CN101829042B - Anti-aging Chinese medicinal mask and preparation method thereof - Google Patents
Anti-aging Chinese medicinal mask and preparation method thereof Download PDFInfo
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- CN101829042B CN101829042B CN2010101796867A CN201010179686A CN101829042B CN 101829042 B CN101829042 B CN 101829042B CN 2010101796867 A CN2010101796867 A CN 2010101796867A CN 201010179686 A CN201010179686 A CN 201010179686A CN 101829042 B CN101829042 B CN 101829042B
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Abstract
The invention provides an anti-aging Chinese medicinal mask. The active ingredient of the mask is an aqueous extract which consists of 15 to 50 weight percent of pilose asiabell root, 15 to 50 weight percent of astragalus and 15 to 60 weight percent of Indian buead, wherein the pilose asiabell root has the effect of invigorating the vital energy and nourishing the blood, the astragalus has the effect of nourishing spleen Qi, and the pilose asiabell root and the astragalus help production of Qi and blood and serve as a monarch medicament; the Indian buead has the effects of invigorating the spleen, excreting dampness and helping spleen transportation and transformation and serves as a ministerial medicament; mint oil has pungent flavor and cooling property and can refresh the mind and serves as an adjuvant medicament; and the four medicaments have the effects of invigorating the spleen, nourishing the blood and clearing dampness, so that the mask has the effects of enriching the blood, beautifying, dissipating fatigue and alleviating aging. The mask also comprises moisturizing nutrients such as wheat germ oil, hyaluronic acid and collagen and the like so as to further improve the beautifying effect.
Description
Technical field
The present invention relates to the cosmetic formulation field, be specifically related to a kind of facial film of Chinese medicine compound extract preparation.
Background technology
Modern's rhythm of life is fast, and pressure is big, poor sleep, and skin lacks maintenance, adds and lives in for a long time in the air conditioner surroundings, causes the moisture of skin disequilibrium; Because environmental pollution is on the rise, dust, ultraviolet have more increased the weight of the aging of skin to the injury of skin again.
Skin aging shows as wrinkle and produces, and cutis laxa, nasolabial fold occur and deepen, and skin goes out various mottles etc.How defying age keeps the young physiological status of body, has become the research topic of a hot topic.Mostly the mechanism of popular anti-aging cosmetics is to remove free radical on the market at present, and like the gentle bloom (vitamin E) of Avene, Laneige snow coagulates newborn elite and reveals (Semen Armeniacae Amarum, Punica granatum L., cocoa extraction elite), Biotherm Fructus Canarii albi youth albumen essence (Olive leaf P.E) etc.; The extra-nutrition thing is like SK-II (Petiolus Trachycarpi tetrapeptide-3, end collagen), Lancome (corn, malt essence, polished rice peptide and sea-plant elite), FANCL (little collagen protein, silk albumen, EPC, maritime pine elite) etc.But free radical causes of senescence; Metalloproteases causes of senescence (replenishing collagen and elastin laminin) all is to set forth the old and feeble origin cause of formation from some aspects; In fact skin aging is multi-level, a many-sided complex process; The slow down aging cosmetics of single mechanism development more than the foundation, its effect is often barely satisfactory.
Summary of the invention
The technical problem that the present invention will solve provide a kind of can resisting age of skin, replenish the Chinese medicine facial film of skin-nourishing thing.
The technical scheme that the present invention addresses the above problem is:
A kind of Chinese medicine facial film of anti aging effect; This facial film is made up of effective components of Chinese medicinal and facial film field acceptable auxiliary, it is characterized in that said effective ingredient comprises that 94～97% (w/w) concentration is Chinese medicine extraction liquid and 0.5～2% (w/w) Oleum menthae of 0.2～2g medical material/mL; Described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Radix Codonopsis 15%～50%, the Radix Astragali 15%～50%, Poria 15%～60%; Every facial film is loaded with described Chinese medicine extraction liquid 80mL.
In the facial film of the present invention, described Chinese medicine extraction liquid is extracted by the Chinese medicine water decocting method of following weight proportion and obtains: Radix Codonopsis 30%～40%, the Radix Astragali 25%～35%, Poria 30%～40%.
In the facial film of the present invention; Described effective ingredient also can comprise and occupies the skin-nourishing thing of imitating composition 0.005～5.5%% (W/W) cosmetic result with further raising facial film of the present invention; Described skin-nourishing thing is selected from Semen Tritici aestivi germ oil, a kind of or two or more in hyaluronic acid and the collagen protein.
Facial film according to the invention can be prepared by following method:
(1) get Poria, Radix Codonopsis and the Radix Astragali, decocte with water twice adds 6～10 times for the first time and decocted 1.5～3 hours, adds 6～10 times for the second time and decocts 1.5～3 hours; Merge decocting liquid twice, filter, be concentrated into 0.2～2g medical material/mL, cold preservation was left standstill 10～24 hours, filtered, and adding water adjustment filter liquor concentration is 0.2～2g medical material/mL, gets Chinese medicine extraction liquid;
(2) carry the ratio of the said Chinese medicine extraction liquid of 80mL in every facial film, get Chinese medicine extraction liquid, Oleum menthae and facial film adjuvant and process facial film by conventional method;
In the above-mentioned steps, described facial film adjuvant comprises dispersant and carrier, wherein,
Described dispersant is selected from propylene glycol, glycerin or ethanol, preferred propylene glycol or glycerin;
Said carrier is gel-type vehicle or non-woven fabrics, and wherein, described gel-type vehicle is one or both in soybean fiber, arabic gum, carrageenan, Konjac glucomannan and the gelatin.
In the method for preparing of facial film of the present invention, described adjuvant also can comprise one or both in the following adjuvant:
1. antiseptic:, can be selected from chlorobutanol, benzyl alcohol, phenethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate and the propylparaben one or both, preferably ethyl hydroxybenzoate or propylparaben to prolong the shelf-life of facial film of the present invention.
2. solubilizing agent: optional to increase the dissolving of skin-nourishing thing from tween 80, SP-115A (Xin Pu company) or 1264 emulsifying agents (Xin Pu company).
When facial film of the present invention selects for use gel-type vehicle to be carrier, promptly be the quartzy facial film that is commonly called as, concrete method for making is following:
(1) scattered dispersant and gel-type vehicle mixture joined in the said Chinese medicine extraction liquid by proportioning, be heated to 80～90 ℃ and fully stirred 15 minutes, transfer to pH5.5～6.5 with the pH regulator agent;
(2) be cooled to 50 ℃ and add Oleum menthae, film forming (promptly processing facial film), packing, sterilization;
Wherein said pH regulator agent is hydrochloric acid, citric acid and phosphate buffer solution.
If the effective ingredient in the said quartzy facial film also comprises the skin-nourishing thing, then the skin-nourishing thing prepares in the process to add with Oleum menthae at facial film and gets final product.
If said quartzy facial film also contains adjuvants such as antiseptic or solubilizing agent, then when the preparation facial film, said adjuvant and gel-type vehicle are disperseed with dispersant, join in the Chinese medicine extraction liquid again.
When facial film of the present invention selects for use non-woven fabrics to be carrier, promptly be the non-woven fabrics facial film that is commonly called as, concrete method for making is following: dispersant and Oleum menthae are added in the said Chinese medicine extraction liquid, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, radiation sterilization.
If the effective ingredient in the said non-woven fabrics facial film also comprises the skin-nourishing thing, then the skin-nourishing thing prepares in the process to add with Oleum menthae at facial film and gets final product.
If said non-woven fabrics facial film also contains adjuvants such as antiseptic or solubilizing agent, then when the preparation facial film, said adjuvant is disperseed with dispersant, join in the Chinese medicine extraction liquid again.
Facial film according to the invention as main active component, can play blood-enriching face-nourishing, allaying tiredness, the effect of slow down aging with the effective ingredient of Poria, Radix Codonopsis and the Radix Astragali and Oleum menthae.
Therefrom medical angle is seen, taste are the foundation of acquired constitution, weakness of the spleen and stomach, and then insufficiency of generating and transforming QI and blood shows as spiritlessness and weakness, deficiency of QI with disinclination to talk, shallow complexion, even senilism.The spleen being in charge of dampness, weakness of the spleen and stomach then fortune is unable, and turbid damp is easy to stagnate.Radix Codonopsis benefiting qi and nourishing blood in the facial film of the present invention, the big enriching spleen-QI of the Radix Astragali, both share and help QI and blood biochemical, are monarch drug; Be aided with Poria spleen invigorating eliminating dampness by diuresis, help spleen fortuneization, be ministerial drug; Help with the hot cool refreshment of Oleum menthae, four medicines make a concerted effort to have strengthening spleen and nourishing blood, ooze the turbid effect of dampness removing, thereby reach blood-enriching face-nourishing, allaying tiredness, the effect of delaying decrepitude of skin again.
In order to understand the present invention better, will further specify the technique effect that the present invention has through clinical experiment report below.
1, patient data: skin elasticity is poor, shallow complexion, inappetence, or feeling of fatigue patient 90 examples, each 45 example of men and women, 30～45 years old age.Be divided into three groups at random: treatment group (Chinese medicine extraction liquid adds the skin nutrient) 30 examples, each 15 example of men and women, 36 ± 8 years old age; Matched group is (carrageenan adds water) 30 examples 1., each 15 example of men and women, 35 ± 8 years old age; Matched group is (Chinese medicine extraction liquid 2.; Do not add the skin nutrient) 30 examples, each 15 example of men and women, 37 ± 7 years old age.
Treatment first three groups patient's sex, age, clinical symptoms integration there are no significant difference (P＞0.05) has comparability.
2, experiment material:
(1) treatment group facial film of the present invention is pressed embodiment 1 preparation:
The treatment group is 1.: contain the skin-nourishing thing in the effective ingredient of used facial film, press embodiment 1 preparation, every weight is 80 grams, specification 10*15cm.
(2) the matched group facial film prepares by following method:
Matched group is 1.:
Prescription: carrageenan 11g, ethyl hydroxybenzoate 2g.
Method for making: water adds carrageenan after being heated to 80-90 ℃, and ethyl hydroxybenzoate fully stirred 15 minutes, regulates pH value to 5.5-6.5, film forming, packing, sterilization.Every weight is 80 grams, specification 10*15cm.
Matched group is 2.: do not contain the skin-nourishing thing in the effective ingredient of used facial film, used facial film is pressed embodiment 16 preparations, and every weight is 80 grams, specification 10*15cm.
3, experimental technique:
The treatment group: the patient lies on the back, and after washing one's face, spreads on face with facial film of the present invention, flush away behind about 15min.3 times weekly, be 2 weeks the course of treatment.
Matched group: the patient lies on the back, and after washing one's face, spreads on face, flush away behind about 15min with matched group facial film (not drug ingredients) 1..3 times weekly, be 2 weeks the course of treatment.
4, clinical symptoms standards of grading: skin elasticity still can, can recover rapidly after pushing but produce less dermatoglyph around the press section to be designated as 1 fen more dermatoglyph and to be designated as 2 fens; Skin elasticity is not good enough, pushes back 1～2s and can recover to be designated as 4 fens; Skin elasticity is poor, pushes the back and could the recuperator be designated as 8 fens above 2s.Shallow complexion is glossy to be designated as 2 fens, and the ochriasis tarnish is designated as 4 fens, and complexion is withered and yellow dark and gloomyly to be had no gloss and be designated as 8 fens.Appetite is good, and non fatigue feeling is designated as 0 fen, and appetite is poor slightly, and feeling of fatigue gently respectively is designated as 2 fens, inappetence, and feeling of fatigue respectively is designated as 4 fens.
5, efficacy assessment standard:
By formula earlier---score value * 100% calculates the improvement rate before clinical symptoms integration score value improvement rate=(symptom integral score value before the treatment-treatment back symptom integral score value)/treatment, adopts criterion evaluation curative effect then.
Produce effects: symptom integral score value improvement rate >=70%;
Effectively: symptom integral score value improvement rate >=50%;
Invalid: symptom does not see that obvious improvement or counter sees deterioration, symptom integral score value improvement rate＜50%.
6, statistical procedures: total data adopts SPSS 13.0 statistics softwares to carry out statistical analysis, and measurement data adopts the t check, and enumeration data adopts x
2Check.
7, result of the test
Table 1 is relatively seen in the clinical symptoms scoring before and after treatment group and the treatment of control group, and curative effect is relatively seen table 2 before and after treatment group and the treatment of control group, and treatment group and the matched group 1. improvement of cardinal symptom sign are relatively seen table 3.Can know that from table 2 facial film defying age total effective rate of the present invention is up to 80.0%, and observe through the treatment group and not have the heating of the skin of discovery, flushing, edema, untoward reaction such as pruritus.
Clinical symptoms scoring before and after table 1 treatment group and the treatment of control group
| Group | n | Before the treatment | After the treatment | Difference |
| The treatment group | 30 | 9.80±1.21 | 4.07±0.87 | 5.73±1.48 |
| Matched group 1. | 30 | 9.60±1.10 | 8.13±1.63 | 1.47±1.46 |
| Matched group 2. | 30 | 9.93±1.11 | 4.36±0.85 | 5.57±1.48 |
Table 2 treatment group and matched group curative effect are relatively
| Group | Case load | Produce effects | Effectively | Invalid | Total effective rate/% |
| The treatment group | 30 | 5 | 19 | 6 | 80.0 |
| Matched group 1. | 30 | 0 | 2 | 28 | 6.7 |
| Matched group 2. | 30 | 4 | 18 | 8 | 73.3 |
1. treatment group and matched group compare, and the evident in efficacy of medicine explained in P＜0.01.
2. treatment group and matched group compare P＞0.05; What main therapeutical effect had been described is Chinese medicine extraction liquid; But the difference of integration can be found out from the treatment front and back; Chinese medicine extraction liquid adds skin-nourishing thing group (i.e. treatment group) and does not add skin nutrient group (matched group 2.) relatively, can play function of anti-skin aging preferably.
Table 3 treatment group and matched group 1. cardinal symptom sign improve relatively
Routine number in the last table is two groups of case loads that improve, and percent is the improvement example number/hundreds of proportions by subtraction of treatment precedent of two groups of symptoms.Through statistical procedures, the equal difference of symptom is (P＜0.01) significantly.
The specific embodiment
Among the following embodiment 1～16, the recipe quantity of each embodiment is the recipe quantity of 12.5 facial films.
Embodiment 1
Prescription:
Radix Codonopsis 164g, Radix Astragali 141g, Poria 165g and Oleum menthae 5g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g and ethyl hydroxybenzoate 2g;
Method for making:
Getting above three flavor medicines is Radix Codonopsis, the Radix Astragali, Poria, and the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 0.5g medical material/ml, cold preservation was left standstill 24 hours; Filter, 0.5g medical material/ml is filtrated in adjustment, gets Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).Because hyaluronic acid than indissoluble, is difficult to homodisperse with medicinal liquid is directly mixed mutually, obtains the hyalomitome acid solution so earlier hyaluronic acid is dissolved in the water, and then mixes with medicinal liquid.
Embodiment 2
Prescription:
Radix Codonopsis 90g, Radix Astragali 270g, Poria 240g and Oleum menthae 1g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g and ethyl hydroxybenzoate 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time, adds 6 times of water gagings for the second time; Each 3 hours, merge the secondary decocting liquid, filter, concentrate written treaty 0.63g medical material/ml; Cold preservation was left standstill 24 hours, filtered, and 0.63g medical material/ml is filtrated in adjustment, got Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 3
Prescription:
Radix Codonopsis 480g, Radix Astragali 280g, Poria 120g and Oleum menthae 10g;
Soybean fiber 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g and benzyl alcohol 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 0.85g medical material/ml, cold preservation was left standstill 24 hours; Filter, 0.85: 1 medicinal liquid (0.85g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, soybean fiber and ethyl hydroxybenzoate; Be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value, be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein to 5.5-6.5; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 4
Prescription:
Radix Codonopsis 348g, Radix Astragali 116g, Poria 696g and Oleum menthae 15g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g and ethyl hydroxybenzoate 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 1.5g medical material/ml, cold preservation was left standstill 24 hours; Filter, 1.5: 1 medicinal liquid (1.5g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan, ethyl hydroxybenzoate; Be heated to 80-90 ℃ and fully stirred 15 minutes, regulate pH value, be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein to 5.5-6.5; Mixing makes dissolving fully, film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 5
Prescription:
Radix Codonopsis 600g, Radix Astragali 600g, Poria 680g and Oleum menthae 5g;
Carrageenan 11g, propylene glycol 50g, hyaluronic acid 0.1g, collagen protein 5g and ethyl hydroxybenzoate 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 10 times of water gagings for the first time; For the second time add 10 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 2g medical material/ml, cold preservation was left standstill 24 hours; Filter, 2: 1 medicinal liquid (2g medical materials/ml), get Chinese medicine extraction liquid are filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 6
Prescription:
Radix Codonopsis 60g, Radix Astragali 60g, Poria 80g and Oleum menthae 5g;
Soybean fiber 13g, propylene glycol 10g, hyaluronic acid 0.5g and ethyl hydroxybenzoate 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, be condensed into 0.2: 1 medicinal liquid (0.2g medical material/ml), hide and left standstill 24 hours; Filter, 0.2: 1 medicinal liquid (0.2g medical material/ml), get Chinese medicine extraction liquid is filtrated in the moisturizing adjustment; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film; Get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate; Being heated to 80-90 ℃ fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add Oleum menthae and 0.5% hyalomitome acid solution, make dissolving fully.Mixing, film forming, packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 7
Prescription:
Radix Codonopsis 188g, Radix Astragali 141g, Poria 141g and Oleum menthae 5g;
Carrageenan 13g, propylene glycol 50g, collagen protein 50g, ethyl hydroxybenzoate 1g and propylparaben 1g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time, adds 6 times of water gagings for the second time; Each 3 hours, merge the secondary decocting liquid, filter, concentrate written treaty 0.56g medical material/ml; Cold preservation was left standstill 24 hours, filtered, and 0.56g medical material/ml is filtrated in adjustment, got Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered propylene glycol, carrageenan, ethyl hydroxybenzoate and the propylparaben of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add Oleum menthae and hyalomitome acid solution, collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
Embodiment 8
Prescription:
Radix Codonopsis 164g, Radix Astragali 118g, Poria 188g and Oleum menthae 5g;
Carrageenan 13g, ethanol 50g, hyaluronic acid 0.1g, ethyl hydroxybenzoate 1g and propylparaben 1g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time, adds 6 times of water gagings for the second time; Each 3 hours, merge the secondary decocting liquid, filter, concentrate written treaty 0.5g medical material/ml; Cold preservation was left standstill 24 hours, filtered, and 0.5g medical material/ml is filtrated in adjustment, got Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered ethanol, carrageenan, ethyl hydroxybenzoate and the propylparaben of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully; Film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 9
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Carrageenan 13g, ethanol 50g, hyaluronic acid 0.25, collagen protein 10g, ethyl hydroxybenzoate 1g and benzyl alcohol 5g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 0.56g medical material/ml, cold preservation was left standstill 24 hours; Filter, 0.56: 1 medicinal liquid (0.56g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered ethanol, carrageenan, ethyl hydroxybenzoate and the benzyl alcohol of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein, mixing makes dissolving fully; Film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 10
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Carrageenan 13g, glycerin 50g, hyaluronic acid 0.25g, collagen protein 10g and chlorobutanol 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 0.56g medical material/ml, cold preservation was left standstill 24 hours; Filter, 0.56: 1 medicinal liquid (0.56g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered glycerin, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 11
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Carrageenan 10g, arabic gum 3g, propylene glycol 50g, hyaluronic acid 0.25g, collagen protein 10g and ethyl hydroxybenzoate 2g.
Method for making:
Get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time, adds 6 times of water gagings for the second time; Each 3 hours, merge the secondary decocting liquid, filter, concentrate written treaty 0.56g medical material/ml; Cold preservation was left standstill 24 hours, filtered, and 0.56g medical material/ml is filtrated in adjustment, got Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get scattered propylene glycol, carrageenan, the arabic gum volume ethyl hydroxybenzoate of Chinese medicine extraction liquid adding and be heated to 80-90 ℃ of abundant the stirring 15 minutes, regulate pH value to 5.5-6.5; Be cooled to about 50 ℃ and add Oleum menthae, 0.5% hyalomitome acid solution and collagen protein thoroughly, mixing makes dissolving fully; Film forming; Packing, sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 12
Prescription:
Radix Codonopsis 429g, Radix Astragali 429g, Poria 485g, Oleum menthae 14g;
Hyaluronic acid 0.36g, collagen protein 18g and propylene glycol 180g.
Method for making: get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 1.87g medical material/ml), cold preservation was left standstill 24 hours to concentrate 1.87: 1 medicinal liquids of written treaty; Filter, 1.87: 1 medicinal liquid 1.87g medical materials/ml) are filtrated in adjustment, Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with the scattered Oleum menthae of propylene glycol, 1% hyalomitome acid solution and collagen protein, fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing, and sterilization promptly gets.
In the above-mentioned steps, described 1% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 1% (w/w).
Embodiment 13
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g and 264 emulsifying agents (Xin Pu company) 4g.
Method for making: get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.52g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.52: 1 medicinal liquid of written treaty; Filter, 0.52: 1 medicinal liquid (0.52g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; Carry the ratio of 80mL Chinese medicine extraction liquid in every facial film; Getting Chinese medicine extraction liquid adds with 1264 scattered emulsifying agents of propylene glycol, Oleum menthae, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and collagen protein; Fully mix, stir, the non-woven fabrics that high-temperature sterilization is good absorbs, packing; Radiation sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 14
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g and SP-115A (Xin Pu company) 4g.
Method for making: get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.52g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.52: 1 medicinal liquid of written treaty; Filter, 0.52: 1 medicinal liquid (0.52g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with the scattered SP-115A of propylene glycol, Oleum menthae, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and collagen protein, fully mix; Stir; The non-woven fabrics that high-temperature sterilization is good absorbs, packing, and radiation sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 15
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Hyaluronic acid 0.1g, collagen protein 5g, Semen Tritici aestivi germ oil 20g, propylene glycol 50g and tween 80 10g.
Method for making: get Radix Codonopsis, the Radix Astragali and Poria, the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, (the 0.52g medical material/ml), cold preservation was left standstill 24 hours to concentrate 0.52: 1 medicinal liquid of written treaty; Filter, 0.52: 1 medicinal liquid (0.52g medical material/ml), get Chinese medicine extraction liquid is filtrated in adjustment; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add with the scattered tween 80 of propylene glycol, Oleum menthae, Semen Tritici aestivi germ oil, 0.5% hyalomitome acid solution and collagen protein, fully mix; Stir; The non-woven fabrics that high-temperature sterilization is good absorbs, packing, and radiation sterilization promptly gets.
In the above-mentioned steps, described 0.5% hyalomitome acid solution is that concentration is the hyaluronic acid aqueous solution of 0.5% (w/w).
Embodiment 16
Prescription:
Radix Codonopsis 150g, Radix Astragali 150g, Poria 170g and Oleum menthae 5g;
Carrageenan 11g, propylene glycol 50g, ethyl hydroxybenzoate 2g.
Method for making:
Getting above three flavor medicines is Radix Codonopsis, the Radix Astragali, Poria, and the decocte with water secondary adds 8 times of water gagings for the first time; For the second time add 6 times of water gagings, each 3 hours, merge the secondary decocting liquid; Filter, concentrate written treaty 0.5g medical material/ml, cold preservation was left standstill 24 hours; Filter, 0.5g medical material/ml is filtrated in adjustment, gets Chinese medicine extraction liquid; In the ratio that every facial film carries the 80mL Chinese medicine extraction liquid, get Chinese medicine extraction liquid and add scattered propylene glycol, carrageenan and ethyl hydroxybenzoate, be heated to 80-90 ℃ and fully stirred 15 minutes; Regulate pH value to 5.5-6.5, be cooled to about 50 ℃ and add Oleum menthae, mixing; Make dissolving fully, film forming, packing; Sterilization promptly gets.
Claims (8)
1. the Chinese medicine facial film of an anti aging effect; This facial film is made up of effective components of Chinese medicinal and facial film field acceptable auxiliary, it is characterized in that said effective ingredient is that Chinese medicine extraction liquid, 0.5～2% (w/w) Oleum menthae of 0.2～2g medical material/mL and the skin-nourishing thing of 0.005～5.5% (W/W) are formed by 94～97% (w/w) concentration; The weight percentage sum of described Chinese medicine extraction liquid, Oleum menthae and skin-nourishing thing is one of percentage hundred; Described Chinese medicine extraction liquid is obtained by the Chinese medicine water decocting method extraction of following weight proportion: Radix Codonopsis 15%～50%, the Radix Astragali 15%～50%, Poria 15%～60%; Described skin-nourishing thing is selected from a kind of or two or more in Semen Tritici aestivi germ oil, hyaluronic acid and the collagen protein; Every facial film is loaded with described Chinese medicine extraction liquid 80mL.
2. facial film according to claim 1 is characterized in that described Chinese medicine extraction liquid is extracted by the Chinese medicine water decocting method of following weight proportion to obtain: Radix Codonopsis 30%～40%, the Radix Astragali 25%～35%, Poria 30%～40%.
3. the method for preparing of claim 1 or 2 said facial films, this method is made up of following steps:
(1) get Poria, Radix Codonopsis and the Radix Astragali, decocte with water twice adds 6～10 times for the first time and decocted 1.5～3 hours, adds 6～10 times for the second time and decocts 1.5～3 hours; Merge decocting liquid twice, filter, be concentrated into 0.2～2g medical material/mL, cold preservation was left standstill 10～24 hours, filtered, and adding water adjustment filter liquor concentration is 0.2～2g medical material/mL, gets Chinese medicine extraction liquid;
(2) carry the ratio of the said Chinese medicine extraction liquid of 80mL in every facial film, get Chinese medicine extraction liquid, Oleum menthae and facial film adjuvant and process facial film by conventional method;
In the above-mentioned steps, described facial film adjuvant comprises dispersant and carrier, wherein,
Described dispersant is selected from propylene glycol, glycerin or ethanol;
Said carrier is gel-type vehicle or non-woven fabrics, and wherein, described gel-type vehicle is one or both in soybean fiber, arabic gum, carrageenan, Konjac glucomannan and the gelatin.
4. like the said method of claim 3, it is characterized in that described dispersant is propylene glycol or glycerin.
5. like the said method of claim 3, it is characterized in that described facial film adjuvant also comprises antiseptic, said antiseptic is one or both in chlorobutanol, benzyl alcohol, phenethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate and the propylparaben.
6. like the said method of claim 5, it is characterized in that described antiseptic is ethyl hydroxybenzoate or propylparaben.
7. like the said method of claim 3, it is characterized in that described facial film adjuvant also comprises solubilizing agent, described solubilizing agent is a tween 80.
8. like the said method of claim 5, it is characterized in that described facial film adjuvant also comprises solubilizing agent, described solubilizing agent is a tween 80.
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| CN2010101796867A CN101829042B (en) | 2010-05-17 | 2010-05-17 | Anti-aging Chinese medicinal mask and preparation method thereof |
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| CN101829042B true CN101829042B (en) | 2012-01-11 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102172289B (en) * | 2011-03-30 | 2012-12-26 | 广州智享生物科技有限公司 | Compound collagen electuary with high absorption and utilization rate and preparation method thereof |
| CN104207994A (en) * | 2014-09-14 | 2014-12-17 | 王小乐 | Healthy facial mask and preparation method thereof |
| CN104257593A (en) * | 2014-10-16 | 2015-01-07 | 武汉嘉润天合信息科技有限公司 | Traditional Chinese medicine compound multi-effect mask solution, mask and producing technology of mask solution |
| CN106265281A (en) * | 2016-08-24 | 2017-01-04 | 刘艺鹏 | Chinese medicine anti-ageing face mask |
| CN109758414A (en) * | 2019-03-27 | 2019-05-17 | 广州纯美化妆品制造有限公司 | It is a kind of to have effects that alleviate face mask of traditional Chinese medicine of dry skin and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1150899A (en) * | 1996-05-23 | 1997-06-04 | 陈星� | Anti-wrinkle lotion |
| CN1201678A (en) * | 1998-06-24 | 1998-12-16 | 苏桄显 | Face nursing cream |
| KR20060073708A (en) * | 2004-11-17 | 2006-06-29 | 최양원 | Manufacturing method of a herb medicine for atopic skin diseases |
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2010
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1150899A (en) * | 1996-05-23 | 1997-06-04 | 陈星� | Anti-wrinkle lotion |
| CN1201678A (en) * | 1998-06-24 | 1998-12-16 | 苏桄显 | Face nursing cream |
| KR20060073708A (en) * | 2004-11-17 | 2006-06-29 | 최양원 | Manufacturing method of a herb medicine for atopic skin diseases |
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