CN102206436A - Vacuum-plating ultraviolet curing intermediate paint - Google Patents
Vacuum-plating ultraviolet curing intermediate paint Download PDFInfo
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- CN102206436A CN102206436A CN2010101405647A CN201010140564A CN102206436A CN 102206436 A CN102206436 A CN 102206436A CN 2010101405647 A CN2010101405647 A CN 2010101405647A CN 201010140564 A CN201010140564 A CN 201010140564A CN 102206436 A CN102206436 A CN 102206436A
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- acrylic resin
- urethane acrylate
- lacquer
- trigger
- ultraviolet light
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Abstract
The invention belongs to the technical field of paints, and particularly relates to a vacuum-plating ultraviolet curing intermediate paint, which includes the following raw materials by weight: 10%-20% of hydroxy acrylic resin, 25%-35% of polyurethane acrylates, 15%-20% of thermoplastic acrylic acid resin, 15%-25% of ethyl acetate, 10%-15% of butyl acetate, 8%-15% of isobutanol, 3%-10% of nano-pigments, 3%-5% of ultraviolet-curing initiators, and 1%-3% of additives. The invention has a fast-curing property, good wearability, pollution resistance, hard-object scratch resistance, high glossiness, low volatility, is environment-friendly and free of pollution, can be widely used to spray electronic or electric appliance products and cosmetic containers.
Description
Technical field:
The invention belongs to technical field of coatings, coat with lacquer in particularly a kind of vacuum plating ultraviolet light polymerization.
Background technology:
At present, various electronics or electric equipment products, cosmetics containers are widely used in people's the life as digital camera, notebook computer, mobile phone, photographic camera, MP4 or the like.The shell of this series products is made by plastics or plastic material mostly, during use often friction destroy the outward appearance of product easily, and hand is when touching the shell of product, meetings such as hand perspiration have certain corrodibility to the shell of product, influence the work-ing life of product.Therefore; all need be after its shell machine-shaping at surperficial sprayed protection and ornamental coating; purpose is to improve its weathering resistance, chemical resistant properties and surface hardness; reduce insulating property; prevent adhesivity and dirt resistance, improve hand feel performance, and improve the artistic effect of decorating; make the plastic casing color abundanter, have the metallic surface effect of emulation.Traditional coating adopts thermoplastic acrylic paint or bicomponent polyurethane coating more, and this class coating exists the wear resistance deficiency, damage resistant not, and production efficiency is low, and chemical-resistant is poor, problems such as environmental pollution.
Summary of the invention:
The objective of the invention is to provide a kind of and solidify fast and have good wear resistance, resistance to soiling, anti-hard thing scratch resistant at the deficiencies in the prior art, the glossiness height, volatility is low, coats with lacquer in the vacuum plating ultraviolet light polymerization of environmental protection.
The object of the present invention is achieved like this:
Coat with lacquer in the vacuum plating ultraviolet light polymerization, it comprises following raw materials by weight percent:
Hydroxylated acrylic resin 10%～20%
Urethane acrylate 25%～35%
Thermoplastic acrylic resin 15%～20%
Vinyl acetic monomer 15%～25%
N-BUTYL ACETATE 10%～15%
Isopropylcarbinol 8%～15%
Nano dye 3%～10%
Trigger for optical solidification 3%～5%
Auxiliary agent 1%～3%.
Preferably, it comprises following raw materials by weight percent:
Hydroxylated acrylic resin 10%～15%
Urethane acrylate 25%～30%
Thermoplastic acrylic resin 15%～20%
Vinyl acetic monomer 15%～20%
N-BUTYL ACETATE 10%～15%
Isopropylcarbinol 8%～15%
Nano dye 3%～10%
Trigger for optical solidification 3%～5%
Auxiliary agent 1%～3%.
Preferably, it comprises following raw materials by weight percent:
Hydroxylated acrylic resin 10%
Urethane acrylate 35%
Thermoplastic acrylic resin 15%
Vinyl acetic monomer 15%
N-BUTYL ACETATE 10%
Isopropylcarbinol 8%
Nano dye 3%
Trigger for optical solidification 3%
Auxiliary agent 1%.
Described urethane acrylate is any one in aliphatic urethane acrylate, aromatic urethane acrylate, the aromatic polyether urethane acrylate.
Described trigger for optical solidification is 2-methyl isophthalic acid-(4-first sulfydryl phenyl)-2-morpholine-1-acetone, 2; 4; 6-trimethylbenzoyl diphenyl phosphine oxide, two (2; 4,6-trimethylbenzoyl) one or more in phenyl phosphine oxide, 2-hydroxy-2-methyl-1-phenyl-acetone, the 1-hydroxy cyclohexyl phenylketone.
Described auxiliary agent comprises that the arbitrary proportion of defoamer, flow agent and dispersion agent mixes.
Its preparation method is that its preparation method is, and is earlier that vinyl acetic monomer, N-BUTYL ACETATE, isopropylcarbinol is mixed according to the above ratio that mixed solvent is standby; Hydroxylated acrylic resin, urethane acrylate, the thermoplastic acrylic resin of getting aforementioned proportion again add container, add trigger for optical solidification and auxiliary agent, formed mixture is after low speed is uniformly dispersed, add the mixed solvent that signature makes, fully stirred then 10～15 minutes, add nano dye at last, the back that is uniformly dispersed is filtered with 400 order grenadines and is got product.
Beneficial effect of the present invention: coat with lacquer in a kind of vacuum plating ultraviolet light polymerization, it comprises following raw materials by weight percent: Hydroxylated acrylic resin 10%～20%, polyurethane acroleic acid 25%～35%, thermoplastic acrylic resin 15%～20%, vinyl acetic monomer 15%～25%, N-BUTYL ACETATE 10%～15%, isopropylcarbinol 8%～15%, nano dye 3%～10%, trigger for optical solidification 3%～5%, auxiliary agent 1%～3%; The present invention is solidified quick and is had good wear resistance, resistance to soiling, anti-hard thing scratch resistant, the glossiness height, volatility is low, environment friendly and pollution-free, can extensively spray and be used for electronics or electric equipment products, cosmetics containers etc., can make the outward appearance of product more attractive in appearance, strengthen whole adhesive force of coatings, strengthen its scratch resistance, wear-resisting and anti-pollution characteristic.In addition, this product can be used for auto lamp, electric hair clip, electric iron etc., has resistance to elevated temperatures.
Embodiment:
The present invention is further illustrated with specific embodiment below, but the present invention is not subjected to the qualification of following embodiment.
Hydroxy acrylate has high adherence, high-flexibility, and the resin low temperature adaptability that has is good, and ferrous metal sticking power is good, corrosive nature is good.
Maximum characteristics of urethane acrylate and performance are: viscosity is low, can make oligopolymer again, also can make reactive thinner and use, and smell is low.If require curing speed fast, can select the higher slightly resin of functionality to strengthen sticking power simultaneously, system has excellent weathering resistance after the film forming, and snappiness and elongation at break have favorable chemical resistance and environmental compatibility, and ply adhesion is good.
The supplier of table 1 urethane acrylate and product grade
| Bayer | The cyanogen spy | Middle mountain Chiba | BASF |
| LS2298/1 | EB264 | UV2100 | 303 |
| LS2285 | EB210 | UV2000 | |
| LS2265 |
A lot of products coat with lacquer the back and move phenomenon because of colour migration can appear in additive color in spraying, in ultraviolet-curing paint, add an amount of thermoplastic propene's acid esters and good help is arranged solving this defective, make more even that the product surface color represents after the application, offer convenience to construction.
The supplier of table 2 thermoplastic acrylic resin and product grade
| Mitsubishi | Same moral | Synchronously |
| BR113 | AC1226 | TP5160 |
| BR2952 | AC10230 | TP5162 |
| AC10268 |
Nano dye is a kind of look essence of color, and the advantage that it compares common pigments is: environmental protection, its every index can reach the ROHS standard, and the influence of environment, human body is reduced greatly.Nano material of the present invention mainly contains following:
The supplier of table 3 nano dye
| Refined in big day | Changxing chemistry | One ring look treasured | Super full chemical industry |
| Shades of colour | Shades of colour | Shades of colour | Shades of colour |
Trigger for optical solidification is the key component of entire ultraviolet photo-cured coating, trigger for optical solidification is a kind of material of energy absorbed radiation energy UV-light, the radiating capacity UV-light is mainly by high voltage mercury lamp, metal halid lamp, electrodeless lamp, the spectrum that xenon lamp etc. send, the trigger for optical solidification absorb light produces curing reaction and crosslinking curing.Trigger for optical solidification of the present invention mainly contains following:
The supplier of table 4 trigger for optical solidification and product grade
| Switzerland's vapour crust | Changzhou China titanium | U.S.'s Sartomer | Beijing English power |
| 819 | 1104 | 1120 | 907 |
| 18 | 1108 | 1130 | TPO |
| 1173 | 1103 | 1173 | |
| 1024 | 184 |
Auxiliary agent mainly is to help moistening ground, makes its surfacing, and auxiliary agent of the present invention mainly contains following:
The supplier of table 5 auxiliary agent and product grade
Embodiment 1
By weight percentage, earlier that vinyl acetic monomer 15%, N-BUTYL ACETATE 10%, isopropylcarbinol 8% is mixed that mixed solvent is standby; Get Hydroxylated acrylic resin 10% again; (urethane acrylate is selected Bayer LS2265 for use to urethane acrylate 35%; be aliphatic urethane acrylate); thermoplastic acrylic resin 15% adds in the container; add trigger for optical solidification 3%[trigger for optical solidification again and select Switzerland's vapour crust 819 for use; be two (2; 4; the 6-trimethylbenzoyl) phenyl phosphine oxide] and defoamer 0.3% (defoamer select for use enlightening high by 920); flow agent 0.5% (flow agent select for use enlightening high by 2100); dispersion agent 0.2% (dispersion agent select for use enlightening high by 681); formed mixture is after low speed is uniformly dispersed; add the aforementioned mixed solvent that makes; fully stirred then 10～15 minutes; add 3% nano dye (nano dye is selected the pigment of all kinds of super full chemical industry for use) at last, the back that is uniformly dispersed gets product with the filtration of 400 order grenadines.
Embodiment 2
By weight percentage, earlier that vinyl acetic monomer 20%, N-BUTYL ACETATE 10%, isopropylcarbinol 10% is mixed that mixed solvent is standby; Get Hydroxylated acrylic resin 10% again, (urethane acrylate is selected the special EB264 of cyanogen for use to urethane acrylate 25%, be the aromatic urethane acrylate), thermoplastic acrylic resin 15% adds in the container, add trigger for optical solidification 3%[trigger for optical solidification again and select Beijing English power 907 for use, be 2-methyl isophthalic acid-(4-first sulfydryl phenyl)-2-morpholine-1-acetone] and defoamer 1% (defoamer is selected Bayer 020 for use), flow agent 0.5% (flow agent is selected Bayer 306 for use), dispersion agent 0.5% (dispersion agent is selected Bayer 168 for use), formed mixture is after low speed is uniformly dispersed, add the aforementioned mixed solvent that makes, fully stirred then 10～15 minutes, add 5% nano dye (nano dye is selected the pigment of all kinds of a ring look treasured for use) at last, the back that is uniformly dispersed gets product with the filtration of 400 order grenadines.
Embodiment 3
By weight percentage, earlier that vinyl acetic monomer 15%, N-BUTYL ACETATE 10%, isopropylcarbinol 8% is mixed that mixed solvent is standby; Get Hydroxylated acrylic resin 17% again, (urethane acrylate is selected middle mountain Chiba UV2100 for use to urethane acrylate 25%, be the aromatic polyether urethane acrylate), thermoplastic acrylic resin 15% adds in the container, (trigger for optical solidification is selected Beijing English power 1173 for use to add trigger for optical solidification 3% again, be 2-hydroxy-2-methyl-1-phenyl-acetone) and defoamer 1% (defoamer is selected moral modest 2700 for use), flow agent 1% (flow agent is selected moral modest 435 for use), dispersion agent 1% (dispersion agent is selected moral modest 912 for use), formed mixture is after low speed is uniformly dispersed, add the aforementioned mixed solvent that makes, fully stirred then 10～15 minutes, add 4% nano dye (nano dye is selected the pigment of all kinds of Changxing chemistry for use) at last, the back that is uniformly dispersed gets product with the filtration of 400 order grenadines.
Embodiment 4
By weight percentage, earlier that vinyl acetic monomer 15%, N-BUTYL ACETATE 10%, isopropylcarbinol 8% is mixed that mixed solvent is standby; Get Hydroxylated acrylic resin 20% again, (urethane acrylate is selected BASF 303 for use to urethane acrylate 25%, be the aromatic urethane acrylate), thermoplastic acrylic resin 15% adds in the container, (trigger for optical solidification is selected Beijing English power 184 for use to add trigger for optical solidification 3% again, be the 1-hydroxy cyclohexyl phenylketone) and defoamer 0.5% (defoamer select for use enlightening high by 920), flow agent 0.2% (flow agent select for use enlightening high by 2100), dispersion agent 0.3% (dispersion agent select for use enlightening high by 681), formed mixture is after low speed is uniformly dispersed, add the aforementioned mixed solvent that makes, fully stirred then 10～15 minutes, add 3% nano dye (nano dye is selected the pigment of all kinds of refining big day for use) at last, the back that is uniformly dispersed gets product with the filtration of 400 order grenadines.
The finished product that embodiment 1～4 is made directly sprays, and spraying air pressure is 4-6kg/cm
2, spray distance is 8-14cm, also can adopt the automation line application, thickness 7-9 μ m.The first seasoning 2-3min in spraying back then enters temperature and is in 55 ± 3 ℃ the baking oven, keeps 3-5min, crosses uv then, and its exposure energy is 600-800mj/cm
3
The above only is preferred embodiment of the present invention, so all equivalences of doing according to the described structure of patent claim of the present invention, feature and principle change or modify, is included in the patent claim of the present invention.
Claims (7)
1. coat with lacquer in the vacuum plating ultraviolet light polymerization, it is characterized in that: it comprises following raw materials by weight percent:
Hydroxylated acrylic resin 10%～20%
Urethane acrylate 25%～35%
Thermoplastic acrylic resin 15%～20%
Vinyl acetic monomer 15%～25%
N-BUTYL ACETATE 10%～15%
Isopropylcarbinol 8%～15%
Nano dye 3%～10%
Trigger for optical solidification 3%～5%
Auxiliary agent 1%～3%.
2. coat with lacquer in the vacuum plating ultraviolet light polymerization according to claim 1, it is characterized in that: it comprises following raw materials by weight percent:
Hydroxylated acrylic resin 10%～15%
Urethane acrylate 25%～30%
Thermoplastic acrylic resin 15%～20%
Vinyl acetic monomer 15%～20%
N-BUTYL ACETATE 10%～15%
Isopropylcarbinol 8%～15%
Nano dye 3%～10%
Trigger for optical solidification 3%～5%
Auxiliary agent 1%～3%.
3. coat with lacquer in the vacuum plating ultraviolet light polymerization according to claim 1, it is characterized in that: it comprises following raw materials by weight percent:
Hydroxylated acrylic resin 10%
Urethane acrylate 35%
Thermoplastic acrylic resin 15%
Vinyl acetic monomer 15%
N-BUTYL ACETATE 10%
Isopropylcarbinol 8%
Nano dye 3%
Trigger for optical solidification 3%
Auxiliary agent 1%.
4. according to coating with lacquer in any described vacuum plating ultraviolet light polymerization of claim 1-3, it is characterized in that: described urethane acrylate is any one in aliphatic urethane acrylate, aromatic urethane acrylate, the aromatic polyether urethane acrylate.
5. according to coating with lacquer in any described vacuum plating ultraviolet light polymerization of claim 1-3; it is characterized in that: described trigger for optical solidification is 2-methyl isophthalic acid-(4-first sulfydryl phenyl)-2-morpholine-1-acetone, 2; 4; 6-trimethylbenzoyl diphenyl phosphine oxide, two (2; 4,6-trimethylbenzoyl) one or more in phenyl phosphine oxide, 2-hydroxy-2-methyl-1-phenyl-acetone, the 1-hydroxy cyclohexyl phenylketone.
6. according to coating with lacquer in any described vacuum plating ultraviolet light polymerization of claim 1-3, it is characterized in that: described auxiliary agent comprises that the arbitrary proportion of defoamer, flow agent and dispersion agent mixes.
7. according to coating with lacquer in any described vacuum plating ultraviolet light polymerization of claim 1-3, it is characterized in that: its preparation method is, and is earlier that vinyl acetic monomer, N-BUTYL ACETATE, isopropylcarbinol is mixed according to the above ratio that mixed solvent is standby; Hydroxylated acrylic resin, urethane acrylate, the thermoplastic acrylic resin of getting aforementioned proportion again add container, add trigger for optical solidification and auxiliary agent, formed mixture is after low speed is uniformly dispersed, add the aforementioned mixed solvent that makes, fully stirred then 10～15 minutes, add nano dye at last, the back that is uniformly dispersed is filtered with 400 order grenadines and is got product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010140564.7A CN102206436B (en) | 2010-03-31 | 2010-03-31 | Vacuum-plating ultraviolet curing intermediate paint |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010140564.7A CN102206436B (en) | 2010-03-31 | 2010-03-31 | Vacuum-plating ultraviolet curing intermediate paint |
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| Publication Number | Publication Date |
|---|---|
| CN102206436A true CN102206436A (en) | 2011-10-05 |
| CN102206436B CN102206436B (en) | 2015-05-20 |
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| CN201010140564.7A Active CN102206436B (en) | 2010-03-31 | 2010-03-31 | Vacuum-plating ultraviolet curing intermediate paint |
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Cited By (8)
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| CN102775902A (en) * | 2012-08-07 | 2012-11-14 | 昆山市万胜化工有限公司 | Finish paint for plastic |
| CN103073989A (en) * | 2012-12-19 | 2013-05-01 | 青岛海诺水务科技股份有限公司 | Ultraviolet-cured paint |
| CN103525288A (en) * | 2013-09-30 | 2014-01-22 | 安徽蓝柯复合材料有限公司 | Ultraviolet curing coating for coating plastic surface and preparation method thereof |
| CN103526632A (en) * | 2013-09-30 | 2014-01-22 | 安徽蓝柯复合材料有限公司 | Priming-free ultraviolet (UV) coating for paper and preparation method of coating |
| CN108624221A (en) * | 2018-05-25 | 2018-10-09 | 深圳市深赛尔股份有限公司 | Painted in a kind of high-performance vacuum plating UV dope and preparation method thereof |
| CN112457764A (en) * | 2020-10-30 | 2021-03-09 | 中山市鑫峰光固化材料有限公司 | Ultraviolet curing coating without thickening and preparation method thereof |
| CN115558401A (en) * | 2021-12-29 | 2023-01-03 | 江苏兴业联合装备技术有限公司 | High-strength SPC (super solvent modified) floor UV (ultraviolet) curing coating and preparation method thereof |
| CN116333584A (en) * | 2022-10-12 | 2023-06-27 | 珠海市三绿实业有限公司 | Coating photosensitive resin for 3D printing model post-treatment and preparation method thereof |
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| CN112457764B (en) * | 2020-10-30 | 2022-08-09 | 中山市鑫峰光固化材料有限公司 | Ultraviolet curing coating without thickening and preparation method thereof |
| CN115558401A (en) * | 2021-12-29 | 2023-01-03 | 江苏兴业联合装备技术有限公司 | High-strength SPC (super solvent modified) floor UV (ultraviolet) curing coating and preparation method thereof |
| CN115558401B (en) * | 2021-12-29 | 2023-08-04 | 江苏兴业联合装备技术有限公司 | High-strength SPC floor UV (ultraviolet) curing coating and preparation method thereof |
| CN116333584A (en) * | 2022-10-12 | 2023-06-27 | 珠海市三绿实业有限公司 | Coating photosensitive resin for 3D printing model post-treatment and preparation method thereof |
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Effective date of registration: 20200803 Address after: Taicang HuaSu road harbor of Suzhou city in Jiangsu province 215400 Port Development Zone No. 6 Patentee after: TAICANG PEIQI PAINT Co.,Ltd. Address before: 523000, Dongguan City, Guangdong province Tangxia Pingshan 188 Industrial Zone Dongguan Pei Qi coating Co., Ltd. Patentee before: Peiqi Paint Co.,Ltd. of Dongguan City |
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Address after: 215400 No. 6, HuaSu Middle Road, taicanggang Port Development Zone, Suzhou, Jiangsu Patentee after: Suzhou Peiqi Material Technology Co.,Ltd. Address before: 215400 No. 6, HuaSu Middle Road, taicanggang Port Development Zone, Suzhou, Jiangsu Patentee before: TAICANG PEIQI PAINT CO.,LTD. |