CN101845268B - 一种水性单组分玻璃透明隔热涂料的制备方法 - Google Patents
一种水性单组分玻璃透明隔热涂料的制备方法 Download PDFInfo
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- CN101845268B CN101845268B CN 201010179816 CN201010179816A CN101845268B CN 101845268 B CN101845268 B CN 101845268B CN 201010179816 CN201010179816 CN 201010179816 CN 201010179816 A CN201010179816 A CN 201010179816A CN 101845268 B CN101845268 B CN 101845268B
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- water
- thermal insulating
- insulating glass
- glass coating
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- 238000000034 method Methods 0.000 title abstract description 9
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- 239000011159 matrix material Substances 0.000 claims description 19
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 17
- 238000002360 preparation method Methods 0.000 claims description 17
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- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 10
- 239000012752 auxiliary agent Substances 0.000 claims description 9
- 239000007822 coupling agent Substances 0.000 claims description 9
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- PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 claims description 6
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
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- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
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- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 5
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- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 4
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 claims description 4
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 2
- IWHMBXAAXBYCDD-UHFFFAOYSA-N dihydroxymethyl acetate Chemical compound CC(=O)OC(O)O IWHMBXAAXBYCDD-UHFFFAOYSA-N 0.000 claims description 2
- 239000012966 redox initiator Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical compound [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 claims description 2
- NNOZGCICXAYKLW-UHFFFAOYSA-N 1,2-bis(2-isocyanatopropan-2-yl)benzene Chemical compound O=C=NC(C)(C)C1=CC=CC=C1C(C)(C)N=C=O NNOZGCICXAYKLW-UHFFFAOYSA-N 0.000 claims 2
- DSSXKBBEJCDMBT-UHFFFAOYSA-M lead(2+);octanoate Chemical compound [Pb+2].CCCCCCCC([O-])=O DSSXKBBEJCDMBT-UHFFFAOYSA-M 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 abstract description 9
- 238000009413 insulation Methods 0.000 abstract description 5
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- 150000004706 metal oxides Chemical class 0.000 abstract 1
- UOHMMEJUHBCKEE-UHFFFAOYSA-N prehnitene Chemical compound CC1=CC=C(C)C(C)=C1C UOHMMEJUHBCKEE-UHFFFAOYSA-N 0.000 description 10
- 238000010276 construction Methods 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
- 150000002148 esters Chemical class 0.000 description 5
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- -1 polypropylene Polymers 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 3
- 238000006386 neutralization reaction Methods 0.000 description 3
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 125000005375 organosiloxane group Chemical group 0.000 description 2
- 229920000570 polyether Polymers 0.000 description 2
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- SVYKKECYCPFKGB-UHFFFAOYSA-N N,N-dimethylcyclohexylamine Chemical compound CN(C)C1CCCCC1 SVYKKECYCPFKGB-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 125000004423 acyloxy group Chemical group 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 239000012975 dibutyltin dilaurate Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- VQPKAMAVKYTPLB-UHFFFAOYSA-N lead;octanoic acid Chemical compound [Pb].CCCCCCCC(O)=O VQPKAMAVKYTPLB-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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CN 201010179816 CN101845268B (zh) | 2010-05-21 | 2010-05-21 | 一种水性单组分玻璃透明隔热涂料的制备方法 |
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CN 201010179816 CN101845268B (zh) | 2010-05-21 | 2010-05-21 | 一种水性单组分玻璃透明隔热涂料的制备方法 |
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CN101845268A CN101845268A (zh) | 2010-09-29 |
CN101845268B true CN101845268B (zh) | 2012-08-22 |
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CN 201010179816 Expired - Fee Related CN101845268B (zh) | 2010-05-21 | 2010-05-21 | 一种水性单组分玻璃透明隔热涂料的制备方法 |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103333600B (zh) * | 2013-05-30 | 2016-12-28 | 中国科学院合肥物质科学研究院 | 一种单组份水性聚氨酯透明隔热涂料的制备方法 |
CN105713501A (zh) * | 2015-12-28 | 2016-06-29 | 太仓耀华玻璃有限公司 | 一种带有聚氨酯涂层的隔热保温真空玻璃及其制造方法 |
CN109364535A (zh) * | 2018-10-29 | 2019-02-22 | 薛向东 | 一种耐高温消泡剂 |
CN110845698A (zh) * | 2019-11-19 | 2020-02-28 | 合众(佛山)化工有限公司 | 一种聚醚胺改性水性聚氨酯树脂及其制备方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4644030A (en) * | 1985-02-01 | 1987-02-17 | Witco Corporation | Aqueous polyurethane - polyolefin compositions |
CN1257897A (zh) * | 1999-12-10 | 2000-06-28 | 朱蓉仪 | 隔热涂料及其制备方法 |
CN1293683A (zh) * | 1998-03-16 | 2001-05-02 | 拜尔安特卫普有限公司 | 制造透明聚氨酯/脲弹性体的方法 |
CN1556162A (zh) * | 2004-01-09 | 2004-12-22 | 南京工业大学 | 纳米透明耐磨复合涂料 |
CN1637035A (zh) * | 2003-11-18 | 2005-07-13 | 气体产品与化学公司 | 水性聚氨酯分散体及其制造和使用方法 |
-
2010
- 2010-05-21 CN CN 201010179816 patent/CN101845268B/zh not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4644030A (en) * | 1985-02-01 | 1987-02-17 | Witco Corporation | Aqueous polyurethane - polyolefin compositions |
CN1293683A (zh) * | 1998-03-16 | 2001-05-02 | 拜尔安特卫普有限公司 | 制造透明聚氨酯/脲弹性体的方法 |
CN1257897A (zh) * | 1999-12-10 | 2000-06-28 | 朱蓉仪 | 隔热涂料及其制备方法 |
CN1637035A (zh) * | 2003-11-18 | 2005-07-13 | 气体产品与化学公司 | 水性聚氨酯分散体及其制造和使用方法 |
CN1556162A (zh) * | 2004-01-09 | 2004-12-22 | 南京工业大学 | 纳米透明耐磨复合涂料 |
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CN101845268A (zh) | 2010-09-29 |
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Owner name: SHANGHAI CONSTRUCTION SCIENCE RESEARCH INST. Free format text: FORMER OWNER: SHANGHAI BUILDING SCIENCE RESEARCH INSTITUTE CO., LTD. Effective date: 20130918 |
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Effective date of registration: 20130918 Address after: 200032 Shanghai city Xuhui District Wanping Road No. 75 first floor Patentee after: SHANGHAI Research Institute OF BUILDING SCIENCES Address before: 200032 Shanghai city Xuhui District Wanping Road No. 75 Patentee before: SHANGHAI RESEARCH INSTITUTE OF BUILDING SCIENCES (Group) Co.,Ltd. |
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