CN101608334A - A kind of titanium alloy anodic oxidation and coloring device - Google Patents
A kind of titanium alloy anodic oxidation and coloring device Download PDFInfo
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- CN101608334A CN101608334A CNA2009101122310A CN200910112231A CN101608334A CN 101608334 A CN101608334 A CN 101608334A CN A2009101122310 A CNA2009101122310 A CN A2009101122310A CN 200910112231 A CN200910112231 A CN 200910112231A CN 101608334 A CN101608334 A CN 101608334A
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Abstract
A kind of titanium alloy anodic oxidation and coloring device relates to a kind of coloring apparatus, especially relates to a kind of titanium alloy anodic oxidation and coloring device.Provide that a kind of light weight body is little, compact construction, function titanium alloy anodic oxidation and coloring device comparatively complete and simple to operate.Be provided with alkaline bath, the hot water washing trough, 5 cold water washing troughs, pickling tank, anodizing tank, the boiling water enclosed slot, 3 electric heaters, 3 temperature sensors, temperature controller, timing controller and direct supply, alkaline bath, the hot water washing trough, the cold water washing trough, pickling tank, 2 cold water washing troughs, anodizing tank, 2 cold water washing troughs and boiling water enclosed slot are placed on the support by linear sequence, lay operating panel on the support, the right and left at pilot wire is provided with temperature controller respectively, direct supply and timing controller, 3 electric heaters are located at alkaline bath respectively, in hot water washing trough and the boiling water enclosed slot.
Description
Technical field
The present invention relates to a kind of coloring apparatus, especially relate to a kind of titanium alloy anodic oxidation and coloring device.
Background technology
Because titanium has that density is little, intensity is high, stable chemical performance and advantage such as corrosion-resistant, therefore since the eighties in 20th century, the titanium material begins to be applied to removable partial denture to be made, and is gradually improved in clinical application.Titanium or titanium alloy is used to medical field because of having good biocompatibility again, and its good biocompatibility is the dense oxidation film that comes from the surface.In a single day titanium is exposed to the oxide film protection layer that just can form one deck densification in the air rapidly, and its thickness is 2～60nm.Oxide film has two big functions: 1) stop titanium matrix metal to body fluid environment release metal ions; 2) structure of zone of oxidation and hydration characteristics make it to be exposed to body fluid generation aquation, promote specific protein in surface adsorption, integrate thereby form bone.Yet the oxide film that forms naturally in air can not meet the demands because rete is unstable and thickness is too thin.In order to improve the performance of rete, carry out surface modification to titanium alloy.The method of surface modification is a lot, and anodic oxidation is the most frequently used a kind of method.
(Zhao Qing .H3PO4+C such as Zhao Qing
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7Titanium alloy anode oxidation coloring process research in the system. Aviation Engineering Institutes Of Nanchang's journal, 2000,14 (1)) reported H3PO4+C
6H
11NaO
7Titanium alloy anode oxidation coloring process research in the system.
Summary of the invention
Purpose of the present invention aims to provide that a kind of light weight body is little, compact construction, function titanium alloy anodic oxidation and coloring device comparatively complete and simple to operate.
The present invention is provided with alkaline bath, the hot water washing trough, 5 cold water washing troughs, pickling tank, anodizing tank, the boiling water enclosed slot, 3 electric heaters, 3 temperature sensors, temperature controller, timing controller and direct supply, alkaline bath, the hot water washing trough, the cold water washing trough, pickling tank, 2 cold water washing troughs, anodizing tank, 2 cold water washing troughs and boiling water enclosed slot are placed on the support by linear sequence, lay operating panel on the support, the right and left at pilot wire is provided with temperature controller respectively, direct supply and timing controller, 3 electric heaters are located at alkaline bath respectively, in hot water washing trough and the boiling water enclosed slot.
Described alkaline bath is provided with the alkaline bath cell body, is provided with water inlet pipe, exhaust duct and air stirring pipe on the alkaline bath cell body, is provided with alkali cleaning thing rod bracing frame at alkaline bath cell body top, is provided with blow-off pipe in alkaline bath cell body bottom.
Preferably be provided with mounting block that is used for fixing water inlet pipe and the mounting block that is used for fixing air stirring pipe in the alkaline bath cell body outside.Wherein the material of alkaline bath cell body, blow-off pipe, water pipe anchor and alkali cleaning thing rod bracing frame is PP, and the material of air stirring pipe, exhaust duct and water inlet pipe is PVC.
Described hot water washing trough is provided with hot water washing trough cell body, is provided with water inlet pipe, rising pipe and exhaust duct on hot water washing trough cell body top, is provided with blow-off pipe in hot water washing trough cell body bottom.
Preferably be provided with mounting block that is used for fixing water inlet pipe and the mounting block that is used for fixing rising pipe in the hot water washing trough cell body outside.Wherein the material of hot water washing trough cell body and water pipe anchor is PP, and the material of rising pipe, exhaust duct and water inlet pipe is PVC.
Described cold water washing trough is provided with the washing bath cell body, is provided with water inlet pipe and rising pipe on washing bath cell body top, is provided with blow-off pipe in the bottom of washing bath cell body.
Preferably be provided with mounting block that is used for fixing water inlet pipe and the mounting block that is used for fixing rising pipe in the washing bath cell body outside.Wherein the material of washing bath cell body and water pipe anchor is PP, and the material of rising pipe and water inlet pipe is PVC.
Described pickling tank is provided with the pickling tank cell body, is provided with water inlet pipe on pickling tank cell body top, is provided with exhaust duct at pickling tank cell body top, is provided with blow-off pipe in pickling tank cell body bottom.
Preferably be provided with the mounting block that is used for fixing water inlet pipe in the pickling tank cell body outside.Wherein the material of pickling tank cell body, blow-off pipe and water pipe anchor is PP, and the material of water inlet pipe is PVC.
Described anodizing tank is provided with the anodizing tank cell body, and anodizing tank cell body top is provided with water inlet pipe and air stirring pipe, is provided with exhaust duct and electrode holder at anodizing tank cell body top, at anodizing tank cell body bottom blow-down pipe.
Preferably be provided with mounting block that is used for fixing water inlet pipe and the mounting block that is used for fixing air stirring pipe in the anodizing tank cell body outside.Wherein the material of anodizing tank cell body, water pipe anchor and electrode holder is PP, and the material of air stirring pipe, exhaust duct and water inlet pipe is PVC.
Described boiling water enclosed slot is provided with boiling water enclosed slot inside groove and boiling water enclosed slot water jacket, is provided with water shoot in boiling water enclosed slot water jacket bottom, and water shoot is connected with boiling water enclosed slot inside groove.Wherein the material of boiling water enclosed slot inside groove is PP, and the material of boiling water enclosed slot water jacket and water shoot is SUS304.Between boiling water enclosed slot inside groove and boiling water enclosed slot water jacket, preferably fill the insulation asbestos.
The present invention is owing to adopt each cell body successively by the frame mode of linear arrangement, therefore little, the compact construction of light weight body not only, and also technological operation is simple.Owing to establish alkaline bath, hot water washing trough, 5 cold water washing troughs, pickling tank, anodizing tank, boiling water enclosed slot, 3 electric heaters, 3 temperature sensors, temperature controller, timing controller and direct supplys, so function is comparatively complete.
Description of drawings
Fig. 1 is that the structure of the embodiment of the invention is formed synoptic diagram.
Fig. 2 is the plan structure synoptic diagram of Fig. 1.
Fig. 3 is that the alkaline bath structure of the embodiment of the invention is formed synoptic diagram.
Fig. 4 becomes synoptic diagram for the hot water washing trough structural group of the embodiment of the invention.
Fig. 5 becomes synoptic diagram for the cold water washing trough structural group of the embodiment of the invention.
Fig. 6 is that the pickling tank structure of the embodiment of the invention is formed synoptic diagram.
Fig. 7 is that the anodizing tank structure of the embodiment of the invention is formed synoptic diagram.
Fig. 8 is that the boiling water enclosed slot structure of the embodiment of the invention is formed synoptic diagram.
Embodiment
Following examples will the present invention is further illustrated in conjunction with the accompanying drawings.
Referring to Fig. 1 and 2, the present invention is provided with alkaline bath 1, hot water washing trough 2,5 cold water washing troughs 31～35, pickling tank 4, anodizing tank 5, anodic oxidation mesa supports frame 6, boiling water enclosed slot 7,3 electric heaters, 3 temperature sensors, temperature controller, timing controller and direct supply, alkaline bath 1, hot water washing trough 2, cold water washing trough 31, pickling tank 4,2 cold water washing troughs 32 and 33, anodizing tank 5,2 cold water washing troughs 34 and 35, boiling water enclosed slot 7 is placed on the support 8 by linear sequence, lay operating panel 9 on the support 8, the right and left at pilot wire is provided with temperature controller respectively, direct supply and timing controller, 3 electric heaters are located at alkaline bath 1 respectively, in hot water washing trough 2 and the boiling water enclosed slot 7.
Referring to Fig. 3, described alkaline bath 1 is provided with alkaline bath cell body 11, on alkaline bath cell body 11, be provided with water inlet pipe 12, exhaust duct 13 and air stirring pipe 14, be provided with alkali cleaning thing rod bracing frame 15 at alkaline bath cell body 11 tops, be provided with blow-off pipe 16 in alkaline bath cell body 11 bottoms.Be provided with anchor 17 that is used for fixing water inlet pipe 12 and the anchor 18 that is used for fixing air stirring pipe 14 in alkaline bath cell body 11 outsides.Wherein the material of alkaline bath cell body 11, blow-off pipe 16, water pipe anchor 17 and 18, alkali cleaning thing rod bracing frame 15 is PP, and the material of air stirring pipe 14, exhaust duct 13 and water inlet pipe 12 is PVC.
Referring to Fig. 4, described hot water washing trough 2 is provided with hot water washing trough cell body 21, is provided with water inlet pipe 22, rising pipe 23 and exhaust duct 24 on hot water washing trough cell body 21 tops, is provided with blow-off pipe 25 in hot water washing trough cell body 21 bottoms.Be provided with anchor 26 that is used for fixing water inlet pipe 22 and the anchor 27 that is used for fixing rising pipe 23 in hot water washing trough cell body 21 outsides.Wherein the material of hot water washing trough cell body 21 and water pipe anchor 26 and 27 is PP, and the material of rising pipe 23, exhaust duct 24 and water inlet pipe 22 is PVC.
Referring to Fig. 5, described cold water washing trough 31～35 is provided with washing bath cell body 311, is provided with water inlet pipe 312 and rising pipe 313 on washing bath cell body 311 tops, is provided with blow-off pipe 314 in the bottom of washing bath cell body 311.Be provided with anchor 315 that is used for fixing water inlet pipe 312 and the anchor 316 that is used for fixing rising pipe 313 in washing bath cell body 311 outsides.Wherein the material of washing bath cell body 311 and water pipe anchor 315 and 316 is PP, and the material of rising pipe 313 and water inlet pipe 312 is PVC.
Referring to Fig. 6, described pickling tank 4 is provided with pickling tank cell body 41, is provided with water inlet pipe 42 on pickling tank cell body 41 tops, is provided with exhaust duct 43 at pickling tank cell body 41 tops, is provided with blow-off pipe 44 in pickling tank cell body 41 bottoms.Be provided with the anchor 45 that is used for fixing water inlet pipe 42 in pickling tank cell body 41 outsides.Wherein the material of pickling tank cell body 41, blow-off pipe 44 and water pipe anchor 45 is PP, and the material of water inlet pipe 42 is PVC.
Referring to Fig. 7, described anodizing tank 5 is provided with anodizing tank cell body 51, anodizing tank cell body 51 tops are provided with water inlet pipe 52 and air stirring pipe 53, are provided with exhaust duct 54 and electrode holder 55 at anodizing tank cell body 51 tops, at anodizing tank cell body 51 bottom blow-down pipes 56.Be provided with anchor 57 that is used for fixing water inlet pipe 52 and the anchor 58 that is used for fixing air stirring pipe 53 in anodizing tank cell body 51 outsides.Wherein the material of anodizing tank cell body 51, water pipe anchor 57 and 58, electrode holder 55 is PP, and the material of air stirring pipe 53, exhaust duct 54 and water inlet pipe 52 is PVC.
Referring to Fig. 8, described boiling water enclosed slot 7 is provided with boiling water enclosed slot inside groove 71 and boiling water enclosed slot water jacket 72, is provided with water shoot 73 in boiling water enclosed slot water jacket 72 bottoms, and water shoot 73 is connected with boiling water enclosed slot inside groove 71.Wherein the material of boiling water enclosed slot inside groove 71 is PP, and the material of boiling water enclosed slot water jacket 72 and water shoot 73 is SUS304.Between boiling water enclosed slot inside groove 71 and boiling water enclosed slot water jacket 72, fill the insulation asbestos.
The present invention establishes 4 operating units, and alkaline bath, hot water washing trough and cold water washing trough are operating unit one, and pickling tank and 2 cold water washing troughs are operating unit two, and anodizing tank is that three, 2 cold water washing troughs of operating unit and boiling water enclosed slot are operating unit four.
Operating unit one is installed: alkaline bath, hot water washing trough and cold water washing trough are placed on the operating table surface bracing frame, buckle operating table surface then, use the tapping screw locking between operating table surface and the bracing frame.
Operating unit two is installed: pickling tank and 2 cold water washing troughs are placed on the operating table surface bracing frame in order, buckle operating table surface then, use the tapping screw locking between operating table surface and the bracing frame.
Operating unit three is installed: anodizing tank is placed on the anodic oxidation mesa supports frame, buckles the anodic oxidation operating table surface then, and operating table surface and bracing frame directly use the tapping screw locking.
Operating unit four is installed: 2 cold water washing troughs and boiling water enclosed slot are placed on the operating table surface bracing frame in order, buckle operating table surface then, use the tapping screw locking between operating table surface and the bracing frame.
Below provide working method of the present invention.
1, tank liquor preparation
1.1 alkali cleaning tank liquor preparation
1.1.1 open the pure water valve, inject about 2/3 volume pure water, close the pure water valve then;
1.1.2 open the exhaust duct valve;
1.1.3 add the medicament that measures;
1.1.4 open the pressurized air valve, stirred 10 minutes;
1.1.5 open the pure water valve switch, inject pure water to prescribed volume valve-off at once;
1.1.6 cover the groove lid.
1.2, acid pickling groove liquid preparation
1.2.1 open the pure water valve, inject about 2/3 volume pure water, close the pure water valve then;
1.2.2 open the exhaust duct valve;
1.2.3 add the medicament that measures, stirred 1 minute with stirring rod;
1.2.4 open the pure water valve switch, inject pure water to prescribed volume valve-off at once;
1.2.5 cover the groove lid.
1.3, anode oxidation groove liquid preparation
1.3.1 open the pure water valve, inject about 2/3 volume pure water, close the pure water valve then;
1.3.2 open the exhaust duct valve;
1.3.3 add the medicament that measures;
1.3.4 open the pressurized air valve, stirred 10 minutes;
1.3.5 open the pure water valve switch, inject pure water to prescribed volume valve-off at once;
1.3.6 cover the groove lid.
Attention: all pharmacy slot pure water inlet valves keep normal off status in tank liquor preparation finishing back.
2, operation steps
2.1 open all groove lids;
2.2 open all induced exhaust valves (the follow-up normally open that keeps);
2.3 open outside blower fan;
2.4 open all washing bath inlet valves, keep changing the water frequency and be 1 groove/hour;
2.5 in the boiling water enclosed slot, add pure water, be advisable with cell body 2/3;
2.6 in the thermopair bracing frame, insert thermopair;
2.7 open all temperature controller switches, configure parameter according to technological specification;
2.8 when treating that temperature is increased to prescribed value, operate according to technical process;
2.9 turn on the power switch, set power parameter according to painted requirement, open the cell body power control switch and get final product;
2.10 after anode oxidation coloration finishes, close the cell body power control switch, take out product;
2.11 after all product anode oxidation colorations finished, powered-down switch and temperature controller switch took out thermopair;
2.12 close the washing bath inlet valve;
2.13 close outside blower fan;
2.14 cover the groove lid, in order to using next time.
3, tank liquor is changed: the medicine groove not directly enters water drain, needs to collect with dedicated container, send relevant qualification processed in units, and washing water etc. can directly enter water drain.When changing groove, operator need dress safety guard, slowly open the bottom land valve, and medicament is slowly flowed out, and hurt sb.'s feelings in order to avoid spill collection container.
4, precaution
3.1. during anodic oxidation, forbid the charged down groove of product, variant production adopts different anchor clamps;
3.2. when changing groove, it is excessive to must guard against valve open, so that medicament spills and hurts sb.'s feelings.
Claims (7)
1. titanium alloy anodic oxidation and coloring device, it is characterized in that being provided with alkaline bath, the hot water washing trough, 5 cold water washing troughs, pickling tank, anodizing tank, the boiling water enclosed slot, 3 electric heaters, 3 temperature sensors, temperature controller, timing controller and direct supply, alkaline bath, the hot water washing trough, the cold water washing trough, pickling tank, 2 cold water washing troughs, anodizing tank, 2 cold water washing troughs and boiling water enclosed slot are placed on the support by linear sequence, lay operating panel on the support, the right and left at pilot wire is provided with temperature controller respectively, direct supply and timing controller, 3 electric heaters are located at alkaline bath respectively, in hot water washing trough and the boiling water enclosed slot.
2. a kind of titanium alloy anodic oxidation and coloring device as claimed in claim 1, it is characterized in that described alkaline bath is provided with the alkaline bath cell body, on the alkaline bath cell body, be provided with water inlet pipe, exhaust duct and air stirring pipe, be provided with alkali cleaning thing rod bracing frame at alkaline bath cell body top, be provided with blow-off pipe in alkaline bath cell body bottom.
3. a kind of titanium alloy anodic oxidation and coloring device as claimed in claim 1, it is characterized in that described hot water washing trough is provided with hot water washing trough cell body, be provided with water inlet pipe, rising pipe and exhaust duct on hot water washing trough cell body top, be provided with blow-off pipe in hot water washing trough cell body bottom.
4. a kind of titanium alloy anodic oxidation and coloring device as claimed in claim 1 is characterized in that described cold water washing trough is provided with the washing bath cell body, is provided with water inlet pipe and rising pipe on washing bath cell body top, is provided with blow-off pipe in the bottom of washing bath cell body.
5. a kind of titanium alloy anodic oxidation and coloring device as claimed in claim 1, it is characterized in that described pickling tank is provided with the pickling tank cell body, be provided with water inlet pipe on pickling tank cell body top, be provided with exhaust duct, be provided with blow-off pipe in pickling tank cell body bottom at pickling tank cell body top.
6. a kind of titanium alloy anodic oxidation and coloring device as claimed in claim 1, it is characterized in that described anodizing tank is provided with the anodizing tank cell body, anodizing tank cell body top is provided with water inlet pipe and air stirring pipe, be provided with exhaust duct and electrode holder at anodizing tank cell body top, at anodizing tank cell body bottom blow-down pipe.
7. a kind of titanium alloy anodic oxidation and coloring device as claimed in claim 1, it is characterized in that described boiling water enclosed slot is provided with boiling water enclosed slot inside groove and boiling water enclosed slot water jacket, be provided with water shoot in boiling water enclosed slot water jacket bottom, water shoot is connected with boiling water enclosed slot inside groove.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101122310A CN101608334B (en) | 2009-07-17 | 2009-07-17 | Titanium alloy anodic oxidation and coloring device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009101122310A CN101608334B (en) | 2009-07-17 | 2009-07-17 | Titanium alloy anodic oxidation and coloring device |
Publications (2)
| Publication Number | Publication Date |
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| CN101608334A true CN101608334A (en) | 2009-12-23 |
| CN101608334B CN101608334B (en) | 2011-03-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2009101122310A Expired - Fee Related CN101608334B (en) | 2009-07-17 | 2009-07-17 | Titanium alloy anodic oxidation and coloring device |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102758236A (en) * | 2012-06-29 | 2012-10-31 | 江苏晨力实业有限公司 | Continuous coloring equipment for stainless steel plates and strips |
| CN103014812A (en) * | 2012-11-23 | 2013-04-03 | 北京星航机电设备厂 | Process for coloring titanium alloy through micro-arc oxidation |
| CN109680325A (en) * | 2018-11-16 | 2019-04-26 | 中国航发西安动力控制科技有限公司 | For being surface-treated the compressed air micropore agitating device of tank liquor |
| CN111218705A (en) * | 2020-01-16 | 2020-06-02 | 西安庄信新材料科技有限公司 | Titanium product anodic oxidation processing apparatus |
| CN112195492A (en) * | 2020-10-27 | 2021-01-08 | 广东美铝科技有限公司 | Aluminium alloy oxidation coloring production line |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1844483B (en) * | 2006-03-15 | 2010-07-07 | 厦门大学 | Process for anode oxidation coloration of titanium and titanium alloy surface |
| CN101407931B (en) * | 2008-11-04 | 2010-08-11 | 四川泛华航空仪表电器厂 | Conductive anodic oxidation process for aluminum and alloy part |
-
2009
- 2009-07-17 CN CN2009101122310A patent/CN101608334B/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102758236A (en) * | 2012-06-29 | 2012-10-31 | 江苏晨力实业有限公司 | Continuous coloring equipment for stainless steel plates and strips |
| CN103014812A (en) * | 2012-11-23 | 2013-04-03 | 北京星航机电设备厂 | Process for coloring titanium alloy through micro-arc oxidation |
| CN109680325A (en) * | 2018-11-16 | 2019-04-26 | 中国航发西安动力控制科技有限公司 | For being surface-treated the compressed air micropore agitating device of tank liquor |
| CN111218705A (en) * | 2020-01-16 | 2020-06-02 | 西安庄信新材料科技有限公司 | Titanium product anodic oxidation processing apparatus |
| CN111218705B (en) * | 2020-01-16 | 2022-01-11 | 西安庄信新材料科技有限公司 | Titanium product anodic oxidation processing apparatus |
| CN112195492A (en) * | 2020-10-27 | 2021-01-08 | 广东美铝科技有限公司 | Aluminium alloy oxidation coloring production line |
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| CN101608334B (en) | 2011-03-23 |
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