CN101349502B - Tunnel kiln for preparing microwave ferrite material - Google Patents

Tunnel kiln for preparing microwave ferrite material Download PDF

Info

Publication number
CN101349502B
CN101349502B CN2008100682912A CN200810068291A CN101349502B CN 101349502 B CN101349502 B CN 101349502B CN 2008100682912 A CN2008100682912 A CN 2008100682912A CN 200810068291 A CN200810068291 A CN 200810068291A CN 101349502 B CN101349502 B CN 101349502B
Authority
CN
China
Prior art keywords
degree
temperature
minute
tunnel
rate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN2008100682912A
Other languages
Chinese (zh)
Other versions
CN101349502A (en
Inventor
李汉国
李海东
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Huayang Communication Technology Co., Ltd.
Original Assignee
SHENZHEN HUAYANG COMMUNICATION TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHENZHEN HUAYANG COMMUNICATION TECHNOLOGY Co Ltd filed Critical SHENZHEN HUAYANG COMMUNICATION TECHNOLOGY Co Ltd
Priority to CN2008100682912A priority Critical patent/CN101349502B/en
Publication of CN101349502A publication Critical patent/CN101349502A/en
Application granted granted Critical
Publication of CN101349502B publication Critical patent/CN101349502B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Abstract

The invention discloses a tunnel kiln for the preparation of microwave ferrite material, which comprises an open kiln body, a microcomputer temperature control device and a delivery mechanism, wherein the delivery mechanism is located in the open kiln body, the open kiln body is provided with a heating element, and the heating temperature of the heating element is controlled by the microcomputer temperature control device. When the tunnel kiln for the preparation of microwave ferrite material in the invention sinters samples, the samples operate along the preset sintering curved line in the open kiln body, and each sample is sintered in the kiln under the same condition, thereby having excellent consistency, and not existing difference among furnaces.

Description

Tunnel kiln for preparing microwave ferrite material
Technical field
The present invention relates to the Ferrite Material preparation and use equipment, relate in particular to a kind of tunnel kiln for preparing microwave ferrite material.
Background technology
At present, domestic sintered microwave ferrite all adopts batch-type furnace or bell jar stove.The batch-type furnace capacity is less, poor temperature uniformity, and the producer that adopts is few at present.The bell jar heat size is bigger, and temperature homogeneity is good, and the producer of employing is more and more, but exposes unsurmountable defective in large-scale production.Though bell jar stove good uniformity in this stove exists evident difference between this stove and next stove.Ferrite phase shifter for example, it inserts phase shift and exist evident difference between stove and stove.Therefore, the sintering technology of bell jar stove has brought many troubles for the batch process of phase shifter, circulator and isolator, because the finite capacity of bell jar stove needs to burn in batches, and it is all different that every batch of burning is come out, thereby this shortcoming is that bell jar stove sintering technology itself can't overcome.
Summary of the invention
The object of the present invention is to provide a kind of tunnel kiln for preparing microwave ferrite material of microwave ferrite sintering high conformity.
For achieving the above object, technical scheme of the present invention is:
A kind of tunnel kiln for preparing microwave ferrite material is provided; comprise open kiln body; the tunnel thorax that described cellar for storing things body is limited; microcomputer temperature control device and be positioned at the connecting gear of described tunnel thorax; described tunnel thorax is divided into low temperature binder removal district; high temperature sintering district and cooling area; low temperature binder removal section length is 370 centimetres; the high temperature sintering section length is 140 centimetres; cooling area length is 160 centimetres; be provided with heating element heater in the described tunnel thorax; described heating element heater is provided with the heating rod catch net outward; described microcomputer temperature control device is preset with the sintering curre data of the described heating element heater heating-up temperature of control; described sintering curre data comprise that the binder removal time of low temperature binder removal is 19 hours; temperature rises to 1300 degree; wherein heat up since 25 degree; 25 the degree to 400 the degree between heating rate be 1.04 the degree/minute; 6 hours times spent; 400 the degree to 1100 the degree between heating rate be 2.91 the degree/minute; 4 hours times spent; 1100 the degree to 1200 the degree between heating rate be 0.83 the degree/minute; 2 hours times spent; 1200 the degree to 1300 the degree between heating rate be 0.24 the degree/minute; 7 hours times spent; the sintering time in high temperature sintering district is 7 hours; temperature constant is at 1300 degree; the temperature fall time of cooling area is 7 hours; wherein 1300 the degree to 1100 the degree between rate of temperature fall be 3.33 the degree/minute; 1 hour time spent; 1100 the degree to 840 the degree between rate of temperature fall be 4.33 the degree/minute; 1 hour time spent; 840 the degree to 600 the degree between rate of temperature fall be 4 the degree/minute; 1 hour time spent; 600 the degree to 400 the degree between rate of temperature fall be 3.33 the degree/minute; 1 hour time spent; 400 the degree to 200 the degree between rate of temperature fall be 3.23 the degree/minute; 1 hour time spent; 200 the degree to 100 the degree between rate of temperature fall be 1.67 the degree/minute; 1 hour time spent; 100 the degree to 0 the degree between rate of temperature fall be 1.67 the degree/minute; 1 hour time spent, each sample that enters described tunnel thorax is under the identical condition in the tunnel thorax and is sintered.
Described open kiln body adopts poly-light brick of high alumina and the preparation of light-weight mullite brick.
Described heating element heater is a carbonization silicon heating rod.
Described open kiln body top is provided with chimney, and the bottom is provided with support.
Described connecting gear is manual connecting gear or autotransmitter structure.
Described manual connecting gear comprises handle and pushing plate, by the motion of handle control driving-belt.
Described microcomputer temperature control device is a KST-33-15 type temperature controller.
During tunnel kiln for preparing microwave ferrite material sintered sample of the present invention, sample moves along pre-set sintering curre in open kiln body, each sample is in to be sintered under the identical condition in kiln and forms, thereby uniformity is better, does not have the difference between stove and the stove.
Description of drawings
Fig. 1 is a tunnel kiln for preparing microwave ferrite material structural representation of the present invention;
Fig. 2 is the microwave ferrite sintering curre.
The primary clustering symbol description
1, handle 2, tunnel thorax 3, Yao Bi
4, support 5, chimney 6, heating rod catch net
7, carbonization silicon heating rod 8, KST-33-15 type temperature controller
9, pushing plate
The specific embodiment
See also Fig. 1, tunnel kiln for preparing microwave ferrite material, comprise open kiln body, KST-33-15 type temperature controller 8 and manual connecting gear, open kiln body top is provided with chimney 5, the bottom is provided with support 4, open kiln body comprises tunnel thorax 2 and kiln wall 3, the kiln wall adopts poly-light brick of high alumina and the preparation of light-weight mullite brick, manually connecting gear comprises handle 1 and pushing plate 9, motion by handle control driving-belt, pushing plate is positioned at tunnel thorax 2, handle 1 is positioned at outside the tunnel thorax 2, and open kiln body is divided into low temperature binder removal district, high temperature sintering district and cooling area, low temperature binder removal section length is 370 centimetres, the high temperature sintering section length is 140 centimetres, and cooling area length is 160 centimetres; Be provided with carbonization silicon heating rod 7 in the open kiln body, carbonization silicon heating rod is provided with heating rod catch net 6 outward, and the heating-up temperature of carbonization silicon heating rod is by 8 controls of KST-33-15 type temperature controller.
KST-33-15 type temperature controller, by the controllable silicon power supply, the temperature control accuracy can be in ± 1 ℃.
If manual connecting gear is replaced with the automation connecting gear, can also further improve consistency of product.
The kiln wall material adopts poly-light brick of one-level high alumina and light-weight mullite brick, high insulating effect, and temperature is even in the stove.Heating element heater adopts the SIC heating rod, and the barred body heating evenly.Because there is the temperature difference in the obstruct of pushing plate between the group up and down, even for making in the same cross section of open kiln body temperature, will organize heater down and improve 25 ℃ of temperature, make open kiln body central portion temp uniformity like this.
The microwave ferrite preparation method:
Before kiln begins to burn, earlier sintering curre is as shown in Figure 2 imported microcomputer, the ferrite sample of forming is put into the sintering alms bowl, pendulum is in the centre near alms bowl as far as possible, pushed ahead an alms bowl every one hour then, sample to be burnt is covered the whole process of tunnel cave, and sample is promptly accused sintering and finished.

Claims (7)

1. a tunnel kiln for preparing microwave ferrite material is characterized in that, comprising:
Tunnel thorax, microcomputer temperature control device that open kiln body, described cellar for storing things body are limited and the connecting gear that is positioned at described tunnel thorax;
Described tunnel thorax is divided into low temperature binder removal district, high temperature sintering district and cooling area, and low temperature binder removal section length is 370 centimetres, and the high temperature sintering section length is 140 centimetres, and cooling area length is 160 centimetres;
Be provided with heating element heater in the described tunnel thorax, described heating element heater is provided with the heating rod catch net outward, and described microcomputer temperature control device is preset with the sintering curre data of the described heating element heater heating-up temperature of control;
Described sintering curre data comprise:
The binder removal time of low temperature binder removal is 19 hours, temperature rises to 1300 degree, wherein heat up since 25 degree, 25 degree to heating rate between 400 degree be 1.04 degree/minute, 6 hours times spent, 400 the degree to 1100 the degree between heating rate be 2.91 the degree/minute, 4 hours times spent, 1100 the degree to 1200 the degree between heating rate be 0.83 the degree/minute, 2 hours times spent, 1200 the degree to 1300 the degree between heating rate be 0.24 the degree/minute, 7 hours times spent;
The sintering time in high temperature sintering district is 7 hours, and temperature constant is at 1300 degree;
The temperature fall time of cooling area is 7 hours, wherein 1300 the degree to 1100 the degree between rate of temperature fall be 3.33 the degree/minute, 1 hour time spent, 1100 the degree to 840 the degree between rate of temperature fall be 4.33 the degree/minute, 1 hour time spent, 840 the degree to 600 the degree between rate of temperature fall be 4 the degree/minute, 1 hour time spent, 600 the degree to 400 the degree between rate of temperature fall be 3.33 the degree/minute, 1 hour time spent, 400 the degree to 200 the degree between rate of temperature fall be 3.23 the degree/minute, 1 hour time spent, 200 the degree to 100 the degree between rate of temperature fall be 1.67 the degree/minute, 1 hour time spent, 100 the degree to 0 the degree between rate of temperature fall be 1.67 the degree/minute, 1 hour time spent;
Each sample that enters described tunnel thorax is under the identical condition in the tunnel thorax and is sintered.
2. tunnel kiln for preparing microwave ferrite material according to claim 1 is characterized in that: described open kiln body adopts poly-light brick of high alumina and the preparation of light-weight mullite brick.
3. tunnel kiln for preparing microwave ferrite material according to claim 1 is characterized in that: described heating element heater is a carbonization silicon heating rod.
4. tunnel kiln for preparing microwave ferrite material according to claim 1 is characterized in that: described open kiln body top is provided with chimney, and the bottom is provided with support.
5. tunnel kiln for preparing microwave ferrite material according to claim 1 is characterized in that: described connecting gear is manual connecting gear or autotransmitter structure.
6. tunnel kiln for preparing microwave ferrite material according to claim 5 is characterized in that: described manual connecting gear comprises handle and pushing plate, by the motion of handle control driving-belt.
7. tunnel kiln for preparing microwave ferrite material according to claim 1 is characterized in that: described microcomputer temperature control device is a KST-33-15 type temperature controller.
CN2008100682912A 2008-07-04 2008-07-04 Tunnel kiln for preparing microwave ferrite material Active CN101349502B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2008100682912A CN101349502B (en) 2008-07-04 2008-07-04 Tunnel kiln for preparing microwave ferrite material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2008100682912A CN101349502B (en) 2008-07-04 2008-07-04 Tunnel kiln for preparing microwave ferrite material

Publications (2)

Publication Number Publication Date
CN101349502A CN101349502A (en) 2009-01-21
CN101349502B true CN101349502B (en) 2010-10-20

Family

ID=40268380

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2008100682912A Active CN101349502B (en) 2008-07-04 2008-07-04 Tunnel kiln for preparing microwave ferrite material

Country Status (1)

Country Link
CN (1) CN101349502B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102243020A (en) * 2011-05-04 2011-11-16 成都晶元新材料技术有限公司 Continuous type microwave auxiliary sintering furnace and method
CN104154742A (en) * 2014-09-03 2014-11-19 江苏宇达环保科技股份有限公司 SCR fully-automatic temperature control roller electrical kiln

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106679412A (en) * 2016-12-30 2017-05-17 重庆凌达磁材科技有限公司 Temperature control type full-automatic two-layer electric heating roller kiln

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102243020A (en) * 2011-05-04 2011-11-16 成都晶元新材料技术有限公司 Continuous type microwave auxiliary sintering furnace and method
CN104154742A (en) * 2014-09-03 2014-11-19 江苏宇达环保科技股份有限公司 SCR fully-automatic temperature control roller electrical kiln
CN104154742B (en) * 2014-09-03 2016-04-13 江苏宇达环保科技股份有限公司 A kind of SCR Full-automatic temp-control roller rod electrical kiln

Also Published As

Publication number Publication date
CN101349502A (en) 2009-01-21

Similar Documents

Publication Publication Date Title
CN102517624A (en) Multi-segment temperature control crystal growing furnace
CN101349502B (en) Tunnel kiln for preparing microwave ferrite material
CN104729293A (en) Flowing atmosphere hot/cold impact sintering resistance furnace
CN109867433B (en) Efficient screening system and method for glass components
CN208949130U (en) A kind of quartz glass plate continuous induction melting furnace of homogeneous heating
CN107976061A (en) A kind of vertical ceramic firing heating unit of continous way and heating means
CN103716923B (en) A kind of ceramic electric heating heating carrier and preparation method thereof
CN110220380A (en) A kind of use for laboratory high throughput vacuum heat treatment furnace
CN201476536U (en) Sintering furnace
CN102226644B (en) High-temperature sintering push plate kiln capable of working continuously
CN103134319A (en) Process of silver alloy intermediate frequency smelting of furnace graphite crucible
CN204574785U (en) Flowing atmosphere thermal shock sintering resistance furnace
CN101157545A (en) Method for doping polycrystalline alumina ceramics
CN101420801A (en) Graphite electrode with quasi-ultra-high power
CN101701853B (en) Method for measuring heat treatment degree by judging final temperature of thermal kiln furnace
CN100489162C (en) Falling crucible method growth process for lead molybdate single crystal
WO1993016571A1 (en) Microwave processing materials
CN103673601A (en) Heterogeneous multi-layer crucible
CN203820923U (en) Zirconia ceramic tile for thermal-insulation layer of sapphire furnace
CN207922844U (en) A kind of vertical ceramic firing heating device of continous way
CN203177679U (en) Multidirectional temperature control device used for sintering furnace
CN101125681A (en) Method for preparing partly stable zirconium dioxide
CN211290997U (en) Single-channel vertical heating furnace
CN202829804U (en) Preparation furnace for optical glass
CN102849919A (en) Optical glass preparation furnace

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee
CP02 Change in the address of a patent holder

Address after: 518000 Guangdong city of Shenzhen province Nanshan District Shekou Shao Di Road No. 1 Chiwan Industrial Park E building two floor

Patentee after: Shenzhen Huayang Communication Technology Co., Ltd.

Address before: Nanshan District Xili Town, Shenzhen city Guangdong province 518000 new village Wang Tong Industrial Zone 25 Building 5 North Building

Patentee before: Shenzhen Huayang Communication Technology Co., Ltd.

C56 Change in the name or address of the patentee

Owner name: HUAYANG TECHNOLOGY DEVELOPMENT CO., LTD.

Free format text: FORMER NAME: SHENZHEN HUAYANG COMMUNICATION TECHNOLOGY CO., LTD.

CP03 Change of name, title or address

Address after: 518000 Guangdong city of Shenzhen province Nanshan District Chiwan Shekou Shao Di Road No. 1 Chiwan Industrial Park E Building 1 floor

Patentee after: Shenzhen Hua Yang Communications, Inc

Address before: 518000 Guangdong city of Shenzhen province Nanshan District Shekou Shao Di Road No. 1 Chiwan Industrial Park E building two floor

Patentee before: Shenzhen Huayang Communication Technology Co., Ltd.

C56 Change in the name or address of the patentee

Owner name: SHENZHEN HUAYANG COMMUNICATION TECHNOLOGY CO., LTD

Free format text: FORMER NAME: HUAYANG TECHNOLOGY DEVELOPMENT CO., LTD.

CP01 Change in the name or title of a patent holder

Address after: 518000 Guangdong city of Shenzhen province Nanshan District Chiwan Shekou Shao Di Road No. 1 Chiwan Industrial Park E Building 1 floor

Patentee after: Shenzhen Huayang Communication Technology Co., Ltd.

Address before: 518000 Guangdong city of Shenzhen province Nanshan District Chiwan Shekou Shao Di Road No. 1 Chiwan Industrial Park E Building 1 floor

Patentee before: Shenzhen Hua Yang Communications, Inc