CN102268816A - Preparation method for water-washable silk quilt with effects of aloe skin care and negative ions - Google Patents
Preparation method for water-washable silk quilt with effects of aloe skin care and negative ions Download PDFInfo
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Abstract
The invention discloses a preparation method for water-washable silk quilt with effects of aloe skin care and negative ions. The quilt is characterized in that: 100% natural silk is adopted; an aloe extract, tourmaline microparticles or a sol finishing solution prepared through a sol-gel method are processed on the quilt cover on the base of the silk quilt core prepared through the prior art. According to the present invention, the 100% natural silk is selected; the silk quilt is finely prepared through the unique scientific process; the silk quilt has characteristics of close fitting, health care and the like; the aloe extract, the tourmaline microparticles or the sol finishing solution prepared through the sol-gel method are processed on the quilt cover on the base of the silk quilt core prepared through the prior art, such that the health function of the silk quilt is further improved; the aloe is adopted in the field of mill, and the skin-care function is assigned to the textile, such that a new creation is provided for the field of the mill.
Description
Technical field
The present invention relates to house and spin series products making field, be specifically related to the preparation method that a kind of aloe skin care anion can be washed cocoon silk quilt.
Background technology
Silk be the occurring in nature collection light, gentle, carefully be the natural fabric of one, have the good reputation of " human body second skin ", be called by industry " fiber queen ".Its main component is the pure natural animal protein fibre, includes the necessary amino acid of multiple human body, have windproof, dehumidify, calm the nerves, the effect of nourishing and balance human skin.Silk compliance and warmth retention property are splendid, and are easy to absorb and sweat gas that the people's that dialyses health produces in deep sleep.Silk is smooth, ventilative, soft, moisture absorption, not perverse itch and characteristics such as antistatic make it become the superior material for making clothes of making underclothes, and has more advantageous quality and advantages such as warming, fluffy soft, ventilative health care next to the shin with silk as the cocoon silk quilt of endoplasm.Cocoon silk quilt is to build the most comfortable quilt.
Through scientific analysis, aloe contains necessary 8 seed amino acids of a large amount of vegetable proteins, vitamin A, B6, B12 and human skin and mineral matter.In 75 kinds of known compositions, prove to account for 2/3 to what beautifying had a peculiar function.Wherein 25 kinds of organized enzymes help the function of body metabolism and moist skin.Through experimental results demonstrate, aloe to strengthen skin elasticity and toughness, make the skin soft smooth, the glamour that retains youth has peculiar effect.
Air is made up of countless molecules, atom, after airborne molecule or atom lose or obtain electronics, just forms charged particle, is called ion; The positively charged cation that cries, the electronegative anion that cries.Anion is verified by clinical practice by domestic and international medical circle expert to people's health, longevity and ecological significant impact.Pollute few place in forest, beach, waterfall, countryside etc., contain a large amount of anion air, its concentration is seriously polluted urban hundred times, here people can feel with fresh air, breathe happy, relaxation and happiness, relaxed and joyful, Here it is, and convalescence center all is located at mountain forest, beach, waterfall basic reason on every side, and this is the effect that numerous anion air produce.Therefore anion air is referred to as " long-lived plain " or " air vitamin " by people.
In addition, the anion that is produced by oxygen in the air has higher activity and very strong redox.This interaction energy destroys the cell membrane of bacterium or the activity of cellular plasm organized enzyme, thereby reaches antibiotic and purpose sterilization.This shows that suck an amount of anion every day, of great advantage to health.
Summary of the invention
Technical problem to be solved by this invention is that some the row special performances with the senile-resistant efficacy of health care skin moisten effect of aloe and anion and cocoon silk quilt combine, and provides the preparation method that a kind of aloe skin care anion can be washed cocoon silk quilt.
This method is selected 100% pure natural silk for use; on the core basis that at present existing technology is made; with aloe extract, the colloidal sol dressing liquid of the inorganic oxide of tourmaline particles or sol-gel process preparation is handled and is put, and the health-care effect of cocoon silk quilt is further promoted.
At the extraction of above-mentioned aloe active ingredient this on the one hand, further can extract, concentrate, distillation, fractionation or decompression distillation, supercritical fluid isolation technics by organic chemistry, extraction aloe composition separates, concentrated effective aloe composition.Or with the vacuumize of aloe material or freeze drying, pulverizing, dispersion, preparation nano aloe particle, key technology is to select suitable dispersant and consumption thereof to guarantee the dispersed and stable of nano particle.
At above-mentioned with the aloe be main component composite finishing agent preparation and use this on the one hand, can the aloe composite finishing agent be uniformly applied in the fiber by technology such as spray, flood, pad, with the uniformity and the durability of assurance antiseptic.
At the selection of above-mentioned dispersant and consumption thereof this on the one hand, through data-searching widely and a large amount of experiments, when the preparation composite finishing agent, receive in the dressing liquid select TW-80, its consumption be aloe total amount 5% as dispersion stabilizer.
In fiber, apply technology at above-mentioned aloe composite finishing agent, under the room temperature condition contain PU (3-5% adds aloe complex antimicrobials 2-4% (o.w.f); bath raio 1: 15 in dressing liquid o.w.f); adjust pH value 4-5, add fiber, begin to be warming up to 50 ℃; tapping behind the 30-40min is handled in insulation; fiber dewatering (moisture content 80%-85%), dry then (110 ℃, 3min); bake (110 ℃, 3min).Under such technology, finishing agent is by setting up firm chemical bond between crosslinking agent and fiber molecule, makes the fabric after the processing have good washing resistance, and do not influence the product feel.
The technology of the present invention is on the other hand improved, use a kind of special water-repelling agent to silk through the row hydrophobic treatments, make the silk fiber periphery apply the last layer hydrophobic substance, in washing, can avoid silk fiber to contact, under the effect of hydrone, be connected to each other and form the feel that hardens thereby be unlikely to silk fiber with the direct of water.
In order to realize the foregoing invention purpose, concrete production stage is as follows:
(1) stuffing is 100% silk
(2) making of core
Technological process: lining inspects → opens tailor's system → raw material by random samples and weigh → and proportioning mixing → shredding comb and parallel cotton fibers prior to spinning → wind send and fills suede/comb and parallel cotton fibers prior to spinning lapping/no glue setting → can and coat → seal quilting → test package → finished product warehouse-in
(3) extraction of aloe active ingredient and preparation
(4) preparation of aloe composite finishing liquid
(5) the aloe postfinishing process uses and pads or impregnation method
(6) put in order behind the anion
(7) use water-repelling agent to silk through the row hydrophobic treatments
The present invention has following beneficial effect and substantive distinguishing features:
The cocoon silk quilt that this method is made keep that original cocoon silk quilt is ventilative, soft, moisture absorption, not perverse itch and characteristics such as antistatic in, because aloe extract has been gone up in the back arrangement and anion makes it have the anti-ageing function of waiting for a long time of skin moisten again concurrently, and aloe is applied to field of textiles, and giving textiles skin makeup function is a new bright spot.Simultaneously, the silk packing material through hydrophobic treatments, can be directly used in washing and not harden, not influence bulking intensity, for use provides can many facilities.
The specific embodiment
Below embodiments of the invention are elaborated: present embodiment has provided detailed embodiment and process being to implement under the prerequisite with the technical solution of the present invention, but protection scope of the present invention is not limited to following embodiment.
Embodiment 1:
The preparation that a kind of aloe skin care anion can be washed cocoon silk quilt:
(1) stuffing is 100% silk.
(2) making of core:
Technological process: lining inspects → opens tailor's system → raw material by random samples and weigh → and proportioning mixing → shredding comb and parallel cotton fibers prior to spinning → wind send and fills suede/comb and parallel cotton fibers prior to spinning lapping/no glue setting → can and coat → seal quilting → test package → finished product warehouse-in.
(3) extraction of aloe active ingredient and preparation:
By organic chemistry extraction, concentrate, distillation, fractionation or decompression distillation, supercritical fluid isolation technics, extraction aloe composition, separate, concentrate effective aloe composition, or with the vacuumize of aloe material or freeze drying, pulverizing, dispersion, preparation nano aloe particle.
(4) preparation of aloe composite finishing liquid
Selecting TW-80 in the dressing liquid is dispersant, its consumption be aloe total amount 5%.
(5) aloe postfinishing process:
Pad technology: pad aloe dressing liquid → dry → bake
Concrete technology is as follows: at first pad the aloe dressing liquid, (3-5% adds aloe complex antimicrobials 2-4% (o.w.f), bath raio 1: 15 in dressing liquid o.w.f) containing PU under the room temperature condition, adjust pH value 4-5, add fiber, begin to be warming up to 50 ℃, tapping behind the insulation processing 30-40min, oven dry is (110 ℃ then, 3min), bake (110 ℃, 3min).
(6) anion postfinishing process:
Lining is immersed in the solution of tourmaline particles and adhesive resin the adhesion amount that makes inorganic matter particulate in the lining and aloe extract reach regulation with the mode of extruding.Perhaps adopt the colloidal sol dressing liquid of the inorganic oxide of sol-gel process preparation, generate the gel layer that contains nano particle or micropore, under the state of friction, make fabric discharge anion at fabric face.
(7) use a kind of special water-repelling agent to silk through the row hydrophobic treatments, make the silk fiber periphery apply the last layer hydrophobic substance, in washing, can avoid silk fiber to contact, under the effect of hydrone, be connected to each other and form the feel that hardens thereby be unlikely to silk fiber with the direct of water.
The anion function that carries out to the cocoon silk quilt that finally makes detects, and the anion burst size has reached 4000～4800/cm
3, magnetic field intensity reaches 03～0.5 Gauss.
Embodiment 2:
The preparation that a kind of aloe skin care anion can be washed cocoon silk quilt:
(1) stuffing is 100% silk.
(2) making of core:
Technological process: lining inspects → opens tailor's system → raw material by random samples and weigh → and proportioning mixing → shredding comb and parallel cotton fibers prior to spinning → wind send and fills suede/comb and parallel cotton fibers prior to spinning lapping/no glue setting → can and coat → seal quilting → test package → finished product warehouse-in.
(3) extraction of aloe active ingredient and preparation:
By organic chemistry extraction, concentrate, distillation, fractionation or decompression distillation, supercritical fluid isolation technics, extraction aloe composition, separate, concentrate effective aloe composition, or with the vacuumize of aloe material or freeze drying, pulverizing, dispersion, preparation nano aloe particle.
(4) preparation of aloe composite finishing liquid
Selecting TW-80 in the dressing liquid is dispersant, its consumption be aloe total amount 5%.
(5) aloe postfinishing process:
Impregnation technology: flood → dewater → dry → bake
Concrete technology is as follows: at first flood the aloe dressing liquid, under the room temperature condition contain PU (3-5% adds aloe complex antimicrobials 2-4% (o.w.f); bath raio 1: 15 in dressing liquid o.w.f); adjust pH value 4-5, add fiber, begin to be warming up to 50 ℃; tapping behind the 30-40min is handled in insulation; fiber dewatering (moisture content 80%-85%), dry then (110 ℃, 3min); bake (110 ℃, 3min).
(6) anion postfinishing process:
Lining is immersed in the solution of tourmaline particles and adhesive resin the adhesion amount that makes inorganic matter particulate in the lining and aloe extract reach regulation with the mode of extruding.Perhaps adopt the colloidal sol dressing liquid of the inorganic oxide of sol-gel process preparation, generate the gel layer that contains nano particle or micropore, under the state of friction, make fabric discharge anion at fabric face.
(7) use a kind of special water-repelling agent to silk through the row hydrophobic treatments, make the silk fiber periphery apply the last layer hydrophobic substance, in washing, can avoid silk fiber to contact, under the effect of hydrone, be connected to each other and form the feel that hardens thereby be unlikely to silk fiber with the direct of water.
The anion function that carries out to the cocoon silk quilt that finally makes detects, and the anion burst size has reached 4500～5000/cm
3, magnetic field intensity reaches 0.2～0.56 Gauss.
More than show and described basic principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that describes in the foregoing description and the specification just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (11)
1. preparation method that aloe skin care anion can be washed cocoon silk quilt; it is characterized in that; select 100% pure natural silk for use; on the silk core basis that at present existing technology is made; with aloe extract, the colloidal sol dressing liquid of the inorganic oxide of tourmaline particles or sol-gel process preparation is handled and is put.
2. the preparation method that a kind of aloe skin care anion according to claim 1 can be washed cocoon silk quilt is characterized in that, its preparation technology's flow process comprises following seven steps:
(1) stuffing is 100% silk;
(2) making of core
Technological process: lining inspects → opens tailor's system → raw material by random samples and weigh → and proportioning mixing → shredding comb and parallel cotton fibers prior to spinning → wind send and fills suede/comb and parallel cotton fibers prior to spinning lapping/no glue setting → can and coat → seal quilting → test package → finished product warehouse-in;
(3) extraction of aloe active ingredient and preparation;
(4) preparation of aloe composite finishing liquid;
(5) aloe postfinishing process: pad aloe dressing liquid → dry → bake;
(6) anion postfinishing process:
(7) with water-repelling agent to silk through the row hydrophobic treatments, at the peripheral last layer hydrophobic substance that applies of silk fiber.
3. the preparation method that a kind of aloe skin care anion according to claim 2 can be washed cocoon silk quilt, it is characterized in that the extracting method in the step (3) can be: organic chemistry extraction, concentrate, a kind of or several combination in distillation, fractionation or decompression distillation, the supercritical fluid isolation technics.
4. the preparation method that a kind of aloe skin care anion according to claim 2 can be washed cocoon silk quilt is characterized in that, in the aloe dressing liquid, selection TW-80 is a dispersant in the step (4), its consumption be aloe total amount 5%.
5. the preparation method that a kind of aloe skin care anion according to claim 2 can be washed cocoon silk quilt, it is characterized in that, finishing technique in the step (5) is specially: at first pad the aloe dressing liquid, containing PU (3-5% under the room temperature condition, o.w.f) add aloe complex antimicrobials 2-4% (o.w.f) in the dressing liquid; bath raio 1: 15; adjust pH value 4-5; add fiber, begin to be warming up to 50 ℃, tapping behind the insulation processing 30-40min; oven dry then (110 ℃; 3min), bake (110 ℃, 3min).
6. the preparation method that a kind of aloe skin care anion according to claim 2 can be washed cocoon silk quilt, it is characterized in that, the anion postfinishing process is specially in the step (6): lining is immersed in the solution of tourmaline particles and adhesive resin the adhesion amount that makes inorganic matter particulate in the lining and aloe extract reach regulation with the mode of pushing.Perhaps adopt the colloidal sol dressing liquid of the inorganic oxide of sol-gel process preparation, generate the gel layer that contains nano particle or micropore, under the state of friction, make fabric discharge anion at fabric face.
7. the preparation method that a kind of aloe skin care anion according to claim 1 can be washed cocoon silk quilt is characterized in that, its preparation technology's flow process comprises following seven steps:
(1) stuffing is 100% silk;
(2) making of core
Technological process: lining inspects → opens tailor's system → raw material by random samples and weigh → and proportioning mixing → shredding comb and parallel cotton fibers prior to spinning → wind send and fills suede/comb and parallel cotton fibers prior to spinning lapping/no glue setting → can and coat → seal quilting → test package → finished product warehouse-in;
(3) extraction of aloe active ingredient and preparation;
(4) preparation of aloe composite finishing liquid;
(5) aloe postfinishing process: dipping aloe dressing liquid → dewater → dry → bake;
(6) anion postfinishing process:
(7) with water-repelling agent to silk through the row hydrophobic treatments, at the peripheral last layer hydrophobic substance that applies of silk fiber.
8. the preparation method that a kind of aloe skin care anion according to claim 7 can be washed cocoon silk quilt, it is characterized in that the extracting method of age can be in the step (3): the organic chemistry extraction, concentrate, a kind of or several combination in distillation, fractionation or decompression distillation, the supercritical fluid isolation technics.
9. the preparation method that a kind of aloe skin care anion according to claim 7 can be washed cocoon silk quilt is characterized in that, in the aloe dressing liquid, selection TW-80 is a dispersant in the step (4), its consumption be aloe total amount 5%.
10. the preparation method that a kind of aloe skin care anion according to claim 7 can be washed cocoon silk quilt, it is characterized in that, finishing technique in the step (5) is specially: at first flood the aloe dressing liquid, containing PU (3-5% under the room temperature condition, o.w.f) add aloe complex antimicrobials 2-4% (o.w.f) in the dressing liquid; bath raio 1: 15; adjust pH value 4-5, add fiber, begin to be warming up to 50 ℃; tapping behind the insulation processing 30-40min; fiber dewatering (moisture content 80%-85%), oven dry then (110 ℃, 3min); bake (110 ℃, 3min).
11. the preparation method that a kind of aloe skin care anion according to claim 7 can be washed cocoon silk quilt, it is characterized in that, the anion postfinishing process is specially in the step (6): lining is immersed in the solution of tourmaline particles and adhesive resin the adhesion amount that makes inorganic matter particulate in the lining and aloe extract reach regulation with the mode of pushing.Perhaps adopt the colloidal sol dressing liquid of the inorganic oxide of sol-gel process preparation, generate the gel layer that contains nano particle or micropore, under the state of friction, make fabric discharge anion at fabric face.
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| CN104631102A (en) * | 2015-02-15 | 2015-05-20 | 浙江兆新织造有限公司 | Aloe anion skin-care quilt cover fabric |
| CN104773703A (en) * | 2015-03-24 | 2015-07-15 | 金东奎 | Method for manufacturing article of daily use for home and travelling, and a mineral filling method thereof |
| CN104970629A (en) * | 2015-06-29 | 2015-10-14 | 界首市贝特纺织有限公司 | Method for preparing aloe silk-like cotton healthy comforter batt |
| CN104997348A (en) * | 2015-06-29 | 2015-10-28 | 界首市贝特纺织有限公司 | Silk corn fiber blended antibacterial health-caring batt |
| CN105019225A (en) * | 2015-08-06 | 2015-11-04 | 苏州丝之源纺织科技有限公司 | Preparation method for silk quilt inner capable of generating anions |
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| CN107916559A (en) * | 2017-11-27 | 2018-04-17 | 无锡昊瑜节能环保设备有限公司 | A kind of Silk Fabric Finishing technique that antistatic finishing agent is fixed using sol-gal process |
| CN108754857A (en) * | 2018-05-15 | 2018-11-06 | 苏州先蚕丝绸有限公司 | Functional silk quilt |
| CN109171351A (en) * | 2018-09-11 | 2019-01-11 | 倪学林 | A kind of washing silk quilt and its manufacture craft |
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| CN104631102A (en) * | 2015-02-15 | 2015-05-20 | 浙江兆新织造有限公司 | Aloe anion skin-care quilt cover fabric |
| CN104773703A (en) * | 2015-03-24 | 2015-07-15 | 金东奎 | Method for manufacturing article of daily use for home and travelling, and a mineral filling method thereof |
| CN104970629A (en) * | 2015-06-29 | 2015-10-14 | 界首市贝特纺织有限公司 | Method for preparing aloe silk-like cotton healthy comforter batt |
| CN104997348A (en) * | 2015-06-29 | 2015-10-28 | 界首市贝特纺织有限公司 | Silk corn fiber blended antibacterial health-caring batt |
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| CN106676882A (en) * | 2016-12-12 | 2017-05-17 | 广西凯喜雅丝绸有限公司 | Method for producing elastic swelling silk cotton quilt |
| CN106667164A (en) * | 2016-12-12 | 2017-05-17 | 广西凯喜雅丝绸有限公司 | Method for producing silk cotton quilt |
| CN107604651A (en) * | 2017-09-22 | 2018-01-19 | 南通优棉濠晨纺织品有限公司 | A kind of negative ion health fabric and its soaking agent and application |
| CN107916559A (en) * | 2017-11-27 | 2018-04-17 | 无锡昊瑜节能环保设备有限公司 | A kind of Silk Fabric Finishing technique that antistatic finishing agent is fixed using sol-gal process |
| CN108754857A (en) * | 2018-05-15 | 2018-11-06 | 苏州先蚕丝绸有限公司 | Functional silk quilt |
| CN109171351A (en) * | 2018-09-11 | 2019-01-11 | 倪学林 | A kind of washing silk quilt and its manufacture craft |
| CN111535028A (en) * | 2020-04-23 | 2020-08-14 | 罗莱生活科技股份有限公司 | Durable skin-care fabric and preparation method and application thereof |
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Inventor after: Jin Yiting Inventor after: Li Yujie Inventor after: Song Chunchang Inventor before: Li Yujie Inventor before: Song Chunchang |