CN101862031A - Preparation of undaria pinnitafida ethanol extracting solution and application thereof to cigarette - Google Patents
Preparation of undaria pinnitafida ethanol extracting solution and application thereof to cigarette Download PDFInfo
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- CN101862031A CN101862031A CN 201010204569 CN201010204569A CN101862031A CN 101862031 A CN101862031 A CN 101862031A CN 201010204569 CN201010204569 CN 201010204569 CN 201010204569 A CN201010204569 A CN 201010204569A CN 101862031 A CN101862031 A CN 101862031A
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Abstract
The invention provides a preparation method of undaria pinnitafida ethanol extracting solution, which mainly comprises the following steps: a. baking the undaria pinnitafida after the preliminary treatment for 2 to 4 h under the condition of 40 to 70 DEG C, and crashing the undaria pinnitafida to 20 to 80 meshes; b. taking a certain amount of undaria pinnitafida dry powder, adding ethanol accounting for 3 to 10 times of the amount of the undaria pinnitafida dry powder, and extracting for 1 to 4 h under the condition of normal temperature to 90 DEG C; and c. carrying out cooling, filtering and concentrating the extracting solution until the dry substance concentration is between 1 and 10 percent to obtain the undaria pinnitafida ethanol extracting solution. The undaria pinnitafida ethanol extracting solution is prepared into feed liquid with different concentrations to be uniformly sprayed on cut tobacco in the cigarette material feeding process. Sensory evaluation results prove that during the combustion of the cigarette, the smoke gas has no peculiar smell, impurity gas and irritation effect of the smoke gas of the cigarette are obviously reduced, and the mouth feeling and the like can be improved. The invention improves the smoking quality of the cigarette without changing the original performance of the cigarette, so the invention has actual production significance and value.
Description
Technical field
The present invention relates to the marine alga extraction and use the particularly preparation method of undaria pinnitafida ethanol extract and the application in cigarette thereof.This The Application of Technology does not change the existing processing technology of cigarette, can improve the sucking quality and the sense organ comfort level of cigarette.
Background technology
Marine alga is grown in the particular surroundings of ocean, contain special composition such as iodide, polyphenolic substance, many halos terpenoid, phytosterin compound, polyunsaturated fatty acid and algal polysaccharides, contain nutritional labelings such as rich in protein, vitamin, mineral matter and trace element in addition, obtaining preliminary Application and Development aspect food, industry, agricultural, medicine, beauty treatment and the health care, for example, be made into algal noodles with wheat flour, water and other condiment with the seaweed plant powder of fresh or salt marsh.Because this algal noodles is rich in nutritional labelings such as iodine, calcium, overcome traditional noodles nutritional labeling defect of insufficient effectively, particularly, has positive effect, with reference to patent: algal noodles and production technology CN1401260 thereof to the endemic control of iodine deficient area; From marine alga, extract iron superoxide dismutase (Fe-SOD), be applied to field of medicaments, with reference to patent: the method CN1415748 that extracts iron superoxide dismutase in the marine alga.
Undaria pinnitafida (Undaria pinnatifida) is under the jurisdiction of Phaeophyta, Phaeophyceae, Alariaceae (Nanjing University of Traditional Chinese Medicine, the Chinese medicine voluminous dictionary, 2006, Shanghai science tech publishing house, 1885-1886), be the traditional food of China, the dual-purpose marine alga of medicine, be described as " marine vegetables ",, worldwide culture as all very high kelp of a kind of economic worth, medical value, area and output are only second to sea-tangle and laver comes the 3rd, cultures the area and mainly concentrate on Japan, Korea S and China.Be about 350,000 tons (bright product) in China's output, mainly be distributed in Liaoning, Shandong, Jiangsu, zhejiang and other places.
It is reported, undaria pinnitafida main component: polysaccharide, volatile oil, glyceride, sterol, amino acid, polypeptide, carotenoid, unrighted acid and halide, trace element etc. (Ji Minghou, marine alga chemistry, Beijing: Science Press, 1997, p212-217).Lipid is based on aliphatic acid such as 18 carbon highly unsaturated fatty acids, 20 carbon unrighted acids in the undaria pinnitafida; Its contained mineral matter element, not only A wide selection of colours and designs but also content are abundant, and wherein content is higher elements such as K, Na, Ca, I, is human body " necessary mineral matter element "; The undaria pinnitafida polysaccharide mainly is a fucoidin, algin and laminaran, have the immunity of enhancing (Yang Xiaolin etc., the immunoregulation effect of fucoidin, China's marine drug, 1995.14 (3): p9-13), antiviral (Hudson, J., et al., Antiviral compounds in extracts of Korean seaweeds:Evidence for multipleactivities.Journal of Applied Phycology, 1998.10 (5): p427-434), antitumor, anticoagulation (Peng Bo and Zhao Jinhua, the anti-freezing of algal polysaccharide sulfate and fibrinolytic, Chinese herbal medicine, 2001.32 (11): p1015-1018), hypoglycemic, anti-oxidant, effects such as treatment hypertension.
At present, domestic undaria pinnitafida also is in the roughing stage, and its application is mainly based on edible and material outlet.Also constantly go deep into for network analysis of undaria pinnitafida chemical composition and application study, do not find the application in tobacco as yet.
Summary of the invention
The object of the invention is the ethanol extract of undaria pinnitafida is put in the cigarette in a certain way, thereby improves the sucking quality and the sense organ comfort level of cigarette.
Purpose of the present invention can be achieved through the following technical solutions:
The preparation method of undaria pinnitafida ethanol extract of the present invention comprises the steps:
After a, undaria pinnitafida are handled premenstruum (premenstrua), place under 40～70 ℃ of conditions and dry by the fire 2～4h,, be crushed to 20～80 orders to moisture below 10%, undaria pinnitafida dry powder;
B, get the undaria pinnitafida dry powder of step a gained, add ethanol it is extracted, amount of alcohol added is 3～10 times of dried Undaria pinnatifida grain weight amount, in normal temperature～90 ℃ extraction;
C, extract are through cooling, filtration, and being concentrated into dry substance concentration is 1～10%, obtains the undaria pinnitafida ethanol extract.
In the present invention, the early stage of undaria pinnitafida, processing comprised the infrared enzyme that goes out, washing, removal of impurities and airing process.
The described extracting method of step b of the present invention can be following four kinds of modes: the one, and under normal temperature condition, adopt the alcohol immersion mode to extract soak time 5-10d.The 2nd, adopt the microwave assisted extraction, range of microwave power 160～480w extracts 2～20min.The 3rd, adopt apparatus,Soxhlet's to extract 3-8 hour.The 4th, adopt supercritical carbon dioxide to extract, entrainer is selected ethanol for use, extracting pressure 20～50MPa, 30～50 ℃ of extraction temperature.The present invention also can adopt other existing known technology to extract.
The used concentration of alcohol of the present invention is 95%.
The application process of undaria pinnitafida ethanol extract of the present invention in cigarette: ethanol extract is mixed with the variable concentrations feed liquid, evenly is sprayed onto on the pipe tobacco, mix operations such as silk, storage, cigarette bag afterwards, finally make Cigarette at cigarette charging process.Concrete usage ratio is: undaria pinnitafida alcohol extract consumption is 0.025%～2.5% of a tobacco quality.Smoking result sees Table 1:
Sample cigarette and blank cigarette that table 1 adds the undaria pinnitafida ethanol extract contrast the experimental result of smokeing panel test
The cigarette that adds the undaria pinnitafida ethanol extract is through the sensory evaluating smoking, and the result shows: during cigarette burning, and the flue gas free from extraneous odour, the assorted gas and the excitant of cigarette smoke obviously reduce, and improve mouthfeel etc.
The present invention is as a kind of new cigarette additive, do not change original performance of cigarette, do not change the original processing technology of cigarette, to a certain extent, cigarette humectation poor performance, flue gas drying, the relatively poor quality defect of comfort level that China's cigarette product exists have been improved, improve the sucking quality of cigarette, therefore had more the meaning and the value of actual production.
The specific embodiment
The present invention is described further below in conjunction with embodiment, but does not limit the present invention.
Embodiment 1:
Undaria pinnitafida is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity, dry,, pulverize and mistake 40 eye mesh screens, at 45 ℃ of following baking 4h with baking oven with 95% ethanol of 4 times of amounts, at 80 ℃ of following refluxing extraction 2h, after the filtration filtrate being concentrated into dry matter content is 10%, and with concentrate, by feed liquid: pipe tobacco weight is 0.05% adding proportion, evenly be sprayed onto on the cigarette shreds at cigarette charging process, roll into cigarette.
Through smokeing panel test, the flue gas free from extraneous odour, more blank cigarette flavor matter is more clear, and assorted gas and excitant make moderate progress.
Embodiment 2:
Undaria pinnitafida is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity, dry, dry by the fire 4h down at 50 ℃, pulverize and cross 20 eye mesh screens with baking oven, by apparatus,Soxhlet's, with 95% ethanol of 4 times of amounts, under 85 ℃ of conditions, extract 5h, after the filtration filtrate being concentrated into dry matter content is 10%, and with concentrate, by feed liquid: pipe tobacco weight is 0.1% adding proportion, evenly be sprayed onto on the cigarette shreds at cigarette charging process, roll into cigarette.
Through smokeing panel test, the flue gas free from extraneous odour, assorted gas, excitant all alleviate.
Embodiment 3:
Undaria pinnitafida is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity, dry, dry by the fire 2h down at 50 ℃, pulverize and cross 20 eye mesh screens with baking oven, by the Microwave Extraction device, under 160w power, with 95% alcohol extract 20min of 3 times of amounts, after the filtration filtrate being concentrated into dry matter content is 10%, with concentrate, by feed liquid: pipe tobacco weight is 1% adding proportion, evenly is sprayed onto on the cigarette shreds, rolls into cigarette.
Through smokeing panel test, the flue gas free from extraneous odour, more blank cigarette flavor matter is more clear, and assorted gas, excitant all alleviate, and have improved the flue gas comfort level.
Embodiment 4:
Undaria pinnitafida is through the infrared enzyme that goes out, and washes clean is behind the rejecting impurity, dry, dry by the fire 4h down at 45 ℃, pulverize and cross 40 eye mesh screens with baking oven, pass through supercritical carbon dioxide extraction apparatus, under the 30MPa extracting pressure, make entrainer with ethanol, behind the extraction 2h, isolate tincture, with tincture by tincture: pipe tobacco weight is 1.5% adding proportion, evenly is sprayed onto on the cigarette shreds at cigarette charging process, mixes silk and also makes cigarette.
Through smokeing panel test, the flue gas free from extraneous odour, fragrance matter is strong, enrich, and the assorted gas and the excitant of flue gas obviously reduce, and the undaria pinnitafida alcohol extract improves the sucking quality of cigarette, improves the flue gas mouthfeel.
Embodiment 5:
Through the infrared enzyme that goes out, clean, the undaria pinnitafida after the pre-treatments such as removal of impurities, airing, under 50 ℃ of conditions, dry by the fire 4h with baking oven, to moisture below 10%, pulverize the back and cross 40 mesh sieves, 95% ethanol that adds 3 times of weight soaks 8d at normal temperatures, and soak after filtering, being concentrated into dry substance concentration is 10%, in pipe tobacco weight is 0.5% ratio, evenly is sprayed onto on the cigarette shreds at cigarette charging process, and makes cigarette.Smoking result shows, add undaria pinnitafida alcohol immersion liquid after, the flue gas free from extraneous odour, assorted gas, all more blank cigarette of excitant alleviate, mouthfeel is improved.
Claims (9)
1. the preparation method of a undaria pinnitafida ethanol extract is characterized in that, it is characterized in that: this method may further comprise the steps:
After a, undaria pinnitafida are handled premenstruum (premenstrua), place under 40～70 ℃ of conditions and dry by the fire 2～4h,, be crushed to 20～80 orders to moisture below 10%, undaria pinnitafida dry powder;
B, get the undaria pinnitafida dry powder of step a gained, add ethanol it is extracted;
C, extract are through cooling, filtration, and being concentrated into dry substance concentration is 1～10%, obtains the undaria pinnitafida ethanol extract.
2. according to the preparation method of the described undaria pinnitafida ethanol extract of claim 1, it is characterized in that: the processing in early stage of undaria pinnitafida comprises the infrared enzyme that goes out, washing, removal of impurities and airing process.
3. the preparation method of undaria pinnitafida ethanol extract according to claim 1 is characterized in that: the described extracting method of step b is under normal temperature condition, adopts the alcohol immersion mode to extract soak time 5-10d.
4. the preparation method of undaria pinnitafida ethanol extract according to claim 1 is characterized in that: the extracting method of step b is to adopt the microwave assisted extraction, and range of microwave power 160～480w extracts 2～20min.
5. the preparation method of undaria pinnitafida ethanol extract according to claim 1 is characterized in that: the extracting method of step b is to adopt apparatus,Soxhlet's to extract 3-8h.
6. the preparation method of undaria pinnitafida ethanol extract according to claim 1 is characterized in that: the extracting method of step b is to adopt supercritical carbon dioxide to extract, and entrainer is selected ethanol for use, extracting pressure 20～50MPa, 30～50 ℃ of extraction temperature.
7. the preparation method of undaria pinnitafida ethanol extract according to claim 1 is characterized in that: used concentration of alcohol is 95%.
8. the application of the described undaria pinnitafida ethanol extract of claim 1 in cigarette, it is characterized in that: undaria pinnitafida ethanol extract dilution back is joined on the cigarette shreds with feed liquid as cigarette, the elimination peculiar smell is arranged, reduce assorted gas, excitant, improve the effect of mouthfeel.
9. the application of undaria pinnitafida ethanol extract according to claim 8 in cigarette is characterized in that: undaria pinnitafida ethanol extract consumption is 0.025%～2.5% of a tobacco quality, evenly is sprayed onto on the pipe tobacco at cigarette charging process.
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| CN 201010204569 CN101862031A (en) | 2010-06-22 | 2010-06-22 | Preparation of undaria pinnitafida ethanol extracting solution and application thereof to cigarette |
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| CN 201010204569 CN101862031A (en) | 2010-06-22 | 2010-06-22 | Preparation of undaria pinnitafida ethanol extracting solution and application thereof to cigarette |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101974096A (en) * | 2010-10-27 | 2011-02-16 | 大连水产养殖集团有限公司 | Method for efficiently extracting polysaccharides from sporophyll of Undaria pinnatifida Suringar |
| CN105748537A (en) * | 2014-12-16 | 2016-07-13 | 吴彰哲 | Use of ethanol extract of undaria pinnatifida in preparation of composition for treating or preventing influenza A virus infection |
| CN109197980A (en) * | 2018-11-14 | 2019-01-15 | 浙江海洋大学 | A kind of preservation method of chilled pomfret |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1682614A (en) * | 2004-04-16 | 2005-10-19 | 中国科学院化学研究所 | Sea weed polysaccharide and its derivatives used for cigarette filter tip additives |
| CN1961762A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Sargassum fusiforme alcohol extract and application thereof in tobacco |
-
2010
- 2010-06-22 CN CN 201010204569 patent/CN101862031A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1682614A (en) * | 2004-04-16 | 2005-10-19 | 中国科学院化学研究所 | Sea weed polysaccharide and its derivatives used for cigarette filter tip additives |
| CN1961762A (en) * | 2006-11-25 | 2007-05-16 | 中国烟草总公司郑州烟草研究院 | Sargassum fusiforme alcohol extract and application thereof in tobacco |
Non-Patent Citations (3)
| Title |
|---|
| 《烟草科技》 20080831 李娟娟等 羊栖菜超临界CO2萃取物成分分析及在卷烟中的应用 , 第8期 * |
| 《食品与发酵工业》 20060131 谭洁怡等 超声波法提取裙带菜中褐藻多糖硫酸酯的工艺研究 第115-117页 第32卷, 第1期 2 * |
| 《食品科学》 20060331 门晓媛等 裙带菜硫酸多糖的制备及其性质研究 第156-161页 1-9 第27卷, 第3期 2 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101974096A (en) * | 2010-10-27 | 2011-02-16 | 大连水产养殖集团有限公司 | Method for efficiently extracting polysaccharides from sporophyll of Undaria pinnatifida Suringar |
| CN105748537A (en) * | 2014-12-16 | 2016-07-13 | 吴彰哲 | Use of ethanol extract of undaria pinnatifida in preparation of composition for treating or preventing influenza A virus infection |
| CN105748537B (en) * | 2014-12-16 | 2021-04-09 | 吴彰哲 | Application of undaria pinnatifida ethanol extract in preparation of composition for treating or preventing influenza A virus infection |
| CN109197980A (en) * | 2018-11-14 | 2019-01-15 | 浙江海洋大学 | A kind of preservation method of chilled pomfret |
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Application publication date: 20101020 |