CN101941872B - Pesticidal foliage fertilizer mixed with plant growth factors and preparation method thereof - Google Patents
Pesticidal foliage fertilizer mixed with plant growth factors and preparation method thereof Download PDFInfo
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- CN101941872B CN101941872B CN2010102577797A CN201010257779A CN101941872B CN 101941872 B CN101941872 B CN 101941872B CN 2010102577797 A CN2010102577797 A CN 2010102577797A CN 201010257779 A CN201010257779 A CN 201010257779A CN 101941872 B CN101941872 B CN 101941872B
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Abstract
The invention discloses a pesticidal foliage fertilizer, which is prepared by grinding and uniformly mixing gibberellin 3, heteroauxin, brassinolide, abscisic acid, jasmonic acid, zeatin, salicylic acid, 1-aminocyclopropane-carboxylic acid. The fertilizer is a novel phytosterol foliage fertilizer with advantages of high efficiency, no toxicity and environmental friendliness, can promote the growth of plants by over 10 percent, and has no environmental pollution.
Description
Technical field
The present invention relates to a kind of Pesticidal foliage fertilizer, particularly Pesticidal foliage fertilizer of the long factor of a kind of mixed plant symphysis and preparation method thereof.
Background technology
Because the characteristics such as foliage fertilizer has that instant effect, utilization ratio are high, consumption is few, using method is easy and effect of increasing production is obvious, and be widely used in the agriculture production.In recent years, all take much count of production and the application of foliage fertilizer both at home and abroad, only at the Chinese commodity foliage fertilizer hundreds of is arranged.But, there is no preferably, have nutrition, coordinate plant growth, desinsection and the multi-functional composite foliage fertilizer such as antibacterial.So we have researched and developed a series of multi-functional composite foliage fertilizer, farming No. 1 foliage fertilizer in north is wherein a kind of, and the research and development application of this kind has been enriched the kind of foliage fertilizer and offered the multiple possible selection of peasant.
Summary of the invention
The object of the present invention is to provide the Pesticidal foliage fertilizer of the long factor of a kind of mixed plant symphysis; The present invention also aims to provide the preparation method of this medicine fertilizer.
Pesticidal foliage fertilizer composition of the present invention, its raw material consists of (weight part):
Plant hormones regulators,gibberellins (3) 7-11 part
Indolylacetic acid 0.01-0.1 part
Brassinolide 0.01-0.1 part
Dormin 0.01-0.1 part
Jasmonic acid 0.01-0.1
Zeatin 0.01-0.1
Whitfield's ointment 0.02-0.1 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.1 part.
Pesticidal foliage fertilizer composition of the present invention, its raw material consists of (weight part):
Plant hormones regulators,gibberellins 38-9.9 part
Indolylacetic acid 0.01-0.05 part
Brassinolide 0.01-0.04 part
Dormin 0.01-0.03 part
Jasmonic acid 0.01-0.04 part
Zeatin 0.01-0.04 part
Whitfield's ointment 0.02-0.04 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.03 part.
Pesticidal foliage fertilizer composition of the present invention, its raw material composition is preferably following weight part:
Plant hormones regulators,gibberellins 39.5-9.9 part
Indolylacetic acid 0.04-0.05 part
Brassinolide 0.02-0.03 part
Dormin 0.01-0.02 part
Jasmonic acid 0.01-0.02 part
Zeatin 0.01-0.02 part
Whitfield's ointment 0.02-0.03 part
1-amino-cyclopropane-1-carboxylic acid 0.01-0.02.
The preparation method of Pesticidal foliage fertilizer composition of the present invention is, it is even that said components is pressed the prescription ground and mixed, namely gets the growth hormone mixture.
Said mixture is prepared as optional one of the face technique of taking off of water dispersant:
A gets this growth hormone mixture 0.5-2.5 weight part (preferred 1-2 weight part), adds dispersion agent 0.1-0.2 weight part (preferred 0.12-0.16) again, and wetting agent 0.05-0.1 weight part (preferred 0.06-0.08) is filled to 10 weight parts.It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent (preferred alcohol) of 1-3 (preferred 1: 2), in 40-70 ℃ (preferred 50 ℃) oven dry, grind evenly drying, packing namely obtains growth hormone mixture water dispersant.
B gets this growth hormone mixture 0.5-2.5 weight part (preferred 1-2 weight part), adds dispersion agent 0.1-0.2 weight part (preferred 0.12-0.16) again, and wetting agent 0.05-0.1 weight part (preferred 0.06-0.08) is filled to 10 weight parts.It is 1 that above each component is dissolved in volume ratio: ground and mixed is even in the organic solvent (preferred alcohol) of 1-3 (preferred 1: 1), in 40-70 ℃ (preferred 50 ℃) oven dry, grind evenly drying, packing namely obtains growth hormone mixture water dispersant.
Used organic solvent can also be selected to indefiniteness a kind of in chloroform, 40-90 ℃ sherwood oil, ether, ethyl acetate, normal hexane, hexanaphthene, benzene, ethyl acetate, methyl alcohol, acetone, the pimelinketone etc. except ethanol.
Used dispersion agent can be a kind of in the alkaline sodium lignosulfonate A of improvement, improvement alkaline sodium lignosulfonate B, desugar sodium lignosulfonate (M-9), desugar condensation sodium lignosulfonate (M series), the methanonaphthalene sulphonic acids dispersion agent (such as dispersion agent NNO, Dispersant MF, dispersing agent C NF, super dispersion agent 550S, Di Sier economic benefits and social benefits); Wetting agent is how sodium sulfonate, succsinic acid alkyl sodium sulfonate a kind of of Saponin/TSM, animal protein factor digest, lipid acid vitriol, this sulfonate of alkyl, single dialkybenze sulfonate, polymerization of carboxylic acid sodium, sodium lignosulfonate, petroleum sodium sulfonate, alkyl biphenyl ether sulfonic acid sodium, dipropyl benzene sulfonic acid sodium salt, butyl; Permeate agent is any one or a few among Fatty Alcohol(C12-C14 and C12-C18) polyoxy ether alkene, permeate agent BA, penetrant m, the penetrant t H; Filler is: a kind of in potter's clay, clay, kaolin, diatomite, talcum powder, pyrophyllite, the White Carbon black.
Novel many growth hormone foliage fertilizer is made (weight part) by following raw material:
Growth hormone mixture water dispersant 0.1-0.3 part
Nutritive element mixture 2-6 part
Plant sterol mixture 2-3.5 part
Weighting agent adds to 10 parts
Novel many growth hormone foliage fertilizer is preferably made (weight part) by following raw material:
0.11 part of growth hormone mixture water dispersant
5 parts in nutritive element mixture
2.5 parts in plant sterol mixture
Weighting agent adds to 10 parts
Novel many growth hormone foliage fertilizer is preferably made (weight part) by following raw material:
0.12 part of growth hormone mixture water dispersant
4 parts in nutritive element mixture
3.5 parts in plant sterol mixture
Weighting agent adds to 10 parts
Novel many growth hormone foliage fertilizer is preferably made (weight part) by following raw material:
0.13 part of growth hormone mixture water dispersant
6 parts in nutritive element mixture
3 parts in plant sterol mixture
Weighting agent adds to 10 parts
Growth hormone mixture water dispersant of the present invention (0.1-0.3 part) nutritive element mixture (2-6 part) and plant sterol mixture (2-3.5 part), all be weight part below, add again a certain amount of filler to 10 part, fully mixing, dry, packing get final product.
Above-mentioned nutritive element mixture (take 20 weight parts as example) comprises urea 5 weight parts, potassium primary phosphate 2 weight parts, boric acid 2 weight parts among the present invention; Disodium ethylene diamine tetraacetate 1.8 weight parts, Manganous chloride tetrahydrate 2 weight parts, calcium chloride 1 weight part, sal epsom 2 weight parts, ferrous sulfate 2 weight parts, zinc sulfate 1 weight part, copper sulfate 0.2 weight part, (above-mentioned raw materials mixing, be dissolved in an amount of water, spraying drying gets final product).
The present invention plants the plant sterol of another functional additive for directly extracting from leguminous plants, comprise that β-sitosterol, Stigmasterol, campesterol, brassicasterol, avenasterol, ergosterol, this sterol of standing grain, citrostadienol, Lip river fly enol, ring jackfruit alcohol, cycloartenol, 2,4-methylene basic ring jackfruit alcohol waits any one or a few.Directly from plant, extract with organic solvent and to obtain.Used organic solvent can also be selected to indefiniteness a kind of in chloroform, 40-90 ℃ sherwood oil, ether, ethyl acetate, normal hexane, hexanaphthene, benzene, ethyl acetate, methyl alcohol, acetone, the cyclohexanone etc. except ethanol.
Among the present invention, also optionally added the auxiliary materials such as synergistic agent, permeate agent and stablizer, its usage ratio is 0.1-2%, and synergistic agent is any in tea saponin, root of langdu chromone, methylenedioxy benzene derivative, the 6-vinyl capraldehyde; Permeate agent is any in emulsifier BP, azone, the triphen phosphorus.Stablizer is a kind of in sodium alkyl benzene sulfonate, the Soxylat A 25-7.
Characteristic of the present invention is to collect coordinate plant growth, desinsection, the several functions such as antibacterial in foliage fertilizer, technical process is ripe, and cheap for manufacturing cost, its various components are nontoxic composition, environmentally safe, can significantly improve the output of farm crop, the Sustainable Production of useful agricultural.
The present invention is take Plant hormones regulators,gibberellins as main, and science other plant hormone of arranging in pairs or groups is made water dispersant, and in the water dispersant, dispersion agent, wetting agent make things convenient for agricultural use.Functional additive trace element mixture, plant sterol mixture can promote the growth of plant, can reach again the effect of killing pests and suppressing bacteria.
The invention provides a kind of efficient, nontoxic, environment amenable new plant growth regulator, the growth that it not only can promote plant is more than 10%, and without any problem of environmental pollution, is a kind of very outstanding plant-growth regulator foliage fertilizer.
Following enforcement or experimental example are used for further specifying, but are not limited to the present invention.
Experimental example 1 pharmacodynamic study data
By pot experiment, studied northern agricultural No. 1 (embodiment 1) foliage fertilizer to the impact of spinach growth characteristic in seedling stage.4 processing are established in test, process 1: contrast (clear water); Process 2: 100 times of liquid of No. 1 nutritive medium dilution of north farming; Process 3: 200 times of liquid of No. 1 nutritive medium dilution of north farming; Process 4: 400 times of liquid of No. 1 nutritive medium dilution of north farming.Adopt pot experiment: the basin alms bowl is black plastic keg (internal diameter 10cm, high 10cm), and soil is to fill basin behind flower nutrition soil and the sole of the foot stone 1:1 mixing, adds water, sowing, and every basin sowing 3-5 grain, the rear thinning of emerging keeps 1 strain, and it is consistent that each processes water and fertilizer management.The spring sowing rape was emerged on November 20th, 2009, and on January 20th, 2010 gathered.Foliage-spray 3 times, every minor tick 10 days, the amount of solution that each every basin sprays is 150mL, makes the positive and negative blade face of plant moistening evenly.Spray the 1st time on December 20th, 2009 (rape 4 leaves 1 heart), spray respectively on December 30, January 10 the 2nd time, the 3rd time.During results, every basin plant all gathers.
Gather behind the seedling, measure respectively leaf area, gross weight, over-ground part weight, root weight, relatively the clear water control group calculates the per-cent that each position of plant increases.Calculation formula is as follows:
The observed value of gain percentage=(sample measurement value-control group observed value) * 100%/sample
Experimental result is as follows:
1. the leaf of spinach area:
North No. 1 100,200,400 times of diluents of farming have the effect of obvious promotion the leaf of spinach area change, and reduce with concentration, and increasing amount also reduces.
2. spinach gross weight
North No. 1 100,200,400 times of diluents of farming have the effect that obvious promotion spinach gross weight increases, and reduce with concentration, and increasing amount also reduces.
3. spinach over-ground part
North No. 1 100,200,400 times of diluents of farming have the effect that obvious promotion spinach over-ground part weight increases, and reduce with concentration, and increasing amount also reduces.
4. Radix spinach is heavy
North No. 1 100,200,400 times of diluents of farming have the effect that obviously alleviates Radix spinach weight, and change in concentration is little on the reduction impact.
Experimental result shows, the leaf area of spinach, gross weight, over-ground part weight and clear water are relatively, increment all reaches more than 19%, the weight of root reduces more than 30% approximately, illustrate that the oriented over-ground part of nutritive substance shifts obviously on the root, for the greengrocery crop, demonstration is a kind of reasonable plant-growth regulator foliage fertilizer.
Embodiment
Embodiment 1: with CA3 (Gibberellins, Plant hormones regulators,gibberellins 3) 1200mg, IAA (Indole-3-acetic acid, indolylacetic acid) 5.6mg, BR (Bressinosteroids, brassinolide) 2.5mg, ABA (Abscisic acid, dormin), 1.2mg, JA (Jasmonic acid jasmonic acid) 1.2mg, Z (Zeatin, zeatin) 2.8mg, SA (Salicylic acid Whitfield's ointment) 1.2mg mixing, add dispersing agent C NF150mg, wetting agent sodium laurylsulfonate 80mg, be dissolved in 95% ethanol, grind, use disk granulation, namely obtain the water dispersant of growth hormone mixture.Add again 4g trace element mixture, 3.5g plant sterol mixture, add weighting agent to 10g, mixing, vacuum packaging namely obtains No. 1 foliage fertilizer of north farming.
Embodiment 2: with CA3 (Gibberellins, Plant hormones regulators,gibberellins 3) 1200mg, IAA (Indole-3-acetic acid, indolylacetic acid) 5.6mg, BR (Bressinosteroids, brassinolide) 2.5mg, ABA (Abscisic acid, dormin), 1.2mg, JA (Jasmonic acid jasmonic acid) 1.2mg, Z (Zeatin, zeatin) 2.8mg, SA (Salicylic acid Whitfield's ointment) 1.2mg mixing, add dispersing agent C NF180mg, wetting agent sodium laurylsulfonate 100mg, be dissolved in 70% ethanol, spraying drying, 110 ℃ of control drying temperatures, make granularity at 0.1-0.5mm, namely obtain the water dispersant of growth hormone mixture.Add again 6g trace element mixture, 2g plant sterol mixture, add weighting agent to 10g, mixing, vacuum packaging namely obtains No. 1 foliage fertilizer of north farming.
Embodiment 3: with CA3 (Gibberellins; Plant hormones regulators,gibberellins 3) 1200mg; IAA (Indole-3-acetic acid; indolylacetic acid) 5.6mg; BR (Bressinosteroids; brassinolide) 2.5mg; ABA (Abscisic acid; dormin); 1.2mg; JA (Jasmonic acid jasmonic acid) 1.2mg; Z (Zeatin; zeatin) 2.8mg; SA (Salicylic acid Whitfield's ointment) 1.2mg mixing; add dispersing agent C NF180mg; wetting agent sodium laurylsulfonate 90mg; be ground; water spray is granulated in rotating pelletizer, and drying namely obtains the water dispersant of growth hormone mixture.Add again 3g trace element mixture, 3g plant sterol mixture, add weighting agent to 10g, mixing, vacuum packaging namely obtains No. 1 foliage fertilizer of north farming.
Claims (1)
1. Pesticidal foliage fertilizer is characterized in that this Pesticidal foliage fertilizer makes by the following method:
With Plant hormones regulators,gibberellins 3 1200mg, indolylacetic acid 5.6mg, brassinolide 2.5mg, dormin 1.2mg, jasmonic acid 1.2mg, zeatin 2.8mg, Whitfield's ointment 1.2mg mixing, add dispersing agent C NF150mg, wetting agent sodium laurylsulfonate 80mg, be dissolved in 95% ethanol, grind, use disk granulation, namely obtain the water dispersant of growth hormone mixture; Add again 4g trace element mixture, 3.5g plant sterol mixture, add weighting agent to 10g, mixing, vacuum packaging namely obtains foliage fertilizer.
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| CN2010102577797A CN101941872B (en) | 2010-08-19 | 2010-08-19 | Pesticidal foliage fertilizer mixed with plant growth factors and preparation method thereof |
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| CN2010102577797A CN101941872B (en) | 2010-08-19 | 2010-08-19 | Pesticidal foliage fertilizer mixed with plant growth factors and preparation method thereof |
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| CN101941872B true CN101941872B (en) | 2013-01-09 |
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