CN102590180B - Method for detecting element of Chinese medicine, Chinese medicinal extract, soil or medicinal composition containing Chinese medicinal extract - Google Patents
Method for detecting element of Chinese medicine, Chinese medicinal extract, soil or medicinal composition containing Chinese medicinal extract Download PDFInfo
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- CN102590180B CN102590180B CN201210029994.0A CN201210029994A CN102590180B CN 102590180 B CN102590180 B CN 102590180B CN 201210029994 A CN201210029994 A CN 201210029994A CN 102590180 B CN102590180 B CN 102590180B
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- 229910052713 technetium Inorganic materials 0.000 description 1
- GKLVYJBZJHMRIY-UHFFFAOYSA-N technetium atom Chemical compound [Tc] GKLVYJBZJHMRIY-UHFFFAOYSA-N 0.000 description 1
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- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
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CN201210029994.0A CN102590180B (en) | 2011-10-31 | 2012-02-11 | Method for detecting element of Chinese medicine, Chinese medicinal extract, soil or medicinal composition containing Chinese medicinal extract |
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CN201210029994.0A CN102590180B (en) | 2011-10-31 | 2012-02-11 | Method for detecting element of Chinese medicine, Chinese medicinal extract, soil or medicinal composition containing Chinese medicinal extract |
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CN102590180B true CN102590180B (en) | 2014-04-02 |
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CN105241741B (en) * | 2015-11-27 | 2018-03-30 | 广西壮族自治区药用植物园 | Detect the pre-treating method of metallic element in common bombax flower powder |
CN109632931B (en) * | 2018-12-29 | 2021-07-30 | 上海微谱化工技术服务有限公司 | Analysis method of midazolam preparation |
CN109632930B (en) * | 2018-12-29 | 2022-01-25 | 上海微谱化工技术服务有限公司 | Analysis method for compatibility of midazolam and production system |
CN110412018A (en) * | 2019-09-09 | 2019-11-05 | 华东师范大学 | The detection method of P elements in a kind of plant |
CN110632162B (en) * | 2019-09-11 | 2021-07-27 | 山西大学 | Method for identifying wild astragalus and cultivated astragalus in ground |
CN110702773B (en) * | 2019-11-20 | 2020-11-03 | 武汉上谱分析科技有限责任公司 | Method for measuring Pb isotope ratio in sulfide by using MC-ICP-MS |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0522828A1 (en) * | 1991-07-10 | 1993-01-13 | CEM Corporation | Microwave heated digesting system |
CN101303307A (en) * | 2008-07-08 | 2008-11-12 | 株洲硬质合金集团有限公司 | Analyses testing method of aluminum, calcium, iron, molybdenum, niobium, titanium, tungsten impurity elements in chromium carbide |
CN101762560A (en) * | 2010-01-29 | 2010-06-30 | 广东省粮食科学研究所 | Pretreating and calibrating method for sequentially determining content of lead and cadmium elements in rice |
-
2012
- 2012-02-11 CN CN201210029994.0A patent/CN102590180B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0522828A1 (en) * | 1991-07-10 | 1993-01-13 | CEM Corporation | Microwave heated digesting system |
CN101303307A (en) * | 2008-07-08 | 2008-11-12 | 株洲硬质合金集团有限公司 | Analyses testing method of aluminum, calcium, iron, molybdenum, niobium, titanium, tungsten impurity elements in chromium carbide |
CN101762560A (en) * | 2010-01-29 | 2010-06-30 | 广东省粮食科学研究所 | Pretreating and calibrating method for sequentially determining content of lead and cadmium elements in rice |
Non-Patent Citations (8)
Title |
---|
ICP-MS研究中药炮制前后18种微量元素总量和溶出特性的变化;金鹏飞 等;《中国药学杂志》;20100630;第45卷(第12期);第895页第1段 * |
付先军 等.电感耦合等离子体质谱法分析14种归肺经中药无机元素.《时珍国医国药》.2009,第20卷(第6期), |
刘彦彦 等.微波消解电感耦合等离子体质谱法测定.《时珍国医国药》.2009,第20卷(第6期), |
微波消解电感耦合等离子体质谱法测定;刘彦彦 等;《时珍国医国药》;20090630;第20卷(第6期);全文 * |
晏马成 等.火焰原子吸收光谱法测定鸦胆子中6种元素的含量.《沈阳药科大学学报》.2011,第28卷(第6期), |
火焰原子吸收光谱法测定鸦胆子中6种元素的含量;晏马成 等;《沈阳药科大学学报》;20110630;第28卷(第6期);第439页第2段 * |
电感耦合等离子体质谱法分析14种归肺经中药无机元素;付先军 等;《时珍国医国药》;20090630;第20卷(第6期);第1488页第2-6段 * |
金鹏飞 等.ICP-MS研究中药炮制前后18种微量元素总量和溶出特性的变化.《中国药学杂志》.2010,第45卷(第12期), |
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