CN102552093A - Sunscreen skin care product and preparation method thereof - Google Patents
Sunscreen skin care product and preparation method thereof Download PDFInfo
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- CN102552093A CN102552093A CN2012100578188A CN201210057818A CN102552093A CN 102552093 A CN102552093 A CN 102552093A CN 2012100578188 A CN2012100578188 A CN 2012100578188A CN 201210057818 A CN201210057818 A CN 201210057818A CN 102552093 A CN102552093 A CN 102552093A
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- sunlight screening
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- skin
- protecting product
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- 230000000475 sunscreen effect Effects 0.000 title abstract 7
- 239000000516 sunscreening agent Substances 0.000 title abstract 6
- 238000002360 preparation method Methods 0.000 title description 6
- 238000004519 manufacturing process Methods 0.000 title description 3
- 229930003944 flavone Natural products 0.000 claims abstract description 63
- 235000011949 flavones Nutrition 0.000 claims abstract description 63
- 150000002213 flavones Chemical class 0.000 claims abstract description 29
- 239000000654 additive Substances 0.000 claims abstract description 17
- 230000000996 additive effect Effects 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 17
- 235000017060 Arachis glabrata Nutrition 0.000 claims abstract description 14
- 235000010777 Arachis hypogaea Nutrition 0.000 claims abstract description 14
- 235000018262 Arachis monticola Nutrition 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 235000020232 peanut Nutrition 0.000 claims abstract description 14
- 241001553178 Arachis glabrata Species 0.000 claims abstract 11
- 238000012216 screening Methods 0.000 claims description 43
- 239000000047 product Substances 0.000 claims description 39
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims description 34
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims description 34
- 235000003417 Plumeria rubra f acutifolia Nutrition 0.000 claims description 31
- 244000040691 Plumeria rubra f. acutifolia Species 0.000 claims description 31
- 150000002212 flavone derivatives Chemical class 0.000 claims description 28
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
- 238000003756 stirring Methods 0.000 claims description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- 239000002131 composite material Substances 0.000 claims description 11
- 239000011347 resin Substances 0.000 claims description 11
- 229920005989 resin Polymers 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 8
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 6
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 239000003463 adsorbent Substances 0.000 claims description 6
- 230000001476 alcoholic effect Effects 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 6
- 230000008030 elimination Effects 0.000 claims description 6
- 238000003379 elimination reaction Methods 0.000 claims description 6
- 238000010828 elution Methods 0.000 claims description 6
- 239000000284 extract Substances 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 238000004108 freeze drying Methods 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 239000003480 eluent Substances 0.000 claims description 5
- 239000003921 oil Substances 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 229940008099 dimethicone Drugs 0.000 claims description 4
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 4
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 4
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 4
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims description 4
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 claims description 4
- 229960003415 propylparaben Drugs 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 239000004793 Polystyrene Substances 0.000 claims description 2
- 229920002223 polystyrene Polymers 0.000 claims description 2
- 238000001179 sorption measurement Methods 0.000 claims description 2
- 241000628997 Flos Species 0.000 abstract description 15
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 9
- -1 flavonoid compounds Chemical class 0.000 abstract description 8
- 230000006870 function Effects 0.000 abstract description 4
- 229930003935 flavonoid Natural products 0.000 abstract description 3
- 235000017173 flavonoids Nutrition 0.000 abstract description 3
- 206010020751 Hypersensitivity Diseases 0.000 abstract description 2
- 208000026935 allergic disease Diseases 0.000 abstract description 2
- 230000007815 allergy Effects 0.000 abstract description 2
- 206010067484 Adverse reaction Diseases 0.000 abstract 1
- 230000006838 adverse reaction Effects 0.000 abstract 1
- 230000009982 effect on human Effects 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- 239000002537 cosmetic Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
- 244000105624 Arachis hypogaea Species 0.000 description 3
- 206010042496 Sunburn Diseases 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 231100000957 no side effect Toxicity 0.000 description 3
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 3
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 2
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- FHISHQWBZFWXSQ-UHFFFAOYSA-K [Al+3].[Cl-].[Cl-].[Cl-].OC Chemical compound [Al+3].[Cl-].[Cl-].[Cl-].OC FHISHQWBZFWXSQ-UHFFFAOYSA-K 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 239000013538 functional additive Substances 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 2
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- 150000003254 radicals Chemical class 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 210000000582 semen Anatomy 0.000 description 2
- 230000009759 skin aging Effects 0.000 description 2
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 description 1
- JMGZEFIQIZZSBH-UHFFFAOYSA-N Bioquercetin Natural products CC1OC(OCC(O)C2OC(OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5)C(O)C2O)C(O)C(O)C1O JMGZEFIQIZZSBH-UHFFFAOYSA-N 0.000 description 1
- 206010048768 Dermatosis Diseases 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- MZSGWZGPESCJAN-MOBFUUNNSA-N Melitric acid A Natural products O([C@@H](C(=O)O)Cc1cc(O)c(O)cc1)C(=O)/C=C/c1cc(O)c(O/C(/C(=O)O)=C/c2cc(O)c(O)cc2)cc1 MZSGWZGPESCJAN-MOBFUUNNSA-N 0.000 description 1
- 241001597008 Nomeidae Species 0.000 description 1
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 206010041303 Solar dermatitis Diseases 0.000 description 1
- 244000046101 Sophora japonica Species 0.000 description 1
- 235000010586 Sophora japonica Nutrition 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- NZZIMKJIVMHWJC-UHFFFAOYSA-N dibenzoylmethane Chemical compound C=1C=CC=CC=1C(=O)CC(=O)C1=CC=CC=C1 NZZIMKJIVMHWJC-UHFFFAOYSA-N 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- TUJPOVKMHCLXEL-UHFFFAOYSA-N eriodictyol Natural products C1C(=O)C2=CC(O)=CC(O)=C2OC1C1=CC=C(O)C(O)=C1 TUJPOVKMHCLXEL-UHFFFAOYSA-N 0.000 description 1
- SBHXYTNGIZCORC-ZDUSSCGKSA-N eriodictyol Chemical compound C1([C@@H]2CC(=O)C3=C(O)C=C(C=C3O2)O)=CC=C(O)C(O)=C1 SBHXYTNGIZCORC-ZDUSSCGKSA-N 0.000 description 1
- 235000011797 eriodictyol Nutrition 0.000 description 1
- IVTMALDHFAHOGL-UHFFFAOYSA-N eriodictyol 7-O-rutinoside Natural products OC1C(O)C(O)C(C)OC1OCC1C(O)C(O)C(O)C(OC=2C=C3C(C(C(O)=C(O3)C=3C=C(O)C(O)=CC=3)=O)=C(O)C=2)O1 IVTMALDHFAHOGL-UHFFFAOYSA-N 0.000 description 1
- SBHXYTNGIZCORC-UHFFFAOYSA-N eriodyctiol Natural products O1C2=CC(O)=CC(O)=C2C(=O)CC1C1=CC=C(O)C(O)=C1 SBHXYTNGIZCORC-UHFFFAOYSA-N 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 229940075507 glyceryl monostearate Drugs 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 235000021374 legumes Nutrition 0.000 description 1
- LRDGATPGVJTWLJ-UHFFFAOYSA-N luteolin Natural products OC1=CC(O)=CC(C=2OC3=CC(O)=CC(O)=C3C(=O)C=2)=C1 LRDGATPGVJTWLJ-UHFFFAOYSA-N 0.000 description 1
- 235000009498 luteolin Nutrition 0.000 description 1
- IQPNAANSBPBGFQ-UHFFFAOYSA-N luteolin Chemical compound C=1C(O)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(O)C(O)=C1 IQPNAANSBPBGFQ-UHFFFAOYSA-N 0.000 description 1
- 239000013521 mastic Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 description 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 150000003921 pyrrolotriazines Chemical class 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- FDRQPMVGJOQVTL-UHFFFAOYSA-N quercetin rutinoside Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 FDRQPMVGJOQVTL-UHFFFAOYSA-N 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
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- 230000002787 reinforcement Effects 0.000 description 1
- 235000005493 rutin Nutrition 0.000 description 1
- IKGXIBQEEMLURG-NVPNHPEKSA-N rutin Chemical group O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@H](OC=2C(C3=C(O)C=C(O)C=C3OC=2C=2C=C(O)C(O)=CC=2)=O)O1 IKGXIBQEEMLURG-NVPNHPEKSA-N 0.000 description 1
- ALABRVAAKCSLSC-UHFFFAOYSA-N rutin Natural products CC1OC(OCC2OC(O)C(O)C(O)C2O)C(O)C(O)C1OC3=C(Oc4cc(O)cc(O)c4C3=O)c5ccc(O)c(O)c5 ALABRVAAKCSLSC-UHFFFAOYSA-N 0.000 description 1
- 229960004555 rutoside Drugs 0.000 description 1
- 201000000849 skin cancer Diseases 0.000 description 1
- 201000008261 skin carcinoma Diseases 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000004215 skin function Effects 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 230000037072 sun protection Effects 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention relates to a sunscreen skin care product, which contains a sunscreen additive, wherein the sunscreen additive is peanut shell general flavones and/or flos sophorae general flavones or a mixture of the peanut shell general flavones, the flos sophorae general flavones and nanometer TiO2; when the peanut shell general flavones are added independently, the weight percentage of the peanut shell general flavones is 0.5 to 5 percent; when the flos sophorae general flavones are added independently, the weight percentage of the flos sophorae general flavones is 0.6 to 6 percent; and when the peanut shell general flavones and the flos sophorae general flavones are added to be compounded or the peanut shell general flavones and the flos sophorae general flavones are added to be compounded with the nanometer TiO2, the total addition amount of the peanut shell general flavones and the flos sophorae general flavones is 0.5 to 6 percent. According to the sunscreen skin care product, peanut shells or flos sophorae which is low in cost and readily available is used as raw materials, and flavonoid compounds which are contained in the peanut shells or the flos sophorae are extracted, and are blended scientifically and reasonably to form the sunscreen skin care product. The flavonoid compounds in the peanut shells or the flos sophorae have good functions of absorbing ultraviolet rays and repairing sunburned skin, and the prepared skin care product does not have adverse reaction such as irritation, allergy and the like or side effect on human bodies, has a good sunscreen effect, and is stable in quality and easy to produce and store.
Description
Technical field
The invention belongs to the sunlight screening skin-protecting product technical field, be specifically related to a kind of sun-proof skin care that contains Pericarppium arachidis hypogaeae and/or pagodatree flower general flavone
Article and preparation method thereof.
Background technology
In recent years, receive the influence of atmospheric pollution, ozone layer is destroyed, and arrives the ultraviolet intensity in ground and constantly strengthens.Over-drastic ultraviolet radiation is one of key factor that causes solar dermatitis, skin carcinoma.Ultraviolet wave-length coverage is 100～400nm, and ultraviolet can be divided into three wave bands, and UVC (100～280) nm can not pass ozone layer and get into earth surface, and is less to the human injury; UVB (280～320) nm transmission capacity is stronger relatively, can arrive skin surface, is the main cause that sunburn skin causes erythema; UVA (320～400) nm penetration power is extremely strong, can directly arrive skin corium and cause skin aging, all kinds of dermatosis, tanned etc.At present, the sun-proof skin care cosmetics on the market generally adopt and add the additive component (like BTA and dibenzoyl methane derivant, tartaric acid dialkyl and pyrrolotriazine derivatives etc.) with physics (like zinc oxide, ferrum oxide, titanium dioxide etc.) or chemical sun-proof function.Though the sun-proof functional component of physics can be blocked, reflected sunlight, be restricted in application facet because of the infiltration blending problem solution of granular boundary and other composition of cosmetics is not ideal.Though the sun-proof functional component of chemistry can absorb harmful light in the sunlight, reaches the purpose that protection skin is not burnt, chemical sun-prevention component material is easy to produce simultaneously, be easy to cosmetics and merge mutually, and steady quality.But they also exist shortcoming: more or less obvious or hiding can the causing damage to human body like chemical substance itself, particularly finding has more irritated medical history, poor stability etc. to human body.
Recently discover that contained flavone compound can effectively absorb ultraviolet and remove free radical in the certain plants, and has the effect of ultraviolet to the damage of skin that prevent.Therefore, the flavone compound that from natural plants, extracts is added in the skin care item as sun protection factor, not only can resist the infringement of ultraviolet to skin, also has the skin of reinforcement system of defense, effects such as prevention skin aging.Along with people's is to the pursuit of green health, the natural plants skin care item are also safe in utilization because of it, action temperature and, little to skin irritation, have no side effect and the effect favor that more and more receives consumer such as remarkable.It is the sun-proof cosmetic skin care article of sun-proof functional additive with plant Stigma Croci extracting solution that Chinese patent 98118665 discloses a kind of, has to absorb ultraviolet preferably and repair the sunburn skin function; But the main place of production of Stigma Croci has only a small amount of cultivation in states such as Greece, Spain, Iran in China, and output is extremely low, and the time and effort consuming of gathering is classified as rare rare Chinese medicine in China, mainly does medicinal.Therefore, be badly in need of the new natural plant sun skin protection cosmetics of exploitation at present with sun-proof function.
Summary of the invention
The object of the invention is to provide a kind of sunlight screening skin-protecting product, and these skin care item are main sun-proof functional additive with Pericarppium arachidis hypogaeae and/or pagodatree flower general flavone, have no side effect to skin is non-stimulated, and sun-proof result is good.
The present invention also provides the method for preparing of this sunlight screening skin-protecting product.
For realizing above-mentioned purpose, the present invention adopts following technical scheme:
A kind of sunlight screening skin-protecting product, it contains sunlight screening additive, and said sunlight screening additive is Pericarppium arachidis hypogaeae and/or pagodatree flower general flavone, perhaps Pericarppium arachidis hypogaeae total flavones, pagodatree flower general flavone and nano-TiO
2The mixture of forming.
Concrete, the weight percentage of this sunlight screening additive in sunlight screening skin-protecting product is generally 0.5～6%.Preferably, when independent interpolation Pericarppium arachidis hypogaeae total flavones, Pericarppium arachidis hypogaeae total flavones weight percentage is 0.5～5%.The pagodatree flower general flavone weight percentage is 0.6～6% when adding pagodatree flower general flavone separately.And when Pericarppium arachidis hypogaeae and the composite interpolation of pagodatree flower general flavone or both and nano-TiO
2During composite interpolation, the total addition level of Pericarppium arachidis hypogaeae and pagodatree flower general flavone is advisable with 0.5～6%.Wherein when Pericarppium arachidis hypogaeae and the composite interpolation of pagodatree flower general flavone, both are better with the composite effect in mass ratio 1～5:1～5; When both and nano-TiO
2During composite interpolation, the three (is Pericarppium arachidis hypogaeae total flavones, pagodatree flower general flavone and nano-TiO
2) mass ratio is good with 1～5:0.2～5:1～5.
Further, provide the concrete prescription of this sunlight screening skin-protecting product, per 100 weight portion sunlight screening skin-protecting products contain the following weight parts raw material:
2～15 parts of A phase white oils
2～8 parts of GTCC
2～8 parts of IPM
1～8 part of dimethicone
1～5 part of octadecanol
0.5～3 part of monoglyceride
0.1～0.2 part of propylparaben
1～10 part of B phase Feligel-329
2～10 parts of C phase glycerol
2～10 parts of propylene glycol
0.1～0.3 part of methyl hydroxybenzoate
Deionized water to 100 part
0.5～6 part of sunlight screening additive
1～5 part of D phase Feligel-338
0.1～0.3 part of E phase citric acid
0.1～0.3 part in F phase essence.
Wherein, the GTCC chemical name is the caprylic/capric triglyceride, and the IPM chemical name is an isopropyl myristate, and monoglyceride is also claimed monoglyceride, glyceryl monostearate.Feligel-329 and Feligel-338 are emulsifying agents, are produced by the male chemical industry company limited in east, Guangzhou.
Preferably, per this sunlight screening skin-protecting product of 100 weight portions contains the following weight parts raw material:
2～8 parts of A phase white oils
2～6 parts of GTCC
2～6 parts of IPM
1～5 part of dimethicone
1～3 part of octadecanol
0.5～3 part of monoglyceride
0.1～0.2 part of propylparaben
1～6 part of B phase Feligel-329
2～6 parts of C phase glycerol
2～6 parts of propylene glycol
0.1～0.3 part of methyl hydroxybenzoate
Deionized water to 100 part
0.5～4 part of sunlight screening additive
1～3 part of D phase Feligel-338
0.1～0.3 part of E phase citric acid
0.1～0.3 part in F phase essence.
Raw material Pericarppium arachidis hypogaeae total flavones in the above-mentioned sunlight screening skin-protecting product is preferably with following method preparation: add 20～40ml concentration, 60～90% alcoholic acid adding proportions according to 1g drying peanut shell powder, both are mixed; In 70～85 ℃ of heating and refluxing extraction 2～3 times, each extraction time 2～3h merges the gained extracting solution, the elimination residue while hot then; Filtrate decompression is concentrated (in order to reclaim ethanol); Cross macroporous adsorbent resin; Be eluted to earlier colourless with distilled water; Reuse 30%～95% ethanol gradient elution detects eluent and collects active component (detect eluent when extremely colourless with the aluminum chloride methanol solution of mass percent 1%, explain that eluting is complete); With the resin elution liquid concentrating under reduced pressure that obtains, lyophilization promptly obtains Pericarppium arachidis hypogaeae total flavones product (its purity is 22.0～30.0%, and purity testing is with reference to Q/HHH030-2009).
Said macroporous adsorbent resin is preferably the polystyrene nonpolar macroporous adsorption resin, and what the present invention adopted is the LSA-30 type macroporous adsorbent resin of being produced by Xi'an Lanxiao Sci-Tech Co., Ltd..
Raw material pagodatree flower general flavone in the above-mentioned sunlight screening skin-protecting product is preferably with following method preparation: add 15～35ml concentration, 50～90% alcoholic acid adding proportions according to the dry Pagodatree Flower of 1g, both are mixed; Supersound extraction is 2～3 times then, and power 700～1000w extracts 20～60min at every turn, merges the gained extracting solution, the elimination residue; Filtrate decompression is concentrated, leave standstill, centrifugalize gets precipitate; With the precipitate lyophilization get the pagodatree flower general flavone product (purity 50.0～75.0%, purity testing with reference to 2005 editions " pagodatree flower general flavone content assaying method in the Chinese pharmacopoeia).
The method for preparing of above-mentioned sunlight screening skin-protecting product, it comprises the steps:
1. with A mutually in after each raw materials mix, be warming up to 75 ℃～85 ℃, stirring and dissolving is complete;
2. with B mutually with C mutually in after each raw materials mix, be warming up to 75 ℃～85 ℃, stirring and dissolving is complete;
3. under stirring, the A after the dissolving is added in B after the dissolving, the C mixed phase, in 75 ℃～85 ℃ homogenizing 2～5min;
4. under stirring, add D phase (mastic that is light after the stirring), then when being cooled to 45 ℃～50 ℃, add E phase citric acid and F essence mutually, mix homogeneously promptly gets.
Pericarppium arachidis hypogaeae is the shell of legume Semen arachidis hypogaeae.Semen arachidis hypogaeae is one of main oil variety of high-quality edible oil, in China various places plantation is arranged all, like Henan, Hebei, Shandong, Jiangsu etc.Behind the harvesting peanut, Pericarppium arachidis hypogaeae is generally given it up, and has caused the wasting of resources.The present invention is that raw material extracts total flavones with the Pericarppium arachidis hypogaeae, and Pericarppium arachidis hypogaeae is turned waste into wealth.Flos Sophorae is the flower of leguminous plant Chinese scholartree, and cultivated area is bigger at home, and is very common, especially in the rural area.In a word, raw materials used Pericarppium arachidis hypogaeae of the present invention or Flos Sophorae are all generally planted in China, and the product seedbed is many, and output is abundant, and is cheap and easy to get.The Pericarppium arachidis hypogaeae total flavones mainly contains luteolin, eriodictyol, 5, flavone compounds such as 7-dihydroxy chromone; Flavonoid substances in the Flos Sophorae mainly is rutin and Quercetin etc., and these flavone compounds have defying age, radioprotective, free radical resisting, antioxidation, antiinflammatory, antiviral, biological activity such as antibacterial.Nano titanium oxide can block, reflected sunlight, and the infiltration blending of itself and other composition of cosmetics is also better, and when itself and Pericarppium arachidis hypogaeae, when pagodatree flower general flavone is composite, the skin care item that make show good sun-proof result.The used nano titanium oxide of the present invention is produced by Haitai Nano Material Co., Ltd., Nanjing.
Compare beneficial effect of the present invention with prior art:
Sunlight screening skin-protecting product of the present invention is to be raw material with plant Pericarppium arachidis hypogaeae cheap and easy to get or Flos Sophorae, extracts the flavone compound that it contains, and gets through scientific and reasonable proportioning.Flavone compound in Pericarppium arachidis hypogaeae or the Flos Sophorae has the function that absorbs ultraviolet preferably and repair sunburn skin; The skin care item that make do not produce untoward reaction such as stimulating allergy to human body and have no side effect; The ultraviolet sun-proof result is good, and constant product quality is easy to produce and store.
The specific embodiment:
Below through embodiment technical scheme of the present invention is elaborated, but protection scope of the present invention is not limited thereto.
Embodiment 1-6
A kind of sunlight screening skin-protecting product, each raw material weight umber that per this sunlight screening skin-protecting product of 100 weight portions contains is seen table 1.
Wherein, sunlight screening additive is the Pericarppium arachidis hypogaeae total flavones in the foregoing description 1; Sunlight screening additive is a pagodatree flower general flavone among the embodiment 2 and 3; Sunlight screening additive is by Pericarppium arachidis hypogaeae and pagodatree flower general flavone is composite forms among the embodiment 4 and 5, and mass ratio was respectively 1:2 and 1:6 when Pericarppium arachidis hypogaeae and pagodatree flower general flavone were composite.Sunlight screening additive is to form by Pericarppium arachidis hypogaeae, pagodatree flower general flavone and nano titanium oxide are composite among the embodiment 6, and three's mass ratio is 1:1.5:2.5.
The Pericarppium arachidis hypogaeae total flavones prepares as follows: add 25ml volumetric concentration 70% alcoholic acid adding proportion according to 1g drying peanut shell powder, both are mixed; In 80 ℃ of heating and refluxing extraction 3 times, each extraction time 2.5h merges the gained extracting solution, the elimination residue while hot then; Filtrate decompression is concentrated; Cross LSA-30 type macroporous adsorbent resin, elder generation is eluted to colourless with distilled water, reuse 30%～95% ethanol gradient elution; Detect eluent and collect active component (detect eluent when extremely colourless with the aluminum chloride methanol solution of mass percent 1%, explain that eluting is complete); With the resin elution liquid concentrating under reduced pressure that obtains, lyophilization promptly obtains purity 26.05% Pericarppium arachidis hypogaeae total flavones product.Pagodatree flower general flavone prepares as follows: add 25ml volumetric concentration 60% alcoholic acid adding proportion according to the dry Pagodatree Flower of 1g, both are mixed; Supersound extraction is 2 times then, and power 800w extracts 40min at every turn, merges the gained extracting solution, the elimination residue; Filtrate decompression is concentrated, leave standstill, centrifugalize gets precipitate; The precipitate lyophilization is got purity 62.16% pagodatree flower general flavone product.
With embodiment 1 is example, and the method for preparing of sunlight screening skin-protecting product of the present invention is detailed, and it comprises the steps:
1. with A mutually in after each raw materials mix, be warming up to 80 ℃, stirring and dissolving is complete;
2. with B mutually with C mutually in after each raw materials mix, be warming up to 80 ℃, stirring and dissolving is complete;
3. under stirring, the A after the dissolving is added in B after the dissolving, the C mixed phase, in 80 ℃ of homogenizing 2～5min;
4. under stirring, add the D phase, then when being cooled to 45 ℃～50 ℃, add E phase citric acid and F essence mutually, mix homogeneously promptly gets.
The sun-proof skin care product that each embodiment makes is measured with reference to QB/T 2410-1998 (" the evaluation methodology ultraviolet absorptivity method of sun care preparations UVB district sun-proof result "); Measure the absorbance of product between wavelength 280～400 nm; And try to achieve the meansigma methods of absorbance A under UVB, the UVA district wavelength respectively according to following formula 1 and formula 2, be designated as A respectively
UVBAnd A
UVA, the result sees table 2.
UVB district 280～320 nm:
A
UVB=(A
280+ A
290+ A
300+ A
310+ A
320)/5 formulas (1)
UVA district 330～400 nm:
A
UVA=(A
330+ A
340+ A
350+ A
360+ A
370+ A
380+ A
390+ A
400)/8 formulas (2)
Claims (9)
1. a sunlight screening skin-protecting product is characterized in that, this sunlight screening skin-protecting product contains sunlight screening additive, and said sunlight screening additive is Pericarppium arachidis hypogaeae and/or pagodatree flower general flavone, perhaps Pericarppium arachidis hypogaeae total flavones, pagodatree flower general flavone and nano-TiO
2The mixture of forming.
2. sunlight screening skin-protecting product as claimed in claim 1 is characterized in that, the weight percentage of this sunlight screening additive in sunlight screening skin-protecting product is 0.5～6%.
3. sunlight screening skin-protecting product as claimed in claim 2 is characterized in that, its weight percentage is 0.5～5% when adding the Pericarppium arachidis hypogaeae total flavones separately; The pagodatree flower general flavone weight percentage is 0.6～6% when adding pagodatree flower general flavone separately; When Pericarppium arachidis hypogaeae and the composite interpolation of pagodatree flower general flavone or both and nano-TiO
2During composite interpolation, the total addition level of Pericarppium arachidis hypogaeae and pagodatree flower general flavone is 0.5～6%.
4. like the arbitrary described sunlight screening skin-protecting product of claim 1 to 3, it is characterized in that per this sunlight screening skin-protecting product of 100 weight portions contains the following weight parts raw material:
2～15 parts of A phase white oils
2～8 parts of GTCC
2～8 parts of IPM
1～8 part of dimethicone
1～5 part of octadecanol
0.5～3 part of monoglyceride
0.1～0.2 part of propylparaben
1～10 part of B phase Feligel-329
2～10 parts of C phase glycerol
2～10 parts of propylene glycol
0.1～0.3 part of methyl hydroxybenzoate
Deionized water to 100 part
0.5～6 part of sunlight screening additive
1～5 part of D phase Feligel-338
0.1～0.3 part of E phase citric acid
0.1～0.3 part in F phase essence.
5. sunlight screening skin-protecting product as claimed in claim 4 is characterized in that, per this sunlight screening skin-protecting product of 100 weight portions contains the following weight parts raw material:
2～8 parts of A phase white oils
2～6 parts of GTCC
2～6 parts of IPM
1～5 part of dimethicone
1～3 part of octadecanol
0.5～3 part of monoglyceride
0.1～0.2 part of propylparaben
1～6 part of B phase Feligel-329
2～6 parts of C phase glycerol
2～6 parts of propylene glycol
0.1～0.3 part of methyl hydroxybenzoate
Deionized water to 100 part
0.5～4 part of sunlight screening additive
1～3 part of D phase Feligel-338
0.1～0.3 part of E phase citric acid
0.1～0.3 part in F phase essence.
6. sunlight screening skin-protecting product as claimed in claim 4 is characterized in that, said Pericarppium arachidis hypogaeae total flavones prepares as follows:
Add 20～40ml concentration, 60～90% alcoholic acid adding proportions according to 1g drying peanut shell powder, both are mixed; In 70～85 ℃ of heating and refluxing extraction 2～3 times, each extraction time 2～3h merges the gained extracting solution, the elimination residue while hot then; Filtrate decompression is concentrated, cross macroporous adsorbent resin, elder generation is eluted to colourless with distilled water, and reuse 30%～95% ethanol gradient elution detects eluent and also collects active component; With the resin elution liquid concentrating under reduced pressure that obtains, lyophilization promptly obtains Pericarppium arachidis hypogaeae total flavones product.
7. sunlight screening skin-protecting product as claimed in claim 6 is characterized in that, said macroporous adsorbent resin is the polystyrene nonpolar macroporous adsorption resin.
8. sunlight screening skin-protecting product as claimed in claim 4 is characterized in that, said pagodatree flower general flavone prepares as follows:
Add 15～35ml concentration, 50～90% alcoholic acid adding proportions according to the dry Pagodatree Flower of 1g, both are mixed; Supersound extraction is 2～3 times then, and power 700～1000w extracts 20～60min at every turn, merges the gained extracting solution, the elimination residue; Filtrate decompression is concentrated, leave standstill, centrifugalize gets precipitate; The precipitate lyophilization is promptly got the pagodatree flower general flavone product.
9. the method for preparing of the said sunlight screening skin-protecting product of claim 4 is characterized in that, comprises the steps:
1. with A mutually in after each raw materials mix, be warming up to 75 ℃～85 ℃, stirring and dissolving is complete;
2. with B mutually with C mutually in after each raw materials mix, be warming up to 75 ℃～85 ℃, stirring and dissolving is complete;
3. under stirring, the A after the dissolving is added in B after the dissolving, the C mixed phase, in 75 ℃～85 ℃ homogenizing 2～5min;
4. under stirring, add the D phase, then when being cooled to 45 ℃～50 ℃, add E phase citric acid and F essence mutually, mix homogeneously promptly gets.
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| CN104722100A (en) * | 2015-03-18 | 2015-06-24 | 李�杰 | Process for dynamically adsorbing peanut shell flavonoid crude extract by AB-8 macroporous resin |
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| CN105842179A (en) * | 2016-05-06 | 2016-08-10 | 南阳师范学院 | Screening method for basking-resisting traditional Chinese medicine |
| CN105769714A (en) * | 2016-05-23 | 2016-07-20 | 河南大学 | Moisturizing skincare product and preparation method thereof |
| CN106176436A (en) * | 2016-08-26 | 2016-12-07 | 桂林丰润莱生物科技股份有限公司 | A kind of hair growth promoting baste and preparation method thereof |
| CN109054112A (en) * | 2018-08-14 | 2018-12-21 | 界首市路虎车业有限公司 | Electronic automobile-used antiultraviolet protection cover material of one kind and preparation method thereof |
| CN115252443A (en) * | 2022-08-03 | 2022-11-01 | 安徽格锐新材料科技有限公司 | Sun-screening compound and dry-wet dual-purpose sun-screening pressed powder containing sun-screening compound |
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