CN101525164B - Sodium percarbonate preparation used for water fast oxygenation and disinfection and preparation method thereof - Google Patents
Sodium percarbonate preparation used for water fast oxygenation and disinfection and preparation method thereof Download PDFInfo
- Publication number
- CN101525164B CN101525164B CN200910074178XA CN200910074178A CN101525164B CN 101525164 B CN101525164 B CN 101525164B CN 200910074178X A CN200910074178X A CN 200910074178XA CN 200910074178 A CN200910074178 A CN 200910074178A CN 101525164 B CN101525164 B CN 101525164B
- Authority
- CN
- China
- Prior art keywords
- preparation
- spc
- agent
- raw material
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a sodium percarbonate preparation used for water fast oxygenation and disinfection and a preparation method thereof, belonging to the technical field of water quality treatment and being used for solving the problem that the prior sodium percarbonate product has bad stability and unobvious oxygenation effect. The technical proposal is as follows: the shape of the preparation is tablet, block, pellet or stick and the like, and the preparation is made from the raw materials with the weight portions as follows: 60 to 98 portions of sodium percarbonate, 0.5 to 8 portions of stabilizing agent, 0.5 to 8 portions of exciting agent and 1 to 9 portions of adhesive. Compared with the prior art, the invention has the advantages as follows: 1. the product can subside to the bottom of the water fast after being put into the water, increases the oxygen content of the water fast and completely and can disinfect the water from bottom to top; 2. the product has good stability and long shelf life and is not decomposed easily under normal state, the effective period can be more than one year; and 3. the invention has simple operation, is convenient for using and is safe and effective.
Description
Technical field
The present invention relates to a kind of oxygenation, sterilizing agent, can carry out oxygenation, disinfectant SPC-D preparation and preparation method to water body fast after especially being dissolved in water body, belong to the water conditioning technical field.
Background technology
In aquaculture; high-density breeding and subatmospheric cause the aquaculture water severe depletion of oxygen through regular meeting; cause the redox potential of water body (especially bottom) to descend; the pH value reduces; organism decomposes not thorough; a large amount of deleterious anaerobism product hydrogen sulfide, methane, ammonia-nitrogen content rise, and can cause the general pool and floating head.At present, normally adopt mechanical enhancement for the oxygenation method of aquaculture water, by stir or air pump to the water body bubbling air, but this can only solve surface or local anoxic, can't make whole water body, particularly water bottom oxygenation.The oxygenation, the sterilization method that the SPC-D powder are used for aquaculture water are also arranged in recent years, SPC-D is a kind of good disinfectant and oxygenation agent, be added to and solve water body oxygenation problem in the water body, but powdered sodium carbonate is difficult to be deposited to the bottom, makes the special water bottom of whole water body reach oxygenation effect.Also have materials such as SPC-D, starch, hard fatty acids magnesium are pressed into bulk, be used for oxygenation, the sterilization of breeding water, but this product stability is relatively poor, the quality guaranteed period is short, has influence on result of use thus.
Summary of the invention
The present invention be used to overcome prior art defective, provide a kind of oxygenation effect rapidly obviously, good stability, water fast oxygenation, disinfectant SPC-D preparation and preparation method thereof of being used for easy to use.
The alleged problem of the present invention is solved by following technical scheme:
A kind of water fast oxygenation, disinfectant SPC-D preparation of being used for, its special feature is: described preparation profile is shapes such as sheet, piece, ball or rod, it is made by the raw material of following mass parts: SPC-D 60～98, stablizer 0.5～8, exciting agent 0.5～8, tackiness agent 1～9, described stablizer are a kind of in Magnesium Silicate q-agent, magnesium chloride or the sal epsom; Described exciting agent is a kind of in hexanodioic acid, citric acid, tartrate or the fumaric acid; Described tackiness agent is a kind of in polyvinylpyrrolidone, Microcrystalline Cellulose or the carboxymethyl cellulose.
Above-mentioned water fast oxygenation, the disinfectant SPC-D preparation of being used for, it is made by the raw material of following mass parts: SPC-D 70～95, magnesium chloride 1～6, hexanodioic acid 1～5, polyvinylpyrrolidone 2～7.
Above-mentioned water fast oxygenation, the disinfectant SPC-D preparation of being used for, it is made by the raw material of following mass parts: SPC-D 90, magnesium chloride 4, hexanodioic acid 4, polyvinylpyrrolidone 6.
A kind ofly prepare the above-mentioned method that is used for water fast oxygenation, disinfectant SPC-D preparation, it carries out according to the following steps:
A. take by weighing raw material by proportioning, SPC-D, exciting agent are pulverized be granularity 20～80 orders, stablizer, tackiness agent pulverize for granularity less than 100 orders, the above-mentioned raw materials thorough drying, water content is below 0.3%;
B. add exciting agent, stablizer, the tackiness agent of formula ratio in mixing tank, mixing is even;
C. in the mixing raw material of above-mentioned b step, add the SPC-D of formula ratio, mix;
D. with above-mentioned mixing raw material press forming, humidity is controlled less than 45%R.H., compacting pressure 2.1～4.2T/cm
2, packing gets product.
The present invention is directed to that the existing SPC-D product stability that is used for water body disinfection oxygenation is relatively poor, the water body lower floor unconspicuous problem of oxygenation effect is improved, its product composition is made up of SPC-D, stablizer, exciting agent, tackiness agent, and product form is shapes such as sheet, piece, ball.Compare with existing SPC-D product, the present invention has following remarkable advantage: 1, this product can be deposited to the bottom rapidly after dropping into water body, increase fast, the oxygen level of water body comprehensively, this is because the present invention is after rendering to the bottom, can produce the active oxygen gas microvesicle rapidly, in the rise process that made progress by the bottom, be dissolved in successively on the way in the water body, therefore, than traditional oxygenating, more can significantly improve the middle lower floor oxygen level of water body; In addition, it can also carry out disinfection to water body from bottom to top,, according to surveying and determination, 0.25% SPC-D effect 3min reaches 99.9% to streptococcus aureus and intestinal bacteria killing rate; 0.5% mass action 15min reaches 92.64% to the killing rate of natural bacteria; 10% effect 5min, 5% effect 10min can destroy the antigenicity of HBsAg; 2, product stability is good, is difficult under the normality decomposing, and the quality guaranteed period is permanent, and validity period can be above 1 year; 3, simple to operate, easy to use, safe and effective.
Embodiment
SPC-D is a kind of good disinfectant and oxygenation agent, is pulverulence under the usual condition, swims in the water body top layer.The present invention adds tackiness agent, stablizer and exciting agent and forms difform preparation through compacting in the SPC-D of pulverulence, its profile is beneficial to preparation and is deposited to the bottom.The stablizer that adds in the product can keep stability of formulation on the one hand under normal conditions, can stop preparation pulverous SPC-D and exciting agent reaction in preparation process on the other hand; The exciting agent that adds in the product can impel preparation snap-out release in the aqueous solution to go out oxygen, to reach rapid oxygenation disinfectant effect; Tackiness agent can adhere to together each component under the situation of pressurized; Selected in addition stablizer and exciting agent just are again releasing agents, can make the intact moulding of tablet, and deviate from from mould like a cork.
Water fast oxygenation, the disinfectant SPC-D preparation of being used for of the present invention carries out 54 ℃ of hot accelerated stability tests according to Ministry of Health's 2002 editions " disinfection technology standards ", and effective constituent (active oxygen) content rate of descent is in 7%, and the quality guaranteed period is 1 year.Above-mentioned performance defined in " disinfection technology standard ": at 54 ℃, under 75% the relative humidity, medicine is preserved 14 days index.Directly render to when the present invention uses in the water body, injected volume restrains with 3000-6000 by every mu of 1 meter depth of water, the multiplicable use of water quality deterioration.
Several embodiment below are provided:
Embodiment 1: take by weighing SPC-D 98kg, stablizer magnesium chloride 8kg, exciting agent citric acid 8kg, tackiness agent carboxymethyl cellulose 9kg;
Embodiment 2: take by weighing SPC-D 60kg, stablizer Magnesium Silicate q-agent 4kg, exciting agent hexanodioic acid 0.5kg, polyvinyl pyrrolidone 2kg;
Embodiment 3: take by weighing SPC-D 65kg, stablizer sal epsom 0.5kg, exciting agent tartrate 3kg, polyvinyl pyrrolidone 1kg;
Embodiment 4: take by weighing SPC-D 70kg, stablizer magnesium chloride 1kg, exciting agent fumaric acid 8kg, polyvinyl pyrrolidone composition 9kg;
Embodiment 5: take by weighing SPC-D 95kg, stablizer magnesium chloride 6kg, exciting agent hexanodioic acid 8kg, tackiness agent Microcrystalline Cellulose 9kg;
Embodiment 6: take by weighing SPC-D 90kg, stablizer magnesium chloride 4kg, exciting agent hexanodioic acid 4kg, polyvinyl pyrrolidone 6kg;
Embodiment 7: take by weighing SPC-D 90kg, stablizer Magnesium Silicate q-agent 7kg, exciting agent fumaric acid 8kg, polyvinyl pyrrolidone composition 9kg;
Take by weighing raw material by the foregoing description, SPC-D, exciting agent are pulverized be granularity 20～80 orders, with stablizer, tackiness agent pulverize for granularity less than 100 orders, the raw material thorough drying, water content is below 0.3%; Add exciting agent, stablizer, the tackiness agent of formula ratio in mixing tank, mixing is even; In said mixture, add the SPC-D of formula ratio again, mix; Above-mentioned mixing raw material is pressed into sheet, bulk, difform preparation such as spherical, bar-shaped, and humidity is controlled less than 45%R.H., pressure 2.1～4.2T/cm
2, packing gets product.
Claims (3)
1. one kind is used for water fast oxygenation, disinfectant SPC-D preparation, it is characterized in that: described preparation profile is sheet, piece, ball or bar-like shape, it is made by the raw material of following mass parts: SPC-D 60～98, stablizer 0.5～8, exciting agent 0.5～8, tackiness agent 1～9, described stablizer are a kind of in Magnesium Silicate q-agent, magnesium chloride or the sal epsom; Described exciting agent is a kind of in hexanodioic acid, citric acid, tartrate or the fumaric acid; Described tackiness agent is a kind of in polyvinylpyrrolidone, Microcrystalline Cellulose or the carboxymethyl cellulose;
Described preparation prepares according to the following steps:
A. take by weighing raw material by proportioning, SPC-D, exciting agent are pulverized be granularity 20～80 orders, stablizer, tackiness agent pulverize for granularity less than 100 orders, the above-mentioned raw materials thorough drying, water content is below 0.3%;
B. add exciting agent, stablizer, the tackiness agent of formula ratio in mixing tank, mixing is even;
C. in the mixing raw material of above-mentioned b step, add the SPC-D of formula ratio, mix;
D. with above-mentioned mixing raw material press forming, humidity is controlled less than 45% RH, compacting pressure 2100～4200kg/cm
2, packing gets product.
2. according to described water fast oxygenation, the disinfectant SPC-D preparation of being used for of claim 1, it is characterized in that it is made by the raw material of following mass parts: SPC-D 70～95, magnesium chloride 1～6, hexanodioic acid 1～5, polyvinylpyrrolidone 2～7.
3. according to described water fast oxygenation, the disinfectant SPC-D preparation of being used for of claim 2, it is characterized in that it is made by the raw material of following mass parts: SPC-D 90, magnesium chloride 4, hexanodioic acid 4, polyvinylpyrrolidone 6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910074178XA CN101525164B (en) | 2009-04-20 | 2009-04-20 | Sodium percarbonate preparation used for water fast oxygenation and disinfection and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910074178XA CN101525164B (en) | 2009-04-20 | 2009-04-20 | Sodium percarbonate preparation used for water fast oxygenation and disinfection and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101525164A CN101525164A (en) | 2009-09-09 |
| CN101525164B true CN101525164B (en) | 2011-01-05 |
Family
ID=41093264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910074178XA Expired - Fee Related CN101525164B (en) | 2009-04-20 | 2009-04-20 | Sodium percarbonate preparation used for water fast oxygenation and disinfection and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101525164B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104828955B (en) * | 2015-05-05 | 2017-03-22 | 山东宝来利来生物工程股份有限公司 | Biological composite oxygen producer and preparation method thereof |
| CN108178276A (en) * | 2016-12-08 | 2018-06-19 | 刘宫介 | A kind of fishery substrate modifier and preparation method thereof |
| CN107285450B (en) * | 2017-06-23 | 2020-07-14 | 贝嘉美（天津）生物技术研发有限公司 | Efficient oxygen increasing agent used in aquaculture and application thereof |
| CN108217955A (en) * | 2017-12-25 | 2018-06-29 | 广东粤海生物科技有限公司 | A kind of stable type oxygenation agent used for aquiculture and preparation method thereof |
| CN108996629A (en) * | 2018-08-31 | 2018-12-14 | 江苏祥豪实业股份有限公司 | Potassium Monopersulfate compound effervescent tablet and preparation method thereof for the improvement of water quality substrate |
| CN109892280A (en) * | 2019-03-27 | 2019-06-18 | 青岛中仁动物药品有限公司 | A kind of tablet and preparation method thereof improving breeding water body dissolved oxygen |
| CN110844993A (en) * | 2019-11-29 | 2020-02-28 | 河南骏化发展股份有限公司 | Composite oxygen increasing agent and preparation method thereof |
-
2009
- 2009-04-20 CN CN200910074178XA patent/CN101525164B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN101525164A (en) | 2009-09-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101525164B (en) | Sodium percarbonate preparation used for water fast oxygenation and disinfection and preparation method thereof | |
| CN101525165B (en) | Calcium peroxide preparation used for water fast oxygenation and preparation method thereof | |
| CN101536710A (en) | Mildewproof anti-staling agent for rice | |
| US9517197B1 (en) | Toothpaste composition containing ganoderma lucidum component and preparation method thereof | |
| KR101506382B1 (en) | Composition of foaming tablet | |
| CN102847185A (en) | Solid transparent fragrant deodorizing agent and preparation method thereof | |
| CN103622069A (en) | Preserved egg curing agent and preparation method thereof | |
| CN105836870A (en) | Household water treatment filter material capable of slowly releasing vitamin C and preparation method thereof | |
| CN107593720A (en) | A kind of compound disinfecting tablet and preparation method thereof | |
| CN103784418A (en) | Fish skin gelatin hollow capsules and preparation method thereof | |
| CN104621678A (en) | Compound antiseptic color-protecting preservative solution and production method thereof | |
| CN104012458B (en) | A kind of method utilizing by-product bulky grain SODIUM PERCARBONATE to prepare oxygenation agent | |
| CN102177863A (en) | Method for inducing hormone soaked loaches | |
| CN105395617A (en) | Foot bath effervescent tablet containing macleaya cordata total alkaloids and preparation method of foot bath effervescent tablet | |
| CN105886159B (en) | Food stage aerobic detergent | |
| CN104366111A (en) | Flake abalone compound feed and production method thereof | |
| CN108096429A (en) | A kind of mouth sprays for alleviating oral peculiar smell and preparation method thereof | |
| CN111771905B (en) | Solid hydrogen peroxide and preparation method and application thereof | |
| CN106305775A (en) | Pond bottom disinfectant for loach pond and preparation method thereof | |
| CN110844993A (en) | Composite oxygen increasing agent and preparation method thereof | |
| CN109329136A (en) | It is a kind of for preventing and treating the probiotics fermention mixture and its Ecological preventive way of the rotten body disease of pond culture hybridized snakehead fish | |
| RU2011108370A (en) | CHEWING COMPOSITION, INCLUDING ALGINATE, BICARBONATE AND CARBONATE | |
| CN111096320A (en) | Selective oxidation chlorine dioxide sustained-release tablet special for culture pond | |
| CN106577741A (en) | Sustained-release agent of insecticide and preparation method thereof | |
| CN102526696A (en) | Composition of gastric mucin capsule and preparation method for composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110105 Termination date: 20130420 |