CN101580557A - Preparation process for extracting inulin from cichory root - Google Patents
Preparation process for extracting inulin from cichory root Download PDFInfo
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- CN101580557A CN101580557A CNA2009100120568A CN200910012056A CN101580557A CN 101580557 A CN101580557 A CN 101580557A CN A2009100120568 A CNA2009100120568 A CN A2009100120568A CN 200910012056 A CN200910012056 A CN 200910012056A CN 101580557 A CN101580557 A CN 101580557A
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Abstract
The invention relates to a preparation process for extracting inulin from cichory root, which mainly comprises the following steps: performing cleaning and extracting, sterilizing and inactivating enzyme, purifying sugar liquid, refining the sugar liquid, dehydrating and concentrating the sugar liquid, dehydrating and drying the sugar liquid, and reclaiming small molecular sugar. The preparation process overcomes the defects of process and equipment layout in the prior designed production process, reduces the total production cost, is safe and reliable, and has high extraction efficiency and rate of finished products.
Description
Technical field
The present invention relates to a kind of plant extract technology, relate in particular to the preparation technology who extracts inulin in a kind of root of Herba Cichorii, belong to the chemical industry extraction process.
Background technology
Inulin (synanthrin) and oligofructose are clear and definite because of its structure, and the physiological hygiene function definitely becomes a kind of important function food, occupies the top standard with Japanology, development and application in the world.Application and development in America and Europe and Korea S are also very fast.The research of the functional oligofructose of China starts from the nineties, start late, but development in recent years is very fast.Southern Yangtze University bears scientific payoffs-Production by Enzymes oligofructose that State Scientific and Technological Commission " 95 " brainstorm project obtains, and is third generation protective foods functional factor, and is called as 21 century high-tech biological products.Through how tame famous university and medical college studies confirm that both at home and abroad, inulin and oligofructose have the effect of superpower propagation human body bifidus bacillus, it is functional substance to the human body beneficial, it is the most representative typical products of 21 century human health for regulating organism balance, recover gastrointestinal function, enhance metabolism, prevent various diseases, safeguarding that HUMAN HEALTH has very important effect.Inulin has the physiological function of water-soluble dietary fibre and biological activity precursor as the edible polysaccharide of a kind of natural function, thereby has been widely used in low in calories, low sugar, the low fat food.
But, the production process of existing production technology often short period of time batch production can, pollute when continuous production liquid glucose will occur several weeks, purify and thoroughly do not cause production efficiency to reduce, the final inulin product that obtains its dissolving back liquid glucose mostly is muddy shape, has a strong impact on quality product.
Summary of the invention
The present invention is directed to above-mentioned problems of the prior art, carry out a large amount of exploratory developments and Test Summary according to the method that the modern plants extracting solution purifies, developed a kind of preparation technology who from root of Herba Cichorii, extracts inulin, solved that the inulin production efficiency of extracting in the prior art is low, the problem of poor product quality, the comprehensive multiple purification of the present invention, isolation technique are integrated, make process design and equipment configuration comparatively rationally with reliable, can reduce total production cost effectively.
Technical scheme of the present invention is as follows:
Extraction process of the present invention comprises the steps:
The cleaning lixiviate is got---and bright root of Herba Cichorii is removed impurity wash; The bright root of Herba Cichorii of cleaning is cut into silk or thin slice; The root of Herba Cichorii that is cut into silk or thin slice is carried out the adverse current lixiviate with hot water get synanthrin, the ratio of weight and number of water consumption and root of Herba Cichorii consumption is water: endive=5-10: 1; The lixiviate water temperature remains on 60-80 degree centigrade, and the lixiviate time of getting is 60-100 minute, extrudes residue after lixiviate is finished and gets lixiviate liquid glucose A;
Sterilising and enzyme inactivating---lixiviate liquid glucose A heat temperature raising to 90-100 degree centigrade, is carried out High Temperature Sterilization and went out enzyme 10-30 minute;
Liquid glucose purifies---the lixiviate liquid glucose A behind the sterilising and enzyme inactivating is carried out chemical flocculation isolation of purified and physical cleaning successively, is mass percent concentration that the calcium hydroxide emulsion of 10%-20% is put into chemical reaction and the flocculation of carrying out nonsugar among the lixiviate liquid glucose A, temperature is controlled at 60-90 degree centigrade, and the control pH value is 10-13; Feed carbon dioxide and excessive calcium hydroxide reaction then and separate out lime carbonate, control PH to 6.5-8.0, material after chemical flocculation is handled carries out micro-filtration, the ultrafiltration of organic or inorganic film again, with the further adsorb organic compound of craboraffin, the ratio of weight and number of craboraffin and material is, craboraffin: material=0.2-1: 100, obtain to purify liquid glucose B;
Liquid glucose is refining---liquid glucose B is carried out yin, yang macroporous ion exchange resin and bitter principle polymeric adsorbent successively, the mineral ion of Ex-all, partial organic substances pigment and the distinctive bitter principle of witloof raw material do not separate to obtain more purified liquid glucose among the liquid glucose B, also having mass percent in the liquid glucose is that the non-synanthrin material as single fruit sugar, dextrose plus saccharose of 10-25% make with extra care purifying and concentrated with nanofiltration membrane again, control solid content (Brix) is 20%, control sugared content in the non-synanthrin at 2-10%, obtain refining liquid glucose C;
Liquid glucose dehydration concentrates---and will make with extra care liquid glucose C and carry out dehydration by evaporation with the heating evaporation water trap and be concentrated into solid content (Brix) and reach 30-40%, obtain concentrated liquid glucose D;
Liquid glucose dehydrates---and will concentrate liquid glucose D and be preheated to 60-85 degree centigrade and dehydrate the device acquisition inulin that dusts with spraying, the purity of inulin can reach 90%-98%.
Small molecular sugar reclaims---and rare liquid glucose of the non-inulenin of small molecules that the nanofiltration purifies and separates is gone out dewaters with reverse osmosis membrane, and to be concentrated into solid content (Brix) be 10-20%, being concentrated into solid content (Brix) with heating evaporation water trap dehydration by evaporation again is 55-65%, obtains the high fructose syrup byproduct.
Described cleaning lixiviate is got in the step, and bright root of Herba Cichorii also can be cut into silk earlier or thin slice is dried into dried witloof raw material, and the ratio of weight and number of water and dried witloof raw material consumption is water during lixiviate: endive=15-25: 1, and the lixiviate time of getting is 100-150 minute.
In the described liquid glucose purifying step, phosphoric acid and excessive calcium hydroxide reaction are separated out calcium phosphate, control PH to 7-8.5.
In the described liquid glucose thermal dehydration enrichment step, available scrapper thin film evaporator, shell and tube ascending, descending film or multistage external circulation evaporator carry out dehydration by evaporation and concentrate.
In the described liquid glucose thermal dehydration drying step, available pressure formula or centrifugal spraying dehydrate device and dust.
Advantage of the present invention and beneficial effect are as follows:
1, the present invention adopts inulin in the water extraction witloof to compare and uses solvent extraction, and its cost and equipment configratioin requirement are low, and safe and reliable.
2, the present invention adopts water adverse current continuous extraction to get, need not boiling, and simple to operate, stable and extraction efficiency is high, the sugared content that does not extract in the raw material slag is than the low 40-60% of non-counter-current.
3, the present invention adopts go out enzyme, chemical purification and physical cleaning combination process of high temperature can remove non-sugared organic substance more up hill and dale, and can control the microbiological pollution of liquid glucose more effectively, the operation that can guarantee production middle-chain is normal, has improved production efficiency and quality product.
4, the witloof raw material is different with Jerusalem artichoke raw material, himself contain biological bitter principle material, and the present invention adopts macroporous adsorbent resin to solve witloof and extracts bitter taste problem in the liquid glucose.
Description of drawings
Fig. 1 is a process flow sheet of the present invention.
Embodiment
Embodiment 1
Extraction process of the present invention comprises the steps:
The cleaning lixiviate is got---and bright root of Herba Cichorii is removed impurity wash; The bright root of Herba Cichorii of cleaning is cut into silk or thin slice; The root of Herba Cichorii that is cut into silk or thin slice is carried out the adverse current lixiviate with hot water get synanthrin, the ratio of weight and number of water consumption and root of Herba Cichorii consumption is water: endive=8: 1; The lixiviate water temperature remains on 65 degrees centigrade, and the lixiviate time of getting is 80 minutes, extrudes residue after lixiviate is finished and gets lixiviate liquid glucose A;
Sterilising and enzyme inactivating---with lixiviate liquid glucose A heat temperature raising to 95 degree centigrade, carry out go out enzyme 20 minutes of High Temperature Sterilization;
Liquid glucose purifies---the lixiviate liquid glucose A behind the sterilising and enzyme inactivating is carried out chemical flocculation isolation of purified and physical cleaning successively, remove more up hill and dale solid substance and organic in, macromolecular substance and partial pigment, is mass percent concentration that 15% calcium hydroxide emulsion is put into chemical reaction and the flocculation of carrying out nonsugar among the lixiviate liquid glucose A, temperature is controlled at 70 degrees centigrade, and the control pH value is 10-13; Feed carbon dioxide and excessive calcium hydroxide reaction then and separate out lime carbonate, control PH to 6.5-8.0, material after chemical flocculation is handled is with further adsorb organic compound of craboraffin and partial pigment, carry out micro-filtration, the ultrafiltration of organic or inorganic film again, the ratio of weight and number of craboraffin and material is, craboraffin: material=0.5: 100 obtains to purify liquid glucose B;
Liquid glucose is refining---liquid glucose B is carried out yin, yang macroporous ion exchange resin and bitter principle polymeric adsorbent successively, the mineral ion of Ex-all, partial organic substances pigment and the distinctive bitter principle of witloof raw material do not separate to obtain more purified liquid glucose among the liquid glucose B, also having mass percent in the liquid glucose is that the non-synanthrin material as single fruit sugar, dextrose plus saccharose of 10-25% make with extra care purifying and concentrated with nanofiltration membrane again, control solid content (Brix) is 20%, control sugared content in the non-synanthrin at 2-10%, obtain refining liquid glucose C;
Liquid glucose dehydration concentrates---and will make with extra care liquid glucose C and carry out dehydration by evaporation with the heating evaporation water trap and be concentrated into solid content (Brix) and reach 35%, obtain concentrated liquid glucose D;
Liquid glucose dehydrates---and will concentrate liquid glucose D and be preheated to 70 degrees centigrade and dehydrate the device acquisition inulin that dusts with press spray, the purity of inulin reaches 94%.
Small molecular sugar reclaims---and rare liquid glucose of the non-inulenin of small molecules that the nanofiltration purifies and separates is gone out dewaters with reverse osmosis membrane, and to be concentrated into solid content (Brix) be 15%, being concentrated into solid content (Brix) with heating evaporation water trap dehydration by evaporation again is 60%, obtains the high fructose syrup byproduct.
Embodiment 2
Described cleaning lixiviate is got in the step, and the ratio of weight and number of water consumption and root of Herba Cichorii consumption is water: endive=5: 1; The lixiviate water temperature remains on 60 degrees centigrade, and the lixiviate time of getting is 100 minutes;
In the described sterilising and enzyme inactivating step,, carry out go out enzyme 30 minutes of High Temperature Sterilization with lixiviate liquid glucose A heat temperature raising to 90 degree centigrade;
In the described liquid glucose purifying step, is mass percent concentration that 10% calcium hydroxide emulsion is put into chemical reaction and the flocculation of carrying out nonsugar among the lixiviate liquid glucose A, temperature is controlled at 60 degrees centigrade, and the control pH value is 10-13, separates out calcium phosphate with the anti-PH to 7-8 of accent of phosphoric acid again;
In the described liquid glucose purification step, control sugared content in the non-synanthrin at 2-5%;
In the described liquid glucose dehydration enrichment step, dehydration by evaporation is concentrated into solid content (Brix) and reaches 30%;
Described liquid glucose dehydrates in the step, will concentrate liquid glucose D and be preheated to 85 degrees centigrade.
In the described small molecular sugar recycling step, it is 10% that dehydration is concentrated into solid content (Brix), and being concentrated into solid content (Brix) with heating evaporation water trap dehydration by evaporation again is 55%; Other step is with embodiment 1.
Embodiment 3
Described cleaning lixiviate is got in the step, and the ratio of weight and number of water consumption and root of Herba Cichorii consumption is water: root of Herba Cichorii=10: 1; The lixiviate water temperature remains on 80 degrees centigrade, and the lixiviate time of getting is 60 minutes;
In the described sterilising and enzyme inactivating step,, carry out go out enzyme 10 minutes of High Temperature Sterilization with lixiviate liquid glucose A heat temperature raising to 100 degree centigrade;
In the described liquid glucose purifying step, be mass percent concentration that 20% calcium hydroxide emulsion is put into chemical reaction and the flocculation of carrying out nonsugar among the lixiviate liquid glucose A, temperature is controlled at 90 degrees centigrade;
In the described liquid glucose dehydration enrichment step, dehydration by evaporation is concentrated into solid content (Brix) and reaches 40%;
Described liquid glucose dehydrates in the step, will concentrate liquid glucose D and be preheated to 80 degrees centigrade;
In the described small molecular sugar recycling step, it is 20% that dehydration is concentrated into solid content (Brix), and being concentrated into solid content (Brix) with above-mentioned heating evaporation water trap dehydration by evaporation again is 65%; Other step is with implementing 1.
Embodiment 4
Described cleaning lixiviate is got in the step, and the witloof raw material is the witloof dry product, and the ratio of weight and number of water and dry product consumption is water during lixiviate: root of Herba Cichorii=20: 1, and the lixiviate time of getting is 150 minutes;
In the described liquid glucose purifying step, phosphoric acid and excessive calcium hydroxide reaction are separated out calcium phosphate, control PH to 7-8.5; In the described liquid glucose dehydration enrichment step, available scrapper thin film evaporator carries out dehydration by evaporation and concentrates; Described liquid glucose dehydrates in the step, and available centrifugal spraying dehydrates device and dusts; Other step is with embodiment 1.
Embodiment 5
Described cleaning lixiviate is got in the step, and the witloof raw material is the witloof dry product, and the ratio of weight and number of water and dried root of Herba Cichorii consumption is water during lixiviate: root of Herba Cichorii=25: 1, and the lixiviate time of getting is 100 minutes; In the described liquid glucose dehydration enrichment step, available multistage external circulation evaporator carries out dehydration by evaporation and concentrates; Other step is with embodiment 1.
Protection scope of the present invention is as the criterion with claim, not limited by specific embodiment.
Claims (5)
1, extracts the preparation technology of inulin in a kind of root of Herba Cichorii, it is characterized in that comprising the steps:
The cleaning lixiviate is got---and bright root of Herba Cichorii is removed impurity wash; The bright root of Herba Cichorii of cleaning is cut into silk or thin slice; The root of Herba Cichorii that is cut into silk or thin slice is carried out the adverse current lixiviate with hot water get synanthrin, the ratio of weight and number of water consumption and endive consumption is water: endive=5-10: 1; The lixiviate water temperature remains on 60-90 degree centigrade, and the lixiviate time of getting is 60-100 minute, extrudes residue after lixiviate is finished and gets lixiviate liquid glucose A;
Sterilising and enzyme inactivating---lixiviate liquid glucose A heat temperature raising to 90-100 degree centigrade, is carried out High Temperature Sterilization and went out enzyme 10-30 minute;
Liquid glucose purifies---the lixiviate liquid glucose A behind the sterilising and enzyme inactivating is carried out chemical flocculation isolation of purified and physical cleaning successively, is mass percent concentration that the calcium hydroxide emulsion of 10%-20% is put into chemical reaction and the flocculation of carrying out nonsugar among the lixiviate liquid glucose A, temperature is controlled at 60-90 degree centigrade, and the control pH value is 10-13; Feed carbon dioxide and excessive calcium hydroxide reaction then and separate out lime carbonate, control PH to 6.5-8.0, material after chemical flocculation is handled carries out micro-filtration, the ultrafiltration of organic or inorganic film again, with the further adsorb organic compound of craboraffin, the ratio of weight and number of craboraffin and material is, craboraffin: material=0.2-1: 100, obtain to purify liquid glucose B;
Liquid glucose is refining---liquid glucose B is carried out yin, yang macroporous ion exchange resin and bitter principle polymeric adsorbent successively, the mineral ion of Ex-all, partial organic substances pigment and the distinctive bitter principle of witloof raw material do not separate to obtain more purified liquid glucose among the liquid glucose B, also having mass percent in the liquid glucose is that the non-synanthrin material as single fruit sugar, dextrose plus saccharose of 10-25% make with extra care purifying and concentrated with nanofiltration membrane again, control solid content (Brix) is 20%, control sugared content in the non-synanthrin at 2-10%, obtain refining liquid glucose C;
Liquid glucose dehydration concentrates---and will make with extra care liquid glucose C and carry out dehydration by evaporation with the heating evaporation water trap and be concentrated into solid content (Brix) and reach 30-40%, obtain concentrated liquid glucose D;
Liquid glucose dehydrates---and will concentrate liquid glucose D and be preheated to 50-80 degree centigrade and dehydrate the device acquisition inulin that dusts with spraying, the purity of inulin can reach 90%-98%.
Small molecular sugar reclaims---and rare liquid glucose of the non-inulenin of small molecules that the nanofiltration purifies and separates is gone out dewaters with reverse osmosis membrane, and to be concentrated into solid content (Brix) be 10-20%, being concentrated into solid content (Brix) with heating evaporation water trap dehydration by evaporation again is 55-65%, obtains the high fructose syrup byproduct.
2, extract the preparation technology of inulin in the root of Herba Cichorii according to claim 1, it is characterized in that described cleaning lixiviate gets in the step, bright root of Herba Cichorii can be cut into silk earlier, thin slice is dried into dried witloof raw material, the ratio of weight and number of water and dried root of Herba Cichorii consumption is during lixiviate, water: endive=15-25: 1, the lixiviate time of getting is 100-150 minute.
3, extract the preparation technology of inulin in the root of Herba Cichorii according to claim 1, it is characterized in that in the described liquid glucose purifying step, phosphoric acid is separated out calcium phosphate with excessive calcium hydroxide reaction, controls PH to 7-8.5.
4, extract the preparation technology of inulin in the root of Herba Cichorii according to claim 1, it is characterized in that available scrapper thin film evaporator, shell and tube ascending, descending film or multistage external circulation evaporator carry out dehydration by evaporation and concentrate in the described liquid glucose dehydration enrichment step.
5, extract the preparation technology of inulin in the root of Herba Cichorii according to claim 1, it is characterized in that described liquid glucose dehydrates in the step, available pressure formula or centrifugal spraying dehydrate device and dust.
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| CN2009100120568A CN101580557B (en) | 2009-06-16 | 2009-06-16 | Preparation process for extracting inulin from cichory root |
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| CN102146144A (en) * | 2011-03-18 | 2011-08-10 | 晨光生物科技集团天津有限公司 | Method for extracting and refining inulin |
| CN102242168A (en) * | 2011-04-25 | 2011-11-16 | 武汉市金德戈糖业有限公司 | Process for producing high fructose syrup with a content of 55% with rice |
| CN102242167A (en) * | 2011-04-25 | 2011-11-16 | 武汉市金德戈糖业有限公司 | Technology for producing fructose-glucose syrup containing 90% of fructose from rice |
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| US5422346A (en) * | 1988-01-06 | 1995-06-06 | California Natural Products | Instant dried dahlia inulin juice and its method of production and usage |
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| CN102146144B (en) * | 2011-03-18 | 2012-07-04 | 晨光生物科技集团天津有限公司 | Method for extracting and refining inulin |
| CN102146144A (en) * | 2011-03-18 | 2011-08-10 | 晨光生物科技集团天津有限公司 | Method for extracting and refining inulin |
| CN102242168A (en) * | 2011-04-25 | 2011-11-16 | 武汉市金德戈糖业有限公司 | Process for producing high fructose syrup with a content of 55% with rice |
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| CN104498330A (en) * | 2015-01-07 | 2015-04-08 | 青海威德生物技术有限公司 | Device for preparing and debitterizing fructo-oligosaccharide |
| CN106349398A (en) * | 2015-11-13 | 2017-01-25 | 翟丹云 | Cichorium intybus inulin extracting method |
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