CN102329410B - 高流动性聚酯与聚醚混合型聚氨酯材料的制备方法 - Google Patents
高流动性聚酯与聚醚混合型聚氨酯材料的制备方法 Download PDFInfo
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- CN102329410B CN102329410B CN201110236101A CN201110236101A CN102329410B CN 102329410 B CN102329410 B CN 102329410B CN 201110236101 A CN201110236101 A CN 201110236101A CN 201110236101 A CN201110236101 A CN 201110236101A CN 102329410 B CN102329410 B CN 102329410B
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- 239000004814 polyurethane Substances 0.000 title claims abstract description 39
- 229920002635 polyurethane Polymers 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- 229920000570 polyether Polymers 0.000 title claims abstract description 24
- 239000000463 material Substances 0.000 title claims abstract description 19
- 229920000728 polyester Polymers 0.000 title claims abstract description 18
- 239000004721 Polyphenylene oxide Substances 0.000 title claims abstract description 10
- 229920005906 polyester polyol Polymers 0.000 claims abstract description 22
- 238000006243 chemical reaction Methods 0.000 claims description 41
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 36
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 21
- 229910052757 nitrogen Inorganic materials 0.000 claims description 18
- 150000002148 esters Chemical class 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 16
- 238000009413 insulation Methods 0.000 claims description 15
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 14
- 229920000642 polymer Polymers 0.000 claims description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 230000008676 import Effects 0.000 claims description 9
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- SVTBMSDMJJWYQN-RXMQYKEDSA-N (4r)-2-methylpentane-2,4-diol Chemical compound C[C@@H](O)CC(C)(C)O SVTBMSDMJJWYQN-RXMQYKEDSA-N 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000004902 Softening Agent Substances 0.000 claims description 6
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 6
- AWFPGKLDLMAPMK-UHFFFAOYSA-N dimethylaminosilicon Chemical compound CN(C)[Si] AWFPGKLDLMAPMK-UHFFFAOYSA-N 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 6
- 238000009472 formulation Methods 0.000 claims description 6
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 claims description 6
- 229960004418 trolamine Drugs 0.000 claims description 6
- 229920005830 Polyurethane Foam Polymers 0.000 claims description 5
- 239000011496 polyurethane foam Substances 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- RLJWTAURUFQFJP-UHFFFAOYSA-N propan-2-ol;titanium Chemical compound [Ti].CC(C)O.CC(C)O.CC(C)O.CC(C)O RLJWTAURUFQFJP-UHFFFAOYSA-N 0.000 claims description 4
- VXUYXOFXAQZZMF-UHFFFAOYSA-N tetraisopropyl titanate Substances CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 claims description 4
- 239000004970 Chain extender Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000006260 foam Substances 0.000 claims description 3
- 239000003381 stabilizer Substances 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 4
- 239000011148 porous material Substances 0.000 abstract description 3
- 229920005862 polyol Polymers 0.000 abstract description 2
- 150000003077 polyols Chemical class 0.000 abstract description 2
- 239000012948 isocyanate Substances 0.000 abstract 1
- 150000002513 isocyanates Chemical class 0.000 abstract 1
- 239000002585 base Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229920001730 Moisture cure polyurethane Polymers 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
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- Polyurethanes Or Polyureas (AREA)
Abstract
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Priority Applications (1)
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CN201110236101A CN102329410B (zh) | 2011-08-17 | 2011-08-17 | 高流动性聚酯与聚醚混合型聚氨酯材料的制备方法 |
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CN201110236101A CN102329410B (zh) | 2011-08-17 | 2011-08-17 | 高流动性聚酯与聚醚混合型聚氨酯材料的制备方法 |
Publications (2)
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CN102329410A CN102329410A (zh) | 2012-01-25 |
CN102329410B true CN102329410B (zh) | 2012-09-19 |
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CN201110236101A Active CN102329410B (zh) | 2011-08-17 | 2011-08-17 | 高流动性聚酯与聚醚混合型聚氨酯材料的制备方法 |
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Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102558486B (zh) * | 2011-12-23 | 2013-10-30 | 上海汇得化工有限公司 | 一种热贴合用干法聚氨酯合成革树脂材料、制备方法及用途 |
CN103289046A (zh) * | 2013-05-31 | 2013-09-11 | 苏州市景荣科技有限公司 | 一种耐磨聚氨酯鞋底材料 |
CN103289048A (zh) * | 2013-06-21 | 2013-09-11 | 苏州市景荣科技有限公司 | 一种耐老化聚氨酯鞋底材料 |
CN103275295A (zh) * | 2013-06-21 | 2013-09-04 | 苏州市景荣科技有限公司 | 一种阻燃聚氨酯鞋底材料 |
CN103342780B (zh) * | 2013-07-11 | 2015-04-08 | 浙江恒泰源聚氨酯有限公司 | 用不饱和树脂和苯乙烯制备高强度聚氨酯的方法 |
CN106632987A (zh) * | 2017-01-10 | 2017-05-10 | 浙江恒泰源聚氨酯有限公司 | 耐水解抗撕裂聚氨酯双组份鞋底原液的制备方法 |
CN108659253A (zh) * | 2017-12-28 | 2018-10-16 | 浙江恒泰源聚氨酯有限公司 | 超低密度双组份聚氨酯鞋底原液的制备方法 |
CN108178821A (zh) * | 2017-12-28 | 2018-06-19 | 浙江恒泰源聚氨酯有限公司 | 耐磨型双组份聚氨酯抗静电板材原液的制备方法 |
CN107964084A (zh) * | 2017-12-28 | 2018-04-27 | 浙江恒泰源聚氨酯有限公司 | 高速耐热型聚氨酯双组份轮胎原液的制备方法 |
CN111234510B (zh) * | 2020-01-16 | 2022-03-29 | 上海汇得科技股份有限公司 | 一种聚氨酯树脂及其制备方法和用途 |
CN113354793A (zh) * | 2021-05-20 | 2021-09-07 | 华大化学集团有限公司 | 一种高回弹鞋垫中底用聚氨酯树脂及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1961790A1 (en) * | 2005-12-12 | 2008-08-27 | DIC Corporation | Aqueous coating composition, organic/inorganic composite coating film and method for producing same |
CN101547985A (zh) * | 2006-10-26 | 2009-09-30 | 亚什兰许可和知识产权有限公司 | 制造柔性层合制品的方法 |
CN101974147A (zh) * | 2010-09-15 | 2011-02-16 | 旭川化学(苏州)有限公司 | 一种聚酯多元醇及超细纤维合成革用聚氨酯树脂 |
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- 2011-08-17 CN CN201110236101A patent/CN102329410B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1961790A1 (en) * | 2005-12-12 | 2008-08-27 | DIC Corporation | Aqueous coating composition, organic/inorganic composite coating film and method for producing same |
CN101547985A (zh) * | 2006-10-26 | 2009-09-30 | 亚什兰许可和知识产权有限公司 | 制造柔性层合制品的方法 |
CN101974147A (zh) * | 2010-09-15 | 2011-02-16 | 旭川化学(苏州)有限公司 | 一种聚酯多元醇及超细纤维合成革用聚氨酯树脂 |
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CN102329410A (zh) | 2012-01-25 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: Preparation of high fluidity polyester polyether polyurethane Effective date of registration: 20210617 Granted publication date: 20120919 Pledgee: China Construction Bank Wenling sub branch Pledgor: Zhejiang Hengtaiyuan Polyurethane Co.,Ltd. Registration number: Y2021330000599 |
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Date of cancellation: 20221213 Granted publication date: 20120919 Pledgee: China Construction Bank Wenling sub branch Pledgor: Zhejiang Hengtaiyuan Polyurethane Co.,Ltd. Registration number: Y2021330000599 |
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Denomination of invention: Preparation method of high fluidity polyester and polyether mixed polyurethane material Effective date of registration: 20230307 Granted publication date: 20120919 Pledgee: China Construction Bank Wenling sub branch Pledgor: Zhejiang Hengtaiyuan Polyurethane Co.,Ltd. Registration number: Y2023980034065 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20120919 Pledgee: China Construction Bank Wenling sub branch Pledgor: Zhejiang Hengtaiyuan Polyurethane Co.,Ltd. Registration number: Y2023980034065 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of high fluidity polyester and polyether mixed polyurethane material Granted publication date: 20120919 Pledgee: China Construction Bank Wenling sub branch Pledgor: Zhejiang Hengtaiyuan Polyurethane Co.,Ltd. Registration number: Y2024980013400 |