CN102250731A - Raw materials of health preserving white spirit, dendrobium health preserving white spirit and manufacturing method thereof - Google Patents
Raw materials of health preserving white spirit, dendrobium health preserving white spirit and manufacturing method thereof Download PDFInfo
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Abstract
The invention relates to the field of health food and particularly relates to raw materials of a health preserving white spirit, a dendrobium health preserving white spirit and a manufacturing method thereof. The raw materials of the health preserving liquor are characterized by comprising the following components in parts by weight: 1-3 parts of dendrobium, 1-3 parts of rhizoma polygonatum and 1-2 parts of medlar. According to the invention, three types of medicine food homology plant raw materials are reasonably collated to serve as the raw materials of the health preserving white spirit for developing dendrobium nectar, and the dendrobium health preserving white spirit provided by the invention is higher in market value; and meanwhile, the preparation process disclosed by the invention is a combination of a modern food new technology and the traditional method, a multilevel coupling clarification technology is adopted, and a chemical clarification technology and an ultrafiltration clarification technology are jointly applied to the production of white spirit products, thus the precipitation can be effectively eliminated, the product quality can be ensured and the technical problem existing in the liquor production in the prior art can be better solved.
Description
Technical field
The present invention relates to field of health care food, specifically relate to a kind of health liquor raw material, and prepared stem of noble dendrobium health liquor; Simultaneously, the invention also discloses the preparation method of stem of noble dendrobium health liquor.
Background technology
The stem of noble dendrobium belongs to the orchid family Dendrobium per nnial herb, has sleeping, defaecation, improves skin, helps digest, multiple efficacies such as antitumor, anti-cataract.At present, the processing technology of China's stem of noble dendrobium product is also relatively weaker, and product category also seldom.
Along with the raising of people's living standard, health liquor with health role is subjected to domestic consumer's approval.At present according to statistics, health liquor just grows steadily with annual tempo more than 30%.To have the plant stem of noble dendrobium of multi-efficiency, and be applied in the health liquor, be a technology that is worth research, still is not reported both at home and abroad at present.
In existing health care liquor production process, also there are some technological difficulties, mainly contain sedimentation problem and functional sex's component target control problem of wine.
For sedimentation problem, the method that usually adopts mainly contains physical method, chemical process and enzyme method at present.Physical method is to adopt ultra-filtration technique to remove to form macromolecular substance such as sedimentary pectin, albumen easily; Or promote precipitation to form by the subzero treatment method, centrifugal then, remove by filter.Chemical process is by regulating potential of hydrogen, adding external source chemicals processing removal.Enzyme method prevents to form precipitation by adding polygalacturonase, tannase etc. with decomposition such as pectin, tannin.But single physics method, chemical method or enzyme process all are difficult to precipitate thoroughly and remove, and influence the quality of health liquor.
For functional sex's component target control problem, mainly contain operating procedure improperly, the pharmaceutical use of the liquor of loss health greatly makes health liquor lose the function of " health care ".
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the present invention aims to provide a kind of health liquor raw material with health role and health liquor.Simultaneously, the invention also discloses a kind of comparatively advanced health liquor production process,, have the meaning of directiveness solving the technical problem that existing health liquor production exists.
The technical solution used in the present invention is as follows:
A kind of health liquor raw material is characterized in that, comprises following components by weight proportion:
1～3 part of the stem of noble dendrobium;
1～3 part of sealwort;
1～2 part of matrimony vine.
Preferred following components by weight proportion:
2 parts of the stems of noble dendrobium;
2 parts of sealworts;
1 part of matrimony vine.
The stem of noble dendrobium belongs to the orchid family Dendrobium per nnial herb, has sleeping, defaecation, improves skin, helps digest, multiple efficacies such as antitumor, anti-cataract.Sealwort is the Liliaceae per nnial herb, has enhance immunity function, antibiotic, step-down, the anti-ageing multiple efficacies effect of waiting for a long time.Matrimony vine is the multi-branched shrub plant of Solanaceae Lycium, has multiple efficacies effects such as lowering blood glucose, lipotropy and atherosclerosis.The stem of noble dendrobium, sealwort and matrimony vine all belong to the medicinal and edible plant raw material that China Ministry of Health announces.Above three kinds of medicinal and edible plant raw materials are carried out reasonably combinedly being developed to health liquor as health liquor raw material, have higher marketable value.
Stem of noble dendrobium health liquor is characterized in that, the extracting solution that obtains with liquor wine base lixiviate health liquor raw material adds liquor wine keynote and prepares.
The ratio of described allotment is an extracting solution: liquor wine base=1: 5～6.
The alcoholic strength that preferably makes stem of noble dendrobium health liquor is 42～45 degree.
As the stem of noble dendrobium health liquor of implementing technical solution of the present invention, its preparation methods steps is:
1., pre-treatment: health liquor raw material is cleaned, pulverizes;
2., lixiviate: in pulverizing product, add the liquor wine base of 7～9 times (weight ratios), immersion, soak solution is after filtration, clarification, ultrafiltration obtain extracting solution;
3., allotment: the ratio that extracting solution and liquor wine keynote are joined is 1: 5～6.
The grinding particle size of described step in 1. is 60～80 orders.
The immersion of described step in 2. is to soak 48h down at 50 ℃.
The clarification of described step in 2. is to add 0.1% PVPP and 0.1% gelatin in soak solution, and at room temperature leaves standstill 4h.
The ultrafiltration of described step in 2. adopted and held back relative molecular mass is 50,000 or 100,000 ps hollow fiber uf membrane ultra-filtration equipment.
Preparation method disclosed by the invention has well solved drinks in the prior art (particularly health liquor) and has produced existing technical problem.Production technique has overcome single physics method, chemical method or enzyme process and has all removed the halfway technical barrier of precipitation, modern food new technology and traditional method are combined, adopt multistage coupling connection clarification technique, chemical clarification technology and ultra filtering clarifying technology coupling connection are applied in the production of health Liquor Products, effectively eliminate precipitation, guaranteed the quality of product.
Aspect the control of functional ingredient, by the polysaccharide molecular weight Determination of distribution, the clear and definite distribution situation of polysaccharide in the stem of noble dendrobium health liquor according to the distribution of molecular weight, adopts suitable ultra-filtration membrane, has prevented the loss of polysaccharide in ultra-filtration process.
Health liquor raw material of the present invention, stem of noble dendrobium health liquor and preparation method thereof have following advantage:
1, can satisfy the demand of human consumer to healthy drinks
Along with the raising of people's living standard, the requirement of liquor is that the direction to health-care nutritive wine develops, and stem of noble dendrobium health liquor integrates nutrition, nourishing function, and long-term drinking can strengthen body immunity, safeguards HUMAN HEALTH.Make the human consumer can enjoy the enjoyment of drinking, can obtain healthyly again, experience natural green nourishing.
2, accelerate to promote the state of the art of China's liquor industry
Solved the key technical problem during liquor is produced,, promoted the scientific-technical progress of the sector, had great importance the further technology level that improves China's liquor production.
3, the agriculture, rural areas and farmers problem of Xie Jueing is increased farmers' income
The preferred Dabie Mountain Herba Dendrobii of fine quality of the present invention, carrying out along with project, can drive increasing peasant income gets rich, driving the growing dendrobium area increases, form new growth engines, and can drive the development of transportation, service sector, packaging industry, construction industry and related industries, to promoting the agriculture, rural areas and farmers problem of rural economy Sustainable development, solution, the paces of accelerating to build a well-off society in an all-round way have vital role.
Description of drawings
Fig. 1 is the polysaccharide molecular weight distribution plan.
Embodiment
The present invention is further illustrated below in conjunction with embodiment.
One, preparation embodiment
Embodiment 1
Alcoholic strength is the stem of noble dendrobium health liquor (the celestial wine of the stem of noble dendrobium) of 45 degree, and preparation process is as follows:
1., pre-treatment: get stem of noble dendrobium 20kg, sealwort 20kg, matrimony vine 10kg, be crushed to 60 orders after cleaning, mixing;
2., soak: in the product of pulverizing, add 400kg liquor wine base (number of degrees are 45 degree), soak 48h down, filter at 50 ℃;
3., clarification: in filtrate, add 0.1% PVPP (cross-linked polyvinylpyrrolidone) and 0.1% gelatin (all being weight percentage), and at room temperature leave standstill 4h;
4., ultrafiltration: adopting and holding back relative molecular mass is that 50,000 ps hollow fiber uf membrane ultra-filtration equipment ultrafiltration obtains extracting solution;
5., allotment: the ratio in extracting solution and liquor wine base (45 degree) allotment is that 15: 85 (weight ratio) allocates.
6., can, seal.
Embodiment 2
Alcoholic strength is the stem of noble dendrobium health liquor (the celestial wine of the stem of noble dendrobium) of 42 degree, and preparation process is as follows:
1., pre-treatment: get stem of noble dendrobium 30kg, sealwort 30kg, matrimony vine 20kg, be crushed to 80 orders after cleaning, mixing;
2., soak: in the product of pulverizing, add 720kg liquor wine base (number of degrees are 42 degree), soak 48h down, filter at 50 ℃;
All the other are with embodiment 1.
Embodiment 3
Alcoholic strength is the stem of noble dendrobium health liquor (the celestial wine of the stem of noble dendrobium) of 45 degree, and preparation process is as follows:
1., pre-treatment: get stem of noble dendrobium 10kg, sealwort 10kg, matrimony vine 10kg, be crushed to 70 orders after cleaning, mixing;
2., soak: in the product of pulverizing, add 210kg liquor wine base (number of degrees are 45 degree), soak 48h down, filter at 50 ℃;
All the other are with embodiment 1.
Two, comparative example
The comparative example 1
The immersion scheme changes soaking at room temperature 168h into, and other are with embodiment 1.
The comparative example 2
The immersion scheme changes reflux 6h into, and other are with embodiment 1.
The comparative example 3
The clarification scheme changes nature into and leaves standstill 24h, and other are with embodiment 1.
The comparative example 4
The clarification scheme changes into and adds 0.1% PVPP, and room temperature leaves standstill 4h, and other are with embodiment 1.
The comparative example 5
The clarification scheme changes into and adds 0.1% gelatin, and room temperature leaves standstill 4h, and other are with embodiment 1.
The comparative example 6
The clarification scheme changes into and adds 0.005% polygalacturonase, handles 4h for 45 ℃, and other are with embodiment 1.
The comparative example 7
The clarification scheme changes into and adds 0.005% polygalacturonase, handles 4h for 45 ℃, adds 0.1% PVPP and 0.1% gelatin then, and room temperature leaves standstill 4h, and other are with embodiment 1.
The comparative example 8
Ultrafiltration is adopted and to be held back relative molecular mass is 100,000 ps hollow fiber uf membrane ultra-filtration equipment, and other are with embodiment 1.
The comparative example 9
The allotment ratio changes 1: 6 into, and other are with embodiment 1.
The comparative example 10
The allotment ratio changes 1: 5 into, and other are with embodiment 1.
Three, analytical results
1, immersion scheme
Analyze transmittance (720nm), soluble solid content, polysaccharide content after embodiment 1 and comparative example 1-2 soak solution filter, see Table 1.
Three kinds of immersion schemes of table 1 are to the influence of transmittance, soluble solid content, polysaccharide content
| Scheme | Transmittance (%) | Soluble solid content (%) | Polysaccharide content (%) |
| Embodiment 1 | 85 | 2.78 | 0.9 |
| The comparative example 1 | 86 | 2.73 | 0.87 |
| The comparative example 2 | 70 | 2.93 | 0.915 |
As shown in Table 1, it is best that low temperature soaks (comparative example 1) transparency of products, but polysaccharide that soaks out and total dissoluble solid content are low slightly, and soak time is long; Refluxing extraction (comparative example 2) polysaccharide and total dissoluble solid extraction yield height, the time is short, but transmittance is low, is unfavorable for back clarification operation; And hot dipping puies forward the method for (embodiment 1) and falls between, and higher polysaccharide and total dissoluble solid extraction yield are arranged, and the time is not oversize, extracting solution transmittance height.
2, clarification scheme
Analyze transmittance (720nm), the storage rate of soluble solid, the total polysaccharides storage rate of embodiment 1 and comparative example 3-7 clarification back liquid, see Table 2.
6 kinds of clarification schemes of table 2 are to the storage rate of transmittance, soluble solid, the influence of total polysaccharides storage rate
| Scheme | Transmittance (%) | Soluble solid storage rate (%) | Total polysaccharides storage rate (%) |
| Embodiment 1 | 93.6 | 97.2 | 89.9 |
| The comparative example 3 | 85.6 | 98.1 | 95.2 |
| The comparative example 4 | 90.2 | 97.5 | 90.3 |
| The comparative example 5 | 89.7 | 95.2 | 89.1 |
| The comparative example 6 | 88.9 | 95.6 | 85.8 |
| The comparative example 7 | 94.5 | 89.8 | 86.9 |
As shown in Table 2, comparative example's 7 clarification back transmittance height, but the storage rate of soluble solid and total polysaccharides storage rate are lower, embodiment 1 existing transmittance preferably, the storage rate of soluble solid and total polysaccharides storage rate are also higher, therefore, adopt to add 0.1% PVPP and 0.1% gelatin, the method that room temperature leaves standstill 4h is carried out clarifying treatment, and effect is best.
3, ultrafiltration Scheme Selection
With the liquid after the clarification among the embodiment 1, through ethanol sedimentation, measure its molecular weight distribution by HPLC, see accompanying drawing 1.
As shown in Figure 1, mixing polysaccharide mainly is made up of three kinds of components of weight-average molecular weight 43200,21520 and 5053, according to bibliographical information, and weight-average molecular weight 43200,21520th, the main polysaccharide of lycium barbarum polysaccharide is formed, and the 5053rd, the main polysaccharide of polygonatum polysaccharide is formed.
According to the polysaccharide molecular weight Determination of distribution, polysaccharide molecular weight is below 50000, therefore, liquid after embodiment 1 and comparative example 8 clarify respectively, adopt 50,000 to handle respectively with the ultra-filtration membrane of 100,000 relative molecular weight cut-offs, analyze the storage rate and the total polysaccharides storage rate of transmittance, soluble solid, see Table 3.
Two kinds of ultra-filtration membranes of table 3 are to the influence of the storage rate and the total polysaccharides storage rate of transmittance, soluble solid
As shown in Table 3,50,000 all have clarifying effect preferably with the ultra-filtration membrane of 100,000 relative molecular weight cut-offs, but the transmittance of the ultra-filtration membrane of 50,000 relative molecular weight cut-offs is more better.
4, allotment ratio
By sensory evaluation marking, and the influence of the content of investigation soluble solid, set up standards of grading, see Table 4.
Table 4 standards of grading
Analyze the scoring of embodiment 1 and comparative example 9-10 product, see Table 5.
3 kinds of allotments of table 5 scheme product score
As shown in Table 5, the allotment ratio is between 1: 5～6 the time, and the quality of health liquor is comparatively desirable, and add 15% vat liquor of (allotment than be 15: 85) has the Oranoleptic indicator of optimum, performance optimal.
Claims (10)
1. a health liquor raw material is characterized in that, comprises following components by weight proportion:
1～3 part of the stem of noble dendrobium;
1～3 part of sealwort;
1～2 part of matrimony vine.
2. health liquor raw material according to claim 1 is characterized in that, comprises following components by weight proportion:
2 parts of the stems of noble dendrobium;
2 parts of sealworts;
1 part of matrimony vine.
3. stem of noble dendrobium health liquor is characterized in that, the extracting solution that obtains with liquor wine base lixiviate claim 1 or 2 described health liquor raw materials adds liquor wine keynote and prepares.
4. stem of noble dendrobium health liquor according to claim 3 is characterized in that, the ratio of described allotment is an extracting solution: liquor wine base=1: 5～6.
5. stem of noble dendrobium health liquor according to claim 3 is characterized in that, the alcoholic strength of described stem of noble dendrobium health liquor is 42～45 degree.
6. the preparation method of stem of noble dendrobium health liquor is characterized in that, may further comprise the steps:
1., pre-treatment: health liquor raw material is cleaned, pulverizes;
2., lixiviate: in pulverizing product, add 7～9 times liquor wine base, immersion, soak solution is after filtration, clarification, ultrafiltration obtain extracting solution;
3., allotment: the ratio that extracting solution and liquor wine keynote are joined is 1: 5～6.
7. preparation method according to claim 6 is characterized in that, the grinding particle size of described step in 1. is 60～80 orders.
8. preparation method according to claim 6 is characterized in that, the immersion of described step in 2. is to soak 48h down at 50 ℃.
9. preparation method according to claim 6 is characterized in that, the clarification of described step in 2. is to add 0.1% PVPP and 0.1% gelatin in soak solution, and at room temperature leaves standstill 4h.
10. preparation method according to claim 6 is characterized in that, the ultrafiltration of described step in 2. adopted and held back relative molecular mass is 50,000 or 100,000 ps hollow fiber uf membrane ultra-filtration equipment.
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102952742A (en) * | 2012-11-01 | 2013-03-06 | 上海中海龙高新技术研究院 | Dendrobium officinale kimura et migo wine and preparation method thereof |
| CN103627614A (en) * | 2013-12-12 | 2014-03-12 | 西双版纳银海福林石斛有限公司 | Dendrobium wine preparation method |
| CN104277953A (en) * | 2013-07-04 | 2015-01-14 | 张征 | Preparation technology of Dendrobium officinale wine |
| CN105039088A (en) * | 2015-09-08 | 2015-11-11 | 南宁荣港生物科技有限公司 | Preparation method for sealwort fermentation wine |
| CN105349359A (en) * | 2015-11-12 | 2016-02-24 | 赤水市丹霞生产力促进中心有限公司 | Health care wine containing dendrobium stem and ginkgo |
| CN107189922A (en) * | 2017-07-26 | 2017-09-22 | 金湘范 | A kind of white spirit based on plant former dew and preparation method thereof |
| CN107904103A (en) * | 2017-12-05 | 2018-04-13 | 浙江民康天然植物制品有限公司 | A kind of dendrobium candidum health liquor and its preparation method and application |
| CN109182012A (en) * | 2018-11-22 | 2019-01-11 | 李云峰 | A kind of anhydrous middle low health white wine blent |
| CN110484414A (en) * | 2019-07-16 | 2019-11-22 | 韶关学院 | It is a kind of using dendrobium nobile alcohol extracting thing as dendrobium wine of raw material and preparation method thereof |
| CN112760189A (en) * | 2021-03-02 | 2021-05-07 | 湖北省医药工业研究院有限公司 | Formula and preparation method of dendrobium wine |
| CN113308327A (en) * | 2021-05-19 | 2021-08-27 | 中酌酒业(江苏)股份有限公司 | Spartina alterniflora yin-nourishing and yang-tonifying dendrobium wine medicine decocting pot and preparation process thereof |
| CN114989923A (en) * | 2022-05-11 | 2022-09-02 | 安徽迎驾贡酒股份有限公司 | Dendrobium wine and preparation method thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102952742A (en) * | 2012-11-01 | 2013-03-06 | 上海中海龙高新技术研究院 | Dendrobium officinale kimura et migo wine and preparation method thereof |
| CN104277953A (en) * | 2013-07-04 | 2015-01-14 | 张征 | Preparation technology of Dendrobium officinale wine |
| CN103627614A (en) * | 2013-12-12 | 2014-03-12 | 西双版纳银海福林石斛有限公司 | Dendrobium wine preparation method |
| CN103627614B (en) * | 2013-12-12 | 2015-03-11 | 西双版纳银海福林石斛有限公司 | Dendrobium wine preparation method |
| CN105039088A (en) * | 2015-09-08 | 2015-11-11 | 南宁荣港生物科技有限公司 | Preparation method for sealwort fermentation wine |
| CN105349359A (en) * | 2015-11-12 | 2016-02-24 | 赤水市丹霞生产力促进中心有限公司 | Health care wine containing dendrobium stem and ginkgo |
| CN107189922A (en) * | 2017-07-26 | 2017-09-22 | 金湘范 | A kind of white spirit based on plant former dew and preparation method thereof |
| CN107904103A (en) * | 2017-12-05 | 2018-04-13 | 浙江民康天然植物制品有限公司 | A kind of dendrobium candidum health liquor and its preparation method and application |
| CN109182012A (en) * | 2018-11-22 | 2019-01-11 | 李云峰 | A kind of anhydrous middle low health white wine blent |
| CN110484414A (en) * | 2019-07-16 | 2019-11-22 | 韶关学院 | It is a kind of using dendrobium nobile alcohol extracting thing as dendrobium wine of raw material and preparation method thereof |
| CN112760189A (en) * | 2021-03-02 | 2021-05-07 | 湖北省医药工业研究院有限公司 | Formula and preparation method of dendrobium wine |
| CN113308327A (en) * | 2021-05-19 | 2021-08-27 | 中酌酒业(江苏)股份有限公司 | Spartina alterniflora yin-nourishing and yang-tonifying dendrobium wine medicine decocting pot and preparation process thereof |
| CN114989923A (en) * | 2022-05-11 | 2022-09-02 | 安徽迎驾贡酒股份有限公司 | Dendrobium wine and preparation method thereof |
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Application publication date: 20111123 |