CN101328426A - Formula of emulsified heavy oil - Google Patents
Formula of emulsified heavy oil Download PDFInfo
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- CN101328426A CN101328426A CNA2007100696516A CN200710069651A CN101328426A CN 101328426 A CN101328426 A CN 101328426A CN A2007100696516 A CNA2007100696516 A CN A2007100696516A CN 200710069651 A CN200710069651 A CN 200710069651A CN 101328426 A CN101328426 A CN 101328426A
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Abstract
The invention relates to a formula of emulsified heavy oil. The formula consists of heavy oil, water and an addition agent, wherein the percentages by weight of the compositions of the formula include: 69.9 to 89.9 percent of the heavy oil, 10 to 30 percent of the water and 0.1 percent of the addition agent; moreover, the addition agent comprises the following compositions in portion by weight: 6 to 20 portions of cobalt iso-octoate, 6 to 20 portions of manganese iso-octoate, 1 to 10 portions of nickel naphthenate, 35 to 65 portions of sorbitan monooleate, 4 to 8 portions of sorbitan polyoxyethylene monooleate, 1 to 2 portions of nonyl phenol polyoxyethylene (6) ether, 4 to 8 portions of sodium hydroxide, 2 to 4 portions of xylene, 1 to 6 portions of methanol and 1 portion of sunset red. The formula has the advantages of reasonable proportioning, advanced technological method, low price, high stability and catalytic and combustion-supporting effects.
Description
Technical field
The present invention relates to a kind of prescription of emulsification heavy oil, the invention belongs to a kind of Emulsification of Fuel Oil preparation and utilisation technology in chemical industry, the energy.
Background technology
" fuel-water emulsifying " technology is exactly a fuel economy oil, reduce to consume, and the advanced power-saving technology of environment protection standard, our country researched and developed and uses its technology intermittently from the sixties, but because multiple factor does not become effective energy-conservation form.During "the 10th five-years", National Development and Reform Committee releases technology for mixing water in heavy oil, but makes slow progress, and the technology that this is energy-conservation and environmental protection is dual is not also brought economic benefit, environmental benefit, social benefit for our country at present.At present domestic still not have flameholding, storage time longer, the emulsification heavy oil report of emulsify well.
Summary of the invention
Technical problem to be solved by this invention provides a kind of reasonable ratio, processing method advanced person, and product price is low, and stability is high, and possesses the prescription of the emulsification heavy oil of catalysis, combustion-supporting effect.
The present invention solves the problems of the technologies described above the prescription that the technical scheme that is adopted is this emulsification heavy oil, its prescription characteristics are: be made up of heavy oil, water and additive, wherein, the weight percent of each component is: heavy oil 69.9%-89.9%, water 10%-30%, additive 0.1%; Additive is by cobalt iso-octoate, manganese iso-octoate, nickel naphthenate, sorbitan monooleate, the anhydrous sorbitol Aceonon 300 MO, tough basic phenol polyethenoxy 6 ethers, sodium hydroxide, dimethylbenzene, methyl alcohol, the red composition of the setting sun, wherein, the shared parts by weight of each component are: cobalt iso-octoate 6-20 part, manganese iso-octoate 6-20 part, nickel naphthenate 1-10 part, the anhydrous sorbitol list has acid esters 35-65 part, anhydrous sorbitol Aceonon 300 MO 4-8 part, tough basic phenol polyethenoxy 6 ether 1-2 parts, sodium hydroxide 4-8 part, dimethylbenzene 2-4 part, methyl alcohol 1-6 part, red 1 part of the setting sun.
Contain polyisobutene imide and sodium alginate in the additive of the present invention, shared parts by weight are: polyisobutene imide 0-10 part, sodium alginate 0-1 part.
The particle of water of the present invention is less than 2.5 microns, and distributive law is more than 95%.
The present invention compares with prior art and has the following advantages and effect: the present invention improves the vaporization rate of gob, makes the more abundant more even of fuel combustion, thereby reaches the energy-conserving and environment-protective purpose.The rate of economizing gasoline that emulsification heavy oil uses can reach 10%-20%, and because the more abundant more even content of oxynitride, oxysulfide and flue dust in the flue gas that reduced of incendiary.Therefore promote emulsification heavy oil for solving energy shortage, improve environment, all have crucial meaning.The present invention's stability is high, and possesses catalysis, combustion-supporting effect.The present invention can be used in the heavy oil of the various qualities and the trade mark, and the formulation ratio of each component is reasonable, and preparation technology is reasonable in design.
Embodiment
The present invention is described in further detail below in conjunction with embodiment, and following examples are explanation of the invention and the present invention is not limited to following examples.
Embodiment 1
The preparation process of additive of the present invention has been described with the lower section:
Get 15 kilograms of cobalt iso-octoates, 10 kilograms of manganese iso-octoates, 5 kilograms of nickel naphthenates, 45 kilograms of sorbitan monooleates, 4.5 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.3 kilograms in tough basic phenol polyethenoxy 6 ethers, 5 kilograms of polyisobutene imide, 7 kilograms in sodium hydroxide, 2.5 kilograms of dimethylbenzene, 4 kilograms of methyl alcohol, 0.4 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 100.7 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
800 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 199 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 2
Get 18 kilograms of cobalt iso-octoates, 8 kilograms of manganese iso-octoates, 3 kilograms of nickel naphthenates, 48 kilograms of sorbitan monooleates, 5 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.7 kilograms in tough basic phenol polyethenoxy 6 ethers, 8 kilograms of polyisobutene imide, 7.5 kilograms in sodium hydroxide, 2.7 kilograms of dimethylbenzene, 4.5 kilograms of methyl alcohol, 0.7 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 108.1 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
720 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 279 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 3
Get 12 kilograms of cobalt iso-octoates, 17 kilograms of manganese iso-octoates, 6 kilograms of nickel naphthenates, 63 kilograms of sorbitan monooleates, 4 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.9 kilograms in tough basic phenol polyethenoxy 6 ethers, 6 kilograms of polyisobutene imide, 4 kilograms in sodium hydroxide, 2 kilograms of dimethylbenzene, 6 kilograms of methyl alcohol, 0.1 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 123 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
709 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 290 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 4
Get 6 kilograms of cobalt iso-octoates, 20 kilograms of manganese iso-octoates, 4 kilograms of nickel naphthenates, 65 kilograms of sorbitan monooleates, 4.2 kilograms of anhydrous sorbitol Aceonon 300 MOs, 2 kilograms in tough basic phenol polyethenoxy 6 ethers, 3 kilograms of polyisobutene imide, 6.5 kilograms in sodium hydroxide, 3.5 kilograms of dimethylbenzene, 4.8 kilograms of methyl alcohol, 1 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 121 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
849 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 150 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 5
Get 7 kilograms of cobalt iso-octoates, 18 kilograms of manganese iso-octoates, 2 kilograms of nickel naphthenates, 40 kilograms of sorbitan monooleates, 6 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1 kilogram in tough basic phenol polyethenoxy 6 ethers, 7.8 kilograms in sodium hydroxide, 3.8 kilograms of dimethylbenzene, 5.5 kilograms of methyl alcohol, 0.8 kilogram of sodium alginate, red 1 kilogram of the setting sun, mix to stir and make 92.9 kilograms additive, standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
870 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 129 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 6
Get 9 kilograms of cobalt iso-octoates, 16 kilograms of manganese iso-octoates, 10 kilograms of nickel naphthenates, 50 kilograms of sorbitan monooleates, 4.8 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.1 kilograms in tough basic phenol polyethenoxy 6 ethers, 1 kilogram of polyisobutene imide, 8 kilograms in sodium hydroxide, 4 kilograms of dimethylbenzene, 1.2 kilograms of methyl alcohol, 0.2 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 106.3 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
899 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 100 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 7
Get 20 kilograms of cobalt iso-octoates, 7 kilograms of manganese iso-octoates, 1 kilogram of nickel naphthenate, 61 kilograms of sorbitan monooleates, 5.5 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.5 kilograms in tough basic phenol polyethenoxy 6 ethers, 10 kilograms of polyisobutene imide, 4 kilograms in sodium hydroxide, 3 kilograms of dimethylbenzene, 5.8 kilograms of methyl alcohol, 0.3 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 120.1 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
789 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 210 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 8
Get 16 kilograms of cobalt iso-octoates, 10 kilograms of manganese iso-octoates, 9 kilograms of nickel naphthenates, 38 kilograms of sorbitan monooleates, 8 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.8 kilograms in tough basic phenol polyethenoxy 6 ethers, 9 kilograms of polyisobutene imide, 4.3 kilograms in sodium hydroxide, 3.3 kilograms of dimethylbenzene, 3.8 kilograms of methyl alcohol, 0.9 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 105.1 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
760 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 239 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 9
Get 13 kilograms of cobalt iso-octoates, 12 kilograms of manganese iso-octoates, 5 kilograms of nickel naphthenates, 35 kilograms of sorbitan monooleates, 7.5 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.2 kilograms in tough basic phenol polyethenoxy 6 ethers, 7 kilograms of polyisobutene imide, 5 kilograms in sodium hydroxide, 2.1 kilograms of dimethylbenzene, 3.2 kilograms of methyl alcohol, 0.6 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 92.6 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
730 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 269 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 10
Get 8 kilograms of cobalt iso-octoates, 19 kilograms of manganese iso-octoates, 4 kilograms of nickel naphthenates, 36 kilograms of sorbitan monooleates, 7.6 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.7 kilograms in tough basic phenol polyethenoxy 6 ethers, 2 kilograms of polyisobutene imide, 6 kilograms in sodium hydroxide, 2.4 kilograms of dimethylbenzene, 1 kilogram of methyl alcohol, 0.5 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 89.2 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
699 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 300 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 11
Get 17 kilograms of cobalt iso-octoates, 13 kilograms of manganese iso-octoates, 3 kilograms of nickel naphthenates, 43 kilograms of sorbitan monooleates, 5.9 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.4 kilograms in tough basic phenol polyethenoxy 6 ethers, 5 kilograms of polyisobutene imide, 5.5 kilograms in sodium hydroxide, 3.1 kilograms of dimethylbenzene, 1.7 kilograms of methyl alcohol, 0.4 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 100 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
889 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 110 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 12
Get 19 kilograms of cobalt iso-octoates, 6 kilograms of manganese iso-octoates, 7 kilograms of nickel naphthenates, 54 kilograms of sorbitan monooleates, 6.5 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.6 kilograms in tough basic phenol polyethenoxy 6 ethers, 4 kilograms of polyisobutene imide, 6.8 kilograms in sodium hydroxide, 3.6 kilograms of dimethylbenzene, 2 kilograms of methyl alcohol, 0.7 kilogram of sodium alginate, red 1 kilogram of the setting sun mixes to stir and makes 112.2 kilograms additive, and is standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
829 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 170 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 13
Get 10 kilograms of cobalt iso-octoates, 11 kilograms of manganese iso-octoates, 8 kilograms of nickel naphthenates, 57 kilograms of sorbitan monooleates, 7 kilograms of anhydrous sorbitol Aceonon 300 MOs, 1.9 kilograms in tough basic phenol polyethenoxy 6 ethers, 6 kilograms of polyisobutene imide, 5.2 kilograms in sodium hydroxide, 2.8 kilograms of dimethylbenzene, 2.5 kilograms of methyl alcohol, red 1 kilogram of the setting sun, mix to stir and make 112.4 kilograms additive, standby.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
719 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 180 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
In above embodiment, be suitable for the heavy oil of the various qualities and the trade mark.
During burning, the emulsification heavy oil that the present invention makes can improve the vaporization rate of gob, makes the more abundant more even of fuel combustion, thereby reaches the energy-conserving and environment-protective purpose.The rate of economizing gasoline that emulsification heavy oil uses can reach 10%-20%, and because the more abundant more even content of oxynitride, oxysulfide and flue dust in the flue gas that reduced of incendiary.Therefore promote emulsification heavy oil for solving energy shortage, improve environment, all have crucial meaning.
Example:
Through the monitoring of local environmental administration, its smoke content descended 55% than former combusting heavy oil after molten continent, Foshan architectural pottery two factories used this emulsification heavy oil, and oxysulfide descends 25%, and CO descends 40%.And, make the product percent of pass of this factory rise 10% because incendiary is more abundant.
Claims (3)
1, a kind of prescription of emulsification heavy oil, the prescription feature is: be made up of heavy oil, water and additive, wherein, the weight percent of each component is: heavy oil 69.9%-89.9%, water 10%-30%, additive 0.1%; Additive is by cobalt iso-octoate, manganese iso-octoate, nickel naphthenate, sorbitan monooleate, the anhydrous sorbitol Aceonon 300 MO, tough basic phenol polyethenoxy 6 ethers, sodium hydroxide, dimethylbenzene, methyl alcohol, the red composition of the setting sun, wherein, the shared parts by weight of each component are: cobalt iso-octoate 6-20 part, manganese iso-octoate 6-20 part, nickel naphthenate 1-10 part, the anhydrous sorbitol list has acid esters 35-65 part, anhydrous sorbitol Aceonon 300 MO 4-8 part, tough basic phenol polyethenoxy 6 ether 1-2 parts, sodium hydroxide 4-8 part, dimethylbenzene 2-4 part, methyl alcohol 1-6 part, red 1 part of the setting sun.
2, the prescription of emulsification heavy oil according to claim 1 is characterized in that: contain polyisobutene imide and sodium alginate in the described additive, shared parts by weight are: polyisobutene imide 0-10 part, sodium alginate 0-1 part.
3, the prescription of emulsification heavy oil according to claim 1 is characterized in that: the particle of described water is less than 2.5 microns, and distributive law is more than 95%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2007100696516A CN101328426B (en) | 2007-06-22 | 2007-06-22 | Composition of emulsified heavy oil |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2007100696516A CN101328426B (en) | 2007-06-22 | 2007-06-22 | Composition of emulsified heavy oil |
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| CN101328426A true CN101328426A (en) | 2008-12-24 |
| CN101328426B CN101328426B (en) | 2012-06-20 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101462914B (en) * | 2009-01-12 | 2011-12-07 | 山西建烨工贸有限公司 | Environment protective emulsive explosive composite emulsifying agent |
| CN102504896A (en) * | 2011-11-09 | 2012-06-20 | 南开大学 | Method for preparing emulsified heavy oil by using microbial agent |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1357605A (en) * | 2001-08-31 | 2002-07-10 | 石生玉 | Additive for synthetic water-diesel oil fuel and its prepn and application |
| CN1169927C (en) * | 2002-09-26 | 2004-10-06 | 武汉理工大学 | Multifunctional heavy oil and fuel oil additive, preparation and use thereof in preparing emulsified oil |
| CN1566279A (en) * | 2003-06-13 | 2005-01-19 | 洪星南 | Environmental protection water-based diesel oil emulsifier |
| CN1219025C (en) * | 2003-11-07 | 2005-09-14 | 陆翼德 | Additive for emulsified oil and method for preparing the same |
-
2007
- 2007-06-22 CN CN2007100696516A patent/CN101328426B/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101462914B (en) * | 2009-01-12 | 2011-12-07 | 山西建烨工贸有限公司 | Environment protective emulsive explosive composite emulsifying agent |
| CN102504896A (en) * | 2011-11-09 | 2012-06-20 | 南开大学 | Method for preparing emulsified heavy oil by using microbial agent |
| CN102504896B (en) * | 2011-11-09 | 2014-02-12 | 南开大学 | Method for preparing emulsified heavy oil by using microbial agent |
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| CN101328426B (en) | 2012-06-20 |
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