CN102579836A - Traditional Chinese medical dendrobium huoshanense composition and preparation method thereof - Google Patents
Traditional Chinese medical dendrobium huoshanense composition and preparation method thereof Download PDFInfo
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- CN102579836A CN102579836A CN2012100537328A CN201210053732A CN102579836A CN 102579836 A CN102579836 A CN 102579836A CN 2012100537328 A CN2012100537328 A CN 2012100537328A CN 201210053732 A CN201210053732 A CN 201210053732A CN 102579836 A CN102579836 A CN 102579836A
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Abstract
The invention discloses a traditional Chinese medical dendrobium huoshanense composition and a preparation method thereof, wherein the traditional Chinese medical dendrobium huoshanense composition is prepared via water or ethanol extraction, concentration and drying of 25-35 percent of dendrobium huoshanense, 20-30 percent of astragalus mongholicus, 20-35 percent of folium cortex eucommiae and 20-30 percent of American ginseng by mass percentage. Based on the traditional Chinese medicine theory, the dendrobium huoshanense and other valuable Chinese herbs are scientifically and reasonably mixed, and the combination and formula are optimized to achieve the purpose of improving healthcare effects.
Description
One, technical field
The present invention relates to a kind of Chinese medicine health care product, specifically a kind of Herba Dendrobii Chinese medicine composition and preparation method thereof.
Two, background technology
Herba Dendrobii is a orchid family Dendrobium plant, and China has 74 kinds and 2 mutation of the orchid family Dendrobium plant now, and wherein 26 kinds have medicinal.Medicinal dendrobium has reinforcing stomach reg fluid, clearing away heat and nourishing YIN, and multiple efficacies such as sore throat relieving makes eye bright, enhancing immunity and alleviating physical fatigue are wherein famous and precious with Herba Dendrobii, and medical value is worth the highest with health care.But because the Herba Dendrobii habitat is extremely harsh and over-drastic excavating, its wild resource has been on the verge of disappearance.The applicant has realized artificial breeding and cultivation through the modern plants tissue culture technology, for the development and use of Herba Dendrobii provide raw material.
The tradition Herba Dendrobii utilize mode single, be taken after being infused in hot water or decoction with boiled water with single medical material mostly.But in the Herba Dendrobii main functional component---dendrobium polysaccharide viscosity is big, and dissolution rate is slow, and dissolution rate is low, so the utilization rate of its active ingredient is extremely low.The theory of having ignored monarch in traditional traditional Chinese medical science simultaneously not with the other drug reasonable compatibility, therefore is difficult to reach health-care effect preferably.
The Herba Dendrobii class compound Chinese medicinal preparation of present domestic research and development and health food are raw material with the Herba Dendrobii mostly, are that the compound Chinese medicinal preparation of raw material is less with the Herba Dendrobii.Number of patent application is that two patents of invention of 201110198864.5 and 201110198866.4 disclose " a kind of prescription and production technology of compound recipe Herba Dendrobii extractum " and " particulate prescription of a kind of compound recipe Herba Dendrobii and production method " respectively.But have all that the product compatibility is single relatively, dosage form is carried and take inconvenience and defective such as functional component content is lower.The prescription of the Herba Dendrobii hard capsule that patent of the present invention relates to and be applied in and domesticly do not see that bibliographical information is arranged.
Along with the continuous quickening of rhythm of life and the increasing of operating pressure, the physical fatigue symptom all has performance in various degree on one's body nearly all adult." white collar " of most domestic just experiencing in various degree psychological fatigue, physical fatigue according to investigations, and further developing of this state will cause the organs function imbalance, the consume of vital essence blood.Therefore, the resisting fatigue problem has caused more and more people's attention, and the eating effect of fatigue resistant health food in the market is unsatisfactory, and prescription is main with yang-tonifying drug mainly, and portioned product also has certain toxic and side effects.Therefore how to make the health food that has these effects and have no side effect, have the very meaning of Chinese medicine through scientific experiments.
Three, summary of the invention
The present invention aims to provide a kind of Herba Dendrobii Chinese medicine composition and preparation method thereof, and the technical solution problem of is to find suitable compatibility composition to improve the utilization rate of Herba Dendrobii active ingredient.
In order to give full play to the health-care effect of Herba Dendrobii to the mankind; Open up its application prospect in health food and medicine; The present invention is the basis with the theory of Chinese medical science; With Herba Dendrobii and Radix Panacis Quinquefolii, Folium Eucommiae and Radix Astragali compatibility, maximally utilised the functional component of Herba Dendrobii, also help storage, transportation.
Technical solution problem of the present invention adopts following technical scheme:
Herba Dendrobii Chinese medicine composition of the present invention, be with the prepared slices of Chinese crude drugs of following mass percent through water or ethanol extraction and the Chinese medicine composition that after concentrated, drying, obtains:
Herba Dendrobii 25-35%, Radix Astragali 20-30%, Folium Eucommiae 20-35%, Radix Panacis Quinquefolii 20-30%.
The method for preparing of Herba Dendrobii Chinese medicine composition of the present invention is to operate according to the following steps:
Take by weighing Herba Dendrobii, the Radix Astragali, Folium Eucommiae and the Radix Panacis Quinquefolii prepared slices of Chinese crude drugs by proportional quantity, washing is also dry;
The Herba Dendrobii prepared slices of Chinese crude drugs are pulverized the 10-20 mesh sieve, added the water of 10-20 times of weight, reflux, extract, three times; Each 3-8 hour; Merge three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains the Herba Dendrobii extract again after vacuum drying, pulverizing;
The Radix Panacis Quinquefolii prepared slices of Chinese crude drugs were pulverized the 10-20 mesh sieve; The ethanol that adds the concentration expressed in percentage by volume 65-85% of 10-20 times of weight; Reflux, extract, three times each 2-4 hour, merges three times extracting solution; Extracting liquid filtering and vacuum concentration to thick paste shape obtains Radix Panacis Quinquefolii extract again after vacuum drying, pulverizing;
The Radix Astragali and the Folium Eucommiae prepared slices of Chinese crude drugs are mixed, add the water of 8-15 times of weight, reflux, extract, three times, each 2-4 hour, merge three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains mixed extract again after vacuum drying, pulverizing;
Herba Dendrobii extract, Radix Panacis Quinquefolii extract and mixed extract are mixed and stir; Be prepared into oral solid formulation by conventional method after adding appropriate amount of auxiliary materials, like granule, tablet, pill, drop pill, hard capsule, solid dispersion, powder, fine granule, pellet, microcapsule, microspheres agent or other pharmaceutically acceptable oral solid formulations.
In the compatibility of the present invention:
The main active dendrobium polysaccharide of Herba Dendrobii has reinforcing YIN-essence benefit essence, thick the intestines and stomach, mend in never sufficient, flat gastric qi, longue meat, Fructus Alpiniae Oxyphyllae remove the multiple medicinal efficacy such as prolong life of shying, make light of one's life by commiting suicide;
Radix Panacis Quinquefolii can improve thinking and body mobility; Not only can strengthen neural excitation, also can strengthen its process of inhibition, make and suppress to be tending towards concentrated; Thereby differentiation makes excited fully and suppresses two kinds of nervous process and is able to balance; Improve people's the intelligence and the work of muscle power and render a service, produce too much free radical when Radix Panacis Quinquefolii can be removed human body strenuous exercise simultaneously, accelerate elimination effect fatigue; The ginsenoside of containing in the Radix Panacis Quinquefolii simultaneously promotes to organize the utilization to sugar, thereby promotes the absorption of body to dendrobium polysaccharide;
The contained chemical constituent of Folium Eucommiae is mainly lignanoids, iridoids, the plain class of phenylpropyl alcohol, flavonoid, aminoacid and trace element and polysaccharide etc., has invigorating the liver and kidney, the pharmacological action of bone and muscle strengthening; Research simultaneously shows that Folium Eucommiae has the mice of enhancing swimming endurance, reduction mouse movement bleeding from anus lactate level has remarkable effect, to as the blood urea nitrogen content of estimating the muscle injury index reduction trend being arranged.Thereby have antifatigue effect, and do not contain the analeptic and the hormone of International Olympic Committee's regulation forbidding.Thereby explain that Folium Eucommiae is a kind of both economy, significant new raw material of effect again that can be used for alleviating physical fatigue efficiency health-care food.
The Radix Astragali has multiple efficacies such as invigorating QI to consolidate the body surface resistance, diuresis detoxification, evacuation of pus, expelling pus and promoting granulation, enhance immunity and alleviating physical fatigue.
Herba Dendrobii is cool in nature in the side, enriching yin and nourishing kidney, and reinforcing stomach reg fluid is mended gas among the taste day after tomorrow simultaneously, with the source of the angry blood of enhancingization, is monarch drug, the little suffering of Folium Eucommiae, temperature is good at the tonifying YANG of temperature compensation Liver and kidney, bone and muscle strengthening; Radix Astragali sweet in the mouth, tepor are gone into lung, spleen, are dared, kidney channel, are longer than benefiting QI for strengthening the superficies, arresting sweating takes off, holds in the palm skin ulcer granulation promoting, inducing diuresis to remove edema admittedly, and two flavors are the in love article of flesh and blood, can high nourishing YIN sun with angry hemospermia marrow, be ministerial drug.Share with the most delicious, again with the boosting qi and nourishing yin of Radix Panacis Quinquefolii, the stack of clearing away heat and promoting production of body fluid effect science; Have good synergism, can improve the bioavailability of compatibe drug and effective ingredient significantly, comprehensively strengthen its health care; All medicines are played altogether; The merit that invigorating both QI and YIN, QI and blood are taken into account, thus reach effect of relieving physical fatigue.
Compared with prior art, the invention has the advantages that:
1, the present invention is the basis with the theory of Chinese medical science, science with Herba Dendrobii and other rare Chinese medicine reasonable compatibility, optimum organization prescription, thus reach the purpose of enhancing health-care effect.
2, product of the present invention is easy to carry, absorb rapidly, and be a kind of modern preparation type that has than high technology content;
3, the present invention has realized the rational exploitation and utilization to this rare Chinese herbal medicine in imminent danger of Herba Dendrobii.
Four, the specific embodiment
Below in conjunction with embodiment the present invention is done further description so that those skilled in the art can better understand the present invention and implementing, but the embodiment that lifts not as qualification of the present invention.
Embodiment 1:
1, component: the raw material of Chinese medicine composition constitutes by mass percentage: Herba Dendrobii 30%, the Radix Astragali 25%, Folium Eucommiae 25%, Radix Panacis Quinquefolii 20%.
2, method for preparing:
A, take by weighing Herba Dendrobii, the Radix Astragali, Folium Eucommiae and Radix Panacis Quinquefolii by proportional quantity, washing is also dry;
B, Herba Dendrobii is pulverized the 10-20 mesh sieve, added the water of 20 times of weight, reflux, extract, three times; Each 6 hours; Merge three times extracting solution, extracting solution filters and vacuum concentration to thick paste shape with filter press, after vacuum drying, pulverizing, obtains the Herba Dendrobii extract again;
C, Radix Panacis Quinquefolii is pulverized the 10-20 mesh sieve, added the ethanol of the concentration expressed in percentage by volume 80% of 10 times of weight, reflux, extract, three times; Each 3 hours; Merge three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains Radix Panacis Quinquefolii extract again after vacuum drying, pulverizing;
D, the Radix Astragali and Folium Eucommiae are mixed, add the water of 8 times of weight, reflux, extract, three times, each 2 hours, merges three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains mixed extract again after vacuum drying, pulverizing;
E, Herba Dendrobii extract, Radix Panacis Quinquefolii extract and mixed extract mixed and stir obtain Herba Dendrobii Chinese medicine composition powder.
Embodiment 2: hard capsule
1, prescription: the Herba Dendrobii Chinese medicine composition powder 65% of (by mass percentage) embodiment 1 preparation, microcrystalline Cellulose 35%.
2, preparation: with the Herba Dendrobii Chinese medicine composition powder and the microcrystalline Cellulose mix homogeneously of embodiment 1 preparation, add the alcohol granulation of concentration expressed in percentage by volume 85% and cross 40 mesh sieves, incapsulate after 60 ℃ of dryings and get final product the 0.25g/ grain.
3, instructions of taking: every day 2 times, each 4.
Embodiment 3:
1, component: the raw material of Chinese medicine composition constitutes by mass percentage: Herba Dendrobii 28%, the Radix Astragali 27%, Folium Eucommiae 22%, Radix Panacis Quinquefolii 23%.
2, method for preparing:
A, take by weighing Herba Dendrobii, the Radix Astragali, Folium Eucommiae and Radix Panacis Quinquefolii by proportional quantity, washing is also dry;
B, Herba Dendrobii is pulverized the 10-20 mesh sieve, added the water of 15 times of weight, reflux, extract, three times; Each 6 hours; Merge three times extracting solution, extracting solution filters and vacuum concentration to thick paste shape with filter press, after vacuum drying, pulverizing, obtains the Herba Dendrobii extract again;
C, Radix Panacis Quinquefolii is pulverized the 10-20 mesh sieve, added the ethanol of the concentration expressed in percentage by volume 85% of 13 times of weight, reflux, extract, three times; Each 4 hours; Merge 4 times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains Radix Panacis Quinquefolii extract again after vacuum drying, pulverizing;
D, the Radix Astragali and Folium Eucommiae are mixed, add the water of 10 times of weight, reflux, extract, three times, each 2 hours, merges three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains mixed extract again after vacuum drying, pulverizing;
E, Herba Dendrobii extract, Radix Panacis Quinquefolii extract and mixed extract mixed and stir obtain Herba Dendrobii Chinese medicine composition powder.
Embodiment 4: hard capsule
1, prescription: the Herba Dendrobii Chinese medicine composition powder 72% of (by mass percentage) embodiment 1 preparation, microcrystalline Cellulose 28%.
2, preparation: with the Herba Dendrobii Chinese medicine composition powder and the microcrystalline Cellulose mix homogeneously of embodiment 1 preparation, add the alcohol granulation of concentration expressed in percentage by volume 90% and cross 40 mesh sieves, incapsulate after 60 ℃ of dryings and get final product the 0.25g/ grain.
3, instructions of taking: every day 2 times, each 4.
Embodiment 5: granule
1, prescription: the Herba Dendrobii Chinese medicine composition powder 62% of (by mass percentage) embodiment 1 preparation, dextrin 17%, maltodextrin 21%.
2, preparation: with Herba Dendrobii Chinese medicine composition powder and dextrin, the maltodextrin mix homogeneously of embodiment 1 preparation, add concentration expressed in percentage by volume 90% alcohol granulation and 40 mesh sieves, processing content after 60 ℃ of dryings is tan granule, the 3g/ bag.
3, instructions of taking: one time 1 bag, 2 times on the one.
Embodiment 6: tablet
1, prescription: the Herba Dendrobii Chinese medicine composition powder 66% of (by mass percentage) embodiment 1 preparation, lactose 13%, starch 18%, magnesium stearate 3%.
2, preparation: with Herba Dendrobii Chinese medicine composition powder and lactose, starch, the magnesium stearate mix homogeneously of embodiment 1 preparation, add concentration expressed in percentage by volume 85% alcohol granulation and 20 mesh sieves, 60 ℃ of dryings are after tablet machine is pressed into tablet, the 0.6g/ sheet.
3, instructions of taking: one time 2,2 times on the one.
Embodiment 7: superfine powder
1, prescription: the Herba Dendrobii Chinese medicine composition powder 90% of (by mass percentage) embodiment 1 preparation, maltodextrin 9.7%, sucralose 0.3%.
2, preparation: behind the Herba Dendrobii Chinese medicine composition powder of embodiment 1 preparation and maltodextrin, sucralose mix homogeneously, be crushed to 2-6 ten thousand purpose superfine powder, in the vial of packing into, the 4g/ bottle.
3, instructions of taking: one time 2 gram, 2 times on the one.
[pharmacodynamic experiment]
The Herba Dendrobii Chinese medicine composition of the present invention's preparation is that test sample book entrusts Nanjing Medical University health analyzing and testing center to carry out the animal experiment study of effect of relieving physical fatigue with the hard capsule.Recommend consumption according to the adult, establish and tried the basic, normal, high dose groups of thing, be respectively 0.17g/kg.bw, 0.34g/kg.bw, 1g/kg.bw (be equivalent to respectively human body RD 5,10,30 times), establish a negative control group simultaneously.Adopt administration by gavage, tried thing for every day the mouse stomach various dose, negative control group gives the distilled water of equivalent, irritates stomach every day 1 time, connects 30d.31d carries out the mensuration of each item resisting fatigue index.
1, swimming with a load attached to the body experiment: after last was tried thing 30min to mice, the load sheet lead of 5% body weight of Mus root of the tail portion placed the swimming case to swim; The about 30cm of the depth of water; 25 ℃ ± 0.5 ℃ of water temperature, the record mice is from the extremely dead time of swimming beginning, as the mice swimming with a load attached to the body time.
2, serum urea is measured: after last is tried thing 30min to mice, temperature be 30 ℃ in not swimming with a load attached to the body 90min, pull out the eyeball blood sampling behind the rest 60min and leave standstill the centrifugal 15min of 2000r/min behind the 3h, get serum and measure serum urea with complete moving biochemistry analyzer.
3, hepatic glycogen is measured: after last is tried thing 30min to mice, put to death animal.Get liver and after the normal saline rinsing, blot with filter paper, take by weighing liver 100mg, remaining operation is carried out hepatic glycogen by the test kit description and is measured.
4, blood lactic acid is measured: last is tried behind the thing 30min from angular vein clump blood sampling 20uL; Not bearing a heavy burden then in temperature is to stop behind the swimming 10min in 30 ℃ the water; Respectively at motion back 0min and the same blood sampling of 20min 20uL, measure blood lactic acid, calculate blood lactic acid TG-AUC.
The initial data of experiments is seen table 1 and table 2.With SPSS software each experiment initial data is carried out homogeneity test of variance, satisfy data information that " variance is neat " require and carry out statistical disposition with the comparative approach in twos of mean between one factor analysis of variance method and a plurality of experimental group and matched group.
Serum urea and hepatic glycogen mensuration result after table 1 supplies test agent to mice swimming with a load attached to the body test, motion (x ± s)
Annotate: compare with negative control group,
*P＜0.05,
*＜0.01
Table 2 is respectively organized blood lactic acid (mg/L) TG-AUC behind the mouse movement (x ± s)
Annotate: compare with negative control group,
*P＜0.05,
*＜0.01
The data analysis result shows; Continuous irrigation stomach 30 days; Basic, normal, high dose groups all can prolong the mice swimming with a load attached to the body time, the generation of serum urea when reducing mice swimming, the generation of blood lactic acid when reducing swimming; Increase the hepatic glycogen deposit, wherein 1g/kg.bw dose groups and the matched group four indices that compares mice all has difference extremely significantly.Judge that thus visible the present invention has the alleviating physical fatigue function in this test dose scope.
Claims (2)
1. Herba Dendrobii Chinese medicine composition is characterized in that: with the prepared slices of Chinese crude drugs of following mass percent through water or ethanol extraction and the Chinese medicine composition that after concentrated, drying, obtains:
Herba Dendrobii 25-35%, Radix Astragali 20-30%, Folium Eucommiae 20-35%, Radix Panacis Quinquefolii 20-30%.
2. the method for preparing of the described Herba Dendrobii Chinese medicine composition of claim 1 is characterized in that operating according to the following steps:
Take by weighing Herba Dendrobii, the Radix Astragali, Folium Eucommiae and the Radix Panacis Quinquefolii prepared slices of Chinese crude drugs by proportional quantity, washing is also dry;
The Herba Dendrobii prepared slices of Chinese crude drugs are pulverized the 10-20 mesh sieve, added the water of 10-20 times of weight, reflux, extract, three times; Each 3-8 hour; Merge three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains the Herba Dendrobii extract again after vacuum drying, pulverizing;
The Radix Panacis Quinquefolii prepared slices of Chinese crude drugs were pulverized the 10-20 mesh sieve; The ethanol that adds the concentration expressed in percentage by volume 65-85% of 10-20 times of weight; Reflux, extract, three times each 2-4 hour, merges three times extracting solution; Extracting liquid filtering and vacuum concentration to thick paste shape obtains Radix Panacis Quinquefolii extract again after vacuum drying, pulverizing;
The Radix Astragali and the Folium Eucommiae prepared slices of Chinese crude drugs are mixed, add the water of 8-15 times of weight, reflux, extract, three times, each 2-4 hour, merge three times extracting solution, extracting liquid filtering and vacuum concentration to thick paste shape obtains mixed extract again after vacuum drying, pulverizing;
Herba Dendrobii extract, Radix Panacis Quinquefolii extract and mixed extract are mixed and stir, be prepared into oral solid formulation by conventional method after adding appropriate amount of auxiliary materials.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104489674A (en) * | 2014-12-16 | 2015-04-08 | 北京康比特体育科技股份有限公司 | Composition for relieving exercise induced fatigue and preparation of composition |
| CN104509620A (en) * | 2014-12-11 | 2015-04-15 | 罗生芳 | Herbal tea containing eucommia folium and preparation method thereof |
| CN104705641A (en) * | 2014-12-11 | 2015-06-17 | 泰州市古月楼餐饮有限公司 | Soup dumpling stuffing and manufacturing method for soup dumpling |
| CN105029394A (en) * | 2014-04-15 | 2015-11-11 | 四川万安石斛产业开发有限公司 | Anti-fatigue health-caring product or medicine composition |
| CN110193034A (en) * | 2019-05-06 | 2019-09-03 | 普正药业集团股份有限公司 | A kind of eucommia leaf extract and its application in alleviation physical fatigue product |
| CN113545483A (en) * | 2021-07-21 | 2021-10-26 | 陕西科技大学 | Spleen and stomach benefiting elderly person coagulating powder and preparation method thereof |
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| CN100354014C (en) * | 2001-12-21 | 2007-12-12 | Psi医疗有限公司 | Medical fibres & fabrics |
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| CN1354014A (en) * | 2001-11-29 | 2002-06-19 | 廖干甫 | Gongbu ointment |
| CN100354014C (en) * | 2001-12-21 | 2007-12-12 | Psi医疗有限公司 | Medical fibres & fabrics |
| CN101611893A (en) * | 2008-06-25 | 2009-12-30 | 刘泳宏 | A kind of natural viscera-nourishing anticancer health-care egg and preparation method |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029394A (en) * | 2014-04-15 | 2015-11-11 | 四川万安石斛产业开发有限公司 | Anti-fatigue health-caring product or medicine composition |
| CN104509620A (en) * | 2014-12-11 | 2015-04-15 | 罗生芳 | Herbal tea containing eucommia folium and preparation method thereof |
| CN104705641A (en) * | 2014-12-11 | 2015-06-17 | 泰州市古月楼餐饮有限公司 | Soup dumpling stuffing and manufacturing method for soup dumpling |
| CN104489674A (en) * | 2014-12-16 | 2015-04-08 | 北京康比特体育科技股份有限公司 | Composition for relieving exercise induced fatigue and preparation of composition |
| CN110193034A (en) * | 2019-05-06 | 2019-09-03 | 普正药业集团股份有限公司 | A kind of eucommia leaf extract and its application in alleviation physical fatigue product |
| CN113545483A (en) * | 2021-07-21 | 2021-10-26 | 陕西科技大学 | Spleen and stomach benefiting elderly person coagulating powder and preparation method thereof |
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| CN102579836B (en) | 2013-06-12 |
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Owner name: JIUXIANZUN HERBA DENDROBII CO., LTD. Free format text: FORMER NAME: ANHUI SHENGNONG BIOTECHNOLOGY TECHNOLOGY CO., LTD. |
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