CN101748307B - 金砷合金材料及其制备方法 - Google Patents
金砷合金材料及其制备方法 Download PDFInfo
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- CN101748307B CN101748307B CN2008102398431A CN200810239843A CN101748307B CN 101748307 B CN101748307 B CN 101748307B CN 2008102398431 A CN2008102398431 A CN 2008102398431A CN 200810239843 A CN200810239843 A CN 200810239843A CN 101748307 B CN101748307 B CN 101748307B
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- gold
- alloy
- arsenic
- stove
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- 239000000956 alloy Substances 0.000 title claims abstract description 92
- VJRVSSUCOHZSHP-UHFFFAOYSA-N [As].[Au] Chemical compound [As].[Au] VJRVSSUCOHZSHP-UHFFFAOYSA-N 0.000 title claims abstract description 53
- 229910000967 As alloy Inorganic materials 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title claims abstract description 41
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 64
- 229910052785 arsenic Inorganic materials 0.000 claims abstract description 32
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000010931 gold Substances 0.000 claims abstract description 29
- 229910052737 gold Inorganic materials 0.000 claims abstract description 26
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 20
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000010453 quartz Substances 0.000 claims abstract description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000007789 gas Substances 0.000 claims abstract description 12
- 238000007670 refining Methods 0.000 claims abstract description 11
- 229910052786 argon Inorganic materials 0.000 claims abstract description 10
- 238000007789 sealing Methods 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims description 41
- 239000000463 material Substances 0.000 claims description 34
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 21
- 229910052710 silicon Inorganic materials 0.000 claims description 21
- 239000010703 silicon Substances 0.000 claims description 21
- 238000000151 deposition Methods 0.000 claims description 18
- 230000008021 deposition Effects 0.000 claims description 18
- 239000013077 target material Substances 0.000 claims description 18
- 238000005477 sputtering target Methods 0.000 claims description 16
- 238000005266 casting Methods 0.000 claims description 11
- 238000004140 cleaning Methods 0.000 claims description 11
- 238000001465 metallisation Methods 0.000 claims description 11
- 230000002378 acidificating effect Effects 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000011888 foil Substances 0.000 claims description 6
- 230000006698 induction Effects 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000001802 infusion Methods 0.000 claims description 4
- 238000003754 machining Methods 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 238000004381 surface treatment Methods 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000003801 milling Methods 0.000 claims description 3
- 230000003068 static effect Effects 0.000 claims description 3
- 239000001117 sulphuric acid Substances 0.000 claims description 3
- 235000011149 sulphuric acid Nutrition 0.000 claims description 3
- 238000013022 venting Methods 0.000 claims description 3
- 230000004927 fusion Effects 0.000 claims description 2
- 150000002343 gold Chemical class 0.000 claims 1
- 238000012423 maintenance Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 7
- 229910001018 Cast iron Inorganic materials 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 238000005303 weighing Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 9
- 239000000470 constituent Substances 0.000 description 8
- 238000005275 alloying Methods 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 238000005070 sampling Methods 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 241000209456 Plumbago Species 0.000 description 4
- 239000012491 analyte Substances 0.000 description 4
- 239000010439 graphite Substances 0.000 description 4
- 238000012856 packing Methods 0.000 description 4
- 238000004821 distillation Methods 0.000 description 3
- 238000009616 inductively coupled plasma Methods 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 238000003723 Smelting Methods 0.000 description 2
- 238000000137 annealing Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 238000012946 outsourcing Methods 0.000 description 1
- 229910000923 precious metal alloy Inorganic materials 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
Landscapes
- Manufacture And Refinement Of Metals (AREA)
Abstract
Description
取样点 | 1 | 2 | 3 | 4 | 平均含量 | 成分偏差 |
As(%w) | 1.94 | 1.98 | 2.11 | 1.88 | 1.98 | ±0.13 |
取样点 | 1 | 2 | 3 | 4 | 平均含量 | 成分偏差 |
As(%w) | 19.38 | 20.22 | 20.56 | 19.55 | 19.93 | ±0.63 |
取样点 | 1 | 2 | 3 | 4 | 平均含量 | 成分偏差 |
As(%w) | 1.12 | 0.96 | 0.87 | 0.99 | 0.99 | ±0.13 |
取样点 | 1 | 2 | 3 | 4 | 平均含量 | 成分偏差 |
As(%w) | 4.85 | 4.96 | 5.02 | 4.90 | 4.93 | ±0.15 |
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2008102398431A CN101748307B (zh) | 2008-12-19 | 2008-12-19 | 金砷合金材料及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2008102398431A CN101748307B (zh) | 2008-12-19 | 2008-12-19 | 金砷合金材料及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN101748307A CN101748307A (zh) | 2010-06-23 |
CN101748307B true CN101748307B (zh) | 2012-07-25 |
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CN2008102398431A Active CN101748307B (zh) | 2008-12-19 | 2008-12-19 | 金砷合金材料及其制备方法 |
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CN (1) | CN101748307B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103323446A (zh) * | 2012-03-23 | 2013-09-25 | 北京有色金属与稀土应用研究所 | 一种金砷合金靶材中砷量的测定方法 |
CN103394674B (zh) * | 2013-07-24 | 2016-01-13 | 西安工程大学 | 薄壁铸件铸造用真空感应炉及铸造薄壁钛合金铸件的方法 |
CN106956107A (zh) * | 2017-05-08 | 2017-07-18 | 宁波金凤焊割机械制造有限公司 | 金属件的机械加工方法 |
CN109022854B (zh) * | 2018-07-25 | 2020-06-26 | 中国兵器科学研究院宁波分院 | 一种非晶软磁材料的母合金熔炼方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3412278A (en) * | 1965-12-01 | 1968-11-19 | Perkin Elmer Corp | Hollow cathodes having a matrix material with particles interspersed |
US3434828A (en) * | 1963-02-01 | 1969-03-25 | Texas Instruments Inc | Gold alloy for attaching a lead to a semiconductor body |
CN1360338A (zh) * | 1993-06-12 | 2002-07-24 | 株式会社半导体能源研究所 | 半导体器件 |
US20030049894A1 (en) * | 1999-05-07 | 2003-03-13 | University Of Delaware | Si-based resonant interband tunneling diodes and method of making interband tunneling diodes |
-
2008
- 2008-12-19 CN CN2008102398431A patent/CN101748307B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3434828A (en) * | 1963-02-01 | 1969-03-25 | Texas Instruments Inc | Gold alloy for attaching a lead to a semiconductor body |
US3412278A (en) * | 1965-12-01 | 1968-11-19 | Perkin Elmer Corp | Hollow cathodes having a matrix material with particles interspersed |
CN1360338A (zh) * | 1993-06-12 | 2002-07-24 | 株式会社半导体能源研究所 | 半导体器件 |
US20030049894A1 (en) * | 1999-05-07 | 2003-03-13 | University Of Delaware | Si-based resonant interband tunneling diodes and method of making interband tunneling diodes |
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CN101748307A (zh) | 2010-06-23 |
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Denomination of invention: Gold-arsenic alloy material and preparation method thereof Effective date of registration: 20131209 Granted publication date: 20120725 Pledgee: Huaxia Bank, Limited by Share Ltd, Beijing branch Pledgor: Beijing Non-ferrous Metal and Rare-earth Application Inst. Registration number: 2013990000947 |
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Date of cancellation: 20150615 Granted publication date: 20120725 Pledgee: Huaxia Bank, Limited by Share Ltd, Beijing branch Pledgor: Beijing Non-ferrous Metal and Rare-earth Application Inst. Registration number: 2013990000947 |
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Denomination of invention: Gold-arsenic alloy material and preparation method thereof Effective date of registration: 20160922 Granted publication date: 20120725 Pledgee: Beijing rural commercial bank, Limited by Share Ltd, Sijiqing branch Pledgor: Beijing Non-ferrous Metal and Rare-earth Application Inst. Registration number: 2016990000811 |
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Date of cancellation: 20170925 Granted publication date: 20120725 Pledgee: Beijing rural commercial bank, Limited by Share Ltd, Sijiqing branch Pledgor: Beijing Non-ferrous Metal and Rare-earth Application Inst. Registration number: 2016990000811 |
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