CN102153391B - Method for producing compound fertilizer from bottom oil of vegetable oil - Google Patents
Method for producing compound fertilizer from bottom oil of vegetable oil Download PDFInfo
- Publication number
- CN102153391B CN102153391B CN2011100415561A CN201110041556A CN102153391B CN 102153391 B CN102153391 B CN 102153391B CN 2011100415561 A CN2011100415561 A CN 2011100415561A CN 201110041556 A CN201110041556 A CN 201110041556A CN 102153391 B CN102153391 B CN 102153391B
- Authority
- CN
- China
- Prior art keywords
- oil
- foot
- vegetable oil
- fermentation
- compound fertilizer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 150000001875 compounds Chemical class 0.000 title claims abstract description 10
- 239000003921 oil Substances 0.000 title abstract description 38
- 235000019198 oils Nutrition 0.000 title abstract description 38
- 235000015112 vegetable and seed oil Nutrition 0.000 title abstract description 14
- 239000008158 vegetable oil Substances 0.000 title abstract description 14
- 239000003337 fertilizer Substances 0.000 title abstract description 9
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 238000000855 fermentation Methods 0.000 claims abstract description 23
- 230000004151 fermentation Effects 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 21
- 230000007935 neutral effect Effects 0.000 claims abstract description 15
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims abstract description 8
- 238000005469 granulation Methods 0.000 claims abstract description 6
- 230000003179 granulation Effects 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 6
- 235000013311 vegetables Nutrition 0.000 claims description 13
- 210000003608 fece Anatomy 0.000 claims description 7
- 239000010871 livestock manure Substances 0.000 claims description 7
- 239000012467 final product Substances 0.000 claims description 2
- 239000000463 material Substances 0.000 abstract description 5
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 abstract 1
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 abstract 1
- 239000001099 ammonium carbonate Substances 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000003344 environmental pollutant Substances 0.000 abstract 1
- 238000011017 operating method Methods 0.000 abstract 1
- 231100000719 pollutant Toxicity 0.000 abstract 1
- 239000004519 grease Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 7
- 238000007127 saponification reaction Methods 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 6
- 239000002699 waste material Substances 0.000 description 6
- 239000002131 composite material Substances 0.000 description 5
- 235000012343 cottonseed oil Nutrition 0.000 description 4
- 239000002385 cottonseed oil Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000011112 process operation Methods 0.000 description 2
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
Landscapes
- Fertilizers (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention discloses a method for producing compound fertilizer from bottom oil of vegetable oil, which comprises the following steps: extracting neutral oil from oil foot of vegetable oil, adding plant ash and ammonium bicarbonate to the neutral oil, thoroughly and uniformly stirring, carrying out stacking fermentation or fermenting in a fermenting tank, and carrying out post treatment, wherein the post treatment comprises granulation, drying and sterile treatment. By using the method, the bottom oil in a vegetable oil mill can be changed into valuables, and pollutants can be changed into beneficial materials, thereby conforming to the current subjects of energy/resource saving and environment protection. Meanwhile, the method has the advantages of simple operating procedures and low production cost, and the compound fertilizer produced by the method meets the industrial standard NY525-2002 of Department of Agriculture.
Description
Technical field
The present invention relates to a kind of method of utilizing the vegetables oil oil foot to produce compound manure.
Background technology
Oil foot behind the vegetable oil mill refinery now is discarded mostly or burns or bury processing, does like this not meeting the principle that present Energy resources take full advantage of, and simultaneously, also physical environment has been caused great pollution.Progress along with the Energy resources recovery and utilization technology, the method of recycling the vegetables oil oil foot is also arranged at present, as utilize vegetable oil residue to synthesize technical matters--" Chinese architecture waterproof " 04 phase of calendar year 2001 of oil foot pitch, comprehensive utilization vegetables oil oil foot method--" grain and grease " 04 phase in 1999--refiltered oil from the vegetables oil oil foot that becomes sour rotten, but so far, the method for utilizing the vegetables oil oil foot to produce compound manure is not arranged.
Summary of the invention
The object of the present invention is to provide a kind of oil foot that can take full advantage of vegetable oil mill to produce the method for compound manure, the method can turn waste into wealth the oil foot of vegetable oil mill, the change pollutent is useful thing, the theme that meets current save energy resource and environmental protection, simultaneously, the method process operations is simple, and production cost is lower.
The method of utilizing the vegetables oil oil foot to produce compound manure of the present invention, its be with the vegetables oil oil foot after extracting neutral oil, add plant ash and bicarbonate of ammonia, stir laggard windrow and put fermentation or in fermentation vat, ferment, aftertreatment gets final product; Described aftertreatment comprises granulation, oven dry, aseptically process; Described vegetables oil oil foot wherein contains a large amount of compound manure effective constituents and a small amount of neutral grease composition from the discarded oil foot that vegetable oil mill produces, and neutral oil can adopt the method for saponification or rinsing with it removal; Described fermentation vat is common marsh gas fermentation pool; Plant ash can be from the fuel waste of bio-power plant.
The described fermentation carried out in room temperature environment and leavening temperature is not higher than 40 ℃,
Described fermentation time is 10-25 days.Summer, general fermentation time was about 15 days, winter fermentation time about 20 days, temperature can be a little more than envrionment temperature during the material fermentation, but temperature is not higher than 40 degrees centigrade.
By weight, the vegetables oil oil foot 50%-60% after extracting neutral oil, plant ash 30%-40%, bicarbonate of ammonia 10-20%.
Method of the present invention can turn waste into wealth the oil foot of vegetable oil mill, and the change pollutent is useful thing, meets the theme of current save energy resource and environmental protection, and simultaneously, the method process operations is simple, and production cost is lower.The present invention effectively has been combined into organic composite fertilizer with waste (pollutent) and the waste after the bio-power plant generating (the insoluble waste that long-pending month of power station day stacked for a long time) of the oil foot (after extracting neutral oil) of vegetable oil mill, and this fertilizer has reached the industry standard NY525-2002 of the Ministry of Agriculture at present.Technique is through adjusting prescription as adding the inorganic nitrogen-sourced high-effective organic and inorganic composite fertilizer products that also can obtain meeting the GB18877-2002 standard such as a certain amount of grouts, urea.
Embodiment
Embodiment 1
Will be from the cottonseed oil foot of vegetable oil mill after neutral grease be removed in saponification, gross weight in fermentation materials, the cottonseed oil foot 60% after the neutral grease is removed in the saponification of learning from else's experience, after discarded plant ash 40% abundant stirring of taking from bio-power plant, add bicarbonate of ammonia 10%, in fermentation vat, ferment, leavening temperature 20-35 ℃, fermentation time is about 15 days, and it is complete rear by granulation to ferment, oven dry, thereby aseptically process obtains the organic composite fertilizer product, product reaches NY525-2002 standard, detected result such as table 1 through check.
Embodiment 2
Will be from the rapeseed oil residue of vegetable oil mill after neutral grease be removed in saponification, gross weight in fermentation materials, the cottonseed oil foot 50% after the neutral grease is removed in the saponification of learning from else's experience, after discarded plant ash 30% abundant stirring of taking from bio-power plant, add bicarbonate of ammonia 20%, in fermentation vat, ferment, leavening temperature 20-35 ℃, fermentation time is about 15 days, and it is complete rear by granulation to ferment, oven dry, thereby aseptically process obtains the organic composite fertilizer product, product reaches NY525-2002 standard, detected result such as table 1 through check.
Embodiment 3
Will be from the soybean oil residue of vegetable oil mill after neutral grease be removed in saponification, gross weight in fermentation materials, the cottonseed oil foot 55% after the neutral grease is removed in the saponification of learning from else's experience, after discarded plant ash 35% abundant stirring of taking from bio-power plant, add bicarbonate of ammonia 10%, in fermentation vat, ferment, leavening temperature 5-10 ℃, fermentation time is about 20 days, and it is complete rear by granulation to ferment, oven dry, thereby aseptically process obtains the organic composite fertilizer product, product reaches NY525-2002 standard, detected result such as table 1 through check.
Table 1
Claims (1)
1. method of utilizing the vegetables oil oil foot to produce compound manure is characterized in that: the vegetables oil oil foot after extracting neutral oil, is added plant ash and bicarbonate of ammonia, stir laggard windrow and put fermentation or ferment in fermentation vat, aftertreatment gets final product; Described aftertreatment comprises granulation, oven dry, aseptically process; By weight, the vegetables oil oil foot 50%-60% after extracting neutral oil, plant ash 30%-40%, bicarbonate of ammonia 10-20%; The described fermentation carried out in room temperature environment and leavening temperature is not higher than 40 ℃; Described fermentation time is 10-25 days.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100415561A CN102153391B (en) | 2011-02-21 | 2011-02-21 | Method for producing compound fertilizer from bottom oil of vegetable oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100415561A CN102153391B (en) | 2011-02-21 | 2011-02-21 | Method for producing compound fertilizer from bottom oil of vegetable oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102153391A CN102153391A (en) | 2011-08-17 |
| CN102153391B true CN102153391B (en) | 2013-10-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011100415561A Expired - Fee Related CN102153391B (en) | 2011-02-21 | 2011-02-21 | Method for producing compound fertilizer from bottom oil of vegetable oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102153391B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242104A (en) * | 2013-05-22 | 2013-08-14 | 徐应先 | Plant liquid fertilizer |
| CN103380689B (en) * | 2013-06-28 | 2015-03-04 | 孙爱军 | Seedling raising method for leaflet type thunbergii |
| CN105439653A (en) * | 2014-09-10 | 2016-03-30 | 范杰 | Biological organic fertilizer and method for producing biological organic fertilizer by utilizing spent bleaching clay residue |
| CN112745171A (en) * | 2021-01-19 | 2021-05-04 | 庞进果 | Water-saving moisturizing nutrient solution and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1077943A (en) * | 1993-05-31 | 1993-11-03 | 赵志来 | Compoiste fertilizer |
| CN1099374A (en) * | 1994-07-30 | 1995-03-01 | 孙明军 | Multiple effect compound flower fertilizer |
| CN1144210A (en) * | 1995-08-25 | 1997-03-05 | 王天珍 | Garbage compound fertilizer |
| CN1587232A (en) * | 2004-09-30 | 2005-03-02 | 李文喜 | Long lasting composite fertilizer |
| CN101624306A (en) * | 2009-07-01 | 2010-01-13 | 刘占义 | Organic fertilizer and preparation process thereof |
| CN101643374A (en) * | 2009-09-09 | 2010-02-10 | 山西大学 | Compound fertilizer |
-
2011
- 2011-02-21 CN CN2011100415561A patent/CN102153391B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1077943A (en) * | 1993-05-31 | 1993-11-03 | 赵志来 | Compoiste fertilizer |
| CN1099374A (en) * | 1994-07-30 | 1995-03-01 | 孙明军 | Multiple effect compound flower fertilizer |
| CN1144210A (en) * | 1995-08-25 | 1997-03-05 | 王天珍 | Garbage compound fertilizer |
| CN1587232A (en) * | 2004-09-30 | 2005-03-02 | 李文喜 | Long lasting composite fertilizer |
| CN101624306A (en) * | 2009-07-01 | 2010-01-13 | 刘占义 | Organic fertilizer and preparation process thereof |
| CN101643374A (en) * | 2009-09-09 | 2010-02-10 | 山西大学 | Compound fertilizer |
Non-Patent Citations (18)
| Title |
|---|
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| 利用大豆油脚或皂脚生产醇酸树脂原料;王公新;《中国油脂》;19981231;第23卷(第06期);第26至27页 * |
| 利用植物油脚合成油脚沥青的技术工艺;孙勤;《中国建筑防水》;20011231(第04期);第26至30页 * |
| 利用植物油脚生产水泥预制构件隔离剂;冯天聪;《中国油脂》;19951231;第20卷(第01期);第62页 * |
| 利用植物油脚-皂脚制备生物柴油的研究;郭应臣等;《南阳师范学院学报》;20070930;第6卷(第09期);第41至44页 * |
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| 浅谈日本对大豆下脚料的综合利用;黄伟宗;《西部粮油科技》;19961231;第21卷(第04期);第52至55页 * |
| 王公新.利用大豆油脚或皂脚生产醇酸树脂原料.《中国油脂》.1998,第23卷(第06期), |
| 王晓辉等.植物油脚的综合利用.《现代化工》.2006,第26卷(第11期), |
| 综合利用植物油油脚方法;孙福;《粮食与油脂》;19991231(第04期);第30页 * |
| 董雅君.植物油脚的综合利用.《安徽科技》.1995,(第02期), |
| 郭应臣等.利用植物油脚-皂脚制备生物柴油的研究.《南阳师范学院学报》.2007,第6卷(第09期), |
| 黄伟宗.浅谈日本对大豆下脚料的综合利用.《西部粮油科技》.1996,第21卷(第04期), |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102153391A (en) | 2011-08-17 |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20110817 Assignee: Wangjiang Hao Hua Oil Co., Ltd. Assignor: Xu Shihua Contract record no.: 2013340000161 Denomination of invention: Method for producing compound fertilizer from bottom oil of vegetable oil Granted publication date: 20131030 License type: Common License Record date: 20131223 |
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| LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
| EC01 | Cancellation of recordation of patent licensing contract |
Assignee: Wangjiang Hao Hua Oil Co., Ltd. Assignor: Xu Shihua Contract record no.: 2013340000161 Date of cancellation: 20171211 |
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| EC01 | Cancellation of recordation of patent licensing contract | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180119 Address after: Yingjiang road 246200 Anhui city of Anqing province Wangjiang County Huayang Town, No. 65 Patentee after: Anhui Heli green organic fertilizer technical limited company Address before: 246200 Anqing City, Anhui Province, Wangjiang County, Yanhe New Village Patentee before: Xu Shihua |
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| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131030 Termination date: 20210221 |
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| CF01 | Termination of patent right due to non-payment of annual fee |