CN102190952A - Environment-friendly water-based single-component metallic-effect refinish paint for automobiles and preparation method thereof - Google Patents
Environment-friendly water-based single-component metallic-effect refinish paint for automobiles and preparation method thereof Download PDFInfo
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- CN102190952A CN102190952A CN2011101360231A CN201110136023A CN102190952A CN 102190952 A CN102190952 A CN 102190952A CN 2011101360231 A CN2011101360231 A CN 2011101360231A CN 201110136023 A CN201110136023 A CN 201110136023A CN 102190952 A CN102190952 A CN 102190952A
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Abstract
The invention relates to an environment-friendly water-based single-component metallic-effect refinish paint for automobiles and a preparation method thereof. The refinish paint comprises the following components in percentage by weight: 30-50% of water-based resin, 3-10% of single-component metallic-effect pigment, 0.1-1.0% of water-based dispersant, 0.3-1.0% of water-based defoaming agent, 3-9% of water-based thickening agent, 1-8% of cosolvent, 0.5-1% of water-based leveling agent, 0.1% of bactericide, 1-2% of pH regulator and 30-45% of deionized water. Compared with the prior art, the invention is harmless to human bodies, and has the advantages of strong metallic texture and the like.
Description
Technical field
The present invention relates to a kind of automobile touch-up paint, especially relate to a kind of environment-friendly water-based automobile single component metal effect retouching paint and preparation method thereof.
Background technology
Widely used on the car repair market at present is the solvent-borne type retouching paint, the solvent of traditional solvent-borne type retouching paint is everlasting more than 40%, automobile solvent-borne type metallic color is at the solvent of application even up to 85%, these solvents are generally volatile organic compounds (VOC), volatile organic compounds (VOC) enters atmosphere, can cause the pollution of environment, simultaneously the healthy of application workman be worked the mischief.Along with the raising of people to the attention degree of health, car refinishing paint is also developing towards health environment-friendly, and market is to just progressively rising to aqueous automobile retouching paint demand.
Summary of the invention
Purpose of the present invention is exactly that a kind of harmless, environment-friendly water-based automobile single component metal effect retouching paint that metal-like is strong and preparation method thereof is provided in order to overcome the defective that above-mentioned prior art exists.
Purpose of the present invention can be achieved through the following technical solutions: the retouching paint of a kind of environment-friendly water-based automobile single component metal effect, it is characterized in that, this retouching paint comprises following component and weight percentage: water-base resin 30~50%, single component metal effect pigments 3~10%, aqueous dispersant 0.1~1.0%, water-based defoamer 0.3~1.0%, water-based thickener 3~9%, solubility promoter 1~8%; Water-based flow agent 0.5~1%, sterilant 0.1%, pH regulator agent 1~2% and deionized water 30~45%.
Described water-base resin is selected from waterborne polyurethane resin, water-borne acrylic resin, one or more in water-compatible amino resin, the aqueous polyester resin.
Described waterborne polyurethane resin is Bayhydrol XP 2648, Bayhydrol xp 2621 or Bayhydrol XP 2650, described water-borne acrylic resin is JF1605, and described water-compatible amino resin is the hexa methoxy trimeric cyanamide, and described aqueous polyester resin is ADM-F206.
Described single component metal effect pigments is aluminium powder or copper powder, comprises STAPA HYDROLAN 2192, STAPAHYDROLAN2153 or STAPAHYDROLAN9157.
Described aqueous dispersant is polymeric dispersant or inorganic dispersant, described polymeric dispersant is TEGO Dispers 715W, TEGO Dispers 740W or TEGO Dispers 745W, described inorganic dispersant is silicate, carbonate or poly-phosphate.
Described water-based defoamer is polyether type defoamer, organic defoamer or silicone antifoam agent, described polyether type defoamer is TEGO Foamex 815N, TEGO Foamex 822 or TEGO Foamex 830, described organic defoamer is whiteruss or lipid acid, and described silicone antifoam agent is the emulsion-type polysiloxane.
Described water-based thickener is the polyacrylic thickening material, cellulose thickener or polyurethanes thickening material, described polyacrylic thickening material is Viscalex HV 30, Rheolate 125 or Rheolate 1, described cellulose thickener is HEC or HPC, and described polyurethanes thickening material is Rheolate 212 or Rheolate288.
Described solubility promoter is selected from propyl carbinol, sec-butyl alcohol, Virahol, ethanol, one or more in propylene glycol monomethyl ether, the dipropylene glycol monomethyl ether.
Described water-based flow agent is a modified polyorganosiloxane class water-based flow agent, silicone based water-based flow agent or micronization wax emulsion class water-based flow agent, described modified polyorganosiloxane class water-based flow agent is SLIP-FS 444, LevelolW-469 or Levaslip W-461, described silicone based water-based flow agent is BYK-341 or BYK335, and described micronization wax emulsion class water-based flow agent is EFKA-906;
Described sterilant is the substituted arene series bactericidal agent, the heterogeneous ring compound sterilant, the aminated compounds sterilant, the organometallic compound sterilant, described substituted arene series bactericidal agent is pentachlorophenol and sodium salt thereof, daconil M or orthoxenol, and described heterogeneous ring compound sterilant is benzoglyoxaline or oxine, described aminated compounds sterilant is two thiocarbamates or Salicylanlide, and described organometallic compound sterilant is an organotin;
Described pH regulator agent is a diethylamine, triethylamine, diethanolamine, trolamine, Pehanorm, diisopropanolamine (DIPA) or dimethyl isobutyl hydramine.
The preparation method of a kind of environment-friendly water-based automobile single component metal effect retouching paint is characterized in that this method may further comprise the steps:
(1) by weight percentage, with single component metal effect pigments 3~10%, aqueous dispersant 0.1~1.0%, solubility promoter and deionized water add successively under whipped state and mix, and are prepared into component a;
(2) with water-base resin 30~50%, water-based defoamer 0.3~1.0%, deionized water adds successively, and stirs; Add water-based thickener 3~9% then, deionized water also continues to stir; Continue to add solubility promoter, making its total content is 1~8%, water-based flow agent 0.5~1%, and sterilant 0.1% and deionized water also stir and are prepared into component b;
(3) under whipped state, component a is added among the component b, and mix, and pH is transferred to 7~10 with pH regulator agent accent.
Compared with prior art, the present invention has the following advantages:
(1) environment-friendly type does not almost have injury to workman's health;
(2) can directly use deionized water, reduce the discharging of VOC as thinner;
(3) resultant metal texture is strong, arranges effective;
(4) can with the solvent borne priming paint and the varnish coordinative construction of routine.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Each component is all by weight percentage in following examples:
Embodiment 1
The preparation method of a kind of aqueous automobile single component metal effect retouching paint, this method comprises following processing step:
(1) earlier with water-based aluminium powder pigment (STAPA HYDROLAN 2152) 4%, waterborne polymeric dispersion agent (TEGO Dispers 715W) 0.4%, solubility promoter propylene glycol monomethyl ether 1% and deionized water 7% add successively under whipped state and mix, and are prepared into component a;
(2) with water-base resin (Bayhydrol XP 2621) 30%, water-based defoamer (TEGO Foamex830) 0.5%, deionized water 17% adds successively, and stirs; Add water-based thickener (Viscalex HV30) 9% then, deionized water 10% also continues to stir; Continue to add water-based solubility promoter propylene glycol monomethyl ether 7%, water-based flow agent (EFKA-906) 1%, sterilant (facing phenylphenol) 0.1% and deionized water 11% also stir and are prepared into component b;
(3) under whipped state, component a is added among the b, and mix, and transfer to 7~10 with pH regulator agent adjustment (diethanolamine) 2%, promptly get product.
Embodiment 2
The preparation method of a kind of aqueous automobile single component metal effect retouching paint, this method comprises following processing step:
(1) earlier with water-based aluminium powder pigment (STAPA HYDROLAN 9157) 7%, waterborne polymeric dispersion agent (TEGO Dispers 740W) 0.6%, solubility promoter propylene glycol monomethyl ether 2% and deionized water 4.8% add successively under whipped state and mix, and are prepared into component a;
(2) with water-base resin (Bayhydrol xp 2621) 35%, water-based defoamer (TEGO Foamex822) 0.5%, deionized water 14% adds successively, and stirs; Add water-based thickener (Viscalex HV30) 7% then, ionized water 10% also continues to stir; Continue to add water-based solubility promoter propylene glycol monomethyl ether 6%, water-based flow agent (EFKA-906) 1%, sterilant (facing phenylphenol) 0.1% and deionized water 11% also stir and are prepared into component b;
(3) under whipped state, component a is added among the b, and mix, and transfer to 7~10 with pH regulator agent adjustment (diethanolamine) 1%, promptly get product.
Embodiment 3
The preparation method of a kind of aqueous automobile single component metal effect retouching paint, this method comprises following processing step:
(1) earlier with water-based aluminium powder pigment (STAPA HYDROLAN 2193) 10%, waterborne polymeric dispersion agent (TEGO Dispers 745W) 0.8%, solubility promoter propylene glycol monomethyl ether 1% and deionized water 3.6% add successively under whipped state and mix, and are prepared into component a;
(2) with water-base resin (Bayhydrol xp 2621) 40%, water-based defoamer (TEGO Foamex822) 0.5%, deionized water 11% adds successively, and stirs; Add water-based thickener (Viscalex HV30) 3% then, ionized water 10% also continues to stir; Continue to add water-based solubility promoter propylene glycol monomethyl ether 7%, water-based flow agent (EFKA-906) 1%, sterilant (facing phenylphenol) 0.1% and deionized water 11% also stir and are prepared into component b;
(3) under whipped state, component a is added among the b, and mix, and transfer to 7~10 with pH regulator agent adjustment (diethanolamine) 1%, promptly get product.
Embodiment 4
The preparation method of a kind of environment-friendly water-based automobile single component metal effect retouching paint, this method may further comprise the steps:
(1) with copper powder 3%, aqueous dispersant (water glass) 1.0%, solubility promoter propyl carbinol 0.5% and deionized water 3.1% add successively under whipped state and mix, and are prepared into component a;
(2) with water-borne acrylic resin (JF1605) 50%, water-based defoamer paraffin 0.3%, deionized water 10% add successively, and stir; Add cellulose thickener (HEC) 4% then, deionized water 15% also continues to stir; Continue to add solubility promoter propyl carbinol 0.5%, silicone based water-based flow agent (BYK-341) 0.5%, sterilant (pentachlorophenol) 0.1% and deionized water 10% also stir and are prepared into component b;
(3) under whipped state, component a is added among the component b, and mix, and pH is transferred to 7~10 with pH regulator agent (Pehanorm) 2% accent.
Embodiment 5
The preparation method of a kind of environment-friendly water-based automobile single component metal effect retouching paint, this method may further comprise the steps:
(1) with aluminium powder (STAPA HYDROLAN 9157) 8%, aqueous dispersant (Rapisol) 0.1%, solubility promoter sec-butyl alcohol 1% and deionized water 4% add successively under whipped state and mix, and are prepared into component a;
(2) with hexa methoxy trimeric cyanamide 48%, water-based defoamer emulsion type polysiloxane 1%, deionized water 10% adds successively, and stirs; Add polyurethanes thickening material (Rheolate 212) 6% then, deionized water 10% also continues to stir; Continue to add solubility promoter sec-butyl alcohol 4%, micronization wax emulsion class water-based flow agent (EFKA-906) 0.8%, sterilant (organotin) 0.1% and deionized water 6% also stir and are prepared into component b;
(3) under whipped state, component a is added among the component b, and mix, and pH is transferred to 7~10 with pH regulator agent (diethylamine) 1% accent.
Claims (10)
1. environment-friendly water-based automobile single component metal effect retouching paint, it is characterized in that, this retouching paint comprises following component and weight percentage: water-base resin 30~50%, single component metal effect pigments 3~10%, aqueous dispersant 0.1~1.0%, water-based defoamer 0.3~1.0%, water-based thickener 3~9%, solubility promoter 1~8%; Water-based flow agent 0.5~1%, sterilant 0.1%, pH regulator agent 1~2% and deionized water 30~45%.
2. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint, it is characterized in that, described water-base resin is selected from waterborne polyurethane resin, water-borne acrylic resin, one or more in water-compatible amino resin, the aqueous polyester resin.
3. a kind of environment-friendly water-based automobile single component metal effect according to claim 2 retouching paint, it is characterized in that, described waterborne polyurethane resin is Bayhydrol XP 2648, Bayhydrol XP 2621 or Bayhydrol XP 2650, described water-borne acrylic resin is JF1605, described water-compatible amino resin is the hexa methoxy trimeric cyanamide, and described aqueous polyester resin is ADM-F206.
4. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint, it is characterized in that, described single component metal effect pigments is aluminium powder or copper powder, comprises STAPA HYDROLAN 2192, STAPAHYDROLAN2153 or STAPAHYDROLAN9157.
5. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint, it is characterized in that, described aqueous dispersant is polymeric dispersant or inorganic dispersant, described polymeric dispersant is TEGO Dispers 715W, TEGO Dispers 740W or TEGO Dispers 745W, described inorganic dispersant is silicate, carbonate or poly-phosphate.
6. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint, it is characterized in that, described water-based defoamer is polyether type defoamer, organic defoamer or silicone antifoam agent, described polyether type defoamer is TEGO Foamex 815N, TEGO Foamex 822 or TEGO Foamex 830, described organic defoamer is whiteruss or lipid acid, and described silicone antifoam agent is the emulsion-type polysiloxane.
7. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint, it is characterized in that, described water-based thickener is the polyacrylic thickening material, cellulose thickener or polyurethanes thickening material, described polyacrylic thickening material is Viscalex HV 30, Rheolate 125 or Rheolate 1, described cellulose thickener are HEC or HPC, and described polyurethanes thickening material is Rheolate 212 or Rheolate288.
8. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint is characterized in that described solubility promoter is selected from propyl carbinol, sec-butyl alcohol, Virahol, ethanol, one or more in propylene glycol monomethyl ether, the dipropylene glycol monomethyl ether.
9. a kind of environment-friendly water-based automobile single component metal effect according to claim 1 retouching paint, it is characterized in that, described water-based flow agent is a modified polyorganosiloxane class water-based flow agent, silicone based water-based flow agent or micronization wax emulsion class water-based flow agent, described modified polyorganosiloxane class water-based flow agent is SLIP-FS 444, Levelol W-469 or Levaslip W-461, described silicone based water-based flow agent is BYK-341 or BYK335, and described micronization wax emulsion class water-based flow agent is EFKA-906;
Described sterilant is the substituted arene series bactericidal agent, the heterogeneous ring compound sterilant, the aminated compounds sterilant, the organometallic compound sterilant, described substituted arene series bactericidal agent is pentachlorophenol and sodium salt thereof, daconil M or orthoxenol, and described heterogeneous ring compound sterilant is benzoglyoxaline or oxine, described aminated compounds sterilant is two thiocarbamates or Salicylanlide, and described organometallic compound sterilant is an organotin;
Described pH regulator agent is a diethylamine, triethylamine, diethanolamine, trolamine, Pehanorm, diisopropanolamine (DIPA) or dimethyl isobutyl hydramine.
10. the preparation method of an environment-friendly water-based automobile single component metal effect as claimed in claim 1 retouching paint is characterized in that this method may further comprise the steps:
(1) by weight percentage, with single component metal effect pigments 3~10%, aqueous dispersant 0.1~1.0%, solubility promoter and deionized water add successively under whipped state and mix, and are prepared into component a;
(2) with water-base resin 30~50%, water-based defoamer 0.3~1.0%, deionized water adds successively, and stirs; Add water-based thickener 3~9% then, deionized water also continues to stir; Continue to add solubility promoter, making its total content is 1~8%, water-based flow agent 0.5~1%, and sterilant 0.1% and deionized water also stir and are prepared into component b;
(3) under whipped state, component a is added among the component b, and mix, and pH is transferred to 7~10 with pH regulator agent accent.
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Application publication date: 20110921 |