CN102626105A - Iodic acid disinfectant - Google Patents

Iodic acid disinfectant Download PDF

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Publication number
CN102626105A
CN102626105A CN2012100874923A CN201210087492A CN102626105A CN 102626105 A CN102626105 A CN 102626105A CN 2012100874923 A CN2012100874923 A CN 2012100874923A CN 201210087492 A CN201210087492 A CN 201210087492A CN 102626105 A CN102626105 A CN 102626105A
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China
Prior art keywords
thimerosal
acid
ethyl alcohol
concentrated sulfuric
absolute ethyl
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CN2012100874923A
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Chinese (zh)
Inventor
张卫元
肖飞
操继跃
陈翠兰
张永丹
周瑜
刘国庆
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WUHAN HVSEN BIOTECHNOLOGY CO Ltd
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WUHAN HVSEN BIOTECHNOLOGY CO Ltd
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Priority to CN2012100874923A priority Critical patent/CN102626105A/en
Publication of CN102626105A publication Critical patent/CN102626105A/en
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Abstract

The invention belongs to the technical field of chemical disinfectants, in particular to an iodic acid disinfectant which is used for disinfecting surgical operation positions, livestock houses, animal product processing places and utensils. The iodic acid disinfectant is prepared by 1.80%-2.50% of potassium iodide, 1.35%-1.50% of refined iodine, 16.0%-17.0% of 85% phosphoric acid, 0.18%-0.28% of 98% concentrated sulfuric acid, 15.00%-25.00% of absolute ethyl alcohol, 0.04%-0.10% of sodium dodecyl benzene sulfonate and the balance water. The prepared iodic acid disinfectant can exert the disinfecting and sterilizing effect well and quickly kill various bacterium propagule, bacterial spore, virus, fungus, mycoplasma and the like in livestock farms.

Description

A kind of acid iodide thimerosal
Technical field
The present invention relates to chemical disinfection liquid technical field, be specifically related to a kind of surgical site, livestock and poultry house, animal products processing space thimerosal of equipment disinfection in one's power that is used for.
Background technology
Along with aquaculture constantly develops, plant's scale intensifies, the high-density rearing at present, and the pathogene of plant is also constantly complicated, and these pathogenic microorganisms can cause the popular of eqpidemic disease under proper condition.The porcine respiratory disease also can be given healthy swinery through the spittle and air borne, causes large-area morbidity.Plant will be in case morbidity will cause serious economy loss.Sterilization is exactly to prevent that external pathogene from importing in the plant, kills or remove pathogene in the external environment, eliminates the eqpidemic disease source, the route of transmission through cutting off eqpidemic disease with the generation that prevents eqpidemic disease or the expansion that prevents infectious disease with spread, ensure safety in production.
Virus particularly aphthovirus (FMD) to slant acidity to contain iodine disinfectant extremely responsive.Aphthovirus has polymorphy, mainly contains 7 main serotypes before the virales and comprises A, O, C, SAT1, SAT2, SAT3 and Asia type.There is not cross immunity originality each other between 7 principal modes.Be that aftosa is not a kind of infectious disease to the artiodactyl beast, but seven big infectious diseases.
FMD virus has extremely strong tolerance external to natural environment.Virus without sending out in the ight soil of fermentation process cloaca can be survived January in summer, can survive the several months in winter.Virus in the frozen article of freezer can keep its vitality for a long time.The dilution of 1g bubble skin poison still can make the animal morbidity for 1,000 ten thousand times.The bubble skin that i.e. pig's feet portion nature diabrosis comes off and the BF 1g of outflow, its virulence can make 100,000 pig infection morbidities completely.
FMD virus is responsive especially to acid.At 4 ℃, during pH6.5, deactivation 90% in 14 hours; During pH5.5, each minute is deactivation 90%; During pH3, the infectious pop-off of virus.The concentration of iodine is 0.005% o'clock, virus moment inactivation.
Based on above-mentioned research, develop and a kind ofly be used for surgical site, livestock and poultry house, animal products processing space the thimerosal of equipment disinfection is significant in one's power.
Summary of the invention
For satisfying the application in the breeding production better, the object of the present invention is to provide a kind of surgical site, livestock and poultry house, animal products processing space thimerosal of equipment disinfection in one's power that is used for.
To achieve these goals, the present invention has taked following technical measures:
A kind of acid iodide thimerosal, this thimerosal are formed by following feedstock production by weight percentage:
KI 1.80%-2.50%,
Smart iodine 1.35%-1.50%,
85% phosphatase 11 6.0%-17.0%,
98% concentrated sulfuric acid 0.18%-0.28%,
Absolute ethyl alcohol 15.00%-25.00%,
Neopelex 0.04%-0.10%,
Surplus is a water.
Preferably, this thimerosal is formed by following feedstock production by weight percentage:
KI 2.00%-2.50%,
Smart iodine 1.42%-1.50%,
85% phosphatase 11 6.20%-16.70%,
98% concentrated sulfuric acid 0.22%-0.26%,
Absolute ethyl alcohol 16.00%-18.00%,
Neopelex 0.08%-0.10%,
Surplus is a water.
Best, this thimerosal is formed by following feedstock production by weight percentage:
KI 2.10%,
Smart iodine 1.47%,
85% phosphatase 11 6.60%,
98% concentrated sulfuric acid 0.24%,
Absolute ethyl alcohol 17.20%,
Neopelex 0.08%,
Surplus is a water.
The preparation method of this thimerosal is following: at first with low amounts of water KI is dissolved, add smart iodine and absolute ethyl alcohol then, jolting makes it fully dissolve back adding 85% phosphoric acid and 98% concentrated sulfuric acid; Add neopelex behind the mixing again; Surplus adds the water polishing, and mixing promptly gets.
Test confirms that prepared sterilization fluid power is brought into play sterilization well, kills the various bacterial propagules of plant, bacterial spore, virus, fungi, mycoplasma etc. rapidly.
Embodiment
Through concrete embodiment the present invention is specified below, but following examples limit protection scope of the present invention never in any form.
Embodiment 1
A kind of acid iodide thimerosal, it is prepared from following raw materials by weight percent:
KI 2.20%,
Smart iodine 1.42%,
85% phosphatase 11 6.20%,
98% concentrated sulfuric acid 0.22%,
Absolute ethyl alcohol 16.00%,
Neopelex 0.08%,
Water 63.88%.
The preparation method is following: after the 2.20g KI is dissolved with low amounts of water; Add smart iodine of 1.42g and 16.00g absolute ethyl alcohol; Jolting makes it fully dissolve back adding 16.20g 85% phosphoric acid and 0.22g 98% concentrated sulfuric acid, adds the 0.08g neopelex behind the mixing, adds water to 100g; Mixing promptly gets acid iodide thimerosal 1 of the present invention.
Embodiment 2
A kind of acid iodide thimerosal, it is prepared from following raw materials by weight percent:
KI 2.50%,
Smart iodine 1.45%,
85% phosphatase 11 6.70%,
98% concentrated sulfuric acid 0.23%,
Absolute ethyl alcohol 17.00%,
Neopelex 0.10%,
Water 62.02%.
The preparation method is following: after the 2.50g KI is dissolved with low amounts of water; Add smart iodine of 1.45g and 17.00g absolute ethyl alcohol; Jolting makes it fully dissolve back adding 16.70g 85% phosphoric acid and 0.23g 98% concentrated sulfuric acid, adds the 0.10g neopelex behind the mixing, adds water to 100g; Mixing promptly gets acid iodide thimerosal 2 of the present invention.
Embodiment 3
A kind of acid iodide thimerosal, it is prepared from following raw materials by weight percent:
KI 2.40%,
Smart iodine 1.50%,
85% phosphatase 11 6.50%,
98% concentrated sulfuric acid 0.26%,
Absolute ethyl alcohol 20.00%,
Neopelex 0.08%,
Water 59.26%.
The preparation method is following: after the 2.40g KI is dissolved with low amounts of water; Add smart iodine of 1.50g and 20.00g absolute ethyl alcohol; Jolting makes it fully dissolve back adding 16.50g 85% phosphoric acid and 0.26g 98% concentrated sulfuric acid, adds the 0.08g neopelex behind the mixing, adds water to 100g; Mixing promptly gets acid iodide thimerosal 3 of the present invention.
Embodiment 4
A kind of acid iodide thimerosal, it is prepared from following raw materials by weight percent:
KI 2.10%,
Smart iodine 1.47%,
85% phosphatase 11 6.60%,
98% concentrated sulfuric acid 0.24%,
Absolute ethyl alcohol 17.20%,
Neopelex 0.08%,
Water 62.31%.
The preparation method is following: after the 2.10g KI is dissolved with low amounts of water; Add smart iodine of 1.47g and 17.20g absolute ethyl alcohol; Jolting makes it fully dissolve back adding 16.60g 85% phosphoric acid and 0.24g 98% concentrated sulfuric acid, adds the 0.08g neopelex behind the mixing, adds water to 100g; Mixing promptly gets acid iodide thimerosal 4 of the present invention.
Test curative effect and the performance study of the acid iodide thimerosal 1-4 that each embodiment makes, the result sees table 1-4
The minimum inhibitory concentration of 1 pair of common virus of table 1 acid iodide thimerosal, bacterium (MIC value, represent) with extension rate
Figure BDA0000147825870000051
The minimum inhibitory concentration of 2 pairs of common virus of table 2 acid iodide thimerosal, bacterium (MIC value, represent) with extension rate
Figure BDA0000147825870000052
The minimum inhibitory concentration of 3 pairs of common virus of table 3 acid iodide thimerosal, bacterium (MIC value, represent) with extension rate
The minimum inhibitory concentration of 4 pairs of common virus of table 4 acid iodide thimerosal, bacterium (MIC value, represent) with extension rate
Figure BDA0000147825870000061
Table 5 acid iodide thimerosal of the present invention and common disinfectants are relatively
The disinfectant kind The acid iodide thimerosal Glutaraldehyde Peracetate Formaldehyde The level Four ammonium Phenols Peroxide Chlorophenol Fluorine water
Use comfortable, not pungent × × × × × × ×
Fungicidal spectrum is wide × × × ×
Economic utility is high × × ×
Safe, nontoxic × × × × × × ×
Temperature influence is little × × × ×
Disinfection force does not receive organic substance influence × × × × × × ×
Effect is held time more than 2 days × × × × × × × ×
Sterilization rapidly × × ×

Claims (3)

1. an acid iodide thimerosal is characterized in that, said thimerosal is formed by following feedstock production by weight percentage:
KI 1.80%-2.50%,
Smart iodine 1.35%-1.50%,
85% phosphatase 11 6.0%-17.0%,
98% concentrated sulfuric acid 0.18%-0.28%,
Absolute ethyl alcohol 15.00%-25.00%,
Neopelex 0.04%-0.10%,
Surplus is a water.
2. acid iodide thimerosal according to claim 1 is characterized in that, said thimerosal is formed by following feedstock production by weight percentage:
KI 2.00%-2.50%,
Smart iodine 1.42%-1.50%,
85% phosphatase 11 6.20%-16.70%,
98% concentrated sulfuric acid 0.22%-0.26%,
Absolute ethyl alcohol 16.00%-18.00%,
Neopelex 0.08%-0.10%,
Surplus is a water.
3. acid iodide thimerosal according to claim 1 is characterized in that, said thimerosal is formed by following feedstock production by weight percentage:
KI 2.10%,
Smart iodine 1.47%,
85% phosphatase 11 6.60%,
98% concentrated sulfuric acid 0.24%,
Absolute ethyl alcohol 17.20%,
Neopelex 0.08%,
Surplus is a water.
CN2012100874923A 2012-03-28 2012-03-28 Iodic acid disinfectant Pending CN102626105A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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CN102626105A true CN102626105A (en) 2012-08-08

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103210958A (en) * 2013-05-15 2013-07-24 上海宇昂新材料科技有限公司 Aquaculture compound iodine solution and preparation method thereof
CN103222476A (en) * 2013-05-15 2013-07-31 上海宇昂新材料科技有限公司 Iodic acid solution for aquaculture and preparation method thereof
CN106376560A (en) * 2016-08-19 2017-02-08 四川恒通动保生物科技有限公司 A charged foam type iodic acid disinfectant and a preparing method thereof
CN107439547A (en) * 2017-09-01 2017-12-08 四川创美克科技有限公司 Complex glucose acid iodine disinfectant and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6045787A (en) * 1998-09-01 2000-04-04 Shanbrom Technologies Llc Protection of labile proteins during iodine disinfection
CN1318979A (en) * 1998-07-27 2001-10-24 马克特辛姆化学工厂有限公司 Environmentally compatible processes, compositions and materials treated thereby
CN1883273A (en) * 2006-07-06 2006-12-27 王德昌 Active disinfectant germicide and method for preparing same
CN1965651A (en) * 2005-11-18 2007-05-23 天津市润拓生物技术有限公司 Disinfectant containing clustered water for animal
CN101006790A (en) * 2006-12-05 2007-08-01 段英利 Refined iodine disinfectant liquor
CN101028003A (en) * 2007-03-30 2007-09-05 高瑞杰 Environment-protective crop alimentary bacteriocide

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1318979A (en) * 1998-07-27 2001-10-24 马克特辛姆化学工厂有限公司 Environmentally compatible processes, compositions and materials treated thereby
US6045787A (en) * 1998-09-01 2000-04-04 Shanbrom Technologies Llc Protection of labile proteins during iodine disinfection
CN1965651A (en) * 2005-11-18 2007-05-23 天津市润拓生物技术有限公司 Disinfectant containing clustered water for animal
CN1883273A (en) * 2006-07-06 2006-12-27 王德昌 Active disinfectant germicide and method for preparing same
CN101006790A (en) * 2006-12-05 2007-08-01 段英利 Refined iodine disinfectant liquor
CN101028003A (en) * 2007-03-30 2007-09-05 高瑞杰 Environment-protective crop alimentary bacteriocide

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103210958A (en) * 2013-05-15 2013-07-24 上海宇昂新材料科技有限公司 Aquaculture compound iodine solution and preparation method thereof
CN103222476A (en) * 2013-05-15 2013-07-31 上海宇昂新材料科技有限公司 Iodic acid solution for aquaculture and preparation method thereof
CN106376560A (en) * 2016-08-19 2017-02-08 四川恒通动保生物科技有限公司 A charged foam type iodic acid disinfectant and a preparing method thereof
CN106376560B (en) * 2016-08-19 2019-09-06 四川恒通动保生物科技有限公司 A kind of charged foam type Iodic acid disinfectant and preparation method thereof
CN107439547A (en) * 2017-09-01 2017-12-08 四川创美克科技有限公司 Complex glucose acid iodine disinfectant and preparation method thereof

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Application publication date: 20120808