CN102604742A - Perfume essential oil for tobacco and preparation method and application thereof - Google Patents
Perfume essential oil for tobacco and preparation method and application thereof Download PDFInfo
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- CN102604742A CN102604742A CN2012100819540A CN201210081954A CN102604742A CN 102604742 A CN102604742 A CN 102604742A CN 2012100819540 A CN2012100819540 A CN 2012100819540A CN 201210081954 A CN201210081954 A CN 201210081954A CN 102604742 A CN102604742 A CN 102604742A
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Abstract
The invention belongs to the technical field of perfumes for tobacco, specifically relating to perfume essential oil for tobacco and a preparation method and application thereof; the preparation method comprises the following steps: making ginger stems and leaves as raw materials, after removing sundries and drying the raw materials, crushing the raw materials into powder, then, processing carbon dioxide supercritical extraction to the steams and leaves powder. According to The invention, the ginger steams and leaves are used as the raw materials so as to prepare the perfume essential oil for the tobacco; a new tobacco perfume preparation way is provided, thus, the ginger steams and leaves turn waste into wealth; simultaneously, the preparation method is characterized by environmental protection, quick process, and high oil productivity.
Description
Technical field
The invention belongs to the tobacco aromatics using technical field, particularly a kind of tobacco aromatics using essential oil.
Background technology
Ginger belongs to Zingiber ginger and belongs to, and per nnial herb is a kind of common common dietotherapeutic article.Ginger bar leaf is the waste during ginger is produced, and annual all have a large amount of bar leaves to be deposited in the field by the peasant.These waste degradeds are slow, and stacking can be stopped up the field traffic, irrigated, grows the insect pest that spreads disease, and can cause topsoil again if dry burning.Therefore,, not only can turn waste into wealth, can also reduce pollution, help environment protection if can utilize to it.
Summary of the invention
The object of the present invention is to provide a kind of tobacco aromatics using essential oil, it is a raw material with ginger bar leaf, has reduced the ginger bar leaf produced pollution when turning waste into wealth.
The technical scheme that the present invention adopts is following:
A kind of tobacco aromatics using essential oil obtains through laxative remedy: with ginger bar leaf is raw material, and the impurity elimination crushed after being dried is the end, afterwards bar leaf powder is carried out carbon dioxide upercritical fluid extraction.
Concrete, the ripe fresh bar leaf of later stage of ginger is chosen Huang Ye and impurity after washing, is drained surface-moisture, pulverizes after the lyophilize then.
Preferably, pulverizing ginger bar leaf is 20-40 order powder.
When carrying out supercritical extraction, extracting pressure 20～25 MPa, 35～40 ℃ of extraction temperature, the extraction time is 60-120min.
CO
2Flow is 20～30 kg/h.
Adopt the two-stage desorb.
Further, first step stripping vessel pressure is that 10～12 MPa, temperature are 40～54 ℃; Second stage stripping vessel pressure is that 6～8 MPa, temperature are 40～54 ℃.
The spices essential oil that said method makes has good application in tobacco, concrete, is added in the pipe tobacco behind the available alcohol dilution.Essential oil suitable in perfuming cigarette is added in an amount of 0.025～0.050%.
The application extracts spices with ginger bar leaf as raw material, and the extract odor component is analyzed, and identifies 38 kinds of compositions (seeing table 1 for details) in the essential oil altogether, accounts for 97.10% of total amount.Be mainly terpenes and alcohols in these materials.Wherein with β-sesquiphellandrene (31.30), farnesene (28.40), 1,8-cineole (5.81), zingiberene (5.32), amphene (5.08), β-phellandrene (4.10), γ-cananga oil alkene (2.10), PC 560 (2.09), caryophyllene (2.02) content are the highest.Terpenes is the important component of food using material, zingiberene, γ-cananga oil alkene, β-phellandrene, the soft flue gas of farnesene ability; PC 560 has pure and fresh and suitable citrus fragrance; Caryophyllene has the hot perfume (or spice) and the banksia rose like Syzygium aromaticum stem oil, distinguish the flavor of sweet and slightly bitter, can improve and the natural stype of promoting or transferring cigarette perfume.1, the 8-cineole is claimed eucalyptol again, in tobacco, can suppress bitter peppery pungency.Also have a spot of aldoketones material in addition, such material has the graceful gentle fragrance of a flower and fruit is fragrant, can improve the cigarette flavor quality, soft flue gas.
Process for extracting of the present invention has that extraction temperature is low, environmental protection, fast and the oil yield rate advantages of higher, and is easy in industry accomplished.
The present invention has following advantage with respect to prior art:
The present invention utilizes ginger bar leaf to be feedstock production tobacco aromatics using essential oil, provides a kind of new tobacco spice to prepare approach, and ginger bar leaf is turned waste into wealth, preparing method's environmental protection simultaneously, quick, and oil yield rate is high.
Embodiment
Below with specific embodiment technical scheme of the present invention is described, but protection scope of the present invention is not limited thereto:
Embodiment 1
The ripe fresh bar leaf of later stage of ginger is chosen Huang Ye and impurity, and after washing, draining surface-moisture, pulverizing after the lyophilize is 20 orders, gets the bar leaf powder 1500 g extraction plant of packing into, places extraction kettle, in the supercritical extraction unit of 5L, extracts.CO
2Flow is 30 kg/h; Extracting pressure 25 MPa; 40 ℃ of extraction temperature; First step stripping vessel pressure is that 10 MPa, temperature are 54 ℃, and second stage stripping vessel pressure is that 8 MPa, temperature are 54 ℃; The extraction time is 100 min.Oil yield 2.63%.
Essential oil to obtaining carries out composition analysis, sees table 1. for details
Table 1
Effect:
Embodiment 1 extract essential oil is diluted to 0.4% according to 0%, 0.025%, 0.05%, 0.100% ratio of tobacco quality with absolute ethyl alcohol; Spray equably with micro sprayer and to be added in the pipe tobacco; Aromatic tobacco is rolled into cigarette to be propped up; Climatic chamber inner equilibrium moisture 48 h at temperature (20 ± 1) ℃, relative humidity (60 ± 2) % smoke panel test.Smoking result is seen table 2.
Table 2
Above result shows that the extract essential oil can obviously improve cigarette flavor, enriches cigarette perfume (or spice), removes assorted gas, improve mouthfeel.
Embodiment 2
The ripe fresh bar leaf of later stage of ginger is chosen Huang Ye and impurity, and after washing, draining surface-moisture, pulverizing after the lyophilize is 40 orders, gets the bar leaf powder 1500 g extraction plant of packing into, places extraction kettle, in the supercritical extraction unit of 5L, extracts.CO
2Flow is 25 kg/h; Extracting pressure 20 MPa; 35 ℃ of extraction temperature; First step stripping vessel pressure is that 11 MPa, temperature are 40 ℃, and second stage stripping vessel pressure is that 6 MPa, temperature are 40 ℃; The extraction time is 80 min.Oil yield 2.41%.
Embodiment 3
The ripe fresh bar leaf of later stage of ginger is chosen Huang Ye and impurity, and after washing, draining surface-moisture, pulverizing after the lyophilize is 30 orders, gets the bar leaf powder 1500 g extraction plant of packing into, places extraction kettle, in the supercritical extraction unit of 5L, extracts.CO
2Flow is 20 kg/h; Extracting pressure 25 MPa; 40 ℃ of extraction temperature; First step stripping vessel pressure is that 12 MPa, temperature are 45 ℃, and second stage stripping vessel pressure is that 8MPa, temperature are 45 ℃; The extraction time is 120 min.Oil yield 2.24%.
The foregoing description is the preferred embodiment of the present invention, but embodiment of the present invention does not receive above-mentioned restriction, and other the change that any the present invention of not deviating from did all should be the substitute mode of equivalence, is included within protection scope of the present invention.
Claims (9)
1. the preparation method of a tobacco aromatics using essential oil is characterized in that, is raw material with ginger bar leaf, and the impurity elimination crushed after being dried is the end, afterwards bar leaf powder is carried out carbon dioxide upercritical fluid extraction.
2. the preparation method of tobacco aromatics using essential oil as claimed in claim 1 is characterized in that, when carrying out supercritical extraction, and extracting pressure 20～25 MPa, 35～40 ℃ of extraction temperature, the extraction time is 60-120min.
3. the preparation method of tobacco aromatics using essential oil as claimed in claim 2 is characterized in that, CO
2Flow is 20～30 kg/h.
4. the preparation method of tobacco aromatics using essential oil as claimed in claim 2 is characterized in that, adopts the two-stage desorb.
5. the preparation method of tobacco aromatics using essential oil as claimed in claim 4 is characterized in that, first step stripping vessel pressure is that 10～12 MPa, temperature are 40～54 ℃; Second stage stripping vessel pressure is that 6～8 MPa, temperature are 40～54 ℃.
6. like the preparation method of the arbitrary described tobacco aromatics using essential oil of claim 1-5, it is characterized in that pulverizing ginger bar leaf is 20-40 order powder.
7. the prepared spices essential oil of the said tobacco aromatics using essential oil of claim 1-6 preparation method.
8. the application of the spices essential oil that makes of the said method of claim 1-6 is characterized in that, essential oil is added in the pipe tobacco after with alcohol dilution.
9. the application of spices essential oil as claimed in claim 8 is characterized in that, essential oil is added in an amount of 0.025～0.050% of pipe tobacco weight in perfuming cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012100819540A CN102604742A (en) | 2012-03-26 | 2012-03-26 | Perfume essential oil for tobacco and preparation method and application thereof |
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| CN2012100819540A CN102604742A (en) | 2012-03-26 | 2012-03-26 | Perfume essential oil for tobacco and preparation method and application thereof |
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| CN102604742A true CN102604742A (en) | 2012-07-25 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103215136A (en) * | 2013-04-12 | 2013-07-24 | 红云红河烟草(集团)有限责任公司 | Preparation method of essence for aromatic wood cigarettes |
| CN103478894A (en) * | 2013-09-27 | 2014-01-01 | 福建中烟工业有限责任公司 | Camellia extract composition with spicy fragrance and application of same to cigarettes |
| CN103519352A (en) * | 2013-11-07 | 2014-01-22 | 袁恩泽 | Electronic cigarette |
| CN109275947A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A kind of supercritical extract processing method suitable for heating pipe tobacco under not combustion state |
Citations (2)
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| CN1251367A (en) * | 1999-08-20 | 2000-04-26 | 广州市轻工研究所 | Process for supercritical carbon dioxide extracting and separating effective components of ginger |
| CN1762956A (en) * | 2005-09-26 | 2006-04-26 | 闫东海 | Supercritical column chromatography method for preparing general gingerol |
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2012
- 2012-03-26 CN CN2012100819540A patent/CN102604742A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1251367A (en) * | 1999-08-20 | 2000-04-26 | 广州市轻工研究所 | Process for supercritical carbon dioxide extracting and separating effective components of ginger |
| CN1762956A (en) * | 2005-09-26 | 2006-04-26 | 闫东海 | Supercritical column chromatography method for preparing general gingerol |
Non-Patent Citations (3)
| Title |
|---|
| 战琨友: "《姜油的化学成分分析与姜辣素的分离纯化研究》", 《山东农业大学博士学位论文》, 15 March 2010 (2010-03-15) * |
| 战琨友等: "《生姜精油、浸膏和油树脂的提取及成分分析》", 《精细化工》, vol. 26, no. 7, 31 July 2009 (2009-07-31), pages 685 - 690 * |
| 王林: "《姜提取技术及其研究进展》", 《中国中医药信息杂志》, vol. 13, no. 11, 30 November 2006 (2006-11-30), pages 96 - 98 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103215136A (en) * | 2013-04-12 | 2013-07-24 | 红云红河烟草(集团)有限责任公司 | Preparation method of essence for aromatic wood cigarettes |
| CN103478894A (en) * | 2013-09-27 | 2014-01-01 | 福建中烟工业有限责任公司 | Camellia extract composition with spicy fragrance and application of same to cigarettes |
| CN103478894B (en) * | 2013-09-27 | 2015-08-12 | 福建中烟工业有限责任公司 | There is the camellia extract composition of pungent note and the application in cigarette thereof |
| CN103519352A (en) * | 2013-11-07 | 2014-01-22 | 袁恩泽 | Electronic cigarette |
| CN109275947A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A kind of supercritical extract processing method suitable for heating pipe tobacco under not combustion state |
| CN109275947B (en) * | 2018-10-08 | 2021-10-15 | 浙江中烟工业有限责任公司 | Supercritical extraction treatment method suitable for tobacco shreds in heating and non-combustion state |
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Application publication date: 20120725 |