CN102321507B - Multi-efficacy facial soap and preparation method thereof - Google Patents

Multi-efficacy facial soap and preparation method thereof Download PDF

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Publication number
CN102321507B
CN102321507B CN2011102901314A CN201110290131A CN102321507B CN 102321507 B CN102321507 B CN 102321507B CN 2011102901314 A CN2011102901314 A CN 2011102901314A CN 201110290131 A CN201110290131 A CN 201110290131A CN 102321507 B CN102321507 B CN 102321507B
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China
Prior art keywords
oil
facial soap
essential oil
grease
water
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Expired - Fee Related
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CN2011102901314A
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Chinese (zh)
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CN102321507A (en
Inventor
纪红兵
黄丽泉
宋军
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Huizhou Lyuya Biomaterial Co ltd
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GUANGZHOU LVQIAO BIOLOGICAL TECHNOLOGY Co Ltd
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Publication of CN102321507A publication Critical patent/CN102321507A/en
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Abstract

The invention discloses a multi-efficacy facial soap and a preparation method thereof. The facial soap is mainly characterized by containing oil grease, water, sodium hydroxide, honey, natural pigment, and microcapsule essential oil, wherein the adopted grease oil is the combination of emu oil and plant oil according to a certain ratio, and the used essential oil is microencapsulated plant essential oil. The facial soap provided by the invention has the efficacies of cleaning, sterilization, moisture preservation, skin whitening, beverage removing, restoration, crease resistance, and the like, is a pure natural product, has no hurt to skin, and has a simple production technology.

Description

A kind of clean facial soap
Technical field
The present invention relates to clean facial soap of a kind of many effects and preparation method thereof, a kind ofly specifically have cleaning, sterilization, preserve moisture, whiten, the clean facial soap of removing beverage, reparation, function such as wrinkle resistant and preparation method thereof.
Background technology
Progress along with science and technology; The rhythm of life is also more and more faster; People do not have the too many time that skin is carried out daily nursing; So the requirement to cleaning product not only is confined to cleaning, but hopes that it has many effects performance, can also play nursing role to skin simultaneously in cleaning skin.
Emu (EMU) from the national bird in Australia, is one of primary bird kind.Its profile is the African ostrich of picture a bit; Kind race can not fly; And the most valuable that the special fat bag of its back that will belong to, fat of Oromaius norvaehollandeae then extracts from emu fat, and fat of Oromaius norvaehollandeae contains natural components such as abundant oleic acid, inferior fatty acid oil, vitamin E, Vitamin A, OMEGA-3, OMEGA-6; Be that collection is preserved moisture, reparation, wrinkle resistant, sun-proof, whiten, function such as removing beverage is many effects biological beauty product of one, be referred to as by medical cosmetology circle " liquid golden ".
Plants essential oil is flower, leaf, stem, root or the fruit from plant, refines the volatile flavor that extraction obtains through methods such as wet distillation, extruding, cold soaking or solvent lixiviates.Plants essential oil is made up of volatile small molecules, directly plants essential oil is added in the perfumed soap, and essential oil is volatile, and also is subject to the influence of environment and goes bad.Can realize the micro encapsulation of essential oil through water-soluble wall materials of natural polymer such as gum arabic, gelatin or beta-cyclodextrins; Encapsulated essential oil can reduce its volatilization degree, also can make its influence of avoiding outside atmosphere simultaneously, and encapsulated essential oil is added in the clean facial soap; In clean facial soap use; After the water-soluble wall material dissolving, essential oil can slowly be released, thereby reaches the effect of nursing.
Spray-drying process is through mechanical effect, need the exsiccant material, and be dispersed into very thin particulate and (increase the moisture evaporation area as mist; Quicken drying process); Contact with warm air, most of moisture is removed, make the solid matter in the material be dried to powder in moment.It is very fast that spray-drying process has drying process, but the convection drying powdered, and flash evapn does not have influence to heat-sensitive substance character such as essential oils, has advantages such as production efficiency height, running cost be low.
Honey is to be led to by honeybee herborization nectary excretory juice.Honey has the promotion skin metabolism, strengthens the vigor and the antimicrbial power of skin, reduces pigmentation, prevents xerosis cutis, makes skin soft, pure white, fine and smooth, and can reduce wrinkle and prevent and treat skin maintenance effects such as skin disorders such as acne.
Therefore; The clean facial soap of forming by emu wet goods natural fats and oils, microencapsulated essential oils, natural pigment, honey etc.; Be have cleaning, sterilization, preserve moisture, whiten, the cleaning product of many effects of removing beverage, reparation, function such as wrinkle resistant, in cleaning skin, also can carry out daily nursing to skin.
Summary of the invention
The object of the present invention is to provide a kind of collect the cleaning and the skin daily nursing be clean facial soap of many effects of one and preparation method thereof.
For realizing above-mentioned purpose, the technical scheme that the present invention adopted is: main raw material has grease, water, sodium hydroxide, honey, natural pigment, microencapsulated essential oils.Wherein said grease be fat of Oromaius norvaehollandeae or fat of Oromaius norvaehollandeae and Oleum Cocois, plam oil, palm-kernel oil, Camellia oil, raisin seed oil, sweet almond oil, Viscotrol C, wheatgerm wet goods vegetables oil one or more make up according to a certain percentage; Described microencapsulated essential oils be rose, santal, tea tree, lavandula angustifolia, Flos Pelargonii, Rosmarinus officinalis, peppermint, eucalyptus globolus, lemongrass etc.; Described microcapsule wall material is natural polymers such as gum arabic, gelatin, beta-cyclodextrin, modified starch, casein, sodium carboxymethylcellulose pyce, Xylo-Mucine, sodium hydroxyethyl cellulose, HPMC.
In above-mentioned clean facial soap of many effects and preparation method thereof, the described method for preparing microencapsulated essential oils is a spray-drying process, and its preparation process may further comprise the steps:
1) with the water-soluble formation wall of natural polymer material solution;
2) essential oil is distributed in the wall material solution;
3) be 70 ~ 90 in temperature in oC, temperature out is 30 ~ 40 oUnder the C, spraying drying obtains microencapsulated essential oils.
In above-mentioned clean facial soap of many effects and preparation method thereof, it is characterized in that the ratio of various components is: grease is 60 ~ 70%, and water is 20 ~ 25%, and sodium hydroxide is 9 ~ 13%, and honey is 1 ~ 3%, and natural pigment is 0.5 ~ 1%, and microencapsulated essential oils is 3 ~ 5%.
In above-mentioned clean facial soap of many effects and preparation method thereof, the making method of clean facial soap may further comprise the steps:
1) water is dissolution of sodium hydroxide, and is cooled to 40 ~ 50 OC
2) grease is heated to dissolving, and is cooled to 40 ~ 50 OC
3) sodium hydroxide solution is slowly poured in the grease, and stirred fast 20 minutes;
4) add microencapsulated essential oils, natural pigment, honey etc. stir;
5) mixture that stirs is poured in the silica gel mould left standstill;
6) treat that soap lye solidifies the back demoulding, places about 4 weeks of shady and cool ventilation place slaking and can use.
Advantage of the present invention and effect:
The present invention is based on the clean facial soap that fat of Oromaius norvaehollandeae and micro encapsulation plants essential oil are made; Fat of Oromaius norvaehollandeae contains natural components such as abundant oleic acid, inferior fatty acid oil, vitamin E, Vitamin A, OMEGA-3, OMEGA-6; Have the consistency splendid with skin texture; Particularly contain a large amount of unsaturated olefin(e) acids, can strengthen skin elasticity, have extremely strong skin seepage force; Obviously the softening skin stratum corneum, calm down wrinkle, remove dead skin, and can replenish the multiple nutritional components that human skin needs most.In addition, effects such as scar, Glycerin are whitened, desalinated to product of the present invention in addition, and without any side effects.The typical result example is following:
1, old xx, the man, 25 years old, face and shank tumble injury accidentally, hospital treatment leaves scar, uses scar cream on the market once, and effect is not remarkable.Use product of the present invention after 20 days, unusual effect is arranged, scar disappears basically after 30 days.
2, yellow xx, the woman, 34 years old, cheek portion had pigmentation for many years, learn that this product has spot-removal function after, adhere to washing one's face every day three times with product of the present invention, use 10 days continuously after, positive effect is arranged, facial pigmentation shoals, so far effect stability.
Embodiment
Case study on implementation 1
(1) preparation technology of microencapsulated essential oils
The 30g gum arabic is dissolved in formation wall material solution in the 100g water, in wall material solution, forms milk sap to 5g Flos Rosae Rugosae quintessence oil dispersed with stirring.In temperature in is 85 OC, temperature out is 38 OCSpraying drying obtains the micro encapsulation Flos Rosae Rugosae quintessence oil under the condition.
(2) preparation technology of clean facial soap
Fat of Oromaius norvaehollandeae 250g, water 77 g, sodium hydroxide 33 g, micro encapsulation Flos Rosae Rugosae quintessence oil 10 g, natural pigment 2.5g, honey 5g.
Making step is:
1) water is dissolution of sodium hydroxide, and is cooled to 40 ~ 50 OC
2) grease is heated to dissolving, and is cooled to 40 ~ 50 OC
3) sodium hydroxide solution is slowly poured in the grease, and stirred about 20min fast;
4) add microencapsulated essential oils, natural pigment, honey etc. stir;
5) mixture is poured in the silica gel mould left standstill;
6) treat that soap lye solidifies the back demoulding, places 4 weeks of shady and cool ventilation place slaking.
Case study on implementation 2
(1) preparation technology of microencapsulated essential oils
The 50g modified starch is dissolved in formation wall material solution in the 100g water, in wall material solution, forms milk sap to 10g Herba Lysimachiae foenumgraeci quintessence oil dispersed with stirring.In temperature in is 88 OC, temperature out is 40 OCSpraying drying obtains the micro encapsulation Herba Lysimachiae foenumgraeci quintessence oil under the condition.
(2) preparation technology of clean facial soap
Fat of Oromaius norvaehollandeae 150 g, sweet oil 100g, water 78g, sodium hydroxide 34g, micro encapsulation Herba Lysimachiae foenumgraeci quintessence oil 10g, honey 7g.
Making step is: with embodiment 1.
Case study on implementation 3
(1) preparation technology of microencapsulated essential oils
The 5g modified starch is dissolved in formation wall material solution in the 100g water, in wall material solution, forms milk sap to 10g tea tree ethereal oil dispersed with stirring.In temperature in is 86 OC, temperature out is 37 OCSpraying drying obtains the micro encapsulation tea tree ethereal oil under the condition.
(2) preparation technology of clean facial soap
Fat of Oromaius norvaehollandeae 100 g, Camellia oil 100 g, palm-kernel oil 50 g, water 80 g, sodium hydroxide 35 g, micro encapsulation tea tree ethereal oil 8 g, honey 10g.
Making step is: with embodiment 1.
Case study on implementation 4
(1) preparation technology of microencapsulated essential oils
The 30g gelatin is dissolved in formation wall material solution in the 100g water, in wall material solution, forms milk sap to 15g rosemary ethereal oil dispersed with stirring.In temperature in is 85 OC, temperature out is 38 OCSpraying drying obtains the micro encapsulation rosemary ethereal oil under the condition.
(2) preparation technology of clean facial soap
Fat of Oromaius norvaehollandeae 125 g, wheatgerm oil 12 g, Oleum Cocois 50 g, palm-kernel oil 63 g, water 86 g, sodium hydroxide 37 g, micro encapsulation rosemary ethereal oil 8 g, honey 8g.
Making step is: with embodiment 1.
Case study on implementation 5
(1) preparation technology of microencapsulated essential oils
The 30g hydroxypropylcellulose is dissolved in formation wall material solution in the 100g water, in wall material solution, forms milk sap to 10g peppermint essential oil dispersed with stirring.In temperature in is 90 OC, temperature out is 40 OCSpraying drying obtains micro encapsulation peppermint essential oil under the condition.
(2) preparation technology of clean facial soap
Fat of Oromaius norvaehollandeae 150 g, raisin seed oil 50 g, Oleum Cocois 50 g, water 84 g, sodium hydroxide 36 g, micro encapsulation peppermint essential oil 10 g, honey 9g.
Making step is: with embodiment 1.
Case study on implementation 6
(1) preparation technology of microencapsulated essential oils
The 20g casein is dissolved in formation wall material solution in the 100g water, in wall material solution, forms milk sap to 8g eucalyptus quintessence oil dispersed with stirring.In temperature in is 70 OC, temperature out is 30 OCSpraying drying obtains the micro encapsulation eucalyptus quintessence oil under the condition.
(2) preparation technology of clean facial soap
Fat of Oromaius norvaehollandeae 150 g, palm-kernel oil 50 g, sweet almond oil 50 g, water 80 g, sodium hydroxide 35 g, micro encapsulation eucalyptus quintessence oil 8 g, honey 10g.
Making step is: with embodiment 1.

Claims (3)

1. clean facial soap; It is characterized in that raw material is grease, water, sodium hydroxide, honey, natural pigment and essential oil; Wherein said grease is that one or more of fat of Oromaius norvaehollandeae or fat of Oromaius norvaehollandeae and Oleum Cocois, plam oil, palm-kernel oil, Camellia oil, raisin seed oil, sweet almond oil, Viscotrol C, wheatgerm oil make up by a certain percentage; Said essential oil is the plants essential oil that micro encapsulation is handled; Microcapsule wall material is a natural macromolecular material; Described natural macromolecular material is gum arabic, gelatin, modified starch, casein, sodium carboxymethylcellulose pyce, Xylo-Mucine, sodium hydroxyethyl cellulose, HPMC, and microencapsulated essential oils adopts spray drying method for preparation, and preparation process is following:
1) with the water-soluble formation wall of natural macromolecular material material solution;
2) essential oil is distributed in the wall material solution;
3) be 70 ~ 90 ° of C in temperature in, temperature out is that spraying drying obtains microencapsulated essential oils under 30 ~ 40 ° of C.
2. clean facial soap according to claim 1, it is characterized in that described plants essential oil be rose, santal, tea tree, lavandula angustifolia, Flos Pelargonii, Rosmarinus officinalis, peppermint, eucalyptus globolus, lemongrass essential oil.
3. clean facial soap according to claim 1, the making method that it is characterized in that clean facial soap be as follows:
1) water is dissolution of sodium hydroxide, and is cooled to 40 ~ 50 ° of C;
2) grease is heated to dissolving, and is cooled to 40 ~ 50 ° of C;
3) sodium hydroxide solution is slowly poured in the grease, and stirred fast 20 minutes;
4) add microencapsulated essential oils, natural pigment, honey stirs;
5) mixture that stirs is poured in the silica gel mould left standstill;
6) treat that soap lye solidifies the back demoulding, places 4 weeks of shady and cool ventilation place slaking to use.
CN2011102901314A 2011-09-28 2011-09-28 Multi-efficacy facial soap and preparation method thereof Expired - Fee Related CN102321507B (en)

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Application Number Priority Date Filing Date Title
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CN102321507B true CN102321507B (en) 2012-11-21

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CN102614099B (en) * 2012-04-10 2013-03-20 张仕英 Method for preparing rose extract for supercritical CO2 extraction cosmetics
CN102863260A (en) * 2012-09-17 2013-01-09 景步根 Kitchen waste recycling and processing method
CN103232910A (en) * 2013-04-28 2013-08-07 广州丹奇日用化工厂有限公司 Transparent handmade soap and preparation method thereof
CN103224848B (en) * 2013-04-28 2015-01-14 广州丹奇日用化工厂有限公司 Hand-made cold process soap and preparation method thereof
CN103242991A (en) * 2013-06-03 2013-08-14 湖北科技学院 Osmanthus handmade soap and manufacturing method thereof
CN103571625A (en) * 2013-06-21 2014-02-12 伊犁紫苏丽人生物科技有限公司 Lavender essential oil microcapsule and preparation process thereof
CN103468440B (en) * 2013-09-12 2015-09-23 上海制皂(集团)如皋有限公司 A kind of skin whitening, moisturizing perfumed soap and preparation method thereof
CN104120050A (en) * 2014-06-25 2014-10-29 曹源 Cleaning and skin care toilet soap and preparation method thereof
CN104388213A (en) * 2014-11-14 2015-03-04 浙江久晟茶业发展有限公司 Handmade camellia oil soap and preparation method thereof
CN105779172A (en) * 2014-12-15 2016-07-20 朱玉霖 Bingposanyan ancient soap and preparation method therefor
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Inventor after: Huang Liquan

Inventor after: Song Jun

Inventor before: Ji Hongbing

Inventor before: Huang Liquan

Inventor before: Song Jun

TR01 Transfer of patent right

Effective date of registration: 20170712

Address after: 516081 Guangdong Province, Huizhou Dayawan science and Technology Innovation Park Road Research Building 5 building A room 108

Patentee after: HUIZHOU LYUYA BIOMATERIAL CO.,LTD.

Address before: 511400, No. 2, No. 501, building 2, 832, Yingbin Road, Yingbin Road, east ring street, Guangzhou, Guangdong, Panyu District

Patentee before: GUANGZHOU LVQIAO BIOLOGICAL TECHNOLOGY Co.,Ltd.

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20121121

Termination date: 20210928

CF01 Termination of patent right due to non-payment of annual fee