CN102406209B - Liquid drink containing active ingredients of rose essential oil and preparation method for liquid drink - Google Patents
Liquid drink containing active ingredients of rose essential oil and preparation method for liquid drink Download PDFInfo
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- CN102406209B CN102406209B CN201110384661.5A CN201110384661A CN102406209B CN 102406209 B CN102406209 B CN 102406209B CN 201110384661 A CN201110384661 A CN 201110384661A CN 102406209 B CN102406209 B CN 102406209B
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Abstract
The invention provides a liquid drink containing active ingredients of rose essential oil and a preparation method for the liquid drink. The active ingredients, namely beta-citronellol, nerol and beta-elemene are separated from the rose essential oil, and are mixed with rose water, a rose petal concentrated solution and water to form the liquid drink containing the active ingredients of the rose essential oil. Other small molecules contained in the rose essential oil are removed from the liquid drink, so that the stimulation to an internal system of a human body and the burn of a digestive tract of the human body are avoided; therefore, the liquid drink can be safely taken without the guidance of aromatherapists or pharmacists, is easily absorbed, and has obvious effects of activating meridians and nourishing blood and qi, balancing skin oil, regulating internal secretion and the like.
Description
Technical field
The present invention relates to a kind of liquid state drink that contains the Rosa Damascana effective ingredient and preparation method thereof.
Background technology
Rosa Damascana has active vim and vigour, balance skin oil and fat, regulate the function such as endocrine, ediblely can support outer Kohakuhi with interior for a long time, promotes decomposition and metabolism melanin, allow the women have pale, be full of flexible healthy skin; Help human body to obtain enough sleeps and rest; Can activate blood circulation and disperse blood clots, the work that restores menstrual flow and invigorates blood circulation, stimulate circulation, strengthen vessel wall elasticity, reduce the congested phenomenon of heart, lower cardiopathic incidence; Improve spleen function, the sharp spleen benefit heart.Also have certain antibiotic, bacteria resistance function; And can promote intestines peristalsis, laxative effective is arranged; Purify alimentary canal, help toxin to mediate and metabolism, can improve gastric disorder causing nausea, vomiting and constipation; Especially can lower alcohol to the toxic action of liver, improve the hepatohemia that excessive alcohol causes.
Rosa Damascana mainly is comprised of the volatile lower-molecular substance of tool, wherein maximum with alcohols material, the essential oil Matter Composition that can detect and report at present has kind more than 270, and the effective ingredient with above-mentioned functions mainly is β-citronellol, nerol and beta-elemene, other composition major part is for small-molecule substance and have extremely strong penetration power, if directly take Rosa Damascana, can cause great stimulation to internal system, the alimentary canal of burning, must use under aromatotherapy teacher or pharmacist's guidance, therefore oral Rosa Damascana generally just just uses under specific illness.
Summary of the invention
The purpose of this invention is to provide the liquid state drink that contains the Rosa Damascana effective ingredient that a kind of aromatotherapy teacher of need not or pharmacist's guidance just can be drunk safely.
Another object of the present invention provides a kind of preparation method of liquid state drink of above-mentioned Rosa Damascana effective ingredient.
The present invention realizes that the technical scheme of above-mentioned purpose is as follows:
Characteristics of the present invention are, adopt the molecular clock method, from Rosa Damascana, isolate β-citronellol, nerol and three kinds of effective ingredients of beta-elemene, liquid drink of the present invention so just can not brought other contained in the Rosa Damascana little molecule into, thereby has avoided stimulation and gastral the burning of Endocrine system.
A kind of liquid state drink that contains the Rosa Damascana effective ingredient, mainly formed by β-citronellol, nerol, beta-elemene, rose and roseleaf concentrate, percentage composition meter by weight, β-citronellol is 0.2%, nerol is 0.01%, and beta-elemene is 0.001%, and rose is 25%, the roseleaf concentrate is 35%, and described roseleaf concentrate is to pass through the concentrate that the water boil lixiviate obtains after roseleaf cure into sauce with table sugar is pickled again.
The above-mentioned preparation method who contains the liquid state drink of Rosa Damascana effective ingredient comprises the steps:
(1) adopts the molecular clock method, from Rosa Damascana, isolate β-citronellol, nerol, beta-elemene;
(2) preparation of rose: rose is added in the distillation still, pass into water vapour, boil distillation, distillate is collected water after water-oil separating, be rose, stores ageing again;
(3) preparation of roseleaf concentrate: roseleaf uses first table sugar pickled, makes it cure into sauce, adds the water boil lixiviate again, and leaching liquor obtains the roseleaf concentrate after filtering;
(4) β-citronellol, nerol and the rose with proportional quantity obtains emulsion A through mixing homogeneous; Beta-elemene, roseleaf concentrate and the water of proportional quantity are obtained emulsion B through mixing homogeneous; With emulsion A and emulsion B mixing and stirring, after sterilization, namely get the liquid state drink that contains the Rosa Damascana effective ingredient again.
Further, step (1) adopts the process conditions of molecular clock method separation β-citronellol to be: 53 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 40Pa, temperature; The process conditions of Purification of Nerol are: 47 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 50Pa, temperature; The process conditions of separating beta-elemene are: 40 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 45Pa, temperature.
Further, the table sugar in the step (3) is white sugar.
Further, the process that cure into sauce described in the step (3) is: pickled good roseleaf is packed in the container, and sealing thermal insulation is deposited, opened every 10～15 days and to stir, and then sealing thermal insulation deposits, and cycling can cure into sauce after 40～150 days.
Further, when step (3) added the water boil lixiviate, the weight ratio of sauce and water was 1:2.
Beneficial effect of the present invention: the present invention keeps the effective ingredient of Rosa Damascana, removed other contained in the Rosa Damascana little molecule, therefore can not produce the human endocrine system stimulates and gastral burning, under without aromatotherapy teacher or pharmacist's guidance, also but safety clothes are used, be easy to absorb, the effects such as active vim and vigour, balance skin oil and fat, adjusting endocrine are obvious.
The specific embodiment
The invention will be further described below in conjunction with specific embodiment.
The separation of effective ingredient β-citronellol, nerol, beta-elemene in the Rosa Damascana: method is to utilize rotating scraped film formula molecular still that Rosa Damascana is carried out two-stage to separate, isolate the condition of β-citronellol: 53 ℃ of first class pressure 0.133～1.33Pa, temperature, 20 ℃ of secondary pressure 40Pa, temperature, 1 drops/sec of Rosa Damascana flow velocity, knifing rotating speed 300～310r/min separates that to obtain purity be β-citronellol of 96%; Isolate the condition of nerol: 47 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 50Pa, temperature, 1 drops/sec of Rosa Damascana flow velocity, knifing rotating speed 300～310r/min separates that to obtain purity be 98% nerol; Isolate the condition of beta-elemene: 40 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 45Pa, temperature, 1 drops/sec of Rosa Damascana flow velocity, knifing rotating speed 300～310r/min separates that to obtain purity be 98% beta-elemene.
The preparation of rose: selected fresh-rose, its quality must be without bad change, free from extraneous odour, fresh-rose is joined in the distillation still, then injected water steam is approximately in 30 minutes, make the distillation still temperature reach 100 ℃, and from observation panel observation fluidized state, adjust the steam valve quantity of steam according to fluidized state.The temperature of condenser delivery port reaches 70 ℃, when the temperature of oil water separator reaches 30 ℃, begins to have distillate to produce.Distill after 90 minutes, fetching boiling water accesses valve mutually, accesses rose with the stainless steel aging tank, stores ageing 6 months.Before using rose, be first 5 microns membrane filtration with its via hole diameter, ozonization is 30 minutes again.
The preparation of roseleaf concentrate: with white sugar that roseleaf is pickled first, be specially fresh roseleaf and white sugar according to 1:2 weight ratio weighing and burden, again mixed material is sent into kneading machine, the material of rubbing is packed in the stainless steel cask, good seal, be placed on daytime under the sun and tan by the sun, add the cotton-wadded quilt covering and heat insulating night, opened stainless steel cask every 10～15 days, again sealing after stirring, cycling, can cure into sauce after 40～150 days, this sauce of 300kg is joined in the reactor, be 1:2 by sauce and water weight ratio again, add entry, after stirring made sauce be dispersed in the water, water flowing was steam heated to 100 ℃, boil 10～15 minutes after, refilter and obtain the roseleaf concentrate, use ozonization 30 minutes before using.
Above-mentioned each component that makes is mixed homogeneous, detailed process is: by liquid drink weighing scale, be β-citronellol of 0.2%, 0.01% nerol and 25% rose with consumption, in the homogenizer that the refrigeration condition is arranged, carry out emulsifying homogeneous, 18～35 ℃ of homogeneous operating temperatures, time 5min obtain emulsion A; Be 35% roseleaf concentrate, 0.001% beta-elemene, 39% water with consumption, adopt the stirring-type homogenizer to carry out emulsifying homogeneous, 18～24 ℃ of homogeneous operating temperatures, time 5min obtain emulsion B; To mix under emulsion A and the emulsion B stirring, Killing germs by microwave is after 3 minutes again, and can is to rustless steel container.
The product that obtains as stated above has following technical indicator:
Outward appearance: clarify flowing liquid under the normal temperature;
Color and luster: be brownish red;
Fragrance: pure, the happy fragrance of a flower is arranged, fragrance is elegant;
Relative density (25/25 ℃): 0.8500～0.9700;
Refraction index (25 ℃): 1.4000～1.5000.
Claims (5)
1. the preparation method of a liquid state drink that contains the Rosa Damascana effective ingredient, described liquid drink mainly is comprised of β-citronellol, nerol, beta-elemene, rose and roseleaf concentrate, percentage composition meter by weight, β-citronellol is 0.2%, nerol is 0.01%, and beta-elemene is 0.001%, and rose is 25%, the roseleaf concentrate is 35%, it is characterized in that comprising the steps:
(1) adopts the molecular clock method, from Rosa Damascana, isolate β-citronellol, nerol, beta-elemene;
(2) preparation of rose: rose is added in the distillation still, pass into water vapour, boil distillation, distillate is collected water after water-oil separating, be rose, stores ageing again;
(3) preparation of roseleaf concentrate: roseleaf uses first table sugar pickled, makes it cure into sauce, adds the water boil lixiviate again, and leaching liquor obtains the roseleaf concentrate after filtering;
(4) β-citronellol, nerol and the rose with proportional quantity obtains emulsion A through mixing homogeneous; Beta-elemene, roseleaf concentrate and the water of proportional quantity are obtained emulsion B through mixing homogeneous; With emulsion A and emulsion B mixing and stirring, after sterilization, namely get the liquid state drink that contains the Rosa Damascana effective ingredient again.
2. the preparation method of the liquid state drink that contains the Rosa Damascana effective ingredient according to claim 1, it is characterized in that, the process conditions that step (1) adopts the molecular clock method to separate β-citronellol are: 53 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 40Pa, temperature; The process conditions of Purification of Nerol are: 47 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 50Pa, temperature; The process conditions of separating beta-elemene are: 40 ℃ of first class pressure 0.133 ~ 1.33Pa, temperature, 20 ℃ of secondary pressure 45Pa, temperature.
3. the preparation method who contains the liquid state drink of Rosa Damascana effective ingredient according to claim 1 is characterized in that, the table sugar in the step (3) is white sugar.
4. the preparation method of the liquid state drink that contains the Rosa Damascana effective ingredient according to claim 1, it is characterized in that, the process that cure into sauce described in the step (3) is: pickled good roseleaf is packed in the container, sealing thermal insulation is deposited, opened every 10～15 days and to stir, and then sealing thermal insulation deposits, and cycling can cure into sauce after 40～150 days.
5. the preparation method who contains the liquid state drink of Rosa Damascana effective ingredient according to claim 1 is characterized in that, when step (3) added the water boil lixiviate, the weight ratio of sauce and water was 1:2.
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| CN201110384661.5A CN102406209B (en) | 2011-11-28 | 2011-11-28 | Liquid drink containing active ingredients of rose essential oil and preparation method for liquid drink |
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| CN201110384661.5A CN102406209B (en) | 2011-11-28 | 2011-11-28 | Liquid drink containing active ingredients of rose essential oil and preparation method for liquid drink |
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| CN102406209A CN102406209A (en) | 2012-04-11 |
| CN102406209B true CN102406209B (en) | 2013-04-10 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102940700A (en) * | 2012-12-08 | 2013-02-27 | 昆明戈尔登纯净水有限公司 | Method for preparing rose extracting solution, rose water taking rose extracting solution as active ingredient, and preparation method of rose water |
| CN103859030B (en) * | 2012-12-12 | 2018-02-27 | 内蒙古伊利实业集团股份有限公司 | A kind of milk beverage of suitable women and preparation method thereof |
| CN103445251A (en) * | 2013-09-21 | 2013-12-18 | 新疆和田阳光沙漠玫瑰有限公司 | Liquid beverage formula containing effective ingredients of rose essential oil |
| CN103610192A (en) * | 2013-10-12 | 2014-03-05 | 浙江工商大学 | Rose function beverage and preparation method thereof |
| CN103584239A (en) * | 2013-11-12 | 2014-02-19 | 新疆和田阳光沙漠玫瑰有限公司 | Formula of rose drink with anti-oxidation function |
| CN103549599A (en) * | 2013-11-12 | 2014-02-05 | 新疆和田阳光沙漠玫瑰有限公司 | Preparation method of rose antioxidant function beverage |
| CN107224423A (en) * | 2017-06-15 | 2017-10-03 | 广西南宁博智生物科技有限公司 | A kind of hydrosol with whitening function |
| CN107603740B (en) * | 2017-09-13 | 2021-02-09 | 健士星生物技术研发(上海)有限公司 | Method for reducing content of methyl eugenol in rose essential oil |
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| WO2001087095A1 (en) * | 2000-05-15 | 2001-11-22 | Unilever Plc | Ambient stable beverage |
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Effective date of registration: 20190529 Address after: 223800 No. 1 Suhu Road, Wusu Industrial Park, Suqian City, Jiangsu Province Patentee after: Sunshine Desert (Jiangsu) Spice Technology Co., Ltd. Address before: 848000 Hetian District of Xinjiang Uygur Autonomous Region and No.9 Tianmushan Road of Tianshi Zhejiang Industrial Park Patentee before: Xinjiang Hetian Sunshine Desert Rose Co.,Ltd. |