CN101480600B - Combined construction of reactor and cold separation pot for producing amino acid product - Google Patents

Combined construction of reactor and cold separation pot for producing amino acid product Download PDF

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Publication number
CN101480600B
CN101480600B CN2008102426840A CN200810242684A CN101480600B CN 101480600 B CN101480600 B CN 101480600B CN 2008102426840 A CN2008102426840 A CN 2008102426840A CN 200810242684 A CN200810242684 A CN 200810242684A CN 101480600 B CN101480600 B CN 101480600B
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China
Prior art keywords
cold analysis
analysis still
cold separation
filter
reactor
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Expired - Fee Related
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CN2008102426840A
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Chinese (zh)
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CN101480600A (en
Inventor
陆昌元
陆剑平
王建峰
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Jiangsu Yuanyang Pharmaceutical Co.,Ltd.
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JIANGSU YUANYANG CHEMISTRY CO Ltd
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Priority to CN2008102426840A priority Critical patent/CN101480600B/en
Publication of CN101480600A publication Critical patent/CN101480600A/en
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Publication of CN101480600B publication Critical patent/CN101480600B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention relates to a combined structure of a reaction kettle and a cold separation kettle which are used for the production of anime acid products. The combined structure belongs to the technical filed of discharge devices of reaction vessels and comprises a reaction kettle body, a conveying mechanism, a filter, a cold separation kettle feed pipe provided with a viewing mirror, and a cold separation kettle arranged on one side of the filter. The combined structure is characterized by further comprising a control pipeline; one end of the control pipeline is connected with the cold separation kettle feed pipe, while the other end is connected with a cold separation kettle feed opening of the cold separation kettle; the control pipeline is provided with a control valve and a window; the cold separation kettle feed pipe is connected with the filter and a feed opening of the reaction kettle body respectively; in addition, the cold separation kettle feed pipe is provided with a second control valve which is positioned below the viewing mirror. The invention has the advantages that the combined structure cannot cause material waste and can ensure the cleanness of materials entering the cold separation kettle.

Description

The combining structure of reactor in the amino acids production and cold analysis still
Technical field
The invention belongs to the drawing mechanism technical field of reaction vessel, be specifically related to the reactor in a kind of amino acids production and the combining structure of cold analysis still.
Background technology
At the amino acids product for example in the production process of creatine, taurine; in reactor because water, material and active carbon three are mixed in together; therefore the reactant introducing filter that will be come from the drain hole of reactor in reactor reaction end back by conveying mechanism filters; with the active carbon filtering, introduce the cold analysis of cold analysis still by filter then.
Fig. 2 is the reactor in the amino acids production in the prior art and the combining structure of cold analysis still, comprise reactor kettle 1, conveying mechanism 2, filter 3, cold analysis still material guiding tube 4 and cold analysis still 5, conveying mechanism 2 connects with discharging opening 11 pipeline connections of the bottom of reactor kettle 1 and with the filter pipeline, one client link of cold analysis still material guiding tube 4 is on filter 3, the other end constitutes free end, and cold analysis still 5 is configured in a side of filter 3.The discharging opening 11 of the material autoreaction still kettle 1 of reaction after finishing is introduced filters 3 through conveying mechanism 2 and is filtered, and the material that will come from filter 3 by the free end of the hand-held cold analysis still material guiding tube 4 of online assignment personnel causes the cold analysis of cold analysis still simultaneously.But because as described above, water, material and active carbon three mix, and therefore the material of initially being drawn by filter 3 is muddy often, thereby can not immediately material be introduced 5 cold analysis of cold analysis still, otherwise can influence the quality of product.Conventional way is that to observe the look of the material of drawing in the cold analysis still material guiding tube 4 by the personnel of working online assorted, as long as it is muddy situation that black is arranged, so just, with the charging aperture 12 on free end plant reactor kettle 1 top of cold analysis still material guiding tube 4, muddy material is returned in the reactor kettle 1.That is to say,, put in advance, just the free end of cold analysis still material guiding tube 4 is placed in the cold analysis still charging aperture 51 of cold analysis still 5 except that behind a part of material at the charging aperture 12 that begins before cold analysis still 5 draws material, to need cold analysis still material guiding tube 4 is inserted in reactor kettle 1.Whether one of existing shortcoming of aforesaid operations mode, very difficult assurance return the material of previous muddiness to the degree in the reactor 1, can occur usually or to return liquid excessive or to return liquid insufficient; Two, can cause loss of material when cold analysis still material guiding tube 4 being moved from the charging aperture 12 of reactor kettle 1 to the process of the cold analysis still charging aperture 51 of cold analysis still 5; Two, working strength of workers is big, and is very harsh to workman's responsibility consciousness; Three, because of material drops down and can exert an influence to the working site in yard.
The applicant thinks that the problems referred to above are because cold analysis still and filter 3 respectively have a style of one's own, and lack each other due to the effectively connection.
Summary of the invention
Task of the present invention is to provide a kind of can prevent loss of material effectively, can avoid again the material of muddiness is introduced the reactor in the amino acids production of cold analysis still and the combining structure of cold analysis still.
Task of the present invention is finished like this, the reactor in a kind of amino acids production and the combining structure of cold analysis still, it comprises the reactor kettle, conveying mechanism with the discharging opening pipeline connection of reactor kettle, filter with the conveying mechanism pipeline connection, that connect and cold analysis still material guiding tube that be furnished with visor and the cold analysis still that is configured in a side of filter with the filter pipeline, be characterised in that: also include a control piper, one end of this control piper connects with described cold analysis still material guiding tube, the other end connects with the cold analysis still charging aperture of described cold analysis still, described control piper is provided with control valve and form, described cold analysis still material guiding tube reaches with described filter respectively and connects with the charging aperture of reactor kettle, and be provided with second control valve on cold analysis still material guiding tube, second control valve is positioned at the below of described visor.
The advantage of technical scheme provided by the present invention: initial at blowing, material muddiness or title black automatically can be introduced in the reactor kettle, and limpid material in time can be introduced the cold analysis still, thereby having abandoned in the prior art by means of the people is the operation format that moves cold analysis still material guiding tube, not only can not cause the waste of material, and can guarantee to enter into the cleaning of the material in the cold analysis still.
Description of drawings
Fig. 1 is a structure chart of the present invention.
Fig. 2 is the reactor in the amino acids production in the prior art and the combination assumption diagram of cold analysis still.
The specific embodiment
Ask for an interview Fig. 1, provided the reactor kettle 1 that has agitating device, on the discharging opening 11 of the bottom of reactor kettle 1, be furnished with baiting valve 111, between baiting valve 111 and the filter 3 by pipeline connection, conveying mechanism 2 is provided on this pipeline, and this conveying mechanism 2 is synthetic by motor 21 and pump 22 assembly.The bottom of filter 3 go out the end that the liquid interface first line of a couplet connects cold analysis still material guiding tube 4, and the other end of cold analysis still material guiding tube 4 is attached to the charging aperture 12 at reactor kettle 1 top, and on the pipeline of cold analysis still material guiding tube 4, be provided with the visor 41 and second control valve 42, wherein, second control valve 42 is positioned at the below of visor, the material that inherent filtration device 3 is drawn is that initial representation is that muddy material takes the lead in behind second control valve 42 entering then in the reactor kettle 1 again through visor 41.As technical essential of the present invention, on the pipeline of cold analysis still material guiding tube 4 and be positioned at second control valve 42 below connect an end of control piper 6, and the other end of control piper 6 connects with the cold analysis still charging aperture 51 of cold analysis still 5, also be provided with first control valve 61 and form 62 on control piper 6, both adjoin first, second control valve 61,42.
To produce taurine is example; taurine material after the reaction in the reactor kettle 1 will being finished is emitted when also cooling is analysed still 5 cold analysis; then open the baiting valve 111 of discharging opening 11; start conveying mechanism 2; by conveying mechanism 2 the taurine material being introduced filter 3 filters; open second control valve 42 simultaneously and close first control valve 61; the muddy material that comes from filter 3 is at the beginning returned to be guided in the reactor kettle 1; when examining by visor 41 when seeing limpid material; then close second control valve 42; open first control valve 61 simultaneously, make limpid taurine material introduce 5 cold analysis of cold analysis stills by control piper 6, after the cold analysis by cold analysis still baiting valve 52 blowings.Said process neither can be introduced the material of muddiness the cold analysis still and influence product quality, can not cause the waste of material again, and the personnel that work online are as long as open or close second control valve 42 and open or close first control valve 61 according to visor 41 in good time in good time, so working strength of workers is minimized.

Claims (1)

1. the reactor in the amino acids production and the combining structure of cold analysis still, it comprises reactor kettle (1), conveying mechanism (2) with discharging opening (11) pipeline connection of reactor kettle (1), filter (3) with conveying mechanism (2) pipeline connection, cold analysis still (5) with filter (3) pipeline connection and cold analysis still material guiding tube (4) that be furnished with visor (41) and the side that is configured in filter (3), it is characterized in that: also include a control piper (6), one end of this control piper (6) connects with described cold analysis still material guiding tube (4), the other end connects with the cold analysis still charging aperture (51) of described cold analysis still (5), described control piper (6) is provided with control valve (61) and form (62), described cold analysis still material guiding tube (4) reaches with described filter (3) respectively and connects with the charging aperture (12) of reactor kettle (1), and be provided with second control valve (42) on cold analysis still material guiding tube (4), second control valve (42) is positioned at the below of described visor (41).
CN2008102426840A 2008-12-30 2008-12-30 Combined construction of reactor and cold separation pot for producing amino acid product Expired - Fee Related CN101480600B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2008102426840A CN101480600B (en) 2008-12-30 2008-12-30 Combined construction of reactor and cold separation pot for producing amino acid product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2008102426840A CN101480600B (en) 2008-12-30 2008-12-30 Combined construction of reactor and cold separation pot for producing amino acid product

Publications (2)

Publication Number Publication Date
CN101480600A CN101480600A (en) 2009-07-15
CN101480600B true CN101480600B (en) 2011-04-13

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CN2008102426840A Expired - Fee Related CN101480600B (en) 2008-12-30 2008-12-30 Combined construction of reactor and cold separation pot for producing amino acid product

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2472780Y (en) * 2001-03-29 2002-01-23 王修立 Single pot type one-step process flow ammonium chloride crystallizing device
CN2820272Y (en) * 2005-08-19 2006-09-27 宜宾天原股份有限公司 Hydrazinehydrate oxidizing liquid concentration crystallizing still
CN201324631Y (en) * 2008-12-30 2009-10-14 江苏远洋化学有限公司 Combinative structure of reaction kettle and crystallization kettle in amino acid product manufacture

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2472780Y (en) * 2001-03-29 2002-01-23 王修立 Single pot type one-step process flow ammonium chloride crystallizing device
CN2820272Y (en) * 2005-08-19 2006-09-27 宜宾天原股份有限公司 Hydrazinehydrate oxidizing liquid concentration crystallizing still
CN201324631Y (en) * 2008-12-30 2009-10-14 江苏远洋化学有限公司 Combinative structure of reaction kettle and crystallization kettle in amino acid product manufacture

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Owner name: JIANGSU YUANYANG PHARMACEUTICAL CO., LTD.

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Effective date: 20120331

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Address after: 215531, Jiangsu, Changshou City province Tong Industrial Park, 204 National Road, 948.5 kilometers

Patentee after: Jiangsu Yuanyang Pharmaceutical Co.,Ltd.

Address before: 215531, Jiangsu, Changshou City province Tong Industrial Park, 204 National Road, 934.5 kilometers

Patentee before: Jiangsu Yuanyang Chemistry Co., Ltd.

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110413

Termination date: 20161230

CF01 Termination of patent right due to non-payment of annual fee