CN101947267B - Solid fragrant anti-dizziness agent and preparation method thereof - Google Patents
Solid fragrant anti-dizziness agent and preparation method thereof Download PDFInfo
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- CN101947267B CN101947267B CN2010105015880A CN201010501588A CN101947267B CN 101947267 B CN101947267 B CN 101947267B CN 2010105015880 A CN2010105015880 A CN 2010105015880A CN 201010501588 A CN201010501588 A CN 201010501588A CN 101947267 B CN101947267 B CN 101947267B
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Abstract
The invention discloses a solid fragrant anti-dizziness agent and a preparation method thereof. The solid fragrant anti-dizziness agent comprises the following components in percentage by mass: 0.75 to 1.50 percent of anti-dizziness essence, 0.50 to 1.50 percent of solid air freshening glue, 8.00 to 10.00 percent of high-efficiency solubilizing agent, 0.40 to 0.60 percent of preservative and the balance of distilled water. The preparation method comprises the following four steps of: blending the anti-dizziness essence, solubilizing the anti-dizziness essence, preparing a gel and mixing the anti-dizziness essence and the gel. Because natural essential oil is taken as the main raw material of the anti-dizziness essence component, the solid fragrant anti-dizziness agent is a purely natural, nontoxic, harmless and safe product; in addition, because the solid fragrant anti-dizziness agent also comprises components such as lavender oil and the like, the solid fragrant anti-dizziness agent can emit fresh and soft flower and grass fragrance and bring fresh and fragrant aroma to the air, can continuously give off pleasant aroma for 5 to 8 days even in a normal environment and is environmental-friendly.
Description
Technical field
The invention belongs to technical field of chemistry, be specifically related to the blending technology of the anti-dizzy essence of a kind of solid aromatic and the method for preparing of solid aromatic antiblooming agent thereof.
Background technology
People are to prevent dizzy discomfort when waiting the vehicles by ship and by bus, can carry some anti-motion sickness drug things etc.At present, the product on the domestic market is a lot, mainly is to be prepared into medicine (anti-motion sickness drug of phenobarbital class, motilium, metoclopramide etc.).But human body is taken in side effect arranged, can occur thirstyly, dizzy, to bring out epileptic's petit mal.The folk prescription quintessence oil of the also useful Herba Menthae quintessence oil in existing home and abroad, Fructus Citri Limoniae citrus oils is done aromatotherapy, can obviously alleviate nauseating, the stomach discomfort symptom of people when carsickness.
Summary of the invention
One of the object of the invention is to provide in order to solve the above problems a kind of nontoxic, safety solid fragrance antiblooming agent.
Two of the object of the invention is to provide a kind of method for preparing of nontoxic, safety solid fragrance antiblooming agent.
Three of the object of the invention is to provide a kind of anti-dizzy essence that is used for antiblooming agent.
Technical scheme of the present invention
A kind of solid aromatic antiblooming agent, the mass percent of its contained each composition is formed as follows:
Anti-dizzy essence 0.75~1.50%
Solid air freshening glue 0.50~1.50%
Efficient solubilizing agents 8.00~10.00%
Antiseptic 0.40~0.60%
Surplus is a distilled water;
Efficient solubilizing agents wherein is to be main with nonionic, amphoteric ionic surfactant, mainly is the organic compound of alcohol, ether structure: polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether (12-13 alkanol polyxyethylated alcohol) etc.; Be preferably 12-13 alkanol polyxyethylated alcohol;
Solid air freshening glue wherein is macromolecular materials such as polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose; Be preferably modified cellulose;
Antiseptic wherein is the mixture of DMDMH (dihydroxymethyl dimethyl hydantoin) and IPBC (3-iodo-2-propynyl butyl carbamate); Be preferably that model is the product of G.P.L in the Chinese daily use chemicals industry.
Wherein said anti-dizzy essence comprises components such as Mentholum, Borneolum Syntheticum, Camphora, eucalyptus quintessence oil, Oleum Caryophylli, thyme oil, Fructus Citri Limoniae oil, Oleum Menthae Rotundifoliae, Oleum lavandula angustifolia, mentha piperita oil, antioxidant; And the mass percent of each component described in the anti-dizzy essence is seen table 1:
The quality percentage composition of each component in the used anti-dizzy essence of table 1
Sequence number | The raw material name | Quality percentage composition (%) |
1 | Mentholum. | 20.00~30.00 |
2 | Borneolum Syntheticum | 5.00~15.00 |
3 | Camphora | 0.30~2.00 |
4 | Eucalyptus quintessence oil | 15.00~20.00 |
5 | Oleum Caryophylli | 2.00~5.00 |
6 | Thyme oil | 1.00~4.00 |
7 | Fructus Citri Limoniae oil | 8.00~15.00 |
8 | Oleum Menthae Rotundifoliae | 15.00~25.00 |
9 | Oleum lavandula angustifolia | 1.00~4.00 |
10 | Mentha piperita oil | 15.00~25.00 |
11 | Antioxidant | 1.00~2.00 |
Wherein said antioxidant is BHT (a 2.6-ditertbutylparacresol);
The mass percent of each component described in the anti-dizzy essence is preferably seen table 2:
The quality percentage composition of each component in the used anti-dizzy essence of table 2
The raw material name | Quality percentage composition (%) |
Mentholum. | 21.00~28.00 |
Borneolum Syntheticum | 5.00~8.30 |
Camphora | 0.30~1.50 |
Eucalyptus quintessence oil | 15.00~17.00 |
Oleum Caryophylli | 3.00~5.00 |
Thyme oil | 2.00~2.10 |
Fructus Citri Limoniae oil | 8.00~9.10 |
Oleum Menthae Rotundifoliae | 14.00~20.00 |
Oleum lavandula angustifolia | 1.20~1.50 |
Mentha piperita oil | 18.00~20.00 |
Antioxidant | 1.00 |
Wherein said antioxidant is BHT (a 2.6-ditertbutylparacresol).
A kind of method for preparing of solid aromatic antiblooming agent comprises being prepared as follows step:
(1), the allotment of anti-dizzy essence
To resist that each component adds in the anticorrosion container (1) successively in the dizzy essence, and be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of anti-dizzy essence
The modulated anti-dizzy essence for preparing of step (1) is carried out solubilising: at first in anticorrosion container (2) adding account for solid aromatic antiblooming agent product gross mass (hereinafter to be referred as: product population) be 8.00~10.00% efficient solubilizing agents; Be heated to 55~60 ℃; After 15 minutes, to clear;
To account for product population be the anti-dizzy essence that 0.75~1.50% step (1) has been allocated to wherein adding then, after stirring 5~10 minutes with agitator, stirs, and at room temperature lets its natural cooling, promptly get the anti-essence of swooning of solubilising;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40~90.50% distilled water, cause the variation of gross weight for preventing distilled water evaporation in the heating process, in this process, can add into accounting for product population is 10.00~15.00% distilled water; Heat; Progressively being sprinkled into while stirring and accounting for product population is 0.50~1.50% solid air freshening glue, and heated and stirred to 85~90 ℃, after 20~30 minutes; After making powder dissolution; Stop heating, its stirring is cooled to temperature about 60 ℃, promptly get the gel colloid;
(4), anti-dizzy essence and gel and close
Add in the gel colloid of step (3) gained that to account for product population be that 0.40~0.60% antiseptic continued stirs; When naturally cooling to 40~50 ℃; Slowly in the gel colloid, pour the anti-dizzy essence of solubilising of step (2) gained into, continue stirred for several minute after, when treating that the temperature natural cooling is got back to 30~40 ℃; Stop to stir, promptly be combined into the solid aromatic antiblooming agent;
Pour it in the anticorrosion mould into, let it naturally cool to room temperature, promptly get solid aromatic antiblooming agent product of the present invention.
Key character of the present invention is the blending technology of anti-dizzy essence in the solid aromatic antiblooming agent.
Beneficial effect of the present invention
The present invention is with the primary raw material of natural essential oils such as Fructus Citri Limoniae oil, mentha piperita oil, Oleum Menthae Rotundifoliae, eucalyptus quintessence oil for anti-dizzy perfume ingredient, and the solid aromatic antiblooming agent product of gained belongs to a kind of pure natural, nontoxic, safety product.Can make solid aromatic antiblooming agent of the present invention give out the fragrant fragrance of pure and fresh soft flowers and plants owing to also contain lavandula angustifolia wet goods composition in the solid aromatic antiblooming agent again; Not only can purify air; And have and drive away effect tired, peace show tender affection for emotion, when bringing pure and fresh, fragrant fragrance of a flower gas to air, dizzy in the time of can also alleviating riding public transportation means, headache; The sensation of feeling sick is brought joyful, comfortable sensation to health.
Solid aromatic antiblooming agent of the present invention is compared with other type products on the market, safety, to human body have no side effect, easy to carry, it is also convenient to use, and is not subject to influences such as temperature, humidity.Under conventional environment, can continue to discharge 5~8 days pleasant fragrance, also pollution-free to environment.
The specific embodiment
Through embodiment, the present invention is further specified, but do not limit the present invention below.
Use Shanghai traditional Chinese medicines group company to produce provides at present:
BHT (2.6-ditertbutylparacresol) is as the antioxidant in the solid aromatic antiblooming agent.
Use Shanghai Fine Chemical Co., Ltd of Supreme Being section to produce provides at present:
Model is that the product of G.P.L is as the antiseptic in the solid aromatic antiblooming agent;
Model is that the product of Cosmacd N II-9 is as the efficient solubilizing agents in the solid aromatic antiblooming agent.
Use Shanghai to tie up U.S. biotechnology Development Co., Ltd produces and provides at present:
Model is that the product of LA01 is as the solid air freshening glue in the solid aromatic antiblooming agent.
Embodiment 1
A kind of solid aromatic antiblooming agent, the mass percent of its contained each composition is formed as follows:
Anti-dizzy essence A 0.75%
Solid air freshening glue 0.50%
Efficient solubilizing agents 8.00%
Antiseptic 0.40%
Surplus is a distilled water 90.35%
The method for preparing of above-mentioned a kind of solid aromatic antiblooming agent comprises being prepared as follows step:
(1), the allotment of anti-dizzy essence A
The mass percent of each raw material is seen table 3 in the anti-dizzy essence A example:
The quality percentage composition of each component in the used anti-dizzy essence A example of table 3
Sequence number | The raw material name | Quality percentage composition (%) A |
1 | Mentholum | 21.00 |
2 | Borneolum Syntheticum | 5.00 |
3 | Camphora | 0.30 |
4 | Eucalyptus quintessence oil | 15.00 |
5 | Oleum Caryophylli | 5.00 |
6 | Thyme oil | 2.10 |
7 | Fructus Citri Limoniae oil | 9.10 |
8 | Oleum Menthae Rotundifoliae | 20.00 |
9 | Oleum lavandula angustifolia | 1.50 |
10 | Mentha piperita oil | 20.00 |
11 | Antioxidant | 1.00 |
According to the quality percentage composition of each component in the table 3, each component is added in the anticorrosion container (1) by sequence number in the table 3 successively, be stirred to 15 minutes and promptly reach even later on.
(2) solubilising of anti-dizzy essence A
The modulated anti-dizzy essence A for preparing carries out solubilising with step (1): at first in anticorrosion container (2) adding to account for product population be 8.00% efficient solubilizing agents, be heated to 55~60 ℃, after 15 minutes, to clear; To account for product population be the anti-dizzy essence A that 0.75% step (1) has been allocated to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature lets its natural cooling, promptly get the anti-essence A of swooning of solubilising;
(3), the colloidal preparation of gel
In anticorrosion container (3), add distilled water 90.35%, cause the variation of gross weight for preventing distilled water evaporation in the heating process, in this process, can add into accounting for product population is 15.00% distilled water; Heat, progressively being sprinkled into while stirring and accounting for product population is 0.50% solid air freshening glue, and heated and stirred to 85~90 ℃; After 30 minutes, make powder dissolution after, stop the heating; Its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), anti-dizzy essence A and gel and close
Add in the gel colloid of step (3) gained that to account for product population be that 0.40% antiseptic continued stirs; When naturally cooling to 40~50 ℃; Slowly in the gel colloid, pour the anti-dizzy essence A of solubilising of step (2) gained into, continue to stir, when treating that the temperature natural cooling is got back to 30~40 ℃; Stop to stir, promptly be combined into the solid aromatic antiblooming agent;
Pour it in the anticorrosion mould into, let it naturally cool to room temperature, promptly get solid aromatic antiblooming agent product of the present invention.
The solid aromatic antiblooming agent of above-mentioned gained has obvious Allyl-4,3-guaiacol salted cake fried in sesame oil gas, and Oleum Menthae Rotundifoliae is fragrant and sweet too heavy, and the icy penetration power is not enough.Fragrance is too single, fragrance inadequately circle with, abundant, not enough passing through sent out, outward appearance is transparent gel-form.After a period of time, fragrance weakens gradually, and the colloid evaporation rate is fast.Anti-dizzy DeGrain.
Embodiment 2
A kind of solid aromatic antiblooming agent, the mass percent of its contained each composition is formed as follows:
Anti-dizzy essence B 1.50%
Solid air freshening glue 1.50%
Efficient solubilizing agents 10.00%
Antiseptic 0.60%
Surplus is a distilled water
The method for preparing of above-mentioned a kind of solid aromatic antiblooming agent comprises being prepared as follows step:
(1), the allotment of anti-dizzy essence B
The mass percent of each raw material is seen table 4 in the anti-dizzy essence B example:
The quality percentage composition of each component in the used anti-dizzy essence B example of table 4
Sequence number | The raw material name | Quality percentage composition (%) B |
1 | Mentholum | 28.00 |
2 | Borneolum Syntheticum | 7.30 |
3 | Camphora | 0.50 |
4 | Eucalyptus quintessence oil | 17.00 |
5 | Oleum Caryophylli | 3.00 |
6 | Thyme oil | 2.00 |
7 | Fructus Citri Limoniae oil | 8.00 |
8 | Oleum Menthae Rotundifoliae | 14.00 |
9 | Oleum lavandula angustifolia | 1.20 |
10 | Mentha piperita oil | 18.00 |
11 | Antioxidant | 1.00 |
According to the percentage composition of each component in the table 4, each component is added in the anticorrosion container (1) by sequence number in the table 4 successively, be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of anti-dizzy essence B
The modulated anti-dizzy essence B for preparing carries out solubilising with step (1): at first in anticorrosion container (2) adding to account for product population be 10.00% efficient solubilizing agents, be heated to 55~60 ℃, after 15 minutes, to clear; To account for product population be the anti-dizzy essence B that 1.50% step (1) has been allocated to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature lets its natural cooling, promptly get the anti-essence B of swooning of solubilising;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 86.40% distilled water, cause the variation of gross weight for preventing distilled water evaporation in the heating process, in this process, can add into accounting for product population is 15.00% distilled water; Heat, progressively being sprinkled into while stirring and accounting for product population is 1.50% solid air freshening glue, and heated and stirred to 85~90 ℃; After 30 minutes, make powder dissolution after, stop the heating; Its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), anti-dizzy essence B and gel and close
Add in the gel colloid of step (3) gained that to account for product population be after 0.60% the antiseptic; Continue to stir, when naturally cooling to 40~50 ℃, slowly in the gel colloid, pour the anti-dizzy essence B of solubilising of step (2) gained into; Continue to stir; When treating that temperature natural cooling is got back to 30~40 ℃, stop to stir, promptly be combined into the solid aromatic antiblooming agent;
Pour it in the anticorrosion mould into, let it naturally cool to room temperature, promptly get solid aromatic antiblooming agent product of the present invention.
The solid aromatic antiblooming agent of above-mentioned gained has the cool flavor of obvious band, mandarin orange Fructus Citri Limoniae delicate fragrance fragrance, slightly with quiet and beautiful fragrance of a flower fragrance.Fragrance pass through to be sent out, cool rhythm penetration power is strong, coordination, pure and mild, mellow and full, be transparent outward appearance, and have certain gel.With the passing of time, fragrance can slowly volatilize, and still can keep fragrance preferably, and colloidal outward appearance also can diminish over time gradually, but the state of its gel can't change.5~7 days pleasant fragrance can be continued to discharge, and anti-dizzy effect can be effectively reached.
Embodiment 3
A kind of solid aromatic antiblooming agent, the mass percent of its contained each composition is formed as follows:
Anti-dizzy essence C 1.13%
Solid air freshening glue 1.00%
Efficient solubilizing agents 9.00%
Antiseptic 0.50%
Surplus is a distilled water
(1), the allotment of anti-dizzy essence C
The mass percent of each raw material is seen table 5 in the anti-dizzy essence C example:
The quality percentage composition of each component in the used anti-dizzy essence C example of table 5
Sequence number | The raw material name | Quality percentage composition (%) |
1 | Mentholum | 25.00 |
2 | Borneolum Syntheticum | 8.30 |
3 | Camphora | 1.50 |
4 | Eucalyptus quintessence oil | 17.00 |
5 | Oleum Caryophylli | 3.00 |
6 | Thyme oil | 2.00 |
7 | Fructus Citri Limoniae oil | 8.00 |
8 | Oleum Menthae Rotundifoliae | 15.00 |
9 | Oleum lavandula angustifolia | 1.20 |
10 | Mentha piperita oil | 18.00 |
11 | Antioxidant | 1.00 |
According to the quality percentage composition of each component in the table 5, each component is added in the anticorrosion container (1) by sequence number in the table 5 successively, be stirred to 15 minutes and promptly reach even later on.
(2), the solubilising of anti-dizzy essence C
The modulated anti-dizzy essence C for preparing carries out solubilising with step (1): at first in anticorrosion container (2) adding to account for product population be 9.00% efficient solubilizing agents, be heated to 55~60 ℃, after 15 minutes, to clear; To account for product population be the anti-dizzy essence C that 1.13% step (1) has been allocated to wherein adding then, after stirring 10 minutes with agitator, stirs, and at room temperature lets its natural cooling, promptly get the anti-essence C of swooning of solubilising;
(3), the colloidal preparation of gel
Add in anticorrosion container (3) that to account for product population be 88.37% distilled water, cause the variation of gross weight for preventing distilled water evaporation in the heating process, in this process, can add into accounting for product population is 15.00% distilled water; Heat, progressively being sprinkled into while stirring and accounting for product population is 1.00% solid air freshening glue, and heated and stirred is to 85-90 ℃; After 30 minutes, make powder dissolution after, stop the heating; Its stirring is cooled to temperature about 60 ℃, promptly gets the gel colloid;
(4), anti-dizzy essence C and gel and close
Add in the gel colloid of step (3) gained that to account for product population be after 0.50% the antiseptic; Continue to stir, when naturally cooling to 40~50 ℃, slowly in the gel colloid, pour the anti-dizzy essence C of solubilising of step (2) gained into; Continue to stir; When treating that temperature natural cooling is got back to 30~40 ℃, stop to stir, promptly be combined into the solid aromatic antiblooming agent;
Pour it in the anticorrosion mould into, let it naturally cool to room temperature, promptly get solid aromatic antiblooming agent product of the present invention.
The solid aromatic antiblooming agent of above-mentioned gained has obvious Borneolum Syntheticum, the Camphora breath, chemical breath is heavier, fragrance is dull, fragrance inadequately circle with, pure and mild, though outward appearance is transparent gel-form, after a period of time, the colloid evaporation rate is fast.The relative embodiment of anti-dizzy effect 2 is more not obvious.
The above content is merely the basic explanation of the present invention under conceiving, and according to technical scheme of the present invention institute
Any equivalent transformation of doing all should belong to protection scope of the present invention.
Claims (12)
1. a solid aromatic antiblooming agent is characterized in that, by percentage to the quality, its composition is:
Surplus is a distilled water;
Efficient solubilizing agents wherein is polyoxypropylene fatty alcohol ether, polyoxyethylene aliphatic alcohol ether;
Solid air freshening glue wherein is polyvinyl alcohol, hydroxypropyl emthylcellulose or modified cellulose;
Antiseptic wherein is the mixture of dihydroxymethyl dimethyl hydantoin and 3-iodo-2-propynyl butyl carbamate;
Wherein said anti-dizzy essence is made up of Mentholum, Borneolum Syntheticum, Camphora, eucalyptus quintessence oil, Oleum Caryophylli, thyme oil, Fructus Citri Limoniae oil, Oleum Menthae Rotundifoliae, Oleum lavandula angustifolia, mentha piperita oil, antioxidant; Said resisting swooned essence by percentage to the quality, and its composition is: Mentholum: 20.00~30.00%; Borneolum Syntheticum: 5.00~15.00%; Camphora: 0.30~2.00%; Eucalyptus quintessence oil: 15.00~20.00%; Oleum Caryophylli: 2.00~5.00%; Thyme oil: 1.00~4.00%; Fructus Citri Limoniae oil: 8.00~15.00%; Oleum Menthae Rotundifoliae: 15.00~25.00%; Oleum lavandula angustifolia: 1.00~4.00%; Mentha piperita oil: 15.00~25.00%; Antioxidant: 1.00~2.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
2. a kind of solid aromatic antiblooming agent as claimed in claim 1 is characterized in that: efficient solubilizing agents wherein is a polyoxyethylene aliphatic alcohol ether; Solid air freshening glue wherein is modified cellulose.
3. according to claim 1 or claim 2 a kind of solid aromatic antiblooming agent is characterized in that by percentage to the quality, its composition is:
Surplus is a distilled water;
Wherein said resisting swooned essence by percentage to the quality, and its composition is:
Mentholum: 21.00~28.00%; Borneolum Syntheticum: 5.00~8.30%; Camphora: 0.30~1.50%; Eucalyptus quintessence oil: 15.00~17.00%; Oleum Caryophylli: 3.00~5.00%; Thyme oil: 2.00~2.10%; Fructus Citri Limoniae oil: 8.00~9.10%; Oleum Menthae Rotundifoliae: 14.00~20.00%; Oleum lavandula angustifolia: 1.20~1.50%; Mentha piperita oil: 18.00~20.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
4. according to claim 1 or claim 2 a kind of solid aromatic antiblooming agent is characterized in that by percentage to the quality, its composition is:
Surplus is a distilled water;
Wherein said resisting swooned essence by percentage to the quality, and its composition is:
Mentholum: 21.00%; Borneolum Syntheticum: 5.00%; Camphora: 0.30%; Eucalyptus quintessence oil: 15.00%; Oleum Caryophylli: 5.00%; Thyme oil: 2.10%; Fructus Citri Limoniae oil: 9.10%; Oleum Menthae Rotundifoliae: 20.00%; Oleum lavandula angustifolia: 1.50%; Mentha piperita oil: 20.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
5. according to claim 1 or claim 2 a kind of solid aromatic antiblooming agent is characterized in that in the quality percentage, its composition is:
Surplus is a distilled water;
Wherein said resisting swooned essence by percentage to the quality, and its composition is:
Mentholum: 28.00%; Borneolum Syntheticum: 7.30%; Camphora: 0.50%; Eucalyptus quintessence oil: 17.00%; Oleum Caryophylli: 3.00%; Thyme oil: 2.00%; Fructus Citri Limoniae oil: 8.00%; Oleum Menthae Rotundifoliae: 14.00%; Oleum lavandula angustifolia: 1.20%; Mentha piperita oil: 18.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
6. according to claim 1 or claim 2 a kind of solid aromatic antiblooming agent is characterized in that by percentage to the quality, its composition is:
Surplus is a distilled water;
Wherein said resisting swooned essence by percentage to the quality, and its composition is:
Mentholum: 25.00%; Borneolum Syntheticum: 8.30%; Camphora: 1.50%; Eucalyptus quintessence oil: 17.00%; Oleum Caryophylli: 3.00%; Thyme oil: 2.00%; Fructus Citri Limoniae oil: 8.00%; Oleum Menthae Rotundifoliae: 15.00%; Oleum lavandula angustifolia: 1.20%; Mentha piperita oil: 18.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
7. according to claim 1 or claim 2 a kind of method for preparing of solid aromatic antiblooming agent is characterized in that the preparation process of this method is:
(1), the allotment of anti-dizzy essence
To resist that each component adds in the anticorrosion container (1) successively in the dizzy essence, and be stirred to 15 minutes and promptly reach even later on;
(2), the solubilising of anti-dizzy essence
The modulated anti-dizzy essence for preparing of step (1) is carried out solubilising:
Add in anticorrosion container (2) at first that to account for solid aromatic antiblooming agent product gross mass be 8.00~10.00% efficient solubilizing agents, be heated to 55~60 ℃, after 15 minutes, to clear;
To account for the product gross mass be the anti-dizzy essence that 0.75~1.50% step (1) has been allocated to wherein adding then, after stirring 5~10 minutes with agitator, stirs, and at room temperature lets its natural cooling, promptly get the anti-essence of swooning of solubilising;
(3), the preparation of gel
Add in anticorrosion container (3) that to account for the product gross mass be 86.40~90.50% distilled water, cause the variation of gross weight for preventing distilled water evaporation in the heating process, in this process, can add into accounting for the product gross mass is 10.00~15.00% distilled water; Heat; Progressively being sprinkled into while stirring and accounting for the product gross mass is 0.50~1.50% solid air freshening glue, and heated and stirred to 85~90 ℃, after 20~30 minutes; After making powder dissolution; Stop heating, its stirring is cooled to temperature about 60 ℃, promptly get the gel colloid;
(4), anti-dizzy essence and gel and close
Add in the gel colloid of step (3) gained that to account for the product gross mass be that 0.40~0.60% antiseptic continued stirs, when naturally cooling to 40~50 ℃, slowly in the gel colloid, pour the anti-dizzy essence of solubilising of step (2) gained into; After continuing stirred for several minute, when treating that the temperature natural cooling is got back to 30~40 ℃, stop to stir; Promptly get the solid aromatic antiblooming agent; Pour in the anticorrosion mould, let it naturally cool to room temperature, promptly get solid aromatic antiblooming agent product.
8. used anti-dizzy essence in according to claim 1 or claim 2 a kind of solid aromatic antiblooming agent is characterized in that by percentage to the quality, its composition is:
Mentholum: 20.00~30.00%; Borneolum Syntheticum: 5.00~15.00%; Camphora: 0.30~2.00%; Eucalyptus quintessence oil: 15.00~20.00%; Oleum Caryophylli: 2.00~5.00%; Thyme oil: 1.00~4.00%; Fructus Citri Limoniae oil: 8.00~15.00%; Oleum Menthae Rotundifoliae: 15.00~25.00%; Oleum lavandula angustifolia: 1.00~4.00%; Mentha piperita oil: 15.00~25.00%; Antioxidant: 1.00~2.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
9. anti-dizzy essence as claimed in claim 8 is characterized in that by percentage to the quality, its composition is: Mentholum: 21.00~28.00%; Borneolum Syntheticum: 5.00~8.30%; Camphora: 0.30~1.50%; Eucalyptus quintessence oil: 15.00~17.00%; Oleum Caryophylli: 3.00~5.00%; Thyme oil: 2.00~2.10%; Fructus Citri Limoniae oil: 8.00~9.10%; Oleum Menthae Rotundifoliae: 14.00~20.00%; Oleum lavandula angustifolia: 1.20~1.50%; Mentha piperita oil: 18.00~20.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
10. anti-dizzy essence as claimed in claim 8 is characterized in that by percentage to the quality, its composition is: Mentholum: 21.00%; Borneolum Syntheticum: 5.00%; Camphora: 0.30%; Eucalyptus quintessence oil: 15.00%; Oleum Caryophylli: 5.00%; Thyme oil: 2.10%; Fructus Citri Limoniae oil: 9.10%; Oleum Menthae Rotundifoliae: 20.00%; Oleum lavandula angustifolia: 1.50%; Mentha piperita oil: 20.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
11. anti-dizzy essence as claimed in claim 8 is characterized in that by percentage to the quality, its composition is: Mentholum: 28.00%; Borneolum Syntheticum: 7.30%; Camphora: 0.50%; Eucalyptus quintessence oil: 17.00%; Oleum Caryophylli: 3.00%; Thyme oil: 2.00%; Fructus Citri Limoniae oil: 8.00%; Oleum Menthae Rotundifoliae: 14.00%; Oleum lavandula angustifolia: 1.20%; Mentha piperita oil: 18.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
12. anti-dizzy essence as claimed in claim 8 is characterized in that by percentage to the quality, its composition is: Mentholum: 25.00%; Borneolum Syntheticum: 8.30%; Camphora: 1.50%; Eucalyptus quintessence oil: 17.00%; Oleum Caryophylli: 3.00%; Thyme oil: 2.00%; Fructus Citri Limoniae oil: 8.00%; Oleum Menthae Rotundifoliae: 15.00%; Oleum lavandula angustifolia: 1.20%; Mentha piperita oil: 18.00%; Antioxidant: 1.00%; Wherein said antioxidant is the 2.6-ditertbutylparacresol.
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CN103405553A (en) * | 2013-08-13 | 2013-11-27 | 上海应用技术学院 | Solid-gel ultra-refreshing fragrant refreshing agent and preparation method thereof |
CN104721867B (en) * | 2013-08-26 | 2018-03-13 | 安徽新华学院 | A kind of preparation method for the air aromatic agent that can slowly discharge oxygen and natural perfume composition |
CN104013707A (en) * | 2014-05-09 | 2014-09-03 | 苏州易川健康科技有限公司 | Compound essential oil |
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CN104399103B (en) * | 2014-11-28 | 2017-05-31 | 华南理工大学 | A kind of natural air freshener and preparation method thereof |
CN104606468A (en) * | 2014-12-31 | 2015-05-13 | 姜晓明 | Traditional Chinese medicine formula for treating dizziness with syndrome of static blood blocking orifices and preparation method of traditional Chinese medicine formula |
CN111388571A (en) * | 2020-03-06 | 2020-07-10 | 吾悦堂教育科技(北京)有限公司 | Compound essential oil for treating rhinitis and cold |
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