CN101845255A - Water-based baking paint for glass substrate and preparation and use methods thereof - Google Patents
Water-based baking paint for glass substrate and preparation and use methods thereof Download PDFInfo
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- CN101845255A CN101845255A CN201010120281A CN201010120281A CN101845255A CN 101845255 A CN101845255 A CN 101845255A CN 201010120281 A CN201010120281 A CN 201010120281A CN 201010120281 A CN201010120281 A CN 201010120281A CN 101845255 A CN101845255 A CN 101845255A
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Abstract
The invention discloses a water-based baking paint for a glass substrate and a preparation method and the application thereof; the formula of the water-based glass baking paint comprises the following components in parts by weight: 45 to 63 percent of water-soluble acrylic resin, 5 to 7 percent of methylated amino resin, 5 to 15 percent of water-based paste, 1.2 to 1.5 percent of coupling agent, 2 to 5 percent of additive and 25 to 30 percent of deionized water. When the baking paint is prepared, first the water-soluble acrylic resin, defoamer, wetting agent, leveling agent, dispersant and some water are sequentially added into a stirring tank to be stirred, is added with the water-based slurry and the like to be stirred and dispersed at high speed; and finally the methylated amino resin, the coupling agent and the rest water are sequentially added in to be stirred into a uniform coating system. The invention also provides a use method of the glass baking paint. When being applied to ground glass, hard glass and other substrates, the coating has the advantages of simple preparation process, convenient construction, strong coating adhesion, high hardness, water resistance, good heat resistance and the like.
Description
Technical field
The present invention relates to a kind of water-based stoving paint and preparation and using method that is used for glass baseplate.
Background technology
The glass material particular optical performance makes it comparatively extensive in the application aspect daily.The glass daily necessities are in the process of using, and people propose high requirement to each opposite sex of glass daily necessities color.Only the manufacturing forming process from glass is difficult to satisfy the requirement of people to color.The aqueous glass baking vanish be primarily aimed at glasswork painted, be used to be coated on glass article surface to itself playing the effect that beautifies modification; Reduced greatly with water as solvent that VOC (organic volatile) belongs to the environment-friendly type coating product in the discharging of air in the prescription.
Summary of the invention
In view of above-mentioned condition, the object of the present invention is to provide a kind of construction technology simple, the environment-friendly water-based glass baking varnish of good adhesion, tinting strength, surperficial special decorative effect and physical and mechanical properties is arranged at glass article surface.
Another object of the present invention is to provide the preparation and the using method of above-mentioned a kind of above-mentioned baking vanish.
The present invention can be achieved through the following technical solutions:
A kind of aqueous glass baking vanish that is used for glass baseplate, it is characterized in that in weight fraction, prescription comprises following component: 45～63 parts water soluble acrylic resin, 5～7 parts methyl-etherified aminoresin, 5～15 parts pigment slurry, 1.2～1.5 parts coupling agent, 2～5 parts auxiliary agent, 25～30 parts water.
Described resin is the water soluble acrylic resin.
Also be included in the methyl-etherified aminoresin that has good solubility in the water in the described prescription.
Also comprise 0.3～0.5 part wetting agent, 1～1.5 part defoamer, 0.3～0.4 part dispersion agent, 0.5 part flow agent in the described prescription; Add the fashionable wax emulsion that also need add 1.5～2.5 parts at responsiveness pigment.
Also comprise 1.2～1.5 parts coupling agent in the described prescription.
Also comprise 5～15 parts pigment slurry in the above-mentioned prescription.
A kind of preparation method of aqueous glass baking vanish comprises the steps:
(1) water soluble acrylic resin, defoamer, wetting agent, flow agent, dispersion agent and portion water are joined in the stirring tank successively, under 400～600r/min speed conditions, stir 3～5min;
(2) add the pigment slurry (as aqueous color paste, water-based silver slurry, water-soluble pearlescent slurry, delustring slurry etc.) that has prepared in advance, under 800～1000r/min speed conditions, high-speed stirring is disperseed 30～40min;
(3) water of adding methyl-etherified aminoresin, coupling agent and residual content stirs the preparation process that 3～5min can finish whole baking vanish.
A kind of using method of aqueous glass baking vanish, may further comprise the steps: the water or the ethanolic soln that take by weighing 0.5～1.2 times of a certain amount of aqueous glass baking vanish adding are diluted to working viscosity, coat on the glass baseplate, dewater to surface drying at 60 ℃～65 ℃ following levelling baking 3min～5min, toast 15min～10min then under 130 ℃～150 ℃ conditions, baking-curing gets aqueous glass baking vanish coating.
The construction process of above-mentioned glass baseplate use is comparatively simple, and when coating glass baseplate, be easy to generate stronger bonding strength, that lovely luster has good ornamental, every physical and mechanical properties is better.Therefore satisfy the service requirements of people to general glass daily necessities.
Embodiment
Below in conjunction with embodiment glass baseplate use glass baking varnish of the present invention and preparation thereof and using method are described in further detail, but the scope of protection of present invention is not limited to the scope that embodiment represents.
Especially, have stronger physicals, below will enumerate specific embodiment and be described further for proving the prepared aqueous glass baking vanish of listing in the above-mentioned formula table of prescription.
Table 1 aqueous glass baking vanish example formulations
Embodiment 1:
Concrete prescription sees the prescription 1 in the formula table 1 for details
According to prescription 1, get 45 parts water soluble acrylic resin successively, 1.0 the defoamer of part, 0.3 the wetting agent of part, 0.5 the flow agent of part, 0.4 dispersion agent of part and 20 parts water join in the stirring tank, under 400～600r/min speed conditions, stirring 3～5min mixes, the aqueous transparent mill base that adds 10 parts, high-speed stirring is disperseed about 30min under 800～1000r/min, the coupling agent that in stirring tank, adds 1.2 parts more successively, 5 parts methyl-etherified aminoresin, 17 parts water, under 300～500 speed conditions, stir 3～5min, form the preparation process that uniform coating system is promptly finished above-mentioned baking vanish.
Above-mentioned aqueous glass baking vanish in use, the water that adds 0.5 times of water-based stoving paint is adjusted to working viscosity, it is applied on the glass baseplate final high temperature baking, baking under 60 ℃～65 ℃ conditions earlier before the high bake, levelling, except that anhydrating or alcohol solvent; Storing time is about 15min under 130 ℃ of conditions, and storing time is about about 10min under 150 ℃ of conditions, forms transparent color and films.Paint film property sees Table 2 prescriptions, 1 physical property measurement table result.
Embodiment 2
Concrete prescription sees the prescription 2 in the formula table 1 for details
According to prescription 2, get 50 parts water soluble acrylic resin successively, 1.2 the defoamer of part, 0.4 the wetting agent of part, 0.5 the flow agent of part, 0.3 dispersion agent of part and 25 parts water join in the stirring tank, under 400～600r/min speed conditions, stirring 3～5mi n mixes, the delustring slurry that adds 8 parts, high-speed stirring is disperseed about 30min under 800～1000r/min, the coupling agent that in stirring tank, adds 1.5 parts more successively, 5.6 the methyl-etherified aminoresin of part, 7.2 the water of part, under 300～500 speed conditions, stir 3～5mi n, form the preparation process that uniform coating system is promptly finished above-mentioned baking vanish.
Above-mentioned aqueous glass baking vanish in use, the water that adds 1 times of water-based stoving paint is adjusted to working viscosity, it is applied on the glass baseplate final high temperature baking, baking under 60 ℃～65 ℃ conditions earlier before the high bake, levelling, except that anhydrating; Storing time is about 15min under 130 ℃ of conditions, forms to cover filming of husky effect.Paint film property sees Table the performance test results under 2 prescriptions 2.
Embodiment 3
According to prescription 3, get 63 parts water soluble acrylic resin successively, 1.5 the defoamer of part, 0.4 the wetting agent of part, 0.5 the flow agent of part, 0.4 dispersion agent of part and 5 parts water join in the stirring tank, under 400～600r/min speed conditions, stirring 3～5min mixes, add 10 parts aqueous transparent mill base and 5 parts pearlite slurry, high-speed stirring is disperseed about 30min under 800～1000r/min, the coupling agent that in stirring tank, adds 1.5 parts more successively, 7 parts methyl-etherified aminoresin, 6.1 the water of part, under 300～500 speed conditions, stir 3～5min, form the preparation process that uniform coating system is promptly finished above-mentioned baking vanish.
Above-mentioned aqueous glass baking vanish in use, the water that adds 0.8 times of water-based stoving paint is adjusted to working viscosity, it is applied on the glass baseplate final high temperature baking, baking under 60 ℃～65 ℃ conditions earlier before the high bake, levelling, except that anhydrating; Storing time is about 10min under 150 ℃ of conditions, and the transparent color that forms the illusion-colour effect is filmed.Paint film property sees Table the performance test results under 2 prescriptions 3.
The present invention carries out physical property measurement to above-mentioned three groups of aqueous glass baking vanish prescriptions; Test process is to carry out with reference to standard GB and industry examination criteria, and test result is as shown in table 2.
Table 2 physical property measurement result
The construction process of above-mentioned aqueous glass baking vanish need not steps such as pre-treatment, so construction process is comparatively simple; And in the time of on coating the different glass base material, be easy to generate stronger bonding strength, bright-coloured color and luster, favorable mechanical physicals, therefore can play effect such as protection decorations grade glasswork.In addition, above-mentioned aqueous glass baking vanish is in use, and is more or less freely to the allotment of pigment, therefore be easy to control color and and glossy change, and then satisfy different outward appearance needs, promote decorate properties; And above-mentioned aqueous glass baking vanish also can have extremely strong water resistance.
From table 1 and table 2, as can be seen, the aqueous glass baking vanish that above-mentioned three groups of aqueous glass baking vanish prescriptions make has splendid performance above glass baseplate.
In addition, those skilled in the art also can do other variation in spirit of the present invention, and certainly, these are according to the present invention's spirit institute.
Claims (8)
1. water-based stoving paint that is used for glass baseplate, it is characterized in that in weight fraction, prescription comprises following component: 45～63 parts water soluble acrylic resin, 5～7 parts methyl-etherified aminoresin, 5～15 parts pigment slurry, 1.2～1.5 parts coupling agent, 2～5 parts auxiliary agent, 25～30 parts water.
2. aqueous glass baking vanish according to claim 1, it is characterized in that comprising in the described prescription 45～63 parts of water soluble acrylic resins, described water soluble acrylic resin's solids content is 48.5 ± 2%, acid number is that 89.7mg/g, hydroxyl value are that 25.5mg/g, pH value are that 7.5-8.5, second-order transition temperature are 42.5 ℃.
3. aqueous glass baking vanish according to claim 1 is characterized in that comprising in the described prescription 5～7 parts in methyl-etherified aminoresin, and described methyl-etherified aminoresin solid content is 80 ± 3%.
4. aqueous glass baking vanish according to claim 1 is characterized in that comprising in the described prescription 5～15 aqueous color paste parts.Described aqueous color paste comprises: aqueous transparent mill base, the real mill base of water-based, water-based silver slurry, pearlite slurry, delustring slurry etc.
5. aqueous glass baking vanish according to claim 1 is characterized in that comprising in the described prescription 1.2～1.5 parts of coupling agents, and described coupling agent is the alkoxyl group non-ionic compound, effective constituent 100%.
6. aqueous glass baking vanish according to claim 1 is characterized in that described prescription comprises flow agent 0.5,0.3～0.5 part of wetting agent, 0.3～0.5 part of dispersion agent, 1.0～1.5 parts of defoamers.
7. aqueous glass baking vanish preparation method according to claim 1 comprises the steps:
(1) water soluble acrylic resin, defoamer, wetting agent, flow agent, dispersion agent and portion water are joined in the stirring tank successively, under 400～600r/min speed conditions, stir 3～5min;
(2) add aqueous color paste, under 800～1000r/min speed conditions, high-speed stirring is disperseed 30～40min;
(3) add methyl-etherified aminoresin, coupling agent and remainder water, stir the preparation process that 3～5min can finish whole baking vanish.
8. the using method of the described described aqueous glass baking vanish of claim 1, it is characterized in that, during construction, described glass baking varnish with 0.5～1.2 times of the ethanolic soln of deionized water or tap water and 50% dilution after, coat on the glass baseplate, dewater to surface drying at 60 ℃～65 ℃ following levellings, baking 3min～5min, under 130 ℃～150 ℃ conditions, toast 10min～15min then.
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| CN201010120281A CN101845255A (en) | 2010-03-09 | 2010-03-09 | Water-based baking paint for glass substrate and preparation and use methods thereof |
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| CN102020896A (en) * | 2010-12-10 | 2011-04-20 | 湖南福湘木业有限责任公司 | Environmental-protection coating and preparation method thereof |
| CN102153928A (en) * | 2011-02-28 | 2011-08-17 | 重庆恒美涂料有限公司 | Aqueous glass paint and preparation method thereof |
| CN102585630A (en) * | 2011-12-19 | 2012-07-18 | 青岛爱尔家佳新材料有限公司 | Water-based glass baking paint and preparation method thereof |
| CN102618139A (en) * | 2012-04-01 | 2012-08-01 | 王立明 | Water-based paint for painting bottles |
| CN102732121A (en) * | 2012-07-26 | 2012-10-17 | 蔡军 | Composition for water-based glass bottle baking varnish |
| CN102888163A (en) * | 2012-10-25 | 2013-01-23 | 南京长江涂料有限公司 | Water-based paint for Christmas glass ornaments, and preparation method and application thereof |
| CN102977708A (en) * | 2012-11-16 | 2013-03-20 | 苏州嘉乐威企业发展有限公司 | Water-soluble stoving varnish suitable for craft glass products and preparation method thereof |
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Application publication date: 20100929 |