CN101966129A - Method for preparing artificial carbonated spring preparation - Google Patents
Method for preparing artificial carbonated spring preparation Download PDFInfo
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- CN101966129A CN101966129A CN 201010226635 CN201010226635A CN101966129A CN 101966129 A CN101966129 A CN 101966129A CN 201010226635 CN201010226635 CN 201010226635 CN 201010226635 A CN201010226635 A CN 201010226635A CN 101966129 A CN101966129 A CN 101966129A
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Abstract
The invention discloses a method for preparing an artificial carbonated spring preparation. The method comprises the following steps of: adding a certain amount of dispersing agent, liquid moisturizing agent and essence into a proper amount of tap water; after the mixture is dispersed uniformly, adding nano calcium carbonate and inorganic salt; after complete emulsification, drying the prepared suspended serous fluid under a proper condition; adding dried and ground citric acid, alum, binder, pigment, whitening agent and moisturizing agent; and after mixing uniformly and then performing processing to prepare the artificial carbonated spring preparation. The product produced by the method maintains ions which is possessed by a natural hot spring and is good for human skin and health, has double effects of whitening skin and strengthening body, and can be widely applied to families, hotels and public baths.
Description
Technical field
The present invention relates to a kind of cosmetic bath article, especially relate to a kind of preparation method of artificial carbonate spring preparation.
Background technology
Natural hot spring is of long standing and well established in the application of aspects such as beauty and skin care, health care; wherein be known as the carbonate spring of " soup of heart "; the effect that not only has good insulation and protection heart; but also the function that has soften cuticle, moistens and bleach; concerning the women, steep at such hot spring as bubble is in natural skin care water.CO 2 aerated body in the carbonate spring, the general thermal water of spring temperature is low, can promote microvascular expansion, makes blood pressure drops, improves cardiovascular function, helps blood circulation; In addition, carbonate spring contains the carbon dioxide composition, can present bubble at skin surface, therefore, also have slight massage effect, phenomenon has the improvement effect for hypertension, arteriosclerosis, infertility, climacteric, rheumatism, arthritis, neurasthenia, trick is ice-cold etc.
The characteristic of carbonate spring is that the spring temperature is low, but steeped later can entire body happy, the warmness pit of the stomach that goes directly.Often the bubble carbonate spring can have greatest benifit to health undoubtedly, but because occurring in nature natural magnesium spring resource-constrained also is not easy to carry and transport, the requirement of the frequent bathing hot spring of most of people can't be met.
Summary of the invention
The objective of the invention is: provide have building body, the preparation method of a kind of artificial carbonate spring preparation of whitening skin and preserving moisture.
Technical scheme of the present invention is: the preparation method of artificial carbonate spring preparation is carried out according to the following steps:
(1) at first certain amount of dispersant TH-904, liquid humectant agent, essence are joined in an amount of tap water, after being uniformly dispersed, add again through grinding, dry and cross the nano-calcium carbonate and the inorganic salt of 120 mesh sieves, behind the fully emulsified 30min, promptly getting solid content is the suspension slurry of main component with the nano-calcium carbonate between 50-60%.
This suspension slurry that (2) will prepare is dry under suitable condition, will add through the functional component of oven dry, the citric acid, Alumen, binding agent, pigment and the Pear Power that grind and moisture-keeping efficacy again, fully carries out tabletting behind the mix homogeneously.
The content of above step nano-calcium carbonate and various inorganic salts is 5-80% by weight, and functional adjuvant is 0.5-20%.Wherein functional adjuvant comprises whitening agent and wetting agent, and wherein content is respectively by weight: whitening agent is 0.5-10%, is preferably 1-5%, most preferably is 1-3%, and wetting agent is 0.5-10%, is preferably 1-5%, most preferably is 1-3%.
The said whitening agent of the present invention by have the melanin of dispeling, suppress the melanin growth, the melanic effect raw material of reduction is formed.Dispeling melanic raw material is four different cetylates, the oil-soluble Radix Glycyrrhizae extract, linoleic acid, cysteine, one of fruit acid or its mixture, the raw material that suppresses the melanin growth is a hydroquinone, arbutin and derivant thereof, its derivant of kojic acid, fruit acid, caffeic acid, the methyl gentisate, Azelaic Acid, glucamine, tunicamycin, phloretin, ascorbic acid, one of isoflavone compounds or its mixture, the melanic raw material that reduces is vitamin C and derivant thereof, vitamin E and derivant thereof, procyanidin, endothelin antagonist, green tea extract, one of haematoxylin or its mixture.
Wetting agent is an ethylene glycol, glycerol (glycerol), diethylene glycol, propylene glycol, 1,3 butylene glycol, sorbitol, mannitol, tetramethylolmethane, lanonol, the hydrogenation lanonol, polyoxyethylene sorbitan ether, Polyethylene Glycol, lauric acid hexyl ester, butyl palmitate, Aloe extract, hydroxyethyl urea, hyaluronic acid, allantoin and derivant thereof, carbamide and derivant thereof, pyrrolidone sodium carboxylate, Sargassum, trehalose, pectic acid, laminine, ceramide, collagen protein, chitin derivativ, Aloe, lactic acid and sodium lactate, one of amino acid humectant or its mixture.
Binding agent is CMC-Na, β-CD, xanthan gum, Radix Acaciae senegalis, pectin, antler glue, agar, sodium alginate, guar gum, gelatin, cellulose, cellulose gum, carboxymethyl hydroxyethyl cellulose, the spermaceti hydroxyethyl-cellulose, ethyl cellulose, hydroxyethyl-cellulose, hydroxypropyl cellulose, hydroxypropyl emthylcellulose, methylcellulose, microcrystalline Cellulose, 30 POVIDONE K 30 BP/USP-30, polyvinyl alcohol, polyoxyethylene, polyacrylic acid and derivant thereof, one of soluble starch or its mixture.
The carbonic acid gas that is produced among the present invention relates to following chemical reaction, and its chemical equation is respectively:
3CaCO
3+2C
6H
8O
7＝Ca
3(C
6H
5O
7)
2+3H
2O+3CO
2↑
3NaHCO
3+C
6H
8O
7＝Na
3C
6H
5O
7+3H
2O+3CO
2↑
2KAl(SO
4)
2+3CaCO
3+3H
2O＝3CaSO
4+2Al(OH)
3+K
2SO
4+3CO
2↑
3K
2CO
3+2C
6H
8O
7＝2K
3C
6H
5O
7+3H
2O+3CO
2↑
The dosage form of the present invention's preparation can be the solid or the graininess of different shape.
The invention has the beneficial effects as follows: be primary raw material with the nano-calcium carbonate, adding on the various inorganic salts and organic acid basis with health care, introduce again and have the melanin of dispeling, the growth of inhibition melanin, the whitening agent of vat black pigment effect and wetting agent with moisture-keeping efficacy; Simultaneously, utilize carbonate and the organic acid neutralization reaction in water to produce an amount of carbonic acid gas, the carbonic acid gas that produces not only can promote the composition of various ions and Pear Power, moisture-keeping efficacy to be dispersed in the water rapidly, and be dissolved in carbonic acid gas in the water through after skin enters human body, can stimulate blood vessel, cause telangiectasis and allow erubescence, thereby improve cutaneous circulation, create the bathing environment that has to the similar effect of natural magnesium spring.The product that the present invention produces except that having of having kept that natural hot spring possessed to human body skin and healthy and helpful magnesium, calcium, sodium, potassium, chlorine, zinc, aluminum, the sulfate radical plasma, also the two-way effect of Pear Power skin and building body can be widely used in family, hotel and the common outdoor bathing place.
The specific embodiment
Embodiment 1:
3.95g TH-904,2g essence, the agent of 2.37g liquid humectant are joined in the 29g water, after stirring, add 39 nano-calcium carbonates, 6g sodium bicarbonate, 7g inorganic salt mixt, behind the fully emulsified 30min, with this serosity dry 12h under 60 ℃ of conditions, after fully pulverizing, add 37g citric acid, 7g Alumen, 0.8g wetting agent, 1g 30 POVIDONE K 30 BP/USP-30 and an amount of pigment, carry out tabletting behind the mix homogeneously.
Embodiment 2:
4.5g TH-904,2g essence, the agent of 2.37g liquid humectant are joined in the 29g water, after stirring, add 45g nano-calcium carbonate, 7g sodium bicarbonate, 7g inorganic salt mixt, behind the fully emulsified 30min, with this serosity dry 12h under 60 ℃ of conditions, after fully pulverizing, add 25g citric acid, 10g Alumen, 1.8g wetting agent, 5g CMC-Na and an amount of pigment carry out tabletting behind the mix homogeneously.
Embodiment 3:
5.0g TH-904,2g essence, the agent of 2.37g liquid humectant are joined in the 29g water, after stirring, add 50g nano-calcium carbonate, 7g sodium bicarbonate, 7g inorganic salt mixt, behind the fully emulsified 30min, with this serosity dry 12h under 60 ℃ of conditions, after fully pulverizing, add 20g citric acid, 10g Alumen, 0.8g wetting agent, 3g CMC-Na, 1g β-CD and an amount of pigment carry out tabletting behind the mix homogeneously.
Embodiment 4:
5.0g TH-904,2g essence, the agent of 2.37g liquid humectant are joined in the 29g water, after stirring, add 50g nano-calcium carbonate, 7g sodium bicarbonate, 7g inorganic salt mixt, behind the fully emulsified 30min, with this serosity dry 12h under 60 ℃ of conditions, after fully pulverizing, add 20g citric acid, 10g Alumen, 0.8g wetting agent, 6g β-CD and an amount of pigment carry out tabletting behind the mix homogeneously.
Embodiment 5:
With 5.0g TH-904,2g essence, 2.37g the liquid humectant agent joins in the 29g water, after stirring, add the 50g nano-calcium carbonate, the 7g sodium bicarbonate, the 7g inorganic salt mixt, the 2g whitening agent, the 4g wetting agent, behind the fully emulsified 30min, under stirring condition in this serosity progressively adding 16g CMC-Na, when sample is become moist irregular particle shape thing shape by liquid state, add the 20g citric acid again, behind 10g Alumen and an amount of pigment, continue to stir, loose until forming, do not have till the fine powder individualism comparison rule, and then sieve dry after, be processed into lamellar with tablet machine.
Embodiment 6:
With 5.0g TH-904,2g essence, 2.37g the liquid humectant agent joins in the 29g water, after stirring, add the 50g nano-calcium carbonate, the 7g sodium bicarbonate, the 7g inorganic salt mixt, the 2g whitening agent, the 4g wetting agent, behind the fully emulsified 30min, under stirring condition in this serosity progressively adding 3g CMC-Na, 26g β-CD, when sample is become moist irregular particle shape thing shape by liquid state, add the 20g citric acid again, behind 10g Alumen and an amount of pigment, continue to stir, loose until forming, do not have till the fine powder individualism comparison rule, and then sieve dry after, be processed into lamellar with tablet machine.
Embodiment 7:
With 5.0g TH-904,2g essence, 2.37g the liquid humectant agent joins in the 29g water, after stirring, add the 50g nano-calcium carbonate, the 7g sodium bicarbonate, the 7g inorganic salt mixt, the 2g whitening agent, the 4g wetting agent, behind the fully emulsified 30min, under stirring condition in this serosity progressively adding 18g xanthan gum, when sample is become moist irregular particle shape thing shape by liquid state, add the 20g citric acid again, behind 10g Alumen and an amount of pigment, continue to stir, loose until forming, do not have till the fine powder individualism comparison rule, and then sieve dry after, be processed into lamellar with tablet machine.
Embodiment 8:
With 5.0g TH-904,2g essence, 2.37g the liquid humectant agent joins in the 29g water, after stirring, add the 50g nano-calcium carbonate, the 7g sodium bicarbonate, the 7g inorganic salt mixt, the 2g whitening agent, the 4g wetting agent, behind the fully emulsified 30min, under stirring condition in this serosity progressively adding 29g cellulose, when sample is become moist irregular particle shape thing shape by liquid state, add the 20g citric acid again, behind 10g Alumen and an amount of pigment, continue to stir, loose until forming, do not have till the fine powder individualism comparison rule, and then sieve dry after, be processed into lamellar with tablet machine.
Embodiment 9:
With 5.0g TH-904,2g essence, 2.37g the liquid humectant agent joins in the 29g water, after stirring, add the 50g nano-calcium carbonate, the 7g sodium bicarbonate, the 7g inorganic salt mixt, the 2g whitening agent, the 4g wetting agent, behind the fully emulsified 30min, under stirring condition in this serosity progressively adding 53g β-CD, when sample is become moist irregular particle shape thing shape by liquid state, add the 20g citric acid again, behind 10g Alumen and an amount of pigment, continue to stir, loose until forming, do not have till the fine powder individualism comparison rule, and then sieve dry after, be processed into lamellar with tablet machine.
Table 1 preparation method is to the influence of sample
Above embodiment describes the effect that preparation method and different proportioning produced of artificial carbonate spring preparation respectively in detail.The content of nano-calcium carbonate and various inorganic salts is 5-80% by weight among the present invention, whitening agent is 0.5-10%, is preferably 1-5%, most preferably is 1-3%, wetting agent is 0.5-10%, is preferably 1-5%, most preferably is 1-3%, and other adds raw material and can adjust accordingly.As the content of nano-calcium carbonate and various inorganic salts be 5% by weight, whitening agent 3%, wetting agent 0.5%, other adds raw material 91.5%; The content of nano-calcium carbonate and various inorganic salts is 80% by weight, whitening agent 1%, wetting agent 3%, other adds raw material 16%; The content of nano-calcium carbonate and various inorganic salts is 30% by weight, whitening agent 0.5%, wetting agent 10%, other adds raw material 59.5%; The content of nano-calcium carbonate and various inorganic salts is 60% by weight, whitening agent 10%, wetting agent 0.5%, other adds raw material 29.5% etc.
Be illustrated effect and the effect that the present invention produced for further proving in conjunction with the experimenter.
Select the age between women between 25-30 year as the experimenter, skin type belongs to the III type, no cosmetic allergic contact dermatitis history.With foot's skin is test zone, uses 1 (0.4g) at every turn, and it is joined the 4L temperature in 37-42 ℃ of water, and being prepared into concentration is 0.01% (pH value 6.5-7.5) aqueous solution.A foot places the container that adds sample, and the another foot is inserted in the light water and compared, so that compare, test difference between the two.Soak every day, soaks 15min at every turn, 60d on probation continuously, and before on probation, reach the situation of change that 30d, 60d after trying out respectively test skin color.
Adopt the situation of change of Lab colorimeter system spectrophotometer (HP-200 color difference meter) test foot skin color.L: be brightness, be worth greatly more that color is deflection white more, otherwise, deflection black.A: be red, green product ,+a is a red direction, and-a is green direction.B: be yellow, blue product ,+b is yellow direction, and-b is blue direction.C: be saturation, in order to represent the deep or light of color of object surface.H: be hue angle, the colored characteristic of dividing mutually each other of expression.In the Lab colorimeter system, represent three kinds of the aberration Δ Eab between the stimulation, i.e. distances between the colour space two color dot with difference Δ L, Δ a, the Δ b of coordinate L, a, b.Δ Eab=[(Δ L)
2+ (Δ is a)
2+ (Δ b)
2]
1/2, in the formula: because Δ Eab is the aggregative index of L, a, b, represented the solid of colourity to change, so be to estimate the more suitable index that the colour of skin changes.
Untoward reaction such as skin allergy all do not take place in the experimenter after using 60d continuously.When experimenter foot skin color was measured, position and indoor light kept self-consistentency as far as possible, and the experimenter is in indoor [temperature (21 ± 2) ℃, humidity (60 ± 5) %], after cleaning and exposing test position 30min, tested again.During test, get 5 points in every experimenter foot, 10 groups of data of each some follow-on test, with its meansigma methods as final test result, and respectively organize data and represent, and, adopt medically extensive use statistical method by AVERAGE in the Excel software and STDEV function with " mean ± standard deviation ", the method of paired t-test is carried out the significance analysis check to experimenter foot skin color parameter, and p＜0.05 has remarkable meaning.
Table 2 uses the comparison of different time foot skin color value
Last table is for using the situation of change of different time foot skin color value, and by last Biao Kede, behind this sample 30d on probation and the 60d, the L-value of foot's skin raises, and has significant difference (t=3.90, t=2.11, p＜0.05).Show that when this sample 30d on probation, L-value increases, during 60d on probation, L-value continues to increase, and shows that the colour of skin changes to white partially direction, and a (t=1.51, t=0.73, p＞0.05), b (t=0.96, t=1.45, p＞0.05), c (t=1.24, t=0.40, p＞0.05), h (t=1.32, t=1.28, p＞0.05) after using 30d and 60d, the difference that there are no significant.
This product bathing commonly used is also soaked, not only can disinfection, skin-moisturizing, skin, blood circulation promoting, and improve skin metabolism, but also can make skin delicate lubricated, it is beautiful to whiten.
The scope of protection of present invention is not limited to the scope of embodiment statement, and all those skilled in the art are thinkable all within protection domain of the present invention without creative work institute.
Claims (10)
1. the preparation method of an artificial carbonate spring preparation is characterized in that: carry out according to the following steps:
(1) at first certain amount of dispersant TH-904, liquid humectant agent, essence are joined in an amount of tap water, after being uniformly dispersed, add again through grinding, dry and cross the nano-calcium carbonate and the inorganic salt of 120 mesh sieves, behind the fully emulsified 30min, promptly getting solid content is the suspension slurry of main component with the nano-calcium carbonate between 50-60%;
This suspension slurry that (2) will prepare is dry under suitable condition, will add through oven dry, the citric acid that grinds, Alumen, binding agent, pigment, whitening agent and wetting agent again, is fully processed after mixing.
2. the preparation method of a kind of artificial carbonate spring preparation according to claim 1 is characterized in that: the content of described nano-calcium carbonate and inorganic salt is 5-80% by weight, and functional adjuvant is 0.5-20%.
3. the preparation method of a kind of artificial carbonate spring preparation according to claim 2 is characterized in that: described functional adjuvant comprises whitening agent and wetting agent, and wherein content is respectively whitening agent 0.5-10% by weight, wetting agent is 0.5-10%.
4. the preparation method of a kind of artificial carbonate spring preparation according to claim 3, it is characterized in that: described whitening agent is by dispeling melanin, suppress the melanin growth, the melanic raw material that reduces is formed, dispeling melanic raw material is four different cetylates, the oil-soluble Radix Glycyrrhizae extract, linoleic acid, cysteine, one of fruit acid or its mixture, the raw material that suppresses the melanin growth is a hydroquinone, arbutin and derivant thereof, its derivant of kojic acid, fruit acid, caffeic acid, the methyl gentisate, Azelaic Acid, glucamine, tunicamycin, phloretin, ascorbic acid, one of isoflavone compounds or its mixture, the melanic raw material that reduces is vitamin C and derivant thereof, vitamin E and derivant thereof, procyanidin, endothelin antagonist, green tea extract, one of haematoxylin or its mixture.
5. the preparation method of a kind of artificial carbonate spring preparation according to claim 3, it is characterized in that: described wetting agent is an ethylene glycol, glycerol (glycerol), diethylene glycol, propylene glycol, 1,3 butylene glycol, sorbitol, mannitol, tetramethylolmethane, lanonol, the hydrogenation lanonol, polyoxyethylene sorbitan ether, Polyethylene Glycol, lauric acid hexyl ester, butyl palmitate, Aloe extract, hydroxyethyl urea, hyaluronic acid, allantoin and derivant thereof, carbamide and derivant thereof, pyrrolidone sodium carboxylate, Sargassum, trehalose, pectic acid, laminine, ceramide, collagen protein, chitin derivativ, Aloe, lactic acid and sodium lactate, one of amino acid humectant or its mixture.
6. the preparation method of a kind of artificial carbonate spring preparation according to claim 1 is characterized in that: described binding agent is CMC-Na, β-CD, xanthan gum, Radix Acaciae senegalis, pectin, antler glue, agar, sodium alginate, guar gum, gelatin, cellulose, cellulose gum, carboxymethyl hydroxyethyl cellulose, the spermaceti hydroxyethyl-cellulose, ethyl cellulose, hydroxyethyl-cellulose, hydroxypropyl cellulose, hydroxypropyl emthylcellulose, methylcellulose, microcrystalline Cellulose, 30 POVIDONE K 30 BP/USP-30, polyvinyl alcohol, polyoxyethylene, polyacrylic acid and derivant thereof, one of soluble starch or its mixture.
7. the preparation method of a kind of artificial carbonate spring preparation according to claim 3 is characterized in that: whitening agent is preferably 1-3% by weight, wetting agent is preferably 1-3%.
8. the preparation method of a kind of artificial carbonate spring preparation according to claim 1 is characterized in that: the carbonic acid gas that is produced relates to following chemical reaction, and its chemical equation is respectively
3CaCO
3+2C
6H
8O
7＝Ca
3(C
6H
5O
7)
2+3H
2O+3CO
2↑
3NaHCO
3+C
6H
8O
7＝Na
3C
6H
5O
7+3H
2O+3CO
2↑
2KAl(SO
4)
2+3CaCO
3+3H
2O＝3CaSO
4+2Al(OH)
3+K
2SO
4+3CO
2↑
3K
2CO
3+2C
6H
8O
7＝2K
3C
6H
5O
7+3H
2O+3CO
2↑
9. according to the preparation method of any described a kind of artificial carbonate spring preparation of claim 1 to 8, it is characterized in that: the dosage form of preparation is the solid of different shape.
10. according to the preparation method of any described a kind of artificial carbonate spring preparation of claim 1 to 8, it is characterized in that: the dosage form of preparation is a graininess.
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|---|---|---|---|
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|---|---|---|---|
| CN 201010226635 CN101966129A (en) | 2010-07-14 | 2010-07-14 | Method for preparing artificial carbonated spring preparation |
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| CN101966129A true CN101966129A (en) | 2011-02-09 |
Family
ID=43545399
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|---|---|---|---|
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103445985A (en) * | 2012-05-28 | 2013-12-18 | 豪特艾本碳酸泉材料有限公司 | Method for producing tablet, and tablet |
| CN104771328A (en) * | 2015-04-02 | 2015-07-15 | 芜湖美的厨卫电器制造有限公司 | Carbonate spring tablet and preparation method thereof |
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|---|---|---|---|---|
| CN1325681A (en) * | 2000-05-25 | 2001-12-12 | 鞍山市汤岗子医院 | Powder for mineral bath |
| CN1466942A (en) * | 2002-06-07 | 2004-01-14 | 株式会社津村 | Granulating substance used as whitening agent and method for manufacturing the same, bath preparation composition containing the same |
| CN1813657A (en) * | 2005-12-15 | 2006-08-09 | 孙振淋 | Application method of nano calcium phosphate like salt for cosmetic product |
| CN101229313A (en) * | 2008-01-16 | 2008-07-30 | 高磊 | Hotspring powder medicine compounds |
-
2010
- 2010-07-14 CN CN 201010226635 patent/CN101966129A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1325681A (en) * | 2000-05-25 | 2001-12-12 | 鞍山市汤岗子医院 | Powder for mineral bath |
| CN1466942A (en) * | 2002-06-07 | 2004-01-14 | 株式会社津村 | Granulating substance used as whitening agent and method for manufacturing the same, bath preparation composition containing the same |
| CN1813657A (en) * | 2005-12-15 | 2006-08-09 | 孙振淋 | Application method of nano calcium phosphate like salt for cosmetic product |
| CN101229313A (en) * | 2008-01-16 | 2008-07-30 | 高磊 | Hotspring powder medicine compounds |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103445985A (en) * | 2012-05-28 | 2013-12-18 | 豪特艾本碳酸泉材料有限公司 | Method for producing tablet, and tablet |
| CN104771328A (en) * | 2015-04-02 | 2015-07-15 | 芜湖美的厨卫电器制造有限公司 | Carbonate spring tablet and preparation method thereof |
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Application publication date: 20110209 |