CN101787221A - Yellow environment-friendly disperse dye composition - Google Patents
Yellow environment-friendly disperse dye composition Download PDFInfo
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- CN101787221A CN101787221A CN201010117996A CN201010117996A CN101787221A CN 101787221 A CN101787221 A CN 101787221A CN 201010117996 A CN201010117996 A CN 201010117996A CN 201010117996 A CN201010117996 A CN 201010117996A CN 101787221 A CN101787221 A CN 101787221A
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Abstract
The invention discloses a yellow environment-friendly disperse dye composition which is mainly composed of the following components in percentage by weight: 50-97% of one or a plurality of dye monomers A disclosed in formula (1), 3-25% of dye monomer B disclosed in formula (2), 0-30% of dye monomer C disclosed in formula (3), 0-30% of one or a plurality of dye monomers D disclosed in formula (4), 0-12% of one or a plurality of dye monomers E disclosed in formula (5) and 0-30% of one or a plurality of dye monomers F disclosed in formula (6). The yellow environment-friendly disperse dye composition of the invention can be independently used as golden yellow and can be mixed with 2BLN blue and 3B red to be spliced into N gray to serve as low-temperature three-primary colors. The yellow environment-friendly disperse dye composition has vivid colored light, wide pH applicable range during dying, high color yield, favorable levelling property, favorable lifting power and favorable fastness of each item and especially has outstanding advantage on color fastness to light and compatibility.
Description
Technical field
The present invention relates to a kind of Yellow environment-friendly disperse dye composition, belong to low temperature modification partially, be applicable to the dyeing and the stamp of polyester material and vinegar fiber material, also be applicable to the dyeing and the stamp of ultra-fine fibre.
Background technology
C.I.Disperse yellow 23# (23# Huang) uses and extensively, and as monochrome, its low price, coloured light is gorgeous, light fastness is superior, and all other indexs are all good.And as colorant match it and 2BLN the blue and red assembly system disperse grey of 3B N, three's compatibleness is fabulous, dyeing rate is in full accord, and the former title of low temperature old three is arranged.But old three former C.I.Disperse yellow 23# can cracking produce carcinogenic suspicious material under given conditions because of it as low temperature, or harmful aromatic amine, are classified as the forbidding dyestuff by European Union member countries such as Germany.
Existing many in the market substitutes occur, as golden yellow SE-3R, yellow E-RGFL etc., but along with the discovery of using, the light fastness of these substitutes is nothing like the 23# Huang, particularly 80-110 ℃ of temperature rise rate is slow excessively, slightly poor with 2BLN indigo plant and the red synchronism of 3B, cause phenomenon such as aberration, look flower end to end easily.
Summary of the invention
The invention provides a kind of Yellow environment-friendly disperse dye composition, this dye composite uses with the 23# Huang in full accord, also slightly improves aspect sublimation fastness, washing fastness.
A kind of Yellow environment-friendly disperse dye composition, percentage composition meter by weight, mainly composed of the following components:
50～97% as the formula (1) one or more dye monomers A:
Y is H or halogen;
3～25% as the formula (2) dye monomer B:
0～30% as the formula (3) dye monomer C:
0～30% as the formula (4) one or more dye monomers D:
X
1Be H or C
1～C
4Alkyl;
0～12% as the formula (5) one or more dye monomers E:
X
2, X
3Be C independently separately
1～C
4Alkyl;
0～30% as the formula (6) one or more dye monomers F:
R
1Be C
1～C
4Alkyl or C
1～C
4Alkyl in a hydrogen replaced by phenyl ring.
Described dye monomer A be preferably following one or both suc as formula the dye monomer shown in (1-1)～(1-2):
Described dye monomer D be preferably following one or more suc as formula the dye monomer shown in (4-1)～(4-3):
Described dye monomer E be preferably following one or more suc as formula the dye monomer shown in (5-1)～(5-3):
Described dye monomer F be preferably following one or both suc as formula the dye monomer shown in (6-1)～(6-2):
A kind of preferred Yellow environment-friendly disperse dye composition, the percentage composition meter is mainly composed of the following components: 85～92% the dye monomer B as the formula (2) suc as formula the dye monomer A shown in (1-1) and 8～15% by weight.The advantage of this composition is that the compatibleness between its dyestuff is fabulous, no matter is all to be better than other dispersed dye as the monochrome use or with 2BLN indigo plant, mixed its compatibleness of the red assembly of 3B.
A kind of preferred Yellow environment-friendly disperse dye composition, the percentage composition meter is mainly composed of the following components: 82～90% the dye monomer C as the formula (3) of dye monomer B and 1～3% as the formula (2) suc as formula the dye monomer A shown in (1-1) and 8～15% by weight.The advantage of this composition is that the compatibleness between its dyestuff is fabulous, and light fastness can maintain an equal level with 23# is yellow.
A kind of preferred Yellow environment-friendly disperse dye composition, the percentage composition meter is mainly composed of the following components: 85～90% the dye monomer E as the formula (5) of dye monomer B and 1～3% as the formula (2) suc as formula the dye monomer A shown in (1-1) and 8～12% by weight.The advantage of this composition is that its washing fastness and sublimation fastness are significantly improved than the 23# Huang.
A kind of preferred Yellow environment-friendly disperse dye composition, percentage composition meter by weight, mainly composed of the following components: 85～90% suc as formula the dye monomer B as the formula (2) and 4～10% of the dye monomer A shown in (1-1) and 4～10% suc as formula the dye monomer F shown in (6-1).The advantage of this composition is that the compatibleness between its dyestuff is fabulous, and light fastness can maintain an equal level with 23# is yellow, and washing fastness and sublimation fastness improve.
Yellow environment-friendly disperse dye composition of the present invention generally needs to add auxiliary agent during application.Described auxiliary agent is dispersed dye dispersion agent, diffusant and tensio-active agents thereof etc. commonly used when composite. preferably include one of following or its mixture: naphthalene sulfonic acidformaldehyde condensation product, sulfonated lignin, alkyl naphthalene sulfonic acid formaldehyde condensation products.As condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF), naphthalene sulfonic acidformaldehyde condensation product (dispersing agent NNO), benzyl naphthalene sulfonic formaldehyde condensation compound (dispersing agent CNF), sodium lignosulfonate (xylogen 85A, 83A) etc.Usually, auxiliary agent is 1.0～5.4: 1 with the ratio of former dyestuff weight.
Yellow environment-friendly disperse dye composition of the present invention can be with the preparation of following method: after the former dyestuff of dye monomer is mixed in proportion, in the presence of auxiliary agent, water or other tensio-active agent, carry out corpusculed with pulverizers such as sand mill or shredders, then spraying drying.Above-mentioned dye monomer all can adopt the commercially available prod.
Yellow environment-friendly disperse dye composition of the present invention can be aqueous, paste behind the corpusculed, can be powdery, particulate state after the spraying drying.Yellow disperse dye composition of the present invention can be done golden yellow use separately, can do the use of low temperature three primary colors with 2BLN indigo plant and the red assembly system disperse grey N that mixes of 3B, and compatibleness blue with 2BLN and that 3B is red is fabulous, and 80 ℃ of-110 ℃ of temperature rise rates are in full accord.This dye composite coloured light is gorgeous, and the scope of application of pH value is extremely wide when dyeing, the dye yield height, and good level-dyeing property, lifting force is good, and every fastness is all good, and especially the advantage of light fastness, compatibleness aspect is more outstanding.
Embodiment
The invention will be further described below in conjunction with embodiment, but protection scope of the present invention is not limited to this.
Embodiment 1～22
According to data shown in the table 1, after dye monomer added water and piece together to mix by certain proportioning and condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF), naphthalene sulfonic acidformaldehyde condensation product (dispersing agent NNO), sodium lignosulfonate (xylogen 85A, 83A), grind dispersion with sand milling, carry out spraying drying then.
Wherein dye monomer (1-1) can be selected the C.I.DISPYELLOW 54# that Zhejiang Province Runtu intercalated Co., Ltd produces for use; The C.I.DISP YELLOW 64# that dye monomer (1-2) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; The C.I.DISP ORANGE 279# that dye monomer (2) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; The C.I.DISP YELLOW 104# that dye monomer (3) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; Dye monomer (4-1) is 2, after 4-dinitrochlorobenzene and the Ursol D reaction, again through diazotization, with the phenol coupling; Dye monomer (4-2) is 2, after 4-dinitrochlorobenzene and the Ursol D reaction, again through diazotization, with the coupling of 3-methylphenol; Dye monomer (4-3) is 2, after 4-dinitrochlorobenzene and the Ursol D reaction, again through diazotization, with the coupling of 3-ethylphenol; The C.I.DISPYELLOW 121# that dye monomer (5-1) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; The C.I.DISPYELLOW 121:1# that dye monomer (5-2) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; The C.I.DISPYELLOW 121:3# that dye monomer (5-3) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; The C.I.DISP ORANGE 25# that dye monomer (6-1) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; The C.I.DISP ORANGE 288# that dye monomer (6-2) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce.
Table 1:
| ??9 | ??(1-1) | ??88 | ??(2) | ??10 | ??(3) | ??2 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | ??83A | ??250 |
| ??10 | ??(1-1)??(1-2) | ??35??50 | ??(2) | ??10 | ??(3) | ??5 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | Dispersant MF | ??270 |
| ??11 | ??(1-1) | ??75 | ??(2) | ??15 | ??(3) | ??10 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | Dispersing agent NNO | ??290 |
| ??12 | ??(1-2) | ??76 | ??(2) | ??4 | ??(3) | ??20 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | ??85A | ??300 |
| ??13 | ??(1-1) | ??65 | ??(2) | ??5 | ??(3) | ??30 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | Dispersing agent NNO | ??320 |
| ??14 | ??(1-1) | ??60 | ??(2) | ??25 | ??(3) | ??13 | ??(4-1) | ??2 | ??---- | ??---- | ??---- | ??---- | ??83A | ??340 |
| ??15 | ??(1-1)??(1-2) | ??36??36 | ??(2) | ??8 | ??(3) | ??5 | ??(4-2) | ??15 | ??---- | ??---- | ??---- | ??---- | Dispersant MF | ??360 |
| ??16 | ??(1-1) | ??65 | ??(2) | ??5 | ??---- | ??---- | ??(4-3) | ??30 | ??---- | ??---- | ??---- | ??---- | Dispersing agent NNO | ??380 |
| ??17 | ??(1-2) | ??68 | ??(2) | ??15 | ??(3) | ??12 | ??(4-1)??(4-3) | ??2??1 | ??(5-1) | ??2 | ??---- | ??---- | ??85A | ??400 |
| ??18 | ??(1-1) | ??70 | ??(2) | ??15 | ??(3) | ??10 | ??---- | ??---- | ??(5-2)??(5-3) | ??2??3 | ??---- | ??---- | Dispersing agent NNO | ??430 |
| ??19 | ??(1-1) | ??50 | ??(2) | ??16 | ??(3) | ??15 | ??(4-2) | ??7 | ??(5-3) | ??12 | ??---- | ??---- | ??83A | ??470 |
| ??20 | ??(1-1)??(1-2) | ??20??35 | ??(2) | ??10 | ??(3) | ??20 | ??---- | ??---- | ??(5-3) | ??10 | ??(6-1) | ??5 | Dispersant MF | ??450 |
| ??21 | ??(1-1) | ??64 | ??(2) | ??5 | ??---- | ??---- | ??(4-2) | ??3 | ??(5-1) | ??8 | ??(6-1)??(6-2) | ??5??15 | Dispersing agent NNO | ??520 |
| ??22 | ??(1-2) | ??67 | ??(2) | ??3 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | ??(6-1) | ??30 | ??85A | ??540 |
| ??23 | ??(1-1) | ??88 | ??(2) | ??10 | ??---- | ??---- | ??---- | ??---- | ??(5-1) | ??2 | ??---- | ??---- | Dispersing agent NNO | ??530 |
| ??24 | ??(1-1) | ??85 | ??(2) | ??8 | ??---- | ??---- | ??---- | ??---- | ??---- | ??---- | ??6-2 | ??7 | ??85A | ??480 |
Disperse dye composition and DISPERSE YELLOW 23# that the foregoing description is made carry out performance test, and testing method is as follows:
Respectively get the dispersed dye that 0.5 gram embodiment 1～24 makes, water is mixed with the dispersed dye suspension that concentration is 0.5g/500ml respectively, getting 20ml mixes with the water of 80ml, regulate dye bath pH to 5 with acetic acid, be warmed up to 60 ℃ then, put into the 2g trevira simultaneously respectively and carry out high-temperature pressure dyeing, in 35 minutes, be warmed up to 130 ℃, be incubated 30 minutes, sampling when being cooled to 80 ℃.
Observe cloth specimen coloured light and adopt GB/T3921-1997, GB/T3920-1997, GB/T5718-1997 to measure its dyefastness.Measurement result sees Table 2.
Table 2
| The embodiment title | Compatibleness | Washing fastness | Crock fastness | Sublimation fastness (180 ℃) | Light fastness |
| Embodiment 1 | ??A | ??4-5 | ??5 | ??4 | ??7-8 |
| Embodiment 2 | ??A | ??4-5 | ??5 | ??4 | ??7-8 |
| Embodiment 3 | ??A | ??4 | ??5 | ??4 | ??7-8 |
| Embodiment 4 | ??A | ??4-5 | ??5 | ??4 | ??7-8 |
| Embodiment 5 | ??A | ??4 | ??5 | ??4 | ??7-8 |
| Embodiment 6 | ??A | ??4-5 | ??5 | ??4 | ??7-8 |
| Embodiment 7 | ??A | ??4-5 | ??4-5 | ??4 | ??8 |
| Embodiment 8 | ??A | ??4-5 | ??5 | ??4 | ??8 |
| Embodiment 9 | ??A | ??4-5 | ??5 | ??4 | ??8 |
| Embodiment 10 | ??A | ??4-5 | ??5 | ??4- | ??8 |
| Embodiment 11 | ??A | ??4 | ??5 | ??4- | ??8 |
| Embodiment 12 | ??A | ??4 | ??5 | ??4- | ??8 |
| Embodiment 13 | ??A | ??4 | ??5 | ??4- | ??8 |
| Embodiment 14 | ??A | ??4 | ??5 | ??4 | ??7-8 |
| Embodiment 15 | ??A | ??4 | ??5 | ??4 | ??7-8 |
| The embodiment title | Compatibleness | Washing fastness | Crock fastness | Sublimation fastness (180 ℃) | Light fastness |
| Embodiment 16 | ??A | ??4-5 | ??5 | ??4-5 | ??7 |
| Embodiment 17 | ??A | ??4-5 | ??5 | ??4 + | ??8 |
| Embodiment 18 | ??A | ??4 | ??4-5 | ??4-5 | ??8 |
| Embodiment 19 | ??A | ??4-5 | ??5 | ??4-5 | ??8 |
| Embodiment 20 | ??A | ??4-5 | ??5 | ??4-5 | ??8 |
| Embodiment 21 | ??A | ??4-5 | ??5 | ??4-5 | ??7-8 |
| Embodiment 22 | ??A | ??4-5 | ??5 | ??4-5 | ??8 - |
| Embodiment 23 | ??A | ??4-5 | ??5 | ??5- | ??7-8 |
| Embodiment 24 | ??A | ??4-5 | ??5 | ??5- | ??8 |
| DISPERSE YELLOW 23# | ??A | ??3-4 | ??4 | ??3 | ??8 |
Claims (9)
1. Yellow environment-friendly disperse dye composition, percentage composition meter by weight, mainly composed of the following components:
50～97% as the formula (1) one or more dye monomers A:
Y is H or halogen;
3～25% as the formula (2) dye monomer B:
0～30% as the formula (3) dye monomer C:
0～30% as the formula (4) one or more dye monomers D:
X
1Be H or C
1～C
4Alkyl;
0～12% as the formula (5) one or more dye monomers E:
X
2, X
3Be C independently separately
1～C
4Alkyl;
0～30% as the formula (6) one or more dye monomers F:
R
1Be C
1～C
4Alkyl or C
1～C
4Alkyl in a hydrogen replaced by phenyl ring.
2. Yellow environment-friendly disperse dye composition as claimed in claim 1 is characterized in that: described dye monomer A be following one or both suc as formula the dye monomer shown in (1-1)～(1-2):
3. Yellow environment-friendly disperse dye composition as claimed in claim 1 is characterized in that: described dye monomer D be following one or more suc as formula the dye monomer shown in (4-1)～(4-3):
4. Yellow environment-friendly disperse dye composition as claimed in claim 1 is characterized in that: described dye monomer E be following one or more suc as formula the dye monomer shown in (5-1)～(5-3):
5. Yellow environment-friendly disperse dye composition as claimed in claim 1 is characterized in that: described dye monomer F be following one or both suc as formula the dye monomer shown in (6-1)～(6-2):
6. Yellow environment-friendly disperse dye composition as claimed in claim 1, it is characterized in that: percentage composition meter by weight, mainly composed of the following components: 85～92% dye monomer B as the formula (2) suc as formula the dye monomer A shown in (1-1) and 8～15%
7. Yellow environment-friendly disperse dye composition as claimed in claim 1, it is characterized in that: percentage composition meter by weight, mainly composed of the following components: 82～90% the dye monomer C as the formula (3) of dye monomer B and 1～3% as the formula (2) suc as formula the dye monomer A shown in (1-1) and 8～15%
8. Yellow environment-friendly disperse dye composition as claimed in claim 1, it is characterized in that: percentage composition meter by weight, mainly composed of the following components: 85～90% dye monomer B as the formula (2) and 1～3% at least a dye monomer E as the formula (5) suc as formula the dye monomer A shown in (1-1) and 8～12%
9. Yellow environment-friendly disperse dye composition as claimed in claim 1, it is characterized in that: percentage composition meter by weight, mainly composed of the following components: 85～90% suc as formula the dye monomer B as the formula (2) and 4～10% of the dye monomer A shown in (1-1) and 4～10% suc as formula the dye monomer F shown in (6-1)
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|---|---|---|---|
| CN 201010117996 CN101787221B (en) | 2010-03-04 | 2010-03-04 | Yellow environment-friendly disperse dye composition |
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| CN101787221A true CN101787221A (en) | 2010-07-28 |
| CN101787221B CN101787221B (en) | 2013-08-14 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102206430A (en) * | 2011-04-06 | 2011-10-05 | 浙江闰土股份有限公司 | Environment-friendly type yellow disperse dyestuff composition |
| CN102732059A (en) * | 2012-07-03 | 2012-10-17 | 浙江闰土股份有限公司 | Composite dye composition, composite disperse dye and preparation method thereof |
| CN103073918A (en) * | 2013-01-21 | 2013-05-01 | 江苏亚邦染料股份有限公司 | Medium temperature type three-primary-color disperse dyes |
| CN103173038A (en) * | 2013-03-08 | 2013-06-26 | 浙江吉华集团股份有限公司 | Environmentally-friendly composite disperse yellow dye |
| CN103965652A (en) * | 2014-05-27 | 2014-08-06 | 董源 | Yellow-to-orange disperse dye composition |
| CN104231670A (en) * | 2014-08-20 | 2014-12-24 | 张家港互益染整有限公司 | Environment-friendly disperse dye |
| CN104497629A (en) * | 2014-12-31 | 2015-04-08 | 浙江闰土股份有限公司 | Yellow liquid disperse dye as well as preparation method and application thereof |
| CN108102426A (en) * | 2017-10-26 | 2018-06-01 | 安徽凯奇化工科技股份有限公司 | A kind of low temperature disperse yellow dye composition and preparation method thereof |
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| US4588517A (en) * | 1982-06-30 | 1986-05-13 | Hitachi, Ltd. | Liquid crystal composition |
| CN101143973A (en) * | 2007-10-26 | 2008-03-19 | 浙江闰土股份有限公司 | Low-temperature environmental protection disperse yellow dye composition |
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2010
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| US4588517A (en) * | 1982-06-30 | 1986-05-13 | Hitachi, Ltd. | Liquid crystal composition |
| CN101143973A (en) * | 2007-10-26 | 2008-03-19 | 浙江闰土股份有限公司 | Low-temperature environmental protection disperse yellow dye composition |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102206430A (en) * | 2011-04-06 | 2011-10-05 | 浙江闰土股份有限公司 | Environment-friendly type yellow disperse dyestuff composition |
| CN102206430B (en) * | 2011-04-06 | 2013-12-11 | 浙江闰土股份有限公司 | Environment-friendly type yellow disperse dyestuff composition |
| CN102732059B (en) * | 2012-07-03 | 2014-09-03 | 浙江闰土股份有限公司 | Composite dye composition, composite disperse dye and preparation method thereof |
| CN102732059A (en) * | 2012-07-03 | 2012-10-17 | 浙江闰土股份有限公司 | Composite dye composition, composite disperse dye and preparation method thereof |
| CN103073918A (en) * | 2013-01-21 | 2013-05-01 | 江苏亚邦染料股份有限公司 | Medium temperature type three-primary-color disperse dyes |
| CN103173038A (en) * | 2013-03-08 | 2013-06-26 | 浙江吉华集团股份有限公司 | Environmentally-friendly composite disperse yellow dye |
| CN103173038B (en) * | 2013-03-08 | 2014-10-08 | 浙江吉华集团股份有限公司 | Environmentally-friendly composite disperse yellow dye |
| CN103965652A (en) * | 2014-05-27 | 2014-08-06 | 董源 | Yellow-to-orange disperse dye composition |
| CN103965652B (en) * | 2014-05-27 | 2016-05-18 | 董源 | A kind of Yellow-to-orange disperse dye composition |
| CN104231670A (en) * | 2014-08-20 | 2014-12-24 | 张家港互益染整有限公司 | Environment-friendly disperse dye |
| CN104231670B (en) * | 2014-08-20 | 2016-05-11 | 张家港互益染整有限公司 | A kind of environment-friendly disperse dye |
| CN104497629A (en) * | 2014-12-31 | 2015-04-08 | 浙江闰土股份有限公司 | Yellow liquid disperse dye as well as preparation method and application thereof |
| CN108102426A (en) * | 2017-10-26 | 2018-06-01 | 安徽凯奇化工科技股份有限公司 | A kind of low temperature disperse yellow dye composition and preparation method thereof |
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