CN102445051B - 一种从氯化氢气体压缩制备液体氯化氢的方法 - Google Patents
一种从氯化氢气体压缩制备液体氯化氢的方法 Download PDFInfo
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- CN102445051B CN102445051B CN 201110338062 CN201110338062A CN102445051B CN 102445051 B CN102445051 B CN 102445051B CN 201110338062 CN201110338062 CN 201110338062 CN 201110338062 A CN201110338062 A CN 201110338062A CN 102445051 B CN102445051 B CN 102445051B
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- Prior art keywords
- hydrogen chloride
- chloride gas
- water content
- adsorption dehumifier
- adsorbent
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- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical group Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 title claims abstract description 117
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 title claims abstract description 111
- 229910000041 hydrogen chloride Inorganic materials 0.000 title claims abstract description 111
- 239000007789 gas Substances 0.000 title claims abstract description 78
- 239000007788 liquid Substances 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 26
- 230000006835 compression Effects 0.000 title claims abstract description 7
- 238000007906 compression Methods 0.000 title claims abstract description 7
- 238000001816 cooling Methods 0.000 claims abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- 238000001179 sorption measurement Methods 0.000 claims description 60
- 239000003463 adsorbent Substances 0.000 claims description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 238000003795 desorption Methods 0.000 claims description 14
- 239000002808 molecular sieve Substances 0.000 claims description 12
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 229910002804 graphite Inorganic materials 0.000 claims description 10
- 239000010439 graphite Substances 0.000 claims description 10
- 229920006395 saturated elastomer Polymers 0.000 claims description 9
- 229910000831 Steel Inorganic materials 0.000 claims description 4
- 239000012267 brine Substances 0.000 claims description 4
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 claims description 4
- 239000010959 steel Substances 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 claims description 2
- 238000005260 corrosion Methods 0.000 abstract description 4
- 230000007797 corrosion Effects 0.000 abstract description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
- 230000008929 regeneration Effects 0.000 description 10
- 238000011069 regeneration method Methods 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 238000001514 detection method Methods 0.000 description 7
- 210000000476 body water Anatomy 0.000 description 6
- 238000001035 drying Methods 0.000 description 4
- 238000010926 purge Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000003905 agrochemical Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000008676 import Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910000789 Aluminium-silicon alloy Inorganic materials 0.000 description 1
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 229910004283 SiO 4 Inorganic materials 0.000 description 1
- CQBLUJRVOKGWCF-UHFFFAOYSA-N [O].[AlH3] Chemical compound [O].[AlH3] CQBLUJRVOKGWCF-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000002274 desiccant Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000005213 imbibition Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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CN 201110338062 CN102445051B (zh) | 2011-10-31 | 2011-10-31 | 一种从氯化氢气体压缩制备液体氯化氢的方法 |
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CN 201110338062 CN102445051B (zh) | 2011-10-31 | 2011-10-31 | 一种从氯化氢气体压缩制备液体氯化氢的方法 |
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Publication Number | Publication Date |
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CN102445051A CN102445051A (zh) | 2012-05-09 |
CN102445051B true CN102445051B (zh) | 2013-07-31 |
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Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN85106189A (zh) * | 1985-08-20 | 1987-04-29 | 北京化纤工学院 | 一种测定氯化氢中痕量水的方法 |
JP4182608B2 (ja) * | 1999-11-10 | 2008-11-19 | 住友化学株式会社 | 塩化水素と水の分離回収方法 |
CN1323938C (zh) * | 2002-01-25 | 2007-07-04 | 齐化集团有限公司 | 氯化氢的提纯工艺 |
KR101374952B1 (ko) * | 2006-01-27 | 2014-03-14 | 바스프 에스이 | (클로로)탄화수소 및 포스겐을 포함하는 염화수소스트림으로부터 (클로로)탄화수소 무함유 염화수소 및포스겐 무함유 (클로로)탄화수소를 회수하는 방법 |
CN201780009U (zh) * | 2010-08-05 | 2011-03-30 | 钱尉兵 | 水冷、深冷二合一石墨冷凝器 |
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Address after: 312074 Zhejiang Province, Shaoxing city Doumen town Ma Xiang Co-patentee after: Zhejiang University of Technology Patentee after: East Lake Shaoxing hi tech Limited by Share Ltd Address before: 312074 Zhejiang Province, Shaoxing city Doumen town Ma Xiang Co-patentee before: Zhejiang University of Technology Patentee before: Shaoxing Donghu Bio-Chemical Co., Ltd. |
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Address after: 359 Jiangzhong Road, Doumen street, Yuecheng District, Shaoxing City, Zhejiang Province Patentee after: SHAOXING DONGHU HIGH-TECH Co.,Ltd. Patentee after: ZHEJIANG University OF TECHNOLOGY Address before: 312074 Zhejiang Province, Shaoxing city Doumen town Ma Xiang Patentee before: SHAOXING DONGHU HIGH-TECH Co.,Ltd. Patentee before: ZHEJIANG University OF TECHNOLOGY |
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