CN102308827B - Pesticide composition containing flufenoxuron and fenproximate - Google Patents
Pesticide composition containing flufenoxuron and fenproximate Download PDFInfo
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- CN102308827B CN102308827B CN 201110108864 CN201110108864A CN102308827B CN 102308827 B CN102308827 B CN 102308827B CN 201110108864 CN201110108864 CN 201110108864 CN 201110108864 A CN201110108864 A CN 201110108864A CN 102308827 B CN102308827 B CN 102308827B
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- flufenoxuron
- pesticide
- mite
- mite ester
- azoles mite
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- 239000000203 mixture Substances 0.000 title claims abstract description 37
- RYLHNOVXKPXDIP-UHFFFAOYSA-N flufenoxuron Chemical compound C=1C=C(NC(=O)NC(=O)C=2C(=CC=CC=2F)F)C(F)=CC=1OC1=CC=C(C(F)(F)F)C=C1Cl RYLHNOVXKPXDIP-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 239000000575 pesticide Substances 0.000 title claims abstract description 27
- 150000002148 esters Chemical class 0.000 claims description 33
- 150000003851 azoles Chemical class 0.000 claims description 21
- -1 flufenoxuron azoles Chemical class 0.000 claims description 15
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 12
- HVLLSGMXQDNUAL-UHFFFAOYSA-N triphenyl phosphite Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)OC1=CC=CC=C1 HVLLSGMXQDNUAL-UHFFFAOYSA-N 0.000 claims description 10
- 241000488581 Panonychus citri Species 0.000 claims description 7
- 239000004530 micro-emulsion Substances 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 4
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 claims description 4
- 239000004480 active ingredient Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
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- 238000012360 testing method Methods 0.000 description 12
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- 241001454293 Tetranychus urticae Species 0.000 description 7
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- 238000005303 weighing Methods 0.000 description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 241000607479 Yersinia pestis Species 0.000 description 6
- 239000000839 emulsion Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 241000675108 Citrus tangerina Species 0.000 description 4
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- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000000642 acaricide Substances 0.000 description 3
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- 238000000205 computational method Methods 0.000 description 3
- 238000009313 farming Methods 0.000 description 3
- 230000000361 pesticidal effect Effects 0.000 description 3
- 238000005070 sampling Methods 0.000 description 3
- 229920001285 xanthan gum Polymers 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- 229920001214 Polysorbate 60 Polymers 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 210000000481 breast Anatomy 0.000 description 2
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- 231100000053 low toxicity Toxicity 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
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- 241000894007 species Species 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- LRWZZZWJMFNZIK-UHFFFAOYSA-N 2-chloro-3-methyloxirane Chemical compound CC1OC1Cl LRWZZZWJMFNZIK-UHFFFAOYSA-N 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- 229920002101 Chitin Polymers 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 206010018498 Goitre Diseases 0.000 description 1
- 241000219146 Gossypium Species 0.000 description 1
- 229920001732 Lignosulfonate Polymers 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 206010034133 Pathogen resistance Diseases 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
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- 235000009508 confectionery Nutrition 0.000 description 1
- 239000013530 defoamer Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
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- 230000000857 drug effect Effects 0.000 description 1
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- 235000013305 food Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 201000003872 goiter Diseases 0.000 description 1
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- 210000004209 hair Anatomy 0.000 description 1
- 208000006278 hypochromic anemia Diseases 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
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- 150000002923 oximes Chemical class 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
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- 229920001568 phenolic resin Polymers 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229940051841 polyoxyethylene ether Drugs 0.000 description 1
- 229920000056 polyoxyethylene ether Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 1
- 230000007115 recruitment Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000001587 sorbitan monostearate Substances 0.000 description 1
- 229940035048 sorbitan monostearate Drugs 0.000 description 1
- 235000011076 sorbitan monostearate Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a pesticide composition containing flufenoxuron and fenproximate. The ratio of flufenoxuron to fenproximate in parts by weight in the pesticide is 1: (1-10). The pesticide composition disclosed by the invention has obvious synergic effect, application dosage of pesticide is reduced, manpower and material resource are saved, and environmental pollution of the pesticide is reduced, thus the pesticide composition is applicable to preventing and controlling red spiders on fruit trees.
Description
Technical field
The present invention relates to a kind of composition pesticide, active ingredient is flufenoxuron and azoles mite ester, is used for control fruit tree two spotted spider mite.
Background technology
The resistance problem of pest is a global problem, is the emphasis problem that the agricultural science and technology worker pays close attention to always.Along with the continuity year in year out of insect chemical control, increase and the non-science of agricultural chemicals usage amount are used agricultural chemicals, pest resistance is serious day by day, and the pest species that produces resistance is on the increase.
Owing to use agricultural chemicals improper, harmful mite is developed immunity to drugs after the sixties, the natural enemy population reduces, and the ecosystem is destroyed, and causes two spotted spider mite to become the most serious harmful mite of harm on the present fruit tree, and often wildness is caused disaster.To become mite, to be clustered in thorn suction juice on oranges and tangerines blade, spray and the fruit as if mite, young mite.Killed blade presents many canescence flecks, and full leaf canescence when serious causes a large amount of fallen leaves and spike top, influences tree vigo(u)r and output.During rampant the generation, fruit surface is covered with canescence chlorosis spot, and full fruit is pale, influences output.
Therefore, be badly in need of the control medicament of the two spotted spider mite of efficient, low toxicity, environmental protection.
Flufenoxuron belongs to the benzoyl area kind insect growth regulator, IGR, is chitin synthesis inhibitor, the equal tool characteristic of its insecticidal activity, insecticidal spectrum and speed of action, and good blade face anelasticity is arranged.Especially mite and the insect to mezzanine level has high activity, be widely used on oranges and tangerines, cotton, grape, soybean, fruit tree, king's rice and the coffee, planting property of control food mite class (thorn goitre mite, short hairs mite, Panonychus citri, rust mite, tetranychus telarius etc.) and many other insects, and good lasting effect is arranged, to predacious mite and insect safety.There is not the cross resistance problem with other existing miticides.
Azoles mite ester is the oximes miticide, and the E body is than Z body acaricidal activity height, and the mode of action has knocking down and suppresses decorticating based on action of contace poison.It is wide to kill the mite spectrum, and has the desinsection effect of curing the disease concurrently.It is fast to kill mite speed.Azoles mite ester is used very extensive in China, brought into play important function in agriculture control of pest mite.But because the mixture listing that contains azoles mite ester is in a large number added in single use and using by turns with other miticides year after year, made the harmful mite in some areas produce pesticide resistance.
Being mixed of different pesticide species is the common methods of the agriculture resistant insect of control.By the formulation of pesticide screening, filter out rational prescription, can effectively improve actual control efficiency, reduce dosage, reduce cost, delay the generation of pest resistance to insecticide, prolong the service life of medicament, be the important means of the insect comprehensive regulation.The control fruit tree two spotted spider mite that is mixed of flufenoxuron and azoles mite ester does not still have report at present and uses.
Summary of the invention
The technical problem that the present invention solves provide a kind of efficient, low toxicity and the lasting period long, can effectively prevent and treat the fruit tree two spotted spider mite, be conducive to the composition pesticide that contains flufenoxuron and azoles mite ester of the insect comprehensive regulation.
For addressing the above problem, the technical solution adopted in the present invention is: a kind of composition pesticide that contains flufenoxuron and azoles mite ester, and the ratio of weight and number of flufenoxuron and azoles mite ester is 1:1～1:10, preferably, the ratio of weight and number of worm urea and azoles mite ester is 1:1～1:5.
Described composition pesticide can be selected suitable auxiliary agent for use according to well known to a person skilled in the art method, is mixed with: the application forms that suitable agricultural such as missible oil, suspending agent, aqueous emulsion, microemulsion is used.
Described composition pesticide also contains the required usual auxiliaries of preparation pesticidal preparations, usual auxiliaries is one or more the mixing in solvent, emulsifier, wetting agent, stabilizing agent, dispersant, thickener, PH conditioning agent, defoamer, antifreezing agent, the packing agent etc., be known substance, be various auxiliary agents commonly used in the pesticidal preparations, can change to some extent according to different situations, be not particularly limited.
Described composition pesticide is used for control fruit tree two spotted spider mite.
Composition pesticide described in the invention can the finished product preparation form provide, and namely each material mixes in the composition, and the composition of composition also can single agent form provide, and directly mixes in bucket or jar before the use, is diluted to desired concn then.
Composition pesticide provided by the invention adopts the method for spraying to use usually, also can adopt agricultural to go up other operation techniques of using as required.
Compared with prior art, the present invention has following beneficial effect: 1, composition pesticide provided by the invention, in certain ratio range, show obvious synergistic effect, the control efficiency of composition is significantly improved than single agent, reduce using dosage, dispenser recruitment and the cost of agricultural chemicals simultaneously, also reduced influence and residue of pesticide to environment.
2, the active ingredient mechanism of action of composition pesticide provided by the invention has nothing in common with each other, and the application of composition can delay or overcome the generation of pest resistance to insecticide, prolongs the service life of medicament, is conducive to the comprehensive regulation of insect.
3, Pesticidal combination provided by the invention is to crops safety.
Embodiment
In order to make purpose of the present invention, technical scheme and advantage more short and sweet, the present invention describes with following specific embodiment, but the present invention only limits to these examples absolutely not.The following stated only is the present invention embodiment preferably, only is used for describing the present invention, can not be interpreted as the restriction to scope of the present invention.Should be pointed out that all any modifications of making within the spirit and principles in the present invention, be equal to replacement and improvement etc., all should be included within protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
In following examples, unless otherwise indicated, all percentages all are weight percentage.
FORMULATION EXAMPLE 1:Take by weighing 2% flufenoxuron, 10% azoles mite ester, 3% farming breast, 600,3% farming breast, 2201,3% lignosulfonates, 0.2% xanthans, 6% ethylene glycol, 0.5% organosilicon, add deionized water and mend to 100%.After the above-mentioned raw materials mixing, emulsification makes 12% flufenoxuron Enpyfoximate dispersant through high speed shear.
FORMULATION EXAMPLE 2:Take by weighing 1% flufenoxuron, 10% azoles mite ester, 5% Nongru-700 #, 2% Tween-60 #, 2% alkylphenol-polyethenoxy base ether formaldehyde condensation products phosphate, 5% propane diols, 0.2% xanthans.After the above-mentioned raw materials mixing, emulsification makes 11% flufenoxuron Enpyfoximate dispersant through high speed shear.
FORMULATION EXAMPLE 3:Take by weighing 6% flufenoxuron, 6% azoles mite ester, 4% agricultural newborn 500#, 3%Span-60#(sorbitan monostearate), 3% agricultural newborn 2201#, 2% triphenyl phosphite, dimethylbenzene mends 100%.Above-mentioned raw materials is mixed back abundant dissolving mixing make 12% flufenoxuron azoles mite emulsifiable concentrate.
FORMULATION EXAMPLE 4:Take by weighing 2% flufenoxuron, 14% azoles mite ester, 4% Nongru-700 #(alkyl phenol formaldehyde resin polyoxyethylene ether), 6% agricultural newborn 2201#, 2% agricultural newborn 1601#, 1.5% triphenyl phosphite, dimethylbenzene mends 100%.Above-mentioned raw materials is mixed the abundant mixing in back make 16% flufenoxuron azoles mite emulsifiable concentrate.
FORMULATION EXAMPLE 5:Take by weighing 5% flufenoxuron, 10% azoles mite ester, the farming of 6% emulsifier newborn 500#, 2% agricultural newborn 2201#, 3% agricultural newborn 600#, 1% methyl alcohol, 6% dimethylbenzene, 1.2% epoxychloropropane, 0.4% aceticanhydride, deionized water is mended to 100%, above-mentioned raw materials is fully dissolved mixing makes 15% flufenoxuron azoles mite ester microemulsion.
FORMULATION EXAMPLE 6:Taking by weighing 3% flufenoxuron, 7% azoles mite ester, 3% agricultural newborn 2201#, 2% Arlacel-60 #, 5% agricultural newborn 1601#, 1% acetone, 6.5% dimethylbenzene, 1% solvent naphtha S-150,0.8% triphenyl phosphite, deionized water mends to 100%.Above-mentioned raw materials is fully dissolved mixing make 10% flufenoxuron azoles mite ester microemulsion.
FORMULATION EXAMPLE 7:Taking by weighing 2% flufenoxuron, 10% azoles mite ester, 6% agricultural newborn 600# phosphate, 2% Tween-60 #, 3% agricultural newborn 600#, 8% dimethylbenzene, 1% triphenyl phosphite, 2% ethylene glycol, 1.5% xanthans, 0.8% polyvinyl alcohol, 0.2% benzoic acid, deionized water mends to 100%.Above-mentioned raw materials is fully dissolved the mixing shearing make 12% flufenoxuron azoles mite ester aqueous emulsion.
Field control effectiveness test embodiment 1:One oranges and tangerines garden carry out citrus red mite field control effectiveness test in September, 2010 in the Huizhou City, Guangdong Province with above-mentioned FORMULATION EXAMPLE 1:12% flufenoxuron Enpyfoximate dispersant.
12% flufenoxuron Enpyfoximate dispersant adopts 1500,2000,2500 times of liquid even spraying, with 1500 times of liquid of 5% flufenoxuron dispersible agent and 2000 times of liquid of 5% Enpyfoximate dispersant medicament in contrast.Investigation insect population radix before the dispenser was investigated residual insect population number in 1 day, 3 days, 7 days, 15 days, 30 days respectively behind the medicine.Five point samplings are adopted in investigation, five leaf investigation records of each some picked at random.The control efficiency computational methods are as follows: control efficiency (%)=(1-CK
1* Pt
1/ CK
2* Pt
2) * 100.Wherein: CK
1Represent the preceding insect population number of check plot medicine; CK
2Represent insect population number behind the medicine of check plot; Pt
1Represent the preceding insect population number for the treatment of region medicine; Pt
2Represent insect population number behind the treatment region medicine.
Table 1 is 12% flufenoxuron Enpyfoximate dispersant control citrus red mite result of the test.
Field control effectiveness test embodiment 2:One oranges and tangerines garden carry out citrus red mite field control effectiveness test in August, 2010 in Chengdu, Sichuan with above-mentioned FORMULATION EXAMPLE 6:10% flufenoxuron azoles mite ester microemulsion.
10% flufenoxuron azoles mite ester microemulsion adopts 1500,2000,2500 times of liquid even spraying, with 1500 times of liquid of 5% flufenoxuron dispersible agent and 2000 times of liquid of 5% Enpyfoximate dispersant medicament in contrast.Investigation insect population radix before the dispenser was investigated residual insect population number in 1 day, 3 days, 7 days, 15 days, 30 days respectively behind the medicine.Five point samplings are adopted in investigation, five leaf investigation records of each some picked at random.The control efficiency computational methods are as follows: control efficiency (%)=(1-CK
1* Pt
1/ CK
2* Pt
2) * 100.Wherein: CK
1Represent the preceding insect population number of check plot medicine; CK
2Represent insect population number behind the medicine of check plot;
Pt
1Represent the preceding insect population number for the treatment of region medicine; Pt
2Represent insect population number behind the treatment region medicine.
Table 2,10% flufenoxuron azoles mite ester microemulsion control citrus red mite result of the test.
Field control effectiveness test embodiment 3:Carry out European red mite field control effectiveness test in October, 2009 in one apple orchard, Tai, Shandong Province with above-mentioned FORMULATION EXAMPLE 7:12% flufenoxuron azoles mite ester aqueous emulsion.
12% flufenoxuron azoles mite ester aqueous emulsion adopts 1500,2000,2500 times of liquid even spraying, with 1500 times of liquid of 5% flufenoxuron dispersible agent and 2000 times of liquid of 5% Enpyfoximate dispersant medicament in contrast.Investigation insect population radix before the dispenser was investigated residual insect population number in 1 day, 3 days, 7 days, 15 days, 30 days respectively behind the medicine.Five point samplings are adopted in investigation, five leaf investigation records of each some picked at random.The control efficiency computational methods are as follows: control efficiency (%)=(1-CK
1* Pt
1/ CK
2* Pt
2) * 100.
Wherein: CK
1Represent the preceding insect population number of check plot medicine; CK
2Represent insect population number behind the medicine of check plot; Pt
1Represent the preceding insect population number for the treatment of region medicine; Pt
2Represent insect population number behind the treatment region medicine.
Table 3 is 12% flufenoxuron azoles mite ester aqueous emulsion control European red mite result of the test.
From the result of the test of above field control effectiveness test embodiment as can be seen, flufenoxuron azoles mite ester composition pesticide of the present invention is outstanding to apple, citrus red mite control efficiency, and composition still is that the persistence of drug effect all has significant improvement than single agent from quick-acting.By to 7 days preventive effect analysis behind the medicine, it is remarkable to handle differences, and there are significant difference in the preventive effect of single agent and flufenoxuron azoles mite ester composition pesticide.Simultaneously, medicament is safe to fruit tree in the process of the test, to not influence of natural enemy.It is a kind of pesticide species that is worth of widely use.
Claims (2)
1. composition pesticide that contains flufenoxuron and azoles mite ester, it is characterized in that, active ingredient wherein is: flufenoxuron and azoles mite ester, percentage by weight is: 3% flufenoxuron, 7% azoles mite ester, 3% agricultural newborn 2201#, 2% Arlacel-60 #, 5% agricultural newborn 1601#, 1% acetone, 6.5% dimethylbenzene, 1% solvent naphtha S-150,0.8% triphenyl phosphite, deionized water are mended to 100%, are 10% flufenoxuron azoles mite ester microemulsion.
2. a kind of composition pesticide that contains flufenoxuron and azoles mite ester according to claim 1 is characterized in that for the control citrus red mite.
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| CN103734193A (en) * | 2013-12-31 | 2014-04-23 | 灵川县金田农资经营部 | Biogas slurry composite pesticide for preventing and treating red spider |
| CN107467044A (en) * | 2015-09-22 | 2017-12-15 | 祝蓉杰 | The compound method of AVM fenpyroximate flufenoxuron suspending agent |
| CN105145605A (en) * | 2015-10-08 | 2015-12-16 | 广西南宁益土生物科技有限责任公司 | Pesticide composition containing fenpyroximate and flufenoxuron |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1486136A (en) * | 2000-11-10 | 2004-03-31 | �ݶ�ũ�����ѧ�ɷݹ�˾ | Active agent combinations with insecticidal and acaricidal properties |
| CN101485325A (en) * | 2009-02-26 | 2009-07-22 | 陕西韦尔奇作物保护有限公司 | Miticide composition containing tebufenpyrad |
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| CN1554233A (en) * | 1994-06-08 | 2004-12-15 | �����ɷ� | Synergistic composition |
| CN1332610C (en) * | 2004-03-24 | 2007-08-22 | 北京华京五方实用纳米科技开发有限公司 | Pesticide microemulsion |
| CN100563447C (en) * | 2005-03-28 | 2009-12-02 | 北京华京五方实用纳米科技开发有限公司 | A kind of aqueous pesticide and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1486136A (en) * | 2000-11-10 | 2004-03-31 | �ݶ�ũ�����ѧ�ɷݹ�˾ | Active agent combinations with insecticidal and acaricidal properties |
| CN101485325A (en) * | 2009-02-26 | 2009-07-22 | 陕西韦尔奇作物保护有限公司 | Miticide composition containing tebufenpyrad |
Non-Patent Citations (2)
| Title |
|---|
| 13种杀螨剂对柑桔红蜘蛛田间防效评价;陆恒等;《广东农业科学》;20091231(第09期);第98页末尾3行、第107段左栏 * |
| 陆恒等.13种杀螨剂对柑桔红蜘蛛田间防效评价.《广东农业科学》.2009,(第09期),第98页末尾3行、第107段左栏. |
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