CN102080315A - Method and device for dyeing by utilizing ultrasonic wave and microwave - Google Patents

Method and device for dyeing by utilizing ultrasonic wave and microwave Download PDF

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Publication number
CN102080315A
CN102080315A CN2011100284673A CN201110028467A CN102080315A CN 102080315 A CN102080315 A CN 102080315A CN 2011100284673 A CN2011100284673 A CN 2011100284673A CN 201110028467 A CN201110028467 A CN 201110028467A CN 102080315 A CN102080315 A CN 102080315A
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dyeing
valve
dyestuff
separator
microwave
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CN102080315B (en
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王慧玲
周彬
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Yancheng Textile Vocational and Technical College
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Yancheng Textile Vocational and Technical College
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B13/00Treatment of textile materials with liquids, gases or vapours with aid of vibration

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  • Chemical & Material Sciences (AREA)
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Abstract

The invention provides a method and device for dyeing by utilizing ultrasonic waves and microwaves. The dyeing device comprises a water storage tank WT001, a dye kettle DT001, a dyeing kettle DT002, a separator ST001, an ultrasonic generator SW001-1, an ultrasonic generator SW001-2, an ultrasonic transducer SW001, an ultrasonic transducer SW002 and a microwave generator MW001. The dyeing method comprises the steps of: preparing dye liquor under the action of ultrasonic waves, dyeing fabric under the action of ultrasonic waves and microwaves, treating the dye liquor after dyeing, and recycling the recovered water and dye. The method and device for dyeing has the following benefits: the dyeing efficiency and the dyeing effect are effectively improved without using assistants, and the dye can be recycled; and simultaneously, the dyeing device has simple structure, is convenient to control, reduces energy consumption and saves water resources.

Description

A kind of colouring method and device thereof that utilizes ultrasonic wave and microwave
Technical field
The present invention relates to a kind of colouring method and device thereof, particularly a kind of colouring method and device thereof that utilizes ultrasonic wave and microwave.
Background technology
At present, the colouring method of textiles, mainly still, dyestuff, auxiliary agent etc. are made into certain density dye liquor in water by being mixed, under certain temperature and pressure, textiles is dyeed, its shortcoming is that water loss is too much in the dyeing course, the energy consumption of wastewater treatment is excessive, dye utilization rate is lower, and the production cost height is unfavorable for low-carbon (LC), ecology, environmental protection.Simultaneously,, make that dyestuff and auxiliary agent separating difficulty are bigger, be unfavorable for the recycling of dyestuff owing to use a large amount of auxiliary agents.In recent years, people have developed and have utilized supercritical CO 2The method that textiles is dyeed, though that it has is pollution-free, need not to last dyeing and weaving thing dry, advantage such as conserve water resource, also exist following deficiency: the one, in the whole dyeing course, be to keep CO 2Supercriticality, pressure need reach about 7.38MPa, this high pressure conditions requires too high to equipment, complicated operation is not suitable for industrialization very much.The 2nd, CO 2Bad the keeping of supercriticality, easily destroyed fall and influence its dyeing efficient.The 3rd, because CO 2Non-polar character, can only dissolve dyestuff nonpolar or that polarity is lower, thus the dyestuff that be fit to use be very restricted, DISPERSE DYES generally commonly used, on the kind of dying very limited.
Summary of the invention
For overcoming the deficiencies in the prior art part, the invention provides a kind of colouring method and device thereof that utilizes ultrasonic wave and microwave, to cut down the consumption of energy, the conserve water resource improves dyeing efficient and Color, and does not make used additives, the recyclable utilization of dyestuff.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of colouring method that utilizes ultrasonic wave and microwave may further comprise the steps:
1) preparation of dye liquor is carried out proportioning with dyestuff and water by the requirement of institute's dyeing and weaving thing, adds among the dyestuff still DT001, under heating, stirring condition, adopt the ultrasonic wave of 20kHz-40kHz that the dyestuff of reuniting is carried out high-frequency mechanical vibration, smash into smaller particles, make dye liquor;
2) coloration of textile materials is put into dyeing caldron DT002 with institute's dyeing and weaving thing, and according to institute's dyeing and weaving thing and quality thereof, bath raio on demand adds the above-mentioned dye liquor that makes among the dyeing caldron DT002; Under the ultrasonic wave of 20kHz-40kHz, 2000-3000MHz microwave condition, textile dyeing 0.2-0.5h;
3) dye liquor among the dyeing caldron DT002 is pumped in the recovery of dyestuff, enters after the filtration among the separator ST001; To separator ST001 extracting vacuum and heating, among the steam importing condenser C001 with evaporation, the water that condensation forms is used for dyeing next time; Reclaim isolated dyestuff among the dyeing caldron DT002, be used for dyeing next time;
4) post processing of DYED FABRICS adds entry in dyeing caldron DT002, the fabric after the dyeing is cleaned one to twice, cleans the waste water that produces and adopts above-mentioned steps 3) handle DYED FABRICS oven dry or airing after the cleaning.
Water in the above-mentioned adding dyestuff still is soft water.
A kind ofly realize the above-mentioned device that utilizes the colouring method of ultrasonic wave and microwave, comprise water storage tank WT001, dyestuff still DT001, dyeing caldron DT002, separator ST001, supersonic generator SW001-1, supersonic generator SW001-2, ultrasonic transducer SW001, ultrasonic transducer SW002 and microwave generator MW001; Described water storage tank WT001 interlinks through measuring pump MP001 and dyestuff still DT001; Dyestuff still DT001 is equipped with heater H 001, agitator SM001 and ultrasonic transducer SW001, and dyestuff still DT001 interlinks through measuring pump MP002 and dyeing caldron DT002; Dyeing caldron DT002 is equipped with ultrasonic transducer SW002 and microwave generator MW001, ultrasonic transducer SW001 links to each other with supersonic generator SW001-1, ultrasonic transducer SW002 links to each other with supersonic generator SW001-2, and dyeing caldron DT002 interlinks by circulating pump CP003 and separator ST001; Separator ST001 is equipped with heater H 002 and vavuum pump VP001, and separator ST001 links to each other with condenser C001 by circulating pump CP004; Condenser C001 links to each other with water storage tank WT001 by check valve VS001.
For improving the operating efficiency of device, realize control automatically, this device also comprises control module PC001, and above-mentioned supersonic generator SW001-1, supersonic generator SW001-2, microwave generator MW001, measuring pump MP001, measuring pump MP002, heater H 001 and heater H 002 all link to each other with this control module PC001.
Further, between above-mentioned water storage tank WT001 and dyeing caldron DT002, also be provided with valve V001, filter F 001, circulating pump CP001, valve V002; Water storage tank WT001, valve V001, filter F 001, circulating pump CP001, measuring pump MP001, valve V002 and dyestuff still DT001 link to each other successively.
Further, also be provided with circulating pump CP002 and valve V003 between dyestuff still DT001 and dyeing caldron DT002, dyestuff still DT001, circulating pump CP002, measuring pump MP002, valve V003 and dyeing caldron DT002 link to each other successively.
Further, also be provided with filter F 002 and valve V004 between dyeing caldron DT002 and separator ST001, dyeing caldron DT002, filter F 002, circulating pump CP003, valve V004 and separator ST001 link to each other successively.
Further, also be provided with valve V006 and filter F 003 between separator ST001 and condenser C001, separator ST001, valve V006, filter F 003, circulating pump CP004 and condenser C001 link to each other successively.
Further, above-mentioned separator ST001 links to each other with dyestuff still DT001 by powder metering device MP003, valve V005, be delivered among the dyestuff still DT001 with the dyestuff that will reclaim, and powder metering device MP003 links to each other with control module PC001.
Beneficial effect of the present invention is: improve dyeing efficient and Color effectively, and do not make used additives, the recyclable utilization of dyestuff.Simultaneously, dyeing apparatus of the present invention is simple in structure, and control is convenient, has reduced energy consumption, has saved water resource.
Description of drawings
Fig. 1 is a structural representation of the present invention.
The specific embodiment
The invention will be further described below in conjunction with drawings and Examples.
Embodiment one
The device of the dyeing that utilizes ultrasonic wave and microwave that the embodiment of the invention adopted comprises water storage tank WT001, dyestuff still DT001, dyeing caldron DT002, separator ST001, supersonic generator SW001-1, supersonic generator SW001-2, ultrasonic transducer SW001, ultrasonic transducer SW002, microwave generator MW001 and control module PC001; Valve V001, filter F 001, circulating pump CP001, measuring pump MP001 and the valve V002 of described water storage tank WT001 through linking to each other successively, and link to each other with dyestuff still DT001.Dyestuff still DT001 is equipped with heater H 001, agitator SM001 and ultrasonic transducer SW001, and dyestuff still DT001 links to each other with dyeing caldron DT002 with valve V003 through circulating pump CP002, the measuring pump MP002 that links to each other successively.Dyeing caldron DT002 is equipped with ultrasonic transducer SW002 and microwave generator MW001, ultrasonic transducer SW002 links to each other with supersonic generator SW001-1, ultrasonic transducer SW003 links to each other with supersonic generator SW001-2, and dyeing caldron DT002 links to each other with separator ST001 through continuous successively filter F 002, circulating pump CP003 and valve V004.Separator ST001 is equipped with heater H 002 and vavuum pump VP001, and separator ST001 links to each other with condenser C001 by the valve V006, filter F 003 and the circulating pump CP004 that link to each other successively.Condenser C001 links to each other with water storage tank WT001 by check valve VS001.Separator ST001 also links to each other with dyestuff still DT001 by powder metering device MP003, valve V005.Above-mentioned supersonic generator SW001-1, supersonic generator SW001-2, microwave generator MW001, measuring pump MP001, measuring pump MP002, powder metering device MP003, heater H 001, heater H 002 all link to each other with this control module PC001.
The described colouring method that utilizes ultrasonic wave and microwave of the embodiment of the invention for adopting said apparatus, is 80 with the direct black BN dyestuff to specification S* 80 S/ 110 * 7758 ", the cotton muslin of 5kg dyes and is example:
1) preparation of dye liquor, open valve V001, soft water in the water storage tank WT001 filters the back under the effect of circulating pump CP001 through filter F 001, water through measuring pump MP001 metering 75L enters among the dyestuff still DT001, and add the direct black BN dyestuff of 25g by the drain hole FL001 on the dyestuff still DT001, valve-off V001 and V002 then, 001 pair of dyestuff still of heater H DT001 carry out the time constant-temperature heating, and temperature is 50 ℃; Agitator SM001 begins constant speed and stirs, and speed is 1000rpm; Supersonic generator SW001 starts working, and its frequency is 20kHz, and power is 2kw.Make the dye liquor that concentration is 0.33g/L behind the 2min;
2) coloration of textile materials is 80 with 5kg, specification S* 80 S/ 110 * 7758 " cotton muslin is put into dyeing caldron DT002 by putting thing mouth FW001; open valve V003 then; the dye liquor among the dyestuff still DT001 enters among the dyeing caldron DT002 through circulating pump CP002 and measuring pump MP002, reach 1: 15 bath raio after, valve-off V003; Supersonic generator SW002 and microwave generator MW001 start working; Frequency of ultrasonic is 20kHz, and the frequency of microwave is 2000MHz; Because hydrone is a polar molecule, it is under the high-frequency electromagnetic field action of quick alternation, its polarity orientation will change along with the variation of external electric field, cause the motion of hydrone to produce mutual friction effect, the field energy of microwave field is converted into heat energy, inside and outside simultaneously the heating, make textiles reach inside and outside effect at short notice with heat, produce thermalization and a series of materializing procedures such as expanded, accelerated the infiltration of dye liquor to textiles, dyeing uniformity improves greatly, can also change the surface texture and the supramolecular structure of fiber, improves dye-uptake and degree of fixation.Simultaneously ultrasonic wave is among fiber surface " cavitation " effect that produces makes the easier space and micropore that is diffused between the fiber of dyestuff, thereby further improved dyeing efficient and dye-uptake.Dyeing temperature is 80 ℃; Dyeing time is 0.3 hour;
3) recovery of dyestuff, open valve V004, the dye liquor among the dyeing caldron DT002 under the effect of circulating pump CP003 through filter F002, behind the impurity such as fiber in the filtering dyeing course under the textiles band, enter in the separator ST001, dye liquor separates with textiles among the dyeing caldron DT002 thereby make; Valve-off V 004, open valve V006 and check valve VS 001, vavuum pump VP001 vacuumizes separator ST001,002 pair of dye liquor of heater H heats simultaneously, make the water in the dye liquor under low-pressure state, gasify and separate with dyestuff than being easier to, steam turns back to water vapor condensation liquefaction among the water storage tank WT001 through condenser C001, one-way cock VS001 under the effect of circulating pump CP004 again.Valve-off V006 opens valve V005, separates also dry dyestuff and gets back among the dyestuff still DT001 after powder metering device MP003 metering, uses for dyeing next time, then valve-off V005.
4) post processing of DYED FABRICS, open valve V007, directly from water storage tank WT001, add water in dyeing caldron DT002, supersonic generator SW002 and microwave generator MW001 wash the cotton muslin and handle 1-2 time, clean the waste water that produces and adopt above-mentioned steps 3) to handle, the dyeing cotton muslin after the cleaning carries out microwave drying or airing.
Cotton muslin after the dyeing, adopting the computer colour photometer to measure its apparent colour degree of depth K/S value is 28.752; Measure its dry friction variable color fastness by the method for GB/T3920-1997 and reach the 4-5 level, 4 grades of staining fastnesses (standard lining cloth cotton), wet friction variable color fastness reaches the 3-4 level, 4 grades of staining fastnesses (standard lining cloth cotton); Soaping fastness is pressed the method for GB/T3921 (1)-1999 and is measured, and is 3 grades, staining fastness (standard lining cloth cotton) 3-4 level.Therefore after the dyeing, colour fastness to rubbing, the color fastness to washing of fabric are good, good level-dyeing property, COLOR FASTNESS height.
Embodiment two
The device of the dyeing that utilizes ultrasonic wave and microwave that present embodiment adopted is with embodiment one.
The described colouring method that utilizes ultrasonic wave and microwave of inventive embodiments for adopting said apparatus, is 100 with neutral black S-GL dyestuff to specification S* 80 S/ 150 * 13088 ", the real silk fabric of 5kg dyes and is example:
1) preparation of dye liquor, open valve V001, water in the water storage tank WT001 filters the back under the effect of circulating pump CP001 through filter F 001, water through measuring pump MP001 metering 60L enters among the dyestuff still DT001, and add the neutral black S-GL dyestuff of 25g by the drain hole FL001 on the dyestuff still DT001, valve-off V001 and V002 then, 001 pair of dyestuff still of heater H DT001 carry out the time constant-temperature heating, and temperature is 50 ℃; Agitator SM001 begins constant speed and stirs, and speed is 1000rpm; Supersonic generator SW001 starts working, and its frequency is 30kHz, and power is 1.5kw.2min makes the dye liquor that concentration is 0.42g/L after the time;
2) coloration of textile materials, with 5kg, specification is 100S * 80S/150 * 13088 " real silk fabric put into dyeing caldron DT002 by putting thing mouth FW001; open valve V003 then; the dye liquor among the dyestuff still DT001 enters among the dyeing caldron DT002 through circulating pump CP002 and measuring pump MP002; after reaching 1: 12 bath raio, valve-off V003; Supersonic generator SW00 and microwave generator MW001 start working; Frequency of ultrasonic is 30kHz, and the frequency of microwave is 2500MHz; Dyeing time is 0.3 hour.Dyeing temperature is 100 ℃;
3) recovery of dyestuff, open valve V004, the dye liquor among the dyeing caldron DT002 under the effect of circulating pump CP003 through filter F002, behind the impurity such as fiber in the filtering dyeing course under the textiles band, enter in the separator ST001, dye liquor separates with textiles among the dyeing caldron DT002 thereby make; Valve-off V004, open valve V006 and check valve VS001, vavuum pump VP001 vacuumizes separator ST001,002 pair of dye liquor of heater H heats simultaneously, make the water in the dye liquor under low-pressure state, gasify and separate with dyestuff than being easier to, steam turns back to water vapor condensation liquefaction among the water storage tank WT001 through condenser C001, one-way cock VS001 under the effect of circulating pump CP004 again.Valve-off V006 opens valve V005, separates also dry dyestuff and gets back among the dyestuff still DT001 after powder metering device MP003 metering, uses for dyeing next time, then valve-off V005.
4) post processing of DYED FABRICS, open valve V007, directly from water storage tank WT001, add water in dyeing caldron DT002, supersonic generator SW002 and microwave generator MW001 wash real silk fabric and handle 1-2 time, clean the waste water that produces and adopt above-mentioned steps 3) to handle, the dyeing of real silk fabric after the cleaning carries out microwave drying or airing.
Real silk fabric after the dyeing, adopting the computer colour photometer to measure its apparent colour degree of depth K/S value is 21.312; Measure its dry friction variable color fastness by the method for GB/T3920-1997 and reach 5 grades, staining fastness (standard lining cloth silk) 4-5 level, wet friction variable color fastness reaches the 4-5 level, staining fastness (standard lining cloth silk) 4-5 level; Soaping fastness is determined as 3 grades by the method for GB/T3921 (1)-1999, staining fastness (standard lining cloth silk) 3-4 level.Therefore after the dyeing, colour fastness to rubbing, the color fastness to washing of fabric are good, good level-dyeing property, COLOR FASTNESS height.
Embodiment three
The device of the dyeing that utilizes ultrasonic wave and microwave that present embodiment adopted is with embodiment one.The described colouring method that utilizes ultrasonic wave and microwave of inventive embodiments for adopting said apparatus, is 80 with Disperse Blue BGL to specification S* 80 S/ 120 * 10058 ", the terylene poplin cloth fabric of 5kg dyes and is example:
1) preparation of dye liquor, open valve V001, water in the water storage tank WT 001 filters the back under the effect of circulating pump CP001 through filter F 001, water through measuring pump MP001 metering 100L enters among the dyestuff still DT001, and add the Disperse Blue BGL of 25g by the drain hole FL001 on the dyestuff still DT001, valve-off V001 and V002 then, 001 pair of dyestuff still of heater H DT001 carry out the time constant-temperature heating, and temperature is 50 ℃; Agitator SM001 begins constant speed and stirs, and speed is 1000rpm; Supersonic generator SW001 starts working, and its frequency is 40kHz, and power is 1kw.2min makes the dye liquor that concentration is 0.25g/L after the time;
2) coloration of textile materials is 80 with 5kg, specification S* 80 S/ 120 * 10058 " terylene poplin cloth fabric is put into dyeing caldron DT002 by putting thing mouth FW001; open valve V003 then; the dye liquor among the dyestuff still DT001 enters among the dyeing caldron DT002 through circulating pump CP002 and measuring pump MP002, reach 1: 20 bath raio after, valve-off V003; Supersonic generator SW00 and microwave generator MW001 start working; Frequency of ultrasonic is 40kHz, and the frequency of microwave is 4000MHz; Dyeing time is 0 one hours.Dyeing temperature is 130 ℃;
3) recovery of dyestuff, open valve V004, with the process filter F002 under the effect of circulating pump CP003 of the dye liquor among the dyeing caldron DT002, behind the impurity such as fiber in the filtering dyeing course under the textiles band, enter in the separator ST001, dye liquor separates with textiles among the dyeing caldron DT002 thereby make; Valve-off V004, open valve V006 and check valve VS001, vavuum pump VP001 vacuumizes separator ST001,002 pair of dye liquor of heater H heats simultaneously, make the water in the dye liquor under low-pressure state, gasify and separate with dyestuff than being easier to, steam turns back to water vapor condensation liquefaction among the water storage tank WT001 through condenser C001, one-way cock VS001 under the effect of circulating pump CP004 again.Valve-off V006 opens valve V005, separates also dry dyestuff and gets back among the dyestuff still DT001 after powder metering device MP003 metering, uses for dyeing next time, then valve-off V005.
4) post processing of DYED FABRICS, open valve V007, directly from water storage tank WT001, add water in dyeing caldron DT002, supersonic generator SW002 and microwave generator MW001 wash terylene poplin cloth fabric and handle 1-2 time, clean the waste water that produces and adopt above-mentioned steps 3) to handle, the dyeing terylene poplin cloth fabric after the cleaning carries out microwave drying or airing.
Terylene poplin cloth fabric after the dyeing, adopting the computer colour photometer to measure its apparent colour degree of depth K/S value is 21.312; Measure its dry friction variable color fastness by the method for GB/T3920-1997 and reach 5 grades, staining fastness (standard lining cloth polyester) 4-5 level, wet friction variable color fastness reaches the 4-5 level, staining fastness (standard lining cloth polyester) 4-5 level; Soaping fastness is determined as 3 grades by the method for GB/T3921 (1)-1999, staining fastness (standard lining cloth polyester) 3-4 level.Therefore after the dyeing, colour fastness to rubbing, the color fastness to washing of fabric are good, good level-dyeing property, COLOR FASTNESS height.

Claims (10)

1. colouring method that utilizes ultrasonic wave and microwave is characterized in that: may further comprise the steps,
1) preparation of dye liquor is carried out proportioning with dyestuff and water by the requirement of institute's dyeing and weaving thing, adds among the dyestuff still DT001, under heating, stirring condition, adopt the ultrasonic wave of 20kHz-40kHz that the dyestuff of reuniting is carried out high-frequency mechanical vibration, smash into smaller particles, make dye liquor;
2) coloration of textile materials is put into dyeing caldron DT002 with institute's dyeing and weaving thing, and according to institute's dyeing and weaving thing and quality thereof, bath raio on demand adds the above-mentioned dye liquor that makes among the dyeing caldron DT002; Under the ultrasonic wave of 20kHz-40kHz, 2000-3000MHz microwave condition, textile dyeing 0.2-0.5h;
3) dye liquor among the dyeing caldron DT002 is pumped in the recovery of dyestuff, enters after the filtration among the separator ST001; To separator ST001 extracting vacuum and heating, among the steam importing condenser C001 with evaporation, the water that condensation forms is used for dyeing next time; Reclaim isolated dyestuff among the dyeing caldron DT002, be used for dyeing next time;
4) post processing of DYED FABRICS adds entry in dyeing caldron DT002, the fabric after the dyeing is cleaned one to twice, cleans the waste water that produces and adopts above-mentioned steps 3) handle DYED FABRICS oven dry or airing after the cleaning.
2. a kind of colouring method that utilizes ultrasonic wave and microwave according to claim 1 is characterized in that: the water in the above-mentioned adding dyestuff still is soft water.
3. realize the described device that utilizes the colouring method of ultrasonic wave and microwave of claim 1 for one kind, it is characterized in that: comprise water storage tank WT001, dyestuff still DT001, dyeing caldron DT002, separator ST 001, supersonic generator SW001-1, supersonic generator SW001-2, ultrasonic transducer SW001, ultrasonic transducer SW002 and microwave generator MW001; Described water storage tank WT001 interlinks through measuring pump MP001 and dyestuff still DT001; Dyestuff still DT001 is equipped with heater H 001, agitator SM001 and ultrasonic transducer SW001, and dyestuff still DT001 interlinks through measuring pump MP002 and dyeing caldron DT002; Dyeing caldron DT002 is equipped with ultrasonic transducer SW002 and microwave generator MW001, ultrasonic transducer SW001 links to each other with supersonic generator SW001-1, ultrasonic transducer SW002 links to each other with supersonic generator SW001-2, and dyeing caldron DT002 interlinks by circulating pump CP003 and separator ST001; Separator ST001 is equipped with heater H 002 and vavuum pump VP001, and separator ST001 links to each other with condenser C001 by circulating pump CP004; Condenser C001 links to each other with water storage tank WT001 by check valve VS001.
4. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 3 is characterized in that: also comprise control module PC001; Above-mentioned supersonic generator SW001-1, supersonic generator SW001-2, microwave generator MW001, measuring pump MP001, measuring pump MP002, heater H 001 and heater H 002 all link to each other with this control module PC001.
5. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 3 is characterized in that: also be provided with valve V001, filter F 001, circulating pump CP001, valve V002 between above-mentioned water storage tank WT001 and dyeing caldron DT002; Water storage tank WT001, valve V001, filter F 001, circulating pump CP001, measuring pump MP001, valve V002 and dyestuff still DT001 link to each other successively.
6. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 3, it is characterized in that: also be provided with circulating pump CP002 and valve V003 between dyestuff still DT001 and dyeing caldron DT002, dyestuff still DT001, circulating pump CP002, measuring pump MP002, valve V003 and dyeing caldron DT002 link to each other successively.
7. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 3, it is characterized in that: also be provided with filter F 002 and valve V004 between dyeing caldron DT002 and separator ST001, dyeing caldron DT002, filter F 002, circulating pump CP003, valve V004 and separator ST001 link to each other successively.
8. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 3, it is characterized in that: also be provided with valve V006 and filter F 003 between separator ST001 and condenser C001, separator ST001, valve V006, filter F 003, circulating pump CP004 and condenser C001 link to each other successively.
9. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 3 is characterized in that: above-mentioned separator ST001 links to each other with dyestuff still DT001 by powder metering device MP003, valve V005.
10. a kind of device that utilizes the colouring method of ultrasonic wave and microwave according to claim 9 is characterized in that: powder metering device MP003 links to each other with control module PC001.
CN201110028467A 2011-01-14 2011-01-14 Method and device for dyeing by utilizing ultrasonic wave and microwave Expired - Fee Related CN102080315B (en)

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CN103255653A (en) * 2013-04-08 2013-08-21 江阴骏华纺织科技有限公司 Dyeing process and dyeing apparatus for collagen fiber regenerated leather
CN105133231A (en) * 2015-08-14 2015-12-09 湖州新隆龙丝绸印花有限公司 Vertical condensation dyeing machine for silk by utilizing microwaves
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CN105133235A (en) * 2015-08-14 2015-12-09 湖州新隆龙丝绸印花有限公司 Automatic vertical water-cooling dyeing machine for silk by utilizing microwaves
CN105256617A (en) * 2015-11-23 2016-01-20 天津工业大学 Reusing method for reverse micelle dyeing system
CN107869015A (en) * 2016-09-27 2018-04-03 卡尔迈耶罗泰尔有限责任公司 For being applied to webs with the apparatus and method of dye liquor
CN107974784A (en) * 2016-10-25 2018-05-01 财团法人金属工业研究发展中心 Microwave dyeing equipment and microwave dyeing method
CN108754961A (en) * 2018-09-17 2018-11-06 吴国平 Plant dyeing system based on ultrasonic wave and microwave technology
CN110983684A (en) * 2019-12-09 2020-04-10 浙江丝绸科技有限公司 Full-process circulating dyeing method and dyeing system for real silk fabric
TWI703254B (en) * 2019-10-11 2020-09-01 大陸商上海複璐帝流體技術有限公司 Supercritical carbon dioxide printing and dyeing process and the system thereof
CN117026555A (en) * 2023-09-19 2023-11-10 江苏格罗瑞节能科技有限公司 Yarn dyeing device and dyeing method thereof

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CN102587057A (en) * 2012-02-22 2012-07-18 杭州智能染整设备有限公司 High-temperature energy-saving dyeing machine
CN102852008A (en) * 2012-09-06 2013-01-02 青岛大学 Method for improving cationic paint dyeing uniformity by using ultrasonic waves
CN102852008B (en) * 2012-09-06 2014-05-21 青岛大学 Method for improving cationic paint dyeing uniformity by using ultrasonic waves
CN103255653A (en) * 2013-04-08 2013-08-21 江阴骏华纺织科技有限公司 Dyeing process and dyeing apparatus for collagen fiber regenerated leather
CN103255653B (en) * 2013-04-08 2015-04-15 江阴骏华纺织科技有限公司 Dyeing process and dyeing apparatus for collagen fiber regenerated leather
CN105133231A (en) * 2015-08-14 2015-12-09 湖州新隆龙丝绸印花有限公司 Vertical condensation dyeing machine for silk by utilizing microwaves
CN105133229A (en) * 2015-08-14 2015-12-09 湖州新隆龙丝绸印花有限公司 Automatic vertical condensation dyeing machine for silk by utilizing microwaves
CN105133230A (en) * 2015-08-14 2015-12-09 湖州新隆龙丝绸印花有限公司 Vertical water-cooling dyeing machine for silk by utilizing microwaves
CN105133235A (en) * 2015-08-14 2015-12-09 湖州新隆龙丝绸印花有限公司 Automatic vertical water-cooling dyeing machine for silk by utilizing microwaves
CN105256617B (en) * 2015-11-23 2017-10-20 天津工业大学 A kind of reuse method of reverse micelle dyeing system
CN105256617A (en) * 2015-11-23 2016-01-20 天津工业大学 Reusing method for reverse micelle dyeing system
CN107869015A (en) * 2016-09-27 2018-04-03 卡尔迈耶罗泰尔有限责任公司 For being applied to webs with the apparatus and method of dye liquor
CN107869015B (en) * 2016-09-27 2023-05-23 卡尔迈耶罗泰尔有限责任公司 Device and method for applying a dye liquor to a textile web
CN107974784A (en) * 2016-10-25 2018-05-01 财团法人金属工业研究发展中心 Microwave dyeing equipment and microwave dyeing method
CN108754961A (en) * 2018-09-17 2018-11-06 吴国平 Plant dyeing system based on ultrasonic wave and microwave technology
TWI703254B (en) * 2019-10-11 2020-09-01 大陸商上海複璐帝流體技術有限公司 Supercritical carbon dioxide printing and dyeing process and the system thereof
CN110983684A (en) * 2019-12-09 2020-04-10 浙江丝绸科技有限公司 Full-process circulating dyeing method and dyeing system for real silk fabric
CN110983684B (en) * 2019-12-09 2022-08-23 浙江丝绸科技有限公司 Full-process circulating dyeing method and dyeing system for real silk fabric
CN117026555A (en) * 2023-09-19 2023-11-10 江苏格罗瑞节能科技有限公司 Yarn dyeing device and dyeing method thereof
CN117026555B (en) * 2023-09-19 2023-12-12 江苏格罗瑞节能科技有限公司 Yarn dyeing device and dyeing method thereof

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