CN101469511B - Superabsorbent soft antibacterial textile - Google Patents
Superabsorbent soft antibacterial textile Download PDFInfo
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- CN101469511B CN101469511B CN2007103025250A CN200710302525A CN101469511B CN 101469511 B CN101469511 B CN 101469511B CN 2007103025250 A CN2007103025250 A CN 2007103025250A CN 200710302525 A CN200710302525 A CN 200710302525A CN 101469511 B CN101469511 B CN 101469511B
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- antibacterial textile
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Abstract
The invention discloses an ultra-water absorbing soft antibiosis textile. The textile comprises a fiber including polyester compounds on the surface and an antibiosis compound adhering on the fiber, wherein the polyester compound is a compound with hydrophilicity and pliability at the same time. The textile product has long-lasting water absorptivity, ultra pliability, excellent dyeing fastness and antibiosis performance, very soft hand-feeling.
Description
Technical field
The present invention relates to a kind of superabsorbent soft antibacterial textile.
Background technology
Continuous progress and development along with human society; To the requirement of textiles not merely is that to rest on resisting cold warming; The raising of products export standard after the China's entry into the WTO; This presses for the fact of solution, its comfortableness, the functional attention that more and more receives people to have caused the comprehensive lifting of state's inner facing material product specification needs thus more.As the textiles of underwear purposes, its comfortableness requires higher, not only requires to have ultra soft hand feeling, and its water imbibition, anti-microbial property are all had very high requirement.Simultaneously can not produce injury to skin, health again, content of formaldehyde requirement such as can not exceed standard is more and more paid attention to by people.
Summary of the invention
The object of the present invention is to provide a kind of water imbibition, flexibility, superabsorbent soft antibacterial textile that anti-microbial property is good.
Solution of the present invention is:
A kind of superabsorbent soft antibacterial textile is characterized in that: in the fiber of forming this textiles, have the fiber that the polyesters compound is contained on the surface, said polyesters compound is the compound that has hydrophily and flexibility simultaneously concurrently; The antibiotic property compound is attached on the fiber.
The antibiotic property compound is attached to being attached to fiber surface on the fiber or being absorbed in the fiber.
The antibiotic property compound is one or more in zinc and compound, silver and compound thereof, titanium and compound thereof, quaternary ammonium salt, the shitosan compounds.
Zinc and compound thereof, silver and compound thereof, titanium and compound thereof, quaternary ammonium salt, shitosan compounds are through silicone based, type siloxane, acrylic compounds or the polyurethane binding surface attached to fiber.
Superabsorbent soft antibacterial textile after No. 0217.103, JIS L washing standard wash 10 times to the quiet bacterium activity value of staphylococcus aureus more than 2.2.
Superabsorbent soft antibacterial textile washs 20 water imbibitions of standard wash for No. 0217.103 below 1 second through JIS L.
The fiber of forming this product is one or more in terylene, cation-modified terylene, nylon, acrylic fibers, cellulose fibre and the regenerated celulose fibre.
Having the fiber with respect to fabric weight 20% at least in the fiber of composition textiles is the fiber that contains the polyesters composition.
Said polyesters composition is one or more in PETG, cationic-dyeable PETG, polytrimethylene terephthalate, cationic-dyeable polytrimethylene terephthalate, polybutylene terephthalate (PBT), the cationic-dyeable polybutylene terephthalate (PBT), and its content accounts for 30% at least in the fiber that contains the polyesters composition.
Production of products process of the present invention comprises the following steps: successively
A. grey cloth is prepared
B. concise
Scouring agent 0.5-6g/l
Temperature 50-95 ℃
C. typing in the middle of: under temperature 150-190 ℃ condition, handle 0.5-3min;
D. dyeing: 5-80min dyes under temperature 50-135 ℃ condition;
E. dry: dry 0.5-2min under temperature 100-140 ℃ condition;
F. the modulation of resin finishing liquid: with hydrophily, flexibility compound (one or more in polyesters, silicone based, the polyurethanes compound); Antibiotic property compound (one or more in zinc and compound thereof, silver and compound thereof, titanium and compound thereof, quaternary ammonium salt, the shitosan compounds); Adhesive (one or more in polyurethanes, silicone based, isocyanates, the acrylic compounds); PH regulator agent (acetic acid, citric acid etc. wherein one or more) and soft water according to following mixed, stir, be modulated into suction soft antibacterial working fluid.
Suction soft antibacterial working fluid (1L)
All the other all are soft water, and ready textiles in the steps A is immersed in the suction soft antibacterial working fluid (flooding about 1.0 kilograms fabric in every liter of working solution) that is modulated into, and through physical action working fluid are adsorbed on fiber surface;
G. heat treatment: heat treatment is 0.5～5 minute under the condition of 80～180 ℃ of temperature, makes suction softener, antiseptic be attached to filamentary surface, fully reaction, curing.
Product of the present invention has durable water imbibition, ultra-flexible and excellent colorfastness; Because the polyster fibre or the cation-modified terylene of soft resin of the suction of polyesters and blending product have good compatibility; And can obtain good feel and durable water imbibition, can not influence colorfastness simultaneously yet.When using the water absorbing agent beyond the polyesters compound of the present invention in order to obtain soft hand feeling, good water imbibition the time use amount of medicament bigger, thereby cause the decline of fastness.Product of the present invention has excellent anti-microbial property, and feel is very soft.
The specific embodiment:
Below in conjunction with accompanying drawing and embodiment the present invention is described further.
Fig. 1 is the flow chart of cation-modified terylene, acrylic fibres dyeing among the embodiment 1.
Fig. 2 is the flow chart of regenerated cellulose dyeing among the embodiment 1.
Fig. 3 is the flow chart of cation-modified terylene, acrylic fibres dyeing among the embodiment 2.
Fig. 4 is the flow chart of regenerated cellulose dyeing among the embodiment 2.
Fig. 5 is the flow chart of cation-modified terylene, acrylic fibres dyeing in the comparative example.
Fig. 6 is the flow chart of regenerated cellulose dyeing among the embodiment.
Embodiment 1:
A kind of machining manufacture of superabsorbent soft antibacterial textile may further comprise the steps:
(1) preparation of textiles to be processed: cation-modified terylene, acrylic fibers, regenerated celulose fibre blended fabric;
(2) kiering (dyeing machine)
Scouring agent TS-G2 2g/l
Temperature * time 80 * 20min
(3) typing in the middle of: under the condition of 180 ℃ of temperature, handle 1.2min;
(4) dyeing:
Cation-modified terylene, acrylic fibres dyeing
NICHILON YELLOW TR 0.1 (Japan's day one-tenth changes into Company products)
NICHILON BLACK TR200% 3.0; (Japan's day one-tenth changes into Company products)
Regenerated cellulose dyeing
Active yellow 3 R S 0.21
Reactive red B-2BF 0.07
Reactive black G2RC (150%) 2.5;
(5) drying: dry 1.2min under the condition of 130 ℃ of temperature;
(6) modulation of resin finishing liquid:
Hydrophily, flexibility compound F 17-hydroxy-corticosterone EARN ASR (Rudoiph's product) 15g/l
Antibiotic property compound TH-1 (solar corona chemical products) 14g/l
Citric acid (pH regulator agent) 0.4g/l
All the other all are soft water, and ready textiles in the step (1) is immersed in the suction soft antibacterial working fluid (flooding about 1.0 kilograms fabric in every liter of working solution) that is modulated into, and through physical action working fluid are adsorbed on fiber surface;
(7) heat treatment: heat treatment is 1 minute under the condition of 130 ℃ of temperature, makes suction softener, antiseptic be attached to filamentary surface, and fully reaction, curing get this product.
Through resulting product of above procedure of processing, have very soft hand feeling, after JISL No. 0217.103 (agent of JAFET standard wash) the washing standard wash 10 times to the quiet bacterium activity value (JIS L 1902 bacterium liquid absorption processes) of staphylococcus aureus more than 2.2.Wash 20 water imbibitions below 1 second (JIS L 1907-1994 drip method).And has excellent colorfastness.
Test result is following:
Embodiment 2:
(1) preparation of textiles to be processed: cation-modified terylene, acrylic fibers, regenerated celulose fibre blended fabric;
(2) concise (continous mode scouring machine)
Scouring agent TS-G2 2g/l
80 ℃ of temperature
(3) typing in the middle of: under the condition of 180 ℃ of temperature, handle 1.2min;
(4) dyeing:
Cation-modified terylene, acrylic fibres dyeing
NICHILON?YELLOW?TR 0.1
NICHILON?BLACK?TR200％ 3.0
Regenerated cellulose dyeing
Active yellow 3 R S 0.21
Reactive red B-2BF 0.07
Reactive black G2RC (150%) 2.5;
(5) drying: dry 1.2min under the condition of 130 ℃ of temperature;
(6) modulation of resin finishing liquid:
Hydrophily, flexibility compound F 17-hydroxy-corticosterone EARN ASR (Rudoiph's product) 15g/l
Antibiotic property compound S ANT-T94 (Japanese Nagase ChemTex product) 20g/l
Citric acid (pH regulator agent) 0.4g/l
All the other all are soft water, and ready textiles in the step (1) is immersed in the suction soft antibacterial working fluid (flooding about 1.0 kilograms fabric in every liter of working solution) that is modulated into, and through physical action working fluid are adsorbed on fiber surface;
(7) heat treatment: heat treatment is 1 minute under the condition of 130 ℃ of temperature, makes suction softener, antiseptic be attached to filamentary surface, and fully reaction, curing get this product.
Through resulting product of above procedure of processing, have very soft hand feeling, 20 water imbibitions of No. 0217.103 standard wash of JISL are below 1 second (JIS L 1907-1994 drip method).And has excellent colorfastness.
Test result is following:
Comparative example:
(1) preparation of textiles to be processed: cation-modified terylene, acrylic fibers, regenerated celulose fibre blended fabric;
(2) concise (dyeing machine)
Scouring agent TS-G2 2g/l
80 ℃ of temperature
(3) typing in the middle of: under the condition of 180 ℃ of temperature, handle 1.2min;
(4) dyeing:
Cation-modified terylene, acrylic fibres dyeing
NICHILON?YELLOW?TR 0.1
NICHILON?BLACK?TR200％ 3.0
Regenerated cellulose dyeing
Active yellow 3 R S 0.21
Reactive red B-2BF 0.07
Reactive black G2RC (150%) 2.5;
(5) drying: dry 1.2min under the condition of 130 ℃ of temperature;
(6) modulation of resin finishing liquid:
Water imbibition organic siliconresin 15g/l
SANT-T94 (Japanese Nagase ChemTex product) 20
Citric acid (pH regulator agent) 0.4g/l
All the other all are soft water, and ready textiles in the step (1) is immersed in the suction soft antibacterial working fluid (flooding about 1.0 kilograms fabric in every liter of working solution) that is modulated into, and through physical action working fluid are adsorbed on fiber surface;
(7) heat treatment: heat treatment is 1 minute under the condition of 130 ℃ of temperature.
Through the resulting product of above procedure of processing, feel is harder, and the initial stage water imbibition is more than 1 second, water imbibition more than 1 second after No. 0217.103 standard wash of JIS L 20 times (JIS L1907-1994 drip method).
Test result is following:
Through finding out that with the contrast of comparative example product of the present invention has good colorfastness, durable water imbibition and ultra soft hand feeling.
Claims (6)
1. superabsorbent soft antibacterial textile is characterized in that: in the fiber of forming this textiles, have the fiber that the polyesters compound is contained on the surface, said polyesters compound is the compound that has hydrophily and flexibility simultaneously concurrently; The antibiotic property compound is attached on the fiber; The antibiotic property compound is one or more in zinc and compound, titanium and compound thereof, quaternary ammonium salt, the shitosan compounds; 20 water imbibitions of JIS L No. 0217.103 washing standard wash are below 1 second; After No. 0217.103, the JIS L washing standard wash 10 times to the quiet bacterium activity value of staphylococcus aureus more than 2.2.
2. superabsorbent soft antibacterial textile according to claim 1 is characterized in that: the antibiotic property compound is attached to being attached to fiber surface on the fiber or being absorbed in the fiber.
3. superabsorbent soft antibacterial textile according to claim 1 and 2 is characterized in that: zinc and compound thereof, titanium and compound thereof, quaternary ammonium salt, shitosan compounds are through silicone based, acrylic compounds or the polyurethane binding surface attached to fiber.
4. superabsorbent soft antibacterial textile according to claim 1 and 2 is characterized in that: the fiber of forming this product is one or more in terylene, cation-modified terylene, nylon, acrylic fibers, cellulose fibre and the regenerated celulose fibre.
5. superabsorbent soft antibacterial textile according to claim 1 and 2 is characterized in that: having the fiber with respect to fabric weight 20% at least in the fiber of composition textiles is the fiber that contains the polyesters composition.
6. superabsorbent soft antibacterial textile according to claim 5; It is characterized in that: said polyesters composition is one or more in PETG, cationic-dyeable PETG, polytrimethylene terephthalate, cationic-dyeable polytrimethylene terephthalate, polybutylene terephthalate (PBT), the cationic-dyeable polybutylene terephthalate (PBT), and its content accounts for 30% at least in the fiber that contains the polyesters composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007103025250A CN101469511B (en) | 2007-12-25 | 2007-12-25 | Superabsorbent soft antibacterial textile |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007103025250A CN101469511B (en) | 2007-12-25 | 2007-12-25 | Superabsorbent soft antibacterial textile |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101469511A CN101469511A (en) | 2009-07-01 |
| CN101469511B true CN101469511B (en) | 2012-07-04 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007103025250A Expired - Fee Related CN101469511B (en) | 2007-12-25 | 2007-12-25 | Superabsorbent soft antibacterial textile |
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Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102031578A (en) * | 2009-09-25 | 2011-04-27 | 上海德福伦化纤有限公司 | Method for producing organic-silicone-modified hydrophilic abnormity polyester fiber |
| CN102796355A (en) * | 2011-06-29 | 2012-11-28 | 深圳光启高等理工研究院 | Antibacterial plastic and preparation method thereof |
| CN102433603A (en) * | 2011-08-09 | 2012-05-02 | 上海贵达科技有限公司 | Antibacterial, hydroscopic and perspiratory polyester fiber with self-hydrophilicity |
| CN103422237A (en) * | 2012-05-25 | 2013-12-04 | 常州老三集团有限公司 | Fabric and dyeing and finishing process thereof |
| CN103668955B (en) * | 2012-09-24 | 2015-07-15 | 上海韬鸿化工科技有限公司 | Padding-process antibacterial polyester fabric and preparation method thereof |
| CN104233601B (en) * | 2013-06-14 | 2017-06-30 | 东丽纤维研究所（中国）有限公司 | A kind of super soft knitted fabric and its processing method |
| CN108049217A (en) * | 2017-12-19 | 2018-05-18 | 上海嘉麟杰纺织品股份有限公司 | A kind of individual layer is felt nice and cool mesh antibacterial fabric colouring method |
| CN109771314A (en) * | 2019-01-02 | 2019-05-21 | 青蛙王子（福建）婴童护理用品有限公司 | Long-acting anti-, antibacterial wet tissue of one kind and preparation method thereof |
| CN109826005A (en) * | 2019-01-28 | 2019-05-31 | 盐城工学院 | A kind of antibacterial fabric finishing method of moisture absorbing and sweat releasing |
| CN110331582A (en) * | 2019-07-03 | 2019-10-15 | 东华大学 | A kind of super hydrophilic anti-bacterial fibre cellulose fiber and preparation method thereof |
| CN113584884B (en) * | 2021-08-25 | 2023-03-31 | 杭州萧山丝化印染有限公司 | Antibacterial functional fabric and preparation method thereof |
| CN114808486B (en) * | 2022-06-09 | 2024-06-25 | 杭州天瑞印染有限公司 | Energy-saving low-consumption steaming-free printing and color fixing process for cotton fabric |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1538003A (en) * | 2003-10-17 | 2004-10-20 | 信阳市环宇内衣服装厂 | Chitin finished fabric and its manufacturing method |
| CN1563553A (en) * | 2004-03-30 | 2005-01-12 | 东华大学 | Nano functional finishing agent for textile, preparation method and application |
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2007
- 2007-12-25 CN CN2007103025250A patent/CN101469511B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1538003A (en) * | 2003-10-17 | 2004-10-20 | 信阳市环宇内衣服装厂 | Chitin finished fabric and its manufacturing method |
| CN1563553A (en) * | 2004-03-30 | 2005-01-12 | 东华大学 | Nano functional finishing agent for textile, preparation method and application |
Non-Patent Citations (1)
| Title |
|---|
| 董永春.聚酯类纺织助剂.《纺织助剂化学与应用》.中国纺织出版社,2007,(第1版),293. * |
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