CN102002254A - Method for extracting greengage peel pigment and control method for pigment stability - Google Patents
Method for extracting greengage peel pigment and control method for pigment stability Download PDFInfo
- Publication number
- CN102002254A CN102002254A CN2010102851518A CN201010285151A CN102002254A CN 102002254 A CN102002254 A CN 102002254A CN 2010102851518 A CN2010102851518 A CN 2010102851518A CN 201010285151 A CN201010285151 A CN 201010285151A CN 102002254 A CN102002254 A CN 102002254A
- Authority
- CN
- China
- Prior art keywords
- pigment
- green plum
- greengage
- pericarp
- peel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000049 pigment Substances 0.000 title claims abstract description 66
- 238000000034 method Methods 0.000 title claims abstract description 26
- 235000011230 Prunus domestica subsp. italica Nutrition 0.000 title abstract 9
- 244000249693 Reneklode Species 0.000 title abstract 9
- 238000000605 extraction Methods 0.000 claims abstract description 12
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 6
- 230000000694 effects Effects 0.000 claims abstract description 6
- 238000005286 illumination Methods 0.000 claims abstract description 4
- 239000002904 solvent Substances 0.000 claims description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 9
- 239000000843 powder Substances 0.000 claims description 9
- 239000000284 extract Substances 0.000 claims description 8
- XLSMFKSTNGKWQX-UHFFFAOYSA-N hydroxyacetone Chemical compound CC(=O)CO XLSMFKSTNGKWQX-UHFFFAOYSA-N 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 7
- 238000004321 preservation Methods 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 238000003860 storage Methods 0.000 claims description 6
- 239000000654 additive Substances 0.000 claims description 5
- 230000000996 additive effect Effects 0.000 claims description 5
- 235000013305 food Nutrition 0.000 claims description 5
- 230000002829 reductive effect Effects 0.000 claims description 4
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 3
- 229920002678 cellulose Polymers 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 230000008595 infiltration Effects 0.000 claims description 3
- 238000001764 infiltration Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 239000012528 membrane Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000006228 supernatant Substances 0.000 claims description 3
- 230000001476 alcoholic effect Effects 0.000 claims description 2
- 239000002932 luster Substances 0.000 abstract description 3
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 230000001276 controlling effect Effects 0.000 abstract 1
- 238000005374 membrane filtration Methods 0.000 abstract 1
- 239000007800 oxidant agent Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 238000001291 vacuum drying Methods 0.000 abstract 1
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 239000000576 food coloring agent Substances 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 2
- 235000009754 Vitis X bourquina Nutrition 0.000 description 2
- 235000012333 Vitis X labruscana Nutrition 0.000 description 2
- 240000006365 Vitis vinifera Species 0.000 description 2
- 235000014787 Vitis vinifera Nutrition 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000004075 alteration Effects 0.000 description 2
- 235000009973 maize Nutrition 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- KZJWDPNRJALLNS-VPUBHVLGSA-N (-)-beta-Sitosterol Natural products O[C@@H]1CC=2[C@@](C)([C@@H]3[C@H]([C@H]4[C@@](C)([C@H]([C@H](CC[C@@H](C(C)C)CC)C)CC4)CC3)CC=2)CC1 KZJWDPNRJALLNS-VPUBHVLGSA-N 0.000 description 1
- CSVWWLUMXNHWSU-UHFFFAOYSA-N (22E)-(24xi)-24-ethyl-5alpha-cholest-22-en-3beta-ol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)C=CC(CC)C(C)C)C1(C)CC2 CSVWWLUMXNHWSU-UHFFFAOYSA-N 0.000 description 1
- VYIRVAXUEZSDNC-TXDLOWMYSA-N (3R,3'S,5'R)-3,3'-dihydroxy-beta-kappa-caroten-6'-one Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC(=O)[C@]1(C)C[C@@H](O)CC1(C)C VYIRVAXUEZSDNC-TXDLOWMYSA-N 0.000 description 1
- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical group COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 description 1
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 1
- KLEXDBGYSOIREE-UHFFFAOYSA-N 24xi-n-propylcholesterol Natural products C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CCC)C(C)C)C1(C)CC2 KLEXDBGYSOIREE-UHFFFAOYSA-N 0.000 description 1
- MIJYXULNPSFWEK-GTOFXWBISA-N 3beta-hydroxyolean-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CCC(C)(C)C[C@H]5C4=CC[C@@H]3[C@]21C MIJYXULNPSFWEK-GTOFXWBISA-N 0.000 description 1
- 241000167854 Bourreria succulenta Species 0.000 description 1
- 244000157790 Buglossoides arvense Species 0.000 description 1
- 235000004256 Buglossoides arvense Nutrition 0.000 description 1
- VYIRVAXUEZSDNC-LOFNIBRQSA-N Capsanthyn Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CC(O)CC2(C)C VYIRVAXUEZSDNC-LOFNIBRQSA-N 0.000 description 1
- LPZCCMIISIBREI-MTFRKTCUSA-N Citrostadienol Natural products CC=C(CC[C@@H](C)[C@H]1CC[C@H]2C3=CC[C@H]4[C@H](C)[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C)C(C)C LPZCCMIISIBREI-MTFRKTCUSA-N 0.000 description 1
- 244000301850 Cupressus sempervirens Species 0.000 description 1
- 244000163122 Curcuma domestica Species 0.000 description 1
- 235000003392 Curcuma domestica Nutrition 0.000 description 1
- ARVGMISWLZPBCH-UHFFFAOYSA-N Dehydro-beta-sitosterol Natural products C1C(O)CCC2(C)C(CCC3(C(C(C)CCC(CC)C(C)C)CCC33)C)C3=CC=C21 ARVGMISWLZPBCH-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- JKLISIRFYWXLQG-UHFFFAOYSA-N Epioleonolsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4CCC3C21C JKLISIRFYWXLQG-UHFFFAOYSA-N 0.000 description 1
- 235000021559 Fruit Juice Concentrate Nutrition 0.000 description 1
- 240000000950 Hippophae rhamnoides Species 0.000 description 1
- 235000003145 Hippophae rhamnoides Nutrition 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- YBRJHZPWOMJYKQ-UHFFFAOYSA-N Oleanolic acid Natural products CC1(C)CC2C3=CCC4C5(C)CCC(O)C(C)(C)C5CCC4(C)C3(C)CCC2(C1)C(=O)O YBRJHZPWOMJYKQ-UHFFFAOYSA-N 0.000 description 1
- MIJYXULNPSFWEK-UHFFFAOYSA-N Oleanolinsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4=CCC3C21C MIJYXULNPSFWEK-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 235000011158 Prunus mume Nutrition 0.000 description 1
- 244000018795 Prunus mume Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 235000009392 Vitis Nutrition 0.000 description 1
- 241000219095 Vitis Species 0.000 description 1
- 238000003811 acetone extraction Methods 0.000 description 1
- 235000013334 alcoholic beverage Nutrition 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001452 anthocyanidin derivatives Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- MJVXAPPOFPTTCA-UHFFFAOYSA-N beta-Sistosterol Natural products CCC(CCC(C)C1CCC2C3CC=C4C(C)C(O)CCC4(C)C3CCC12C)C(C)C MJVXAPPOFPTTCA-UHFFFAOYSA-N 0.000 description 1
- LGJMUZUPVCAVPU-UHFFFAOYSA-N beta-Sitostanol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CC)C(C)C)C1(C)CC2 LGJMUZUPVCAVPU-UHFFFAOYSA-N 0.000 description 1
- NJKOMDUNNDKEAI-UHFFFAOYSA-N beta-sitosterol Natural products CCC(CCC(C)C1CCC2(C)C3CC=C4CC(O)CCC4C3CCC12C)C(C)C NJKOMDUNNDKEAI-UHFFFAOYSA-N 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- WRANYHFEXGNSND-LOFNIBRQSA-N capsanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CCC(O)C2(C)C WRANYHFEXGNSND-LOFNIBRQSA-N 0.000 description 1
- 235000018889 capsanthin Nutrition 0.000 description 1
- 235000019693 cherries Nutrition 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 235000008504 concentrate Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000003373 curcuma longa Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 235000018927 edible plant Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 230000001077 hypotensive effect Effects 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 230000031700 light absorption Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013310 margarine Nutrition 0.000 description 1
- 239000003264 margarine Substances 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 235000019462 natural additive Nutrition 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 229940100243 oleanolic acid Drugs 0.000 description 1
- 235000012658 paprika extract Nutrition 0.000 description 1
- 239000001688 paprika extract Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 230000000176 photostabilization Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- HZLWUYJLOIAQFC-UHFFFAOYSA-N prosapogenin PS-A Natural products C12CC(C)(C)CCC2(C(O)=O)CCC(C2(CCC3C4(C)C)C)(C)C1=CCC2C3(C)CCC4OC1OCC(O)C(O)C1O HZLWUYJLOIAQFC-UHFFFAOYSA-N 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- KZJWDPNRJALLNS-VJSFXXLFSA-N sitosterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](CC)C(C)C)[C@@]1(C)CC2 KZJWDPNRJALLNS-VJSFXXLFSA-N 0.000 description 1
- 229950005143 sitosterol Drugs 0.000 description 1
- NLQLSVXGSXCXFE-UHFFFAOYSA-N sitosterol Natural products CC=C(/CCC(C)C1CC2C3=CCC4C(C)C(O)CCC4(C)C3CCC2(C)C1)C(C)C NLQLSVXGSXCXFE-UHFFFAOYSA-N 0.000 description 1
- 235000015500 sitosterol Nutrition 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 235000013976 turmeric Nutrition 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Preparation Of Fruits And Vegetables (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to a method for extracting greengage peel pigment and a control method for pigment stability. The method comprises the following steps of: with greengage peel as a raw material, obtaining greengage peel pigment leach liquor through vacuum drying, smashing, dissolving, ultrasonic-wave-assisted extraction and membrane filtration; and controlling greengage peel pigment in the extracted greengage peel pigment leach liquor by regulating influencing factors, such as pH value of environment, temperature, illumination, an oxidizing agent, a reducing agent and the like to ensure the stability of greengage pigment. The method is simple and easy; and the obtained greengage peel pigment has good effect and stable color and luster and lays the foundation for further developing and applying greengage fruit pigment.
Description
Technical background
The present invention relates to a kind of natural extraction field of pigment, be specifically related to the control method of a kind of green plum pericarp pigment extracting method and stability.
Background technology
Food colorant is pigment again, in China, long use history is arranged since ancient times.The green plum pericarp pigment is a kind of natural colorant, is a kind of of food colorant, and the color and luster nature has certain nutrient value and pharmacological function.The natural food tinting material is on Application in Food mainly concentrates on beverage, candy, assembled alcoholic drinks, ice cream, cake, jelly, fruit juice concentrate, can, cooked meat product, margarine oil's wet goods product painted.
Pigment application facet example is a lot, as, Lei Ting etc. propose in the progress of research foodstuff additive, anticancer, inhibition tumour that turmeric, maize are used for; Sailor yellow has hypotensive effect; Capsanthin, Chrysan Yellow, sea-buckthorn Huang, maize, anthocyanidin have antioxygenation; Tea green element, mulberry fruit are red, Red kojic rice, Pericarpium Vitis viniferae are red has an accent blood fat; Asian puccoon is red to have anti-inflammatory effect; Xenthophylls has eye-protecting function.Once the cypress congruence pointed out that the solvent that it is soluble in water, the acetone isopolarity is stronger but was insoluble to non-polar solvents such as ether, ethyl acetate when the red earth grape pigment of research.Red earth grape skin color is red-violet colour and more stable in acidity to neutral environment, and thermotolerance is better, and photostabilization is also better; And in alkaline environment, brown stain can appear in solution, and it is range limited that pigment is utilized.Metal ion also has destruction to it.
Green plum (Japanese Apricot) is a kind of temperate zone rose department cherry genus plant plum, has another name called the plum fruit, does the branch plum, and be a kind of medicinal and edible plant, it is nutritious, the pharmaceutical use height.Green plum contains a large amount of secondary metabolites, as, Sitosterol, Oleanolic Acid sample material reach the flavone component that anti-angiocardiopathy, tumor disease is had certain effect.At present, the research of green plum reports mainly based on the plum pulp, and about rarely seen report of the research of green plum pericarp pigment and research.The green plum pericarp pigment is a kind of as natural pigment, has exploitation potential and value.Present method is put forth effort on the extraction of green plum pericarp pigment and the characteristic and the stabilization technique of green plum pericarp pigment.
Though, it is at present domestic more to the green plum processed and applied,, to the extraction and the application of green plum pigment, and color stability do not have Application and Development, still belongs to blank field.Can believe that the value of green plum pigment on development of functional food more and more is subjected to market and human consumer's favor.
Summary of the invention
The present invention is intended to develop a kind of natural additive for foodstuff with nourishing function, increases the utilization rate of green plum to greatest extent, makes the pericarp of green plum obtain deep development.Technical problem to be solved is to carry out the extraction of green plum pericarp pigment and keep its stability, develops novel natural pigment additive.
Technical scheme of the present invention is as follows:
A kind of extracting method of green plum pericarp pigment is characterized in that: concrete steps are as follows:
(1) clean green plum pericarp is carried out drying with Vacuumdrier, drying temperature is 50-60 ℃: be 4-6h time of drying;
(2) dried green plum fruit peel powder is broken into powder;
(3) pulverous green plum pericarp is dissolved in the solvent, fully mixing, infiltration 1-2h;
(4) with ultrasonic wave above-mentioned solution is helped and carry, extracting temperature is 25-40 ℃, and extraction time is 2.5-4h;
(5) the upper strata extracting solution with step (4) gained separates with whizzer, and the rotating speed of whizzer is 4 000-10000r/min;
(6) supernatant liquid with centrifugal gained filters with 0.60-0.70 μ m mixed cellulose ester membrane, gets the pigment vat liquor;
(7) the pigment vat liquor of step (6) gained is concentrated obtain pigment medicinal extract shape material, low temperature, sealing, lucifuge preservation, and reclaim solvent.
The extracting method of described green plum pericarp pigment is characterized in that: the solvent described in the step (3) is the alcoholic solution of 80-100% acetone, and wherein the mass ratio of green plum pericarp dry powder and hydroxyacetone solution is 1: (10-17).
The control method of the stability of the green plum pericarp pigment that a kind of claim 1 is extracted is characterized in that: may further comprise the steps:
(1) step 1 is extracted the pigment medicinal extract shape material that obtains, low temperature, sealing, lucifuge preservation;
(2) pH value of adjusting storage environment is 3-4.5;
(2) guarantee that the temperature of storage environment is below 50 ℃;
(3) avoid illumination, especially avoid ultraviolet irradiation;
(4) add foodstuff additive with reductibility effect, as, sulfurous acid (20-50ppm), Vc (20-60ppm), etc. may command green plum pigment stable;
(5) suitably add the food grade reductive agent, avoid using oxygenant, can guarantee that the green plum pericarp pigment is stable.With acetone is to extract solvent extraction green plum pericarp pigment, at ultraviolet region maximum absorption band is arranged, at the 275nm place; And also there is less absorption peak at 410nm and 665nm place.With the aberration a value of green plum pericarp pigment extracting solution serves as to investigate index, pigment extract to be colour strength the strongest, lovely luster.Absorbancy is 1.967, and L is 93.40, and a is-4.02, and b is 13.47.
The present invention is a starting materials with the green plum pericarp, with acetone is to extract solvent extraction green plum pericarp pigment, determines optimum extraction solvent and optimised process, has set up the method for green plum pericarp pigment extractive technique and maintenance pigment stability.Compare with traditional natural pigment extracting method,, have its unique advantage with acetone extraction green plum pigment:
(1) simple, fast and cost low;
(2) the pigment extraction effect is good, and aberration, light absorption value are more satisfactory, and absorbancy is 1.967, and L is 93.40, and a is-4.02, and b is 13.47;
(3) make full use of the green plum resource, reduced environmental pollution;
(4) increased the kind of natural pigment, the production space of having widened pigment;
(5) compare with the supercritical extraction method, this law utilization ratio height, easy and simple to handle;
(6) gained green plum pericarp pigment, the utilization scope is wide.Can be used for food coloring, also can be used for makeup.The mixed economy that improves resource utilization and green plum is worth.
Simple to operate, characteristics such as extraction efficiency is high, environmentally safe that this method has.
Specific embodiment
Non-limiting implementation process is as follows:
1, the extraction of green plum pericarp pigment, concrete steps are as follows:
(1) clean green plum pericarp is carried out drying with Vacuumdrier, drying temperature is 50-60 ℃: be 4-6h time of drying;
(2) dried green plum fruit peel powder is broken into powder;
(3) pulverous green plum pericarp is dissolved in the solvent, fully mixing, infiltration 1-2h;
(4) with ultrasonic wave above-mentioned solution is helped under certain temperature and carry, extracting temperature is 25-40 ℃, and extraction time is 2.5-4h;
(5) the upper strata extracting solution with step (4) gained separates with whizzer, and the rotating speed of whizzer is 4 000-10000r/min;
(6) supernatant liquid with centrifugal gained filters with 0.60-0.70 μ m mixed cellulose ester membrane, gets the pigment vat liquor;
(7) the pigment vat liquor of step (6) gained is concentrated obtain pigment medicinal extract shape material, low temperature, sealing, lucifuge preservation, and reclaim solvent.
Solvent described in the step (3) is a 80-100% hydroxyacetone solution, and wherein the mass ratio of green plum pericarp dry powder and hydroxyacetone solution is 1: (10-17).
2, the control method of the stability of green plum pericarp pigment may further comprise the steps:
(1) step 1 is extracted the pigment medicinal extract shape material that obtains, low temperature, sealing, lucifuge preservation;
(2) pH value of adjusting storage environment is 3-4.5;
(2) guarantee that the temperature of storage environment is below 50 ℃;
(3) avoid illumination, especially avoid ultraviolet irradiation;
(4) add foodstuff additive with reductibility effect, as, sulfurous acid (20-50ppm), Vc (20-60ppm), etc. may command green plum pigment stable;
(5) suitably add the food grade reductive agent, avoid using oxygenant, can guarantee that the green plum pericarp pigment is stable.
Claims (3)
1. the extracting method of a green plum pericarp pigment, it is characterized in that: concrete steps are as follows:
(1) clean green plum pericarp is carried out drying with Vacuumdrier, drying temperature is 50-60 ℃, and be 4-6h time of drying;
(2) dried green plum fruit peel powder is broken into powder;
(3) pulverous green plum pericarp is dissolved in the solvent, fully mixing, infiltration 1-2h;
(4) with ultrasonic wave above-mentioned solution is helped and carry, extracting temperature is 25-40 ℃, and extraction time is 2.5-4h;
(5) the upper strata extracting solution with step (4) gained separates with whizzer, and the rotating speed of whizzer is 4 000-10000r/min;
(6) supernatant liquid with centrifugal gained filters with 0.60-0.70 μ m mixed cellulose ester membrane, gets the pigment vat liquor;
(7) the pigment vat liquor of step (6) gained is concentrated obtain pigment medicinal extract shape material, low temperature, sealing, lucifuge preservation, and reclaim solvent.
2. the extracting method of green plum pericarp pigment according to claim 1 is characterized in that: the solvent described in the step (3) is the alcoholic solution of 80-100% acetone, and wherein the mass ratio of green plum pericarp dry powder and hydroxyacetone solution is 1: (10-17).
3. the control method of the stability of the green plum pericarp pigment that extracts of a claim 1 is characterized in that: may further comprise the steps:
(1) step 1 is extracted the pigment medicinal extract shape material that obtains, low temperature, sealing, lucifuge preservation;
(2) pH value of adjusting storage environment is 3-4.5;
(2) guarantee that the temperature of storage environment is below 50 ℃;
(3) avoid illumination, especially avoid ultraviolet irradiation;
(4) add foodstuff additive with reductibility effect, as, sulfurous acid (20-50ppm), Vc (20-60ppm), etc. may command green plum pigment stable;
(5) suitably add the food grade reductive agent, avoid using oxygenant, can guarantee that the green plum pericarp pigment is stable.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102851518A CN102002254A (en) | 2010-09-15 | 2010-09-15 | Method for extracting greengage peel pigment and control method for pigment stability |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102851518A CN102002254A (en) | 2010-09-15 | 2010-09-15 | Method for extracting greengage peel pigment and control method for pigment stability |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102002254A true CN102002254A (en) | 2011-04-06 |
Family
ID=43809969
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010102851518A Pending CN102002254A (en) | 2010-09-15 | 2010-09-15 | Method for extracting greengage peel pigment and control method for pigment stability |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102002254A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104631152A (en) * | 2013-10-09 | 2015-05-20 | 南通大学 | Red cigarette acetate fiber |
| CN106046846A (en) * | 2016-05-26 | 2016-10-26 | 惠州同富康生物科技有限公司 | Method for extracting peel pigment from green plums |
| CN107903656A (en) * | 2017-12-14 | 2018-04-13 | 成都新柯力化工科技有限公司 | A kind of method from green plum pericarp extraction natural food pigment |
| CN113318023A (en) * | 2021-05-31 | 2021-08-31 | 攀枝花学院 | Bougainvillea spectabilis extract and antioxidant blush based on the same |
-
2010
- 2010-09-15 CN CN2010102851518A patent/CN102002254A/en active Pending
Non-Patent Citations (4)
| Title |
|---|
| 徒晓茜: "天然色素的提取和分离", 《印染助剂》 * |
| 李阿娜 等: "青梅果皮色素的提取工艺", 《经济林研究》 * |
| 杨永利 等: "西梅果皮色素的提取工艺及其稳定性研究", 《食品科学》 * |
| 闫宁环 等: "西梅果皮色素提取及其稳定性研究", 《西北农林科技大学学报（自然科学版）》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104631152A (en) * | 2013-10-09 | 2015-05-20 | 南通大学 | Red cigarette acetate fiber |
| CN104631152B (en) * | 2013-10-09 | 2016-04-27 | 南通大学 | Red cigarette acetate fiber |
| CN106046846A (en) * | 2016-05-26 | 2016-10-26 | 惠州同富康生物科技有限公司 | Method for extracting peel pigment from green plums |
| CN107903656A (en) * | 2017-12-14 | 2018-04-13 | 成都新柯力化工科技有限公司 | A kind of method from green plum pericarp extraction natural food pigment |
| CN113318023A (en) * | 2021-05-31 | 2021-08-31 | 攀枝花学院 | Bougainvillea spectabilis extract and antioxidant blush based on the same |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102766125B (en) | Extraction and purification method for black rice anthocyanin | |
| CN103160139A (en) | Extraction method for natural pigment | |
| CN106665890A (en) | Preparation method of walnut oil | |
| CN101429347A (en) | Process for producing beet red pigment | |
| CN102002254A (en) | Method for extracting greengage peel pigment and control method for pigment stability | |
| CN103073914B (en) | Method for extracting maize yellow pigment from maize protein | |
| CN102206426A (en) | Comprehensive utilization of pigment of purple sweet potato in purple sweet potato and method for comprehensively utilizing component thereof | |
| CN103602096A (en) | Method for extracting red pigment of pitaya | |
| CN102924968B (en) | Process for extracting high-purity and high-chroma red date pigment | |
| CN104974071A (en) | Preparation method of zeaxanthine | |
| CN105349253A (en) | Method for extraction of Cornus walteri seed oil by combination of superhigh pressure treatment and subcritical double solvent extraction | |
| CN102477026A (en) | Extraction method of rose anthocyanidin | |
| CN110694297B (en) | Extraction method of plant anthocyanin and roselle anthocyanin extract | |
| CN103980384A (en) | Preparation method of water-soluble pectin of shaddock albedo | |
| CN105273433A (en) | Natural pigment extraction technology | |
| CN104327599B (en) | A kind of colo(u)r coating tinting material | |
| CN105943429A (en) | Preparation method of grape fruit extracting solution | |
| CN104894896A (en) | Method for dyeing silk with natural red series tea dye | |
| CN110272405A (en) | A kind of extracting method of anthocyanidin | |
| CN105295427A (en) | Capsochrome extracting process | |
| CN103820218A (en) | Method for microwave extracting rapeseed grease | |
| CN104448911A (en) | Extraction process for corn yellow pigment | |
| CN110108653A (en) | A kind of capsorubin analysis on change method in fresh capsicum preprocessing process | |
| CN108047946A (en) | Edible coating | |
| CN102936425A (en) | Method for preparing plant dye of pericarpium citri reticulatae powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110406 |