CN101993767B - 一种含纳米碳酸钙的复合磺酸钙润滑脂及其生产方法 - Google Patents
一种含纳米碳酸钙的复合磺酸钙润滑脂及其生产方法 Download PDFInfo
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- CN101993767B CN101993767B CN201010537753.8A CN201010537753A CN101993767B CN 101993767 B CN101993767 B CN 101993767B CN 201010537753 A CN201010537753 A CN 201010537753A CN 101993767 B CN101993767 B CN 101993767B
- Authority
- CN
- China
- Prior art keywords
- percent
- calcium carbonate
- lubricating grease
- stirring
- calcium sulfonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000004519 grease Substances 0.000 title claims abstract description 83
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 70
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 239000011575 calcium Substances 0.000 title claims abstract description 39
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 39
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 title claims abstract description 36
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 35
- 238000004519 manufacturing process Methods 0.000 title abstract description 11
- 239000002199 base oil Substances 0.000 claims abstract description 31
- 239000002131 composite material Substances 0.000 claims abstract description 25
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004327 boric acid Substances 0.000 claims abstract description 16
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 8
- 150000004671 saturated fatty acids Chemical class 0.000 claims abstract description 6
- 230000009466 transformation Effects 0.000 claims abstract 5
- 230000001050 lubricating effect Effects 0.000 claims description 69
- 239000002994 raw material Substances 0.000 claims description 49
- 238000006243 chemical reaction Methods 0.000 claims description 34
- 238000003756 stirring Methods 0.000 claims description 33
- 238000010438 heat treatment Methods 0.000 claims description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 230000003078 antioxidant effect Effects 0.000 claims description 9
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 8
- 239000011707 mineral Substances 0.000 claims description 8
- XQVWYOYUZDUNRW-UHFFFAOYSA-N N-Phenyl-1-naphthylamine Chemical compound C=1C=CC2=CC=CC=C2C=1NC1=CC=CC=C1 XQVWYOYUZDUNRW-UHFFFAOYSA-N 0.000 claims description 6
- KEQFTVQCIQJIQW-UHFFFAOYSA-N N-Phenyl-2-naphthylamine Chemical compound C=1C=C2C=CC=CC2=CC=1NC1=CC=CC=C1 KEQFTVQCIQJIQW-UHFFFAOYSA-N 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- WJUMWVJBOZKPPU-UHFFFAOYSA-N 2,3-bis(6-methylheptyl)-N-phenylaniline Chemical group C(CCCCC(C)C)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCC(C)C WJUMWVJBOZKPPU-UHFFFAOYSA-N 0.000 claims description 4
- 238000007872 degassing Methods 0.000 claims description 4
- 150000001412 amines Chemical group 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 150000004665 fatty acids Chemical class 0.000 claims description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
- 239000010721 machine oil Substances 0.000 claims description 2
- 239000002245 particle Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 12
- 229940114072 12-hydroxystearic acid Drugs 0.000 description 6
- 238000004566 IR spectroscopy Methods 0.000 description 6
- 238000012544 monitoring process Methods 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000013065 commercial product Substances 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 229910021532 Calcite Inorganic materials 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000002086 nanomaterial Substances 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000010705 motor oil Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201010537753.8A CN101993767B (zh) | 2010-11-09 | 2010-11-09 | 一种含纳米碳酸钙的复合磺酸钙润滑脂及其生产方法 |
Applications Claiming Priority (1)
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CN201010537753.8A CN101993767B (zh) | 2010-11-09 | 2010-11-09 | 一种含纳米碳酸钙的复合磺酸钙润滑脂及其生产方法 |
Publications (2)
Publication Number | Publication Date |
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CN101993767A CN101993767A (zh) | 2011-03-30 |
CN101993767B true CN101993767B (zh) | 2014-04-16 |
Family
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Family Applications (1)
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CN201010537753.8A Expired - Fee Related CN101993767B (zh) | 2010-11-09 | 2010-11-09 | 一种含纳米碳酸钙的复合磺酸钙润滑脂及其生产方法 |
Country Status (1)
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CN (1) | CN101993767B (zh) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9976102B2 (en) | 2011-10-31 | 2018-05-22 | Nch Corporation | Composition and method of manufacturing calcium sulfonate greases using alkali metal hydroxide and delayed addition of non-aqueous converting agents |
US9458406B2 (en) | 2011-10-31 | 2016-10-04 | Nch Corporation | Calcium hydroxyapatite based sulfonate grease compositions and method of manufacture |
KR101797940B1 (ko) * | 2011-10-31 | 2017-11-15 | 엔씨에이취 코오포레이션 | 수산화인회석칼슘계 설폰산칼슘 그리스 조성물 및 제조 방법 |
US9976101B2 (en) | 2011-10-31 | 2018-05-22 | Nch Corporation | Method of manufacturing calcium sulfonate greases using delayed addition of non-aqueous converting agents |
CN103146465B (zh) * | 2013-03-15 | 2014-12-31 | 天津市津冠润滑脂有限公司 | 一种高性能复合磺酸钙基润滑脂及其制备方法 |
CA3010739C (en) | 2016-01-07 | 2019-02-19 | Nch Corporation | Manufacturing calcium sulfonate greases using alkali metal hydroxide and delayed addition of non-aqueous converting agents |
US10087391B2 (en) | 2016-05-18 | 2018-10-02 | Nch Corporation | Composition and method of manufacturing calcium magnesium sulfonate greases without a conventional non-aqueous converting agent |
US10519393B2 (en) | 2016-05-18 | 2019-12-31 | Nch Corporation | Composition and method of manufacturing calcium magnesium sulfonate greases |
US10087388B2 (en) | 2016-05-18 | 2018-10-02 | Nch Corporation | Composition and method of manufacturing calcium sulfonate and calcium magnesium sulfonate greases using a delay after addition of facilitating acid |
US10087387B2 (en) | 2016-05-18 | 2018-10-02 | Nch Corporation | Composition and method of manufacturing calcium magnesium sulfonate greases |
US10392577B2 (en) | 2016-05-18 | 2019-08-27 | Nch Corporation | Composition and method of manufacturing overbased sulfonate modified lithium carboxylate grease |
CN107090343A (zh) * | 2017-05-25 | 2017-08-25 | 曹平 | 一种高能导电润滑膏 |
CN108192696B (zh) * | 2017-12-29 | 2020-09-01 | 上海峰竺复合新材料科技有限公司 | 一种碳酸钙晶须改性复合磺酸钙润滑脂及其制备方法 |
CN109762632B (zh) * | 2019-01-15 | 2021-12-10 | 广西碳酸钙产业化工程院有限公司 | 含碳酸钙高性能复合磺酸钙基润滑脂及其制备方法 |
CN109627805B (zh) * | 2019-01-15 | 2021-04-30 | 广西大学 | 改性纳米碳酸钙的制备方法及其应用 |
US11661563B2 (en) | 2020-02-11 | 2023-05-30 | Nch Corporation | Composition and method of manufacturing and using extremely rheopectic sulfonate-based greases |
CN114958469B (zh) * | 2022-06-30 | 2023-02-21 | 南京科润工业介质股份有限公司 | 一种含纳米磺酸钙的微量润滑油 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101153239A (zh) * | 2007-08-27 | 2008-04-02 | 无锡市高润杰化学有限公司 | 一种复合磺酸钙基润滑脂及生产方法 |
CN101469288A (zh) * | 2007-12-25 | 2009-07-01 | 中国科学院兰州化学物理研究所 | 一种开式齿轮润滑剂组合物 |
-
2010
- 2010-11-09 CN CN201010537753.8A patent/CN101993767B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101153239A (zh) * | 2007-08-27 | 2008-04-02 | 无锡市高润杰化学有限公司 | 一种复合磺酸钙基润滑脂及生产方法 |
CN101469288A (zh) * | 2007-12-25 | 2009-07-01 | 中国科学院兰州化学物理研究所 | 一种开式齿轮润滑剂组合物 |
Non-Patent Citations (1)
Title |
---|
深圳市蓝域化工科技有限公司.HBS复合转化促进剂说明书.《HBS复合转化促进剂说明书》.深圳市蓝域化工科技有限公司,2010, * |
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Publication number | Publication date |
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CN101993767A (zh) | 2011-03-30 |
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PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C53 | Correction of patent for invention or patent application | ||
CB02 | Change of applicant information |
Address after: 214000 Xishan Economic Development Zone, Jiangsu, spring road, No. 28, No. Applicant after: Wuxi Huiyuan Advanced Lubricating Oil Co., Ltd. Address before: 214000 Xishan Economic Development Zone, Jiangsu, spring road, No. 28, No. Applicant before: Wuxi Huiyuan Packaging Technology Co., Ltd. |
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COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: WUXI HUIYUAN PACKAGING TECHNOLOGY CO., LTD. TO: JIANGSU HUIYUAN PETROLEUM TECHNOLOGY CO., LTD. |
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ASS | Succession or assignment of patent right |
Owner name: WUXI HUIYUAN SUPER LUBRICATING OIL CO., LTD. Effective date: 20120806 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20120806 Address after: 214000 Xishan Economic Development Zone, Jiangsu, spring road, No. 28, No. Applicant after: Wuxi Huiyuan Advanced Lubricating Oil Co., Ltd. Co-applicant after: Wuxi Huiyuan Super Lubrication Oil Co., Ltd. Address before: 214000 Xishan Economic Development Zone, Jiangsu, spring road, No. 28, No. Applicant before: Wuxi Huiyuan Advanced Lubricating Oil Co., Ltd. |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140416 Termination date: 20191109 |
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CF01 | Termination of patent right due to non-payment of annual fee |