CN102070331B - Preparation method of premixed raw material of ferrite magnet presintering material and production device thereof - Google Patents
Preparation method of premixed raw material of ferrite magnet presintering material and production device thereof Download PDFInfo
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- CN102070331B CN102070331B CN200910272847A CN200910272847A CN102070331B CN 102070331 B CN102070331 B CN 102070331B CN 200910272847 A CN200910272847 A CN 200910272847A CN 200910272847 A CN200910272847 A CN 200910272847A CN 102070331 B CN102070331 B CN 102070331B
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Abstract
The invention relates to a preparation method of a premixed raw material of a ferrite magnet presintering material, belonging to the production field of the raw material of manufacturing industry. The method comprises the following steps: firstly, sending coarse slurry which is prepared by mixing premixed coarse material in a tube mill, performing continuous mixing and grinding in the tube mill to prepare uniform, regular and fine premixed raw material, then sending the premixed raw material to a large capacity precisely-controlled tank, and performing homogenizing treatment to the premixed raw material through the longitudinal circular stirring of pump delivery, the transverse stirring of the agitation impeller and the edge stirring of the vertical fins on the tank wall; and secondly, detecting the components, and adjusting accurately to prepare the premixed raw material with accurate components and uniform grain size. The method of the invention adopts continuous production and does not adopt the traditional and extensive batch production method of the ball mill, thus the production efficiency can be obviously increased, the labor intensity of the operator and the production cost can be reduced, the working environment can be improved, the grain size and components of the premixed raw material slurry product can be highly consistent and accurate and a solid foundation can be laid for the improvement of the quality grades of the downstream magnetic products.
Description
Technical field
The preparation method and the production unit thereof of the premix raw material of a kind of permanent ferrite prefiring material of the present invention belong to production raw material production field, particularly the feedstock production process of wet production permanent ferrite prefiring material.
Background technology
When preparing the premix raw material of permanent ferrite prefiring material; Its key is to control the homogeneity of premix raw material granularity and the accuracy of batch mixing composition, if granularity heterogeneity, the batch mixing composition ratio of the premix raw material of preparation are inaccurate, pre-burning material sintering temperature is different in the time of will causing subsequent production; Therefore cause a large amount of waste products; Even the inadequate thermal sintering of pre-burning material after the adjustment sintering temperature, sintering temperature and influences the quality of its derived product the most at last also with difference when follow-up making magnetic device.The primary raw materials iron oxide red of said this premix raw material is the acid washing iron red recovered material that comes from metallurgy industry.Therefore, the core of guaranteeing to produce the grade quality of permanent ferrite prefiring material is to improve grade quality, the homogeneity of premix raw material granularity and the accuracy of batch mixing composition of its premix raw material.But existing production can not meet the demands.At present, the preparation method of the premix raw material of permanent ferrite prefiring material summarizes has following two kinds:
One, ball milling mechanism material
The industry generally adopts ball milling mechanism material method, uses the ball mill abrasive material, adopts the multimachine running for satisfying to produce, and ball mill quantity is many; Every table grinder batching needs to open and close the ball mill door, after release mesh, from the ball mill blanking, to stirring hold-up vessel; This method is batch production, expects loading and unloading and grinds length consuming time for every jar, and fully by MC; Labor strength is big, and mechanical floor space is big, the easy contaminate environment of slip.More than batch, in batches little, each batch quality, grade are disperseed, though sampling Detection often, the quality and the grade of the material that grinds are inconsistent, are difficult to meet the demands.
Two, ball mill, sand mill are united the system material
Adopt ball milling, sand milling to unite the system material, the input and output material mode that ball mill is opened and closed door changes batch mixing in advance into, gets into ball mill through pipeline again; And increase follow-up sand mill auxiliary abrasive; Improve production efficiency though this method solves than ball milling mechanism material, improved the homogeneity of batch mixing, but still be batch production; Still exist mechanical floor space big, the still easy contaminate environment of slip.
Summary of the invention
The preparation method who the purpose of this invention is to provide a kind of premix raw material of permanent ferrite prefiring material; Produce preparation to realize premix raw material continuity; Improve the accuracy of premix raw material granularity homogeneity and batch mixing composition, and, the production efficiency that system is expected improved; Reduce labor strength, improve operating environment.
The present invention realizes through following technical scheme:
The preparation method of the premix raw material of permanent ferrite prefiring material of the present invention; At first; Adopt surge pump to send into tube mill pro rata premix coarse fodder and water blended coarse fodder slurry; This coarse fodder slurry through the continuous mixed grinding of steel ball, becomes the fine-grained premix raw material of even standard in tube mill, it is sent in the smart control jar of large vol again; And vertical circulation stirring of in jar, carrying through pump power, the horizontal stirring of paddle wheel and the side stirring of the vertical fin of tank skin, the premix raw material is carried out homogenizing handle; Then this premix raw material is carried out composition detection, and after doing the accurate adjustment of composition according to detected result, satisfying preparation, to become composition accurate, the premix raw material of the permanent ferrite prefiring material that granularity is consistent.
The preparing method's of the premix raw material of permanent ferrite prefiring material tube grinds material equipment according to the present invention, comprises the pit type mixer, tube mill; Stock chest; Large vol essence control jar and pump are communicated with through pipeline between this pit type mixer, tube mill, stock chest, the smart control jar of large vol, and slip is by pump delivery; Characteristics are that the smart control jar of large vol has the vertical recycle pump of slip and pipeline, paddle wheel, and tank skin is provided with vertical fin.
The preparing method's of the premix raw material of permanent ferrite prefiring material the technology according to the present invention may further comprise the steps:
1, premix coarse fodder and water blended coarse fodder slurry is levigate through mixing continuously in tube mill, becomes the fine granularity premix raw material of even standard;
2, the fine granularity premix raw material of above-mentioned even standard circulates vertically through pump power in the smart control of large vol jar that stirrings, large stretch of impeller laterally stir and the side of the vertical fin of tank skin stirs, and fine granularity premix raw material is carried out the homogenizing processing;
3, the premix raw material of handling through above-mentioned steps 2 homogenizing is carried out composition detection, and, composition is precisely adjusted according to detected result.
The inventive method already provides a kind of successive working method for this; Make the industry take off fully pendulum Traditional use ball mill intermittence extensive style working method, in the inventive method and device scheme, adopted the smart control of large vol jar to design; Its tank skin vertically is provided with fin; In jar big blade stirring wheel and pump power circulating line are set, premix raw material slip obtains the homogenizing processing that sufficient mechanical type stirs, stirs in this jar, then carry out composition detection and meticulous adjustment again; Therefore guaranteed that the granularity of the former slip product of premix and the height one of composition make peace precisely, for the grade quality of raising downstream magnet product has been established solid foundation; In addition, the present invention has significantly improved production efficiency, greatly reduces operator's labour intensity, and has reduced production cost, has improved operating environment.
Description of drawings
Fig. 1, tube of the present invention grind the materials device synoptic diagram
Embodiment
Combine tube of the present invention to grind materials device accompanying drawing and embodiment at present, further specify the present invention and how to implement:
The preparing method's of the premix raw material of permanent ferrite prefiring material tube grinds material equipment according to the present invention, and about 30 cubic metres of the smart control of the large vol of employing tank volume can hold every batch and feed intake 40 tons.Concrete grammar step such as following embodiment are said.
Embodiment:
1, red iron oxide coarse fodder, Strontium carbonate powder, water are pressed processing compound, pour pit type mixer 1 into, mix 1 hour;
2, the slip that mixes is transported to tube mill 4 and is ground by pump 2, transport pipe 3, and tube mill is pressed the different configuration of raw material steel ball, grinds granularity by inlet amount control.
3, grind the qualified material of back granularity and leave stock chest 7 in; Be transported to the smart control jar 10 of large vol through pump 8, transport pipe 9, an essence control jar opening for feed 11; Start paddle wheel 12, smart control jar slurry circulation pipeline 13 simultaneously; The stirring of the smart control jar 10 tank skin fins of large vol in addition is to the processing of stirring of slip.
4, slip carries out composition analysis in the hold-up vessel to stirring with the xrf analysis appearance, and accurately adjusts according to analytical results, and until being specification product, it is subsequent use to supply to go on foot operation down.
Claims (3)
1. the preparation method of the premix raw material of permanent ferrite prefiring material at first, starches premix coarse fodder and water blended coarse fodder; Adopt surge pump to send into tube mill; This coarse fodder slurry through the continuous mixed grinding of steel ball, becomes the fine-grained premix raw material of even standard in tube mill, it is sent in the smart control jar of large vol again; And vertical circulation stirring of in this jar, carrying through pump power, the horizontal stirring of paddle wheel and the side stirring of the vertical fin of tank skin, the premix raw material is carried out homogenizing handle; Then this premix raw material is carried out composition detection, and after doing the accurate adjustment of composition according to detected result, satisfying preparation, to become composition accurate, the premix raw material that granularity is consistent.
2. be used for the said permanent ferrite prefiring material of claim 1 the premix raw material the preparation method the tube grind material equipment, comprise the pit type mixer, tube mill; Stock chest, large vol essence control jar and pump are communicated with through pipeline between this pit type mixer, tube mill, stock chest, the smart control jar of large vol; Slip is carried by pump power; It is characterized in that the smart control jar of large vol has the vertical circulating line of slip, paddle wheel, tank skin are provided with vertical fin.
3. the preparation method of the premix raw material of permanent ferrite prefiring material according to claim 1 may further comprise the steps:
1), premix coarse fodder and water blended coarse fodder slurry is levigate through mixing continuously in tube mill, becomes the fine granularity premix raw material of even standard;
2), the fine granularity premix raw material of above-mentioned even standard, circulate vertically through pump power in the smart control of large vol jar that stirrings, paddle wheel laterally stir and the side of the vertical fin of tank skin stirs, fine granularity premix raw material is carried out the homogenizing processing;
3), the premix raw material of handling through above-mentioned steps 2 homogenizing is carried out composition detection, and, composition is precisely adjusted according to detected result.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910272847A CN102070331B (en) | 2009-11-24 | 2009-11-24 | Preparation method of premixed raw material of ferrite magnet presintering material and production device thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910272847A CN102070331B (en) | 2009-11-24 | 2009-11-24 | Preparation method of premixed raw material of ferrite magnet presintering material and production device thereof |
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| Publication Number | Publication Date |
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| CN102070331A CN102070331A (en) | 2011-05-25 |
| CN102070331B true CN102070331B (en) | 2012-10-03 |
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| CN200910272847A Expired - Fee Related CN102070331B (en) | 2009-11-24 | 2009-11-24 | Preparation method of premixed raw material of ferrite magnet presintering material and production device thereof |
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| CN111060535B (en) * | 2019-12-12 | 2022-09-23 | 湖南航天磁电有限责任公司 | Ferrite molding ground paste moisture content on-line measuring system |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5098619A (en) * | 1989-10-02 | 1992-03-24 | Hitachi Metals International, Ltd. | Process for forming high quality ferrite magnets |
| EP1209136A1 (en) * | 2000-11-28 | 2002-05-29 | Minebea Co., Ltd. | Production process of recycled Mn-Zn ferrite |
| CN101289315A (en) * | 2008-04-30 | 2008-10-22 | 武汉景宏工贸有限公司 | Process and device for producing slurry of permanent ferrite prefiring material by wet method |
| CN101354939A (en) * | 2008-05-04 | 2009-01-28 | 横店集团东磁股份有限公司 | Method for preparing superfine permanent ferrite forming slurry |
| CN201260946Y (en) * | 2008-05-22 | 2009-06-24 | 武汉钢铁集团耐火材料有限责任公司 | Permanent ferrite powder material slurry mixing and grinding device |
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2009
- 2009-11-24 CN CN200910272847A patent/CN102070331B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5098619A (en) * | 1989-10-02 | 1992-03-24 | Hitachi Metals International, Ltd. | Process for forming high quality ferrite magnets |
| EP1209136A1 (en) * | 2000-11-28 | 2002-05-29 | Minebea Co., Ltd. | Production process of recycled Mn-Zn ferrite |
| CN101289315A (en) * | 2008-04-30 | 2008-10-22 | 武汉景宏工贸有限公司 | Process and device for producing slurry of permanent ferrite prefiring material by wet method |
| CN101354939A (en) * | 2008-05-04 | 2009-01-28 | 横店集团东磁股份有限公司 | Method for preparing superfine permanent ferrite forming slurry |
| CN201260946Y (en) * | 2008-05-22 | 2009-06-24 | 武汉钢铁集团耐火材料有限责任公司 | Permanent ferrite powder material slurry mixing and grinding device |
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| CN102070331A (en) | 2011-05-25 |
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Granted publication date: 20121003 Termination date: 20161124 |