CN102399302A - Ultrasonic extraction method of pectin - Google Patents
Ultrasonic extraction method of pectin Download PDFInfo
- Publication number
- CN102399302A CN102399302A CN201110338104XA CN201110338104A CN102399302A CN 102399302 A CN102399302 A CN 102399302A CN 201110338104X A CN201110338104X A CN 201110338104XA CN 201110338104 A CN201110338104 A CN 201110338104A CN 102399302 A CN102399302 A CN 102399302A
- Authority
- CN
- China
- Prior art keywords
- pectin
- centrifugal
- acid
- extraction
- extracting according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 229920001277 pectin Polymers 0.000 title claims abstract description 28
- 235000010987 pectin Nutrition 0.000 title claims abstract description 28
- 239000001814 pectin Substances 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000002137 ultrasound extraction Methods 0.000 title abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 244000017020 Ipomoea batatas Species 0.000 claims abstract description 7
- 235000002678 Ipomoea batatas Nutrition 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 5
- 238000001471 micro-filtration Methods 0.000 claims abstract description 5
- 239000000049 pigment Substances 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 230000001105 regulatory effect Effects 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 5
- 238000005406 washing Methods 0.000 claims abstract description 5
- 102000004190 Enzymes Human genes 0.000 claims abstract description 3
- 108090000790 Enzymes Proteins 0.000 claims abstract description 3
- 230000003625 amylolytic effect Effects 0.000 claims abstract description 3
- 238000001035 drying Methods 0.000 claims abstract description 3
- 244000061456 Solanum tuberosum Species 0.000 claims description 15
- 235000002595 Solanum tuberosum Nutrition 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 15
- 239000002893 slag Substances 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 229920002472 Starch Polymers 0.000 claims description 6
- 239000000284 extract Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 235000019698 starch Nutrition 0.000 claims description 6
- 239000008107 starch Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 150000003384 small molecules Chemical class 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 3
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- 238000002791 soaking Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000007062 hydrolysis Effects 0.000 abstract description 3
- 238000006460 hydrolysis reaction Methods 0.000 abstract description 3
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 238000000874 microwave-assisted extraction Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 4
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- MYKOKMFESWKQRX-UHFFFAOYSA-N 10h-anthracen-9-one;sulfuric acid Chemical compound OS(O)(=O)=O.C1=CC=C2C(=O)C3=CC=CC=C3CC2=C1 MYKOKMFESWKQRX-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- 244000276331 Citrus maxima Species 0.000 description 1
- 235000001759 Citrus maxima Nutrition 0.000 description 1
- AEMOLEFTQBMNLQ-BKBMJHBISA-N alpha-D-galacturonic acid Chemical compound O[C@H]1O[C@H](C(O)=O)[C@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-BKBMJHBISA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Molecular Biology (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Sustainable Development (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Claims (6)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110338104.XA CN102399302B (en) | 2011-10-31 | 2011-10-31 | A kind of ultrasonic extracting method of pectin |
CN201610000917.0A CN105418793A (en) | 2011-10-31 | 2011-10-31 | Method for extracting pectin |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110338104.XA CN102399302B (en) | 2011-10-31 | 2011-10-31 | A kind of ultrasonic extracting method of pectin |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610000917.0A Division CN105418793A (en) | 2011-10-31 | 2011-10-31 | Method for extracting pectin |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102399302A true CN102399302A (en) | 2012-04-04 |
CN102399302B CN102399302B (en) | 2016-06-01 |
Family
ID=45882000
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610000917.0A Pending CN105418793A (en) | 2011-10-31 | 2011-10-31 | Method for extracting pectin |
CN201110338104.XA Expired - Fee Related CN102399302B (en) | 2011-10-31 | 2011-10-31 | A kind of ultrasonic extracting method of pectin |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610000917.0A Pending CN105418793A (en) | 2011-10-31 | 2011-10-31 | Method for extracting pectin |
Country Status (1)
Country | Link |
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CN (2) | CN105418793A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103304681A (en) * | 2013-06-20 | 2013-09-18 | 中国农业科学院农产品加工研究所 | Method for extracting pectin |
CN104086667A (en) * | 2014-06-11 | 2014-10-08 | 安徽农业大学 | Method for preparing pectin from citrus fruit peel residues by employing ultrasonic-assisted extraction |
CN104513324A (en) * | 2014-12-17 | 2015-04-15 | 广西壮族自治区农业科学院农产品加工研究所 | Method for extracting pectin from pitaya stem |
CN105566512A (en) * | 2015-12-14 | 2016-05-11 | 山东省果树研究所 | Extracting method of persimmon fruit pectin |
CN106519067A (en) * | 2016-11-19 | 2017-03-22 | 朱莉 | Comprehensive utilization method for sweet potato residues |
CN108641014A (en) * | 2018-05-23 | 2018-10-12 | 广东医科大学 | A kind of clausenae Lansium pectin preparation method and the clausenae Lansium pectin using this method preparation |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3511952B2 (en) * | 1999-01-19 | 2004-03-29 | 不二製油株式会社 | Pectin, its production method, acidic protein food using the same, and its production method |
CN101041699A (en) * | 2006-03-22 | 2007-09-26 | 中国农业科学院农产品加工研究所 | Sweet potato pectin and production technique thereof |
CN101805416A (en) * | 2010-03-16 | 2010-08-18 | 上海交通大学 | Preparation method of canna edulis ker pectin |
CN101942036A (en) * | 2009-07-08 | 2011-01-12 | 李浩贤 | Method for extracting pectin from pineapple peel assisted by ultrasonic wave |
CN101891840B (en) * | 2010-08-09 | 2012-03-14 | 黑龙江北大荒斯达奇生物科技有限公司 | Method for extracting pectin by utilizing potato scraps |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007119366A1 (en) * | 2006-03-17 | 2007-10-25 | Fuji Oil Company, Limited | Process for production of pectin, and gelling agent and gelatinous food using the same |
-
2011
- 2011-10-31 CN CN201610000917.0A patent/CN105418793A/en active Pending
- 2011-10-31 CN CN201110338104.XA patent/CN102399302B/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3511952B2 (en) * | 1999-01-19 | 2004-03-29 | 不二製油株式会社 | Pectin, its production method, acidic protein food using the same, and its production method |
CN101041699A (en) * | 2006-03-22 | 2007-09-26 | 中国农业科学院农产品加工研究所 | Sweet potato pectin and production technique thereof |
CN101942036A (en) * | 2009-07-08 | 2011-01-12 | 李浩贤 | Method for extracting pectin from pineapple peel assisted by ultrasonic wave |
CN101805416A (en) * | 2010-03-16 | 2010-08-18 | 上海交通大学 | Preparation method of canna edulis ker pectin |
CN101891840B (en) * | 2010-08-09 | 2012-03-14 | 黑龙江北大荒斯达奇生物科技有限公司 | Method for extracting pectin by utilizing potato scraps |
Non-Patent Citations (3)
Title |
---|
李新华等: "《粮油加工工艺学》", 30 September 2011, article ""粮油加工工艺学"", pages: 294 * |
杨希娟等: ""马铃薯渣中提取果胶的工艺优化及产品成分分析"", 《食品科学》, vol. 32, no. 4, 25 February 2011 (2011-02-25), pages 25 - 30 * |
王俊儒等: "《天然产物提取分离与鉴定技术》", 31 May 2006, article ""天然产物提取分离与鉴定技术"", pages: 14-16 * |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103304681A (en) * | 2013-06-20 | 2013-09-18 | 中国农业科学院农产品加工研究所 | Method for extracting pectin |
CN103304681B (en) * | 2013-06-20 | 2016-03-16 | 中国农业科学院农产品加工研究所 | A kind of method extracting pectin |
CN104086667A (en) * | 2014-06-11 | 2014-10-08 | 安徽农业大学 | Method for preparing pectin from citrus fruit peel residues by employing ultrasonic-assisted extraction |
CN104513324A (en) * | 2014-12-17 | 2015-04-15 | 广西壮族自治区农业科学院农产品加工研究所 | Method for extracting pectin from pitaya stem |
CN105566512A (en) * | 2015-12-14 | 2016-05-11 | 山东省果树研究所 | Extracting method of persimmon fruit pectin |
CN105566512B (en) * | 2015-12-14 | 2018-03-30 | 山东省果树研究所 | A kind of extracting method of persimmon fruit pectin |
CN106519067A (en) * | 2016-11-19 | 2017-03-22 | 朱莉 | Comprehensive utilization method for sweet potato residues |
CN108641014A (en) * | 2018-05-23 | 2018-10-12 | 广东医科大学 | A kind of clausenae Lansium pectin preparation method and the clausenae Lansium pectin using this method preparation |
Also Published As
Publication number | Publication date |
---|---|
CN105418793A (en) | 2016-03-23 |
CN102399302B (en) | 2016-06-01 |
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Legal Events
Date | Code | Title | Description |
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DD01 | Delivery of document by public notice |
Addressee: Niu Qian Document name: Notification of Passing Preliminary Examination of the Application for Invention |
|
C06 | Publication | ||
PB01 | Publication | ||
DD01 | Delivery of document by public notice |
Addressee: Niu Qian Document name: Notification of Publication of the Application for Invention |
|
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Niu Qian Inventor after: Bai Guangdong Inventor after: Zhang Guangyou Inventor after: Li Hongguang Inventor after: He Xintao Inventor before: Niu Qian |
|
COR | Change of bibliographic data | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20160506 Address after: 230031, room 15, building 648, 101 North Fuyang Road, Luyang District, Anhui, Hefei Applicant after: Hefei Jiquan Pharmaceutical Technology Co.,Ltd. Address before: 236800, 68 families, 10 Guangming Road, Qiaocheng District, Anhui, Bozhou Applicant before: Niu Qian |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20191011 Address after: No. 15-1-702, Tianrun upper floor, Tangwang Avenue, Qiaocheng District, Bozhou City, Anhui Province Patentee after: Bozhou runnuo Enterprise Management Consulting Co.,Ltd. Address before: 230031, room 15, building 648, 101 North Fuyang Road, Luyang District, Anhui, Hefei Patentee before: Hefei Jiquan Pharmaceutical Technology Co.,Ltd. |
|
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160601 Termination date: 20211031 |