CN101664165A - Process for extracting non-pectin soluble pomace dietary fibers - Google Patents
Process for extracting non-pectin soluble pomace dietary fibers Download PDFInfo
- Publication number
- CN101664165A CN101664165A CN200810139768A CN200810139768A CN101664165A CN 101664165 A CN101664165 A CN 101664165A CN 200810139768 A CN200810139768 A CN 200810139768A CN 200810139768 A CN200810139768 A CN 200810139768A CN 101664165 A CN101664165 A CN 101664165A
- Authority
- CN
- China
- Prior art keywords
- pomace
- dietary fibers
- concentrate
- pectin
- soluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention discloses a process for extracting non-pectin soluble pomace dietary fibers, which adopts an alkaline extraction-ultra-fine pulverization method to modify dietary fibers so as to convertpart of IDF into SDF, and then performs processes of concentration, sediment cleaning, drying, grinding and the like on an extracted solution so as to prepare the soluble dietary fibers of pomace. The extraction process sufficiently utilizes the pomace after extracting pectin, and reduces environmental pollution simultaneously.
Description
Technical field:
The present invention relates to apple deep process technology field, is a kind of extraction process of non-pectin soluble pomace dietary fibers specifically.
Technical background:
Dietary fiber has different physiological roles, it can angiocardiopathy preventing, prevention gall stone, prevention diabetes, prevention constipation and obesity, prevention skin disease, and can reduce the carcinoma of the rectum and colon cancer odds etc., be called as " the 7th nutrient " after starch, protein, fat, vitamin, mineral matter and water.
According to deliquescent difference, dietary fiber is divided into soluble dietary fiber (SDF) and insoluble diedairy fiber (IDF) two big classes.Wherein IDF can comprise pectin and other non-pectin dietary fiber.SDF is different with health-care effect with the physiological function that IDF is had in human body in the dietary fiber, and this physicochemical property with them is close relevant.The dietary fiber composition requirement SDF of balance accounts for more than 10% of TDF quantity, otherwise can only be known as inserts type dietary fiber.And it is minimum to have extracted in the pomace of pectin the SDF ratio, can't reach the requirement of diet balance, and this just need carry out modification and extraction to these natural dietary fiber sources, and the content that improves SDF is to bring into play its physiological function better.At present, the oven dry that generally just simply neutralizes is handled to the pomace that has extracted pectin, thereby causes wastage of material.
Summary of the invention:
The objective of the invention is to overcome the deficiency of above-mentioned prior art, and provide a kind of extraction process of non-pectin soluble pomace dietary fibers, the pomace that mainly solves the intact pectin of existing extraction just simply neutralizes to dry and handles, and causes problems such as wastage of material.
In order to achieve the above object, the present invention is achieved in that a kind of extraction process of non-pectin soluble pomace dietary fibers, and its special character is that it comprises following processing step:
A, raw material: the useless pomace that has extracted pectin;
B, alkaline process extract: add 9% NaOH solution of 10 times of weight of pomace, temperature remains on 80 ℃, extracts 2.5h;
C, ultramicro grinding: the alkali extract is carried out ultramicro grinding by colloid mill, and colloid mill stator and rotor clearance are set at 20 μ m;
D, centrifugation: the extract through ultramicro grinding carries out centrifugation through centrifugal separator, collects supernatant;
E, concentrate: the supernatant of gained is carried out vacuum concentrate, 82.5 ℃ of thickening temperatures concentrate pressure 0.75 atmospheric pressure, 3.4 times of cycles of concentration;
F, precipitation, cleaning: be that 75% ethanol precipitates above-mentioned concentrate with concentration, and clean 2～3 times;
G, drying: adopt the fluidized bed drying mode that above-mentioned precipitation is cleaned thing and carry out drying, baking temperature is 70 ± 5 ℃, and the time is 135～150min;
H, grinding: dried matter is ground to below the 250 μ m, gets soluble pomace dietary fibers.
Compared with the prior art the extraction process of a kind of non-pectin soluble pomace dietary fibers of the present invention has outstanding substantive distinguishing features and marked improvement, 1, adopting alkali to carry---superfine grinding method carries out modification to dietary fiber, make part IDF change SDF into, in having improved pomace in the SDF extracted amount, also improve the physicochemical characteristic of apple IDF, thereby improved its biologically active and physiological regulation function; 2, raw material is utilized more fully, thereby reduce wastage of material.
The specific embodiment:
In order to understand better and to implement, describe the present invention in detail below in conjunction with embodiment:
Embodiment 1,9% the NaOH solution that the useless pomace that has extracted pectin is added 10 times of weight of pomace, temperature remains on 80 ℃, extract 2.5h, the alkali extract is carried out ultramicro grinding by colloid mill, colloid mill stator and rotor clearance are set at 20 μ m, carry out centrifugation through the extract of ultramicro grinding through centrifugal separator, collect supernatant, the supernatant of gained is carried out vacuum concentrate, 82.5 ℃ of thickening temperatures, concentrate pressure 0.75 atmospheric pressure, 3.4 times of cycles of concentration are that 75% ethanol precipitates concentrate with concentration then, and clean 2 times, adopt the fluidized bed drying mode that sediment is carried out drying, baking temperature is 70 ℃, and the time is 142.5min, dried matter is ground to below the 250 μ m, gets soluble pomace dietary fibers.
Embodiment 2,9% the NaOH solution that the useless pomace that has extracted pectin is added 10 times of weight of pomace, temperature remains on 80 ℃, extract 2.5h, the alkali extract is carried out ultramicro grinding by colloid mill, colloid mill stator and rotor clearance are set at 20 μ m, carry out centrifugation through the extract of ultramicro grinding through centrifugal separator, collect supernatant, the supernatant of gained is carried out vacuum concentrate, 82.5 ℃ of thickening temperatures, concentrate pressure 0.75 atmospheric pressure, 3.4 times of cycles of concentration are that 75% ethanol precipitates concentrate with concentration then, and clean 3 times, adopt the fluidized bed drying mode that sediment is carried out drying, baking temperature is 65 ℃, and the time is 150min, dried matter is ground to below the 250 μ m, gets soluble pomace dietary fibers.
Embodiment 3,9% the NaOH solution that the useless pomace that has extracted pectin is added 10 times of weight of pomace, temperature remains on 80 ℃, extract 2.5h, the alkali extract is carried out ultramicro grinding by colloid mill, colloid mill stator and rotor clearance are set at 20 μ m, carry out centrifugation through the extract of ultramicro grinding through centrifugal separator, collect supernatant, the supernatant of gained is carried out vacuum concentrate, 82.5 ℃ of thickening temperatures, concentrate pressure 0.75 atmospheric pressure, 3.4 times of cycles of concentration are that 75% ethanol precipitates concentrate with concentration then, and clean 2 times, adopt the fluidized bed drying mode that sediment is carried out drying, baking temperature is 75 ℃, and the time is 135min, dried matter is ground to below the 250 μ m, gets soluble pomace dietary fibers.
Claims (1)
1, a kind of extraction process of non-pectin soluble pomace dietary fibers is characterized in that it comprises following processing step:
A, raw material: the useless pomace that has extracted pectin;
B, alkaline process extract: add 9% NaOH solution of 10 times of weight of pomace, temperature remains on 80 ℃, extracts 2.5h;
C, ultramicro grinding: the alkali extract is carried out ultramicro grinding by colloid mill, and colloid mill stator and rotor clearance are set at 20 μ m;
D, centrifugation: the extract through ultramicro grinding carries out centrifugation through centrifugal separator, collects supernatant;
E, concentrate: the supernatant of gained is carried out vacuum concentrate, 82.5 ℃ of thickening temperatures concentrate pressure 0.75 atmospheric pressure, 3.4 times of cycles of concentration;
F, precipitation, cleaning: be that 75% ethanol precipitates above-mentioned concentrate with concentration, and clean 2～3 times;
G, drying: adopt the fluidized bed drying mode that above-mentioned precipitation is cleaned thing and carry out drying, baking temperature is 70 ± 5 ℃, and the time is 135～150min;
H, grinding: dried matter is ground to below the 250 μ m, gets soluble pomace dietary fibers.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101397681A CN101664165B (en) | 2008-09-05 | 2008-09-05 | Process for extracting non-pectin soluble pomace dietary fibers |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101397681A CN101664165B (en) | 2008-09-05 | 2008-09-05 | Process for extracting non-pectin soluble pomace dietary fibers |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101664165A true CN101664165A (en) | 2010-03-10 |
| CN101664165B CN101664165B (en) | 2012-06-20 |
Family
ID=41801070
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008101397681A Active CN101664165B (en) | 2008-09-05 | 2008-09-05 | Process for extracting non-pectin soluble pomace dietary fibers |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101664165B (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415579A (en) * | 2011-10-15 | 2012-04-18 | 成都大学 | Stuffed sausage containing soluble dietary fibers and manufacturing method thereof |
| CN103989103A (en) * | 2014-05-29 | 2014-08-20 | 湖北省农业科学院农产品加工与核农技术研究所 | Preparation method of mulberry pomace water-soluble dietary fiber and application thereof |
| CN104172200A (en) * | 2014-07-23 | 2014-12-03 | 中国农业科学院农产品加工研究所 | Method for increasing content of soluble dietary fibers in apple pomace |
| CN105361187A (en) * | 2015-09-28 | 2016-03-02 | 华中农业大学 | Modified cereal dietary fiber and preparation method thereof |
| CN109793243A (en) * | 2017-11-16 | 2019-05-24 | 镇江市丹徒区南山溪园茶叶专业合作社 | A kind of processing method that microwave assisting method extracts apple skin soluble dietary fiber |
| CN110521749A (en) * | 2019-07-25 | 2019-12-03 | 深圳市麦轩食品有限公司 | A kind of low sugar content and high fiber content moon cake and preparation method thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100361952B1 (en) * | 1999-12-06 | 2002-11-23 | 주식회사 한국야쿠르트 | A method for preparing low rancidify noodle using apple pomace dietary fiber |
| CN1206940C (en) * | 2002-09-17 | 2005-06-22 | 中国科学院过程工程研究所 | Celluse fruit and vegetable dregs food containing enriched bifidus factor and preparation process thereof |
| JP2004154035A (en) * | 2002-11-06 | 2004-06-03 | Combi Corp | Method for producing lactobacillus fermented food product, lactobacillus fermented food product and defecation improver both obtained by the method |
| CN1899091A (en) * | 2006-07-08 | 2007-01-24 | 南昌大学 | Method for producing fruit diet fiber of high soluble diet fiber content |
-
2008
- 2008-09-05 CN CN2008101397681A patent/CN101664165B/en active Active
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415579A (en) * | 2011-10-15 | 2012-04-18 | 成都大学 | Stuffed sausage containing soluble dietary fibers and manufacturing method thereof |
| CN103989103A (en) * | 2014-05-29 | 2014-08-20 | 湖北省农业科学院农产品加工与核农技术研究所 | Preparation method of mulberry pomace water-soluble dietary fiber and application thereof |
| CN103989103B (en) * | 2014-05-29 | 2015-12-09 | 湖北省农业科学院农产品加工与核农技术研究所 | A kind of preparation method of mulberry fruit dregs water-soluble dietary fiber and application thereof |
| CN104172200A (en) * | 2014-07-23 | 2014-12-03 | 中国农业科学院农产品加工研究所 | Method for increasing content of soluble dietary fibers in apple pomace |
| CN105361187A (en) * | 2015-09-28 | 2016-03-02 | 华中农业大学 | Modified cereal dietary fiber and preparation method thereof |
| CN105361187B (en) * | 2015-09-28 | 2018-07-06 | 华中农业大学 | A kind of modified grain dietary fiber and preparation method thereof |
| CN109793243A (en) * | 2017-11-16 | 2019-05-24 | 镇江市丹徒区南山溪园茶叶专业合作社 | A kind of processing method that microwave assisting method extracts apple skin soluble dietary fiber |
| CN110521749A (en) * | 2019-07-25 | 2019-12-03 | 深圳市麦轩食品有限公司 | A kind of low sugar content and high fiber content moon cake and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101664165B (en) | 2012-06-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101664165B (en) | Process for extracting non-pectin soluble pomace dietary fibers | |
| CN101617787B (en) | Process for continuously extracting a plurality of products from highland barley | |
| CN102199223A (en) | Extraction method of lentinan, eritadenine and mushroom dietary fiber | |
| CN103263514B (en) | Method for extracting flavones, low-molecule pectin and cellulose from orange peels in combined way | |
| CN103113483A (en) | Method for extracting various active ingredients from dendrobium officinale | |
| CN104757564B (en) | A kind of method utilizing Pericarppium arachidis hypogaeae to prepare dietary fiber | |
| CN104130333A (en) | Method for synchronous production of anthocyanidin, starch, cellulose and protein by using purple sweet potato | |
| CN101715910B (en) | Composition of banana oligosaccharide and dietary fibre, preparation method and application thereof | |
| CN106167530A (en) | A kind of combined-enzyme method extracts the method for ganoderan | |
| CN102757515A (en) | Method for extracting high-purity flavonoid and pectin from citrus peel | |
| CN101548989A (en) | Mactra veneriformis extract, preparation method and application thereof | |
| CN105504081A (en) | Method for increasing leaching rate of polysaccharide components in dendrobium candidum | |
| CN105249482A (en) | Method for extracting dietary fibers from rose dregs | |
| CN106108031A (en) | Garlic skin dietary fiber and high temperature steaming thereof and enzymolysis modified technology of preparing and application | |
| CN103059151A (en) | Process for extracting water-soluble polysaccharide of Chinese yam | |
| CN101695364A (en) | Method for preparing dietary fiber by apricot residue | |
| CN104543125A (en) | Cyclocarya paliurus pu-erh tea and preparation method thereof | |
| CN106723089A (en) | The method of insoluble diedairy fiber in high efficiency extraction sweet potato waste | |
| CN102308888B (en) | Preparation methods of welsh onion oil and dietary fibers of welsh onion | |
| CN101709095B (en) | Banana ligoglucoside and preparation method and application thereof | |
| CN107501425A (en) | Fragrant solomonseal rhizome polyoses are carried out using radix polygonati officinalis leftover bits and pieces and wash the preparation method of the clear sugar element of pancreas | |
| CN105031289A (en) | Dendrobium officinale and lucid ganoderma capsules and preparation method thereof | |
| CN105433394A (en) | Preparation method of pineapple residue soluble dietary fiber | |
| CN102146143A (en) | Method for preparing pectin and cellulose from extracting residues of ginseng and American ginseng and application thereof | |
| CN107043649A (en) | The method that nearly solid enzymatic hydrolysis joint physical squeezing produces camellia seed oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: YANTAI ANDRE PECTIC CO., LTD. Free format text: FORMER OWNER: ANDELI PECTIN CO., LTD., YANTAI Effective date: 20110603 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20110603 Address after: 264100 No. 889 Xincheng street, Muping District, Shandong, Yantai Applicant after: Yantai Andre Pectin Co., Ltd. Address before: 264100 No. 889 Xincheng street, Muping District, Shandong, Yantai Applicant before: Andeli Pectin Co., Ltd., Yantai |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 889 Xincheng street, Muping District, Yantai City, Shandong Province Patentee after: Yantai DSM Andry pectin Co.,Ltd. Address before: 264100 No. 889 Xincheng street, Muping District, Shandong, Yantai Patentee before: YANTAI ANDRE PECTIN Co.,Ltd. |