CN101250812A - Xanthochromia-resistance dacron afterprocessing oil solution and manufacturing method thereof - Google Patents
Xanthochromia-resistance dacron afterprocessing oil solution and manufacturing method thereof Download PDFInfo
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- CN101250812A CN101250812A CNA2008100611442A CN200810061144A CN101250812A CN 101250812 A CN101250812 A CN 101250812A CN A2008100611442 A CNA2008100611442 A CN A2008100611442A CN 200810061144 A CN200810061144 A CN 200810061144A CN 101250812 A CN101250812 A CN 101250812A
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Abstract
The invention discloses terylene afterprocessing oil agent for preventing xanthochromia, which is mainly formed by smoothing agent, emulsifying agent, cleaning agent and addition agent, and is characterized in that weight percentage of each component is smoothing agent 85%-90%, emulsifying agent 5%-10%, cleaning agent 2%-4% and addition agent 1%-1.5%. According to the weight percentage of each component, the method for preparation is that firstly packing emulsifying agent and cleaning agent with precise measure into an autoclave to heat from 50 DEG C to 80 DEG C, secondly packing smoothing agent into the autoclave to mix for 40-60 min, thirdly charging addition agent to mix homogeneously, and then cooling, filtering and packaging. The terylene after-processing oil agent for preventing xanthochromia has the advantages that interfacial force is low, permeability and diffusibility are good, the applying oil process is quick and homogeneous, the volume for applying oil is easy to be controlled, after-processing is smooth and has no imperfect effect on weave process and causticity component, and the invention is easy for washing and not influence on coloration and topical finish, and is good in cohesion property and forming of silk can, high in oil film strength, and strong in ability of preventing xanthochromia, thereby being favorable to store silks.
Description
Technical field
The present invention relates to a kind of process technology of synthetic fiber, particularly a kind of Xanthochromia-resistance dacron afterprocessing oil solution and manufacture method thereof.
Background technology
At present, the production and the manufacturing of processing finish behind the terylene mainly are to adopt 5
#White oil, 32
#Machinery oil and certain emulsifying agent, antistatic additive and additive compound form, and at high temperature season, terylene thread is subjected under solar radiation or the hot environment to take place easily xanthochromia, and the quality of silk is had certain influence.
Summary of the invention
The objective of the invention is provides a kind of stable performance for the deficiency that solves above-mentioned technology, satisfies processing request behind the terylene thread, effectively improves the Xanthochromia-resistance dacron afterprocessing oil solution and the manufacture method thereof of terylene thread period of storage and external quality.
In order to achieve the above object, a kind of Xanthochromia-resistance dacron afterprocessing oil solution provided by the invention, mainly form by smooth agent, emulsifying agent, detergent, additive, the percentage by weight that it is characterized in that each component is: smooth agent 85% to 90%, emulsifying agent 5% to 10%, detergent 2% to 4%, additive 1% to 1.5%.
Described smooth agent is the technical white oil of three hydrogenation, the mixture of one or more in the unit alcohol aliphatic alcohol ester.The effect of smooth agent can keep between fiber and the fiber, the suitable coefficient of friction between fiber and other contact components, the cohesive force of increase fiber, the unwinding when helping the fiber winding shaping and weaving.
Described emulsifying agent is polyoxyethylene nonylphenol ether, oleic acid polyoxyethylene, C
12-14One or more mixtures of alcohol polyoxyethylene ether, sorbitan fatty acid ester.The effect of emulsifying agent is that with the various components in the finish, particularly emulsified object smooth agent reaches balance by physical and chemical process, makes finish become even, transparent, stable oily liquid in use, and is not stratified, labile acid.
Described detergent is one or more the mixture in coconut oil alkanolamide, the polyoxyethylene nonylphenol ether.The effect of detergent be make finish guarantee terylene thread after process and the process of weaving cotton cloth in associated uses after, be convenient to the dyeing factory washing, be beneficial to carrying out smoothly of dyeing, do not form phenomenons such as oil mark, uneven dyeing.
Described additive be methyl-silicone oil and prevent splash agent, one or more the mixture in the organic acid.The adding of additive can guarantee the goodish penetrability of finish, fiber is oiled smoothly and meets the requirements of oil mass, prevents that simultaneously finish is splashed on the ground, influences the board health, can also guarantee the stability of using and storing of finish.
A kind of Xanthochromia-resistance dacron afterprocessing oil solution provided by the invention can be smooth agent 88% especially: wherein 15 of three hydrogenation
#White oil 80%, the different monooctyl ester 8% of stearic acid; Emulsifying agent 8%: wherein polyoxyethylene nonylphenol ether 6%, C
12-14Alcohol polyoxyethylene ether 2%; Detergent 2%: wherein the coconut oil alkanolamide 2%; Additive 2%: methyl-silicone oil 0.5% prevents splash agent 1.5%.
A kind of Xanthochromia-resistance dacron afterprocessing oil solution provided by the invention can be a smooth agent 90%: select 10 of three hydrogenation for use especially
#White oil; Emulsifying agent 6%: select sorbitan fatty acid ester 4% for use, polyoxyethylene nonylphenol ether 2%; Detergent 2%: select Nonyl pheno-10 ether for use; Additive 2%: select methyl-silicone oil 1% for use, prevent splash agent 1%.
The manufacture method of Xanthochromia-resistance dacron afterprocessing oil solution of the present invention is: by the percentage by weight of each component, elder generation is with emulsifying agent, the detergent suction reactor of accurate measurement, being heated to 50 ℃ to 80 ℃ stirs, again with in the smooth agent suction reactor, stir after 40 minutes to 60 minutes, add additive, the back cooling stirs, filter packing.
The resulting a kind of Xanthochromia-resistance dacron afterprocessing oil solution of the present invention compared with prior art has following distinguishing feature and good effect:
1, surface tension is low, and the infiltration diffusion is good, can evenly oil rapidly, the oil mass that goes up easy to control; 2, back processing is smooth and easy, and weaving process has no adverse effects, and can wash easily, does not influence dyeing and back arrangement; 3, coherent is good, the film strength height, and the silk tube is shaped; 4, non-corrosiveness composition does not all have corrosion to people and equipment, and anti-xanthochromia ability is strong, and is favourable to the storage of silk.
Xanthochromia-resistance dacron afterprocessing oil solution of the present invention is applicable to the production line of POY, DTY two step method.Meet the DTY processing oil tanker mode that oils, can satisfy that POY adds that DTY when playing reels smoothly and the smooth unwinding processing request of DTY when weaving.Between the megathermal period, guarantee that the storage of DTY silk is subjected to solar radiation and not flavescence simultaneously.Use through the Duo Jia chemical fibre factory, reaction is good.
The specific embodiment
The invention will be further described in conjunction with the accompanying drawings below by embodiment.
Embodiment:
A kind of Xanthochromia-resistance dacron afterprocessing oil solution that present embodiment provides, mainly be made up of smooth agent, emulsifying agent, detergent, additive, the percentage by weight of each component is: smooth agent 85% to 90%, emulsifying agent 5% to 10%, detergent 2% to 4%, additive 1% to 1.5%.
A kind of Xanthochromia-resistance dacron afterprocessing oil solution and manufacture method thereof that present embodiment is described, by weight percentage earlier, determine the ratio of each component:
Embodiment 1 prescription is formed:
Smooth agent 88%: wherein 15
#White oil (three hydrogenation) 80%, the different monooctyl ester 8% of stearic acid;
Emulsifying agent 8%: wherein polyoxyethylene nonylphenol ether 6%, C
12-14Alcohol polyoxyethylene ether 2%;
Detergent 2%: wherein the coconut oil alkanolamide 2%;
Additive 2%: methyl-silicone oil 0.5% prevents splash agent 1.5%.
Embodiment 2 prescriptions are formed:
Smooth agent 90%: select 10 for use
#White oil (three hydrogenation);
Emulsifying agent 6%: select sorbitan fatty acid ester 4% for use, polyoxyethylene nonylphenol ether 2%;
Detergent 2%: select Nonyl pheno (10) ether for use;
Additive 2%: select methyl-silicone oil 1% for use, prevent splash agent 1%.
After the described ratio batching of above-mentioned two embodiment, the manufacture method of its Xanthochromia-resistance dacron afterprocessing oil solution is:
With emulsifying agent, detergent suction reactor, open and stir, be warmed up to about 60 ℃.Stir, again with smooth agent suction reactor, maintain the temperature at about 60 ℃, stirred 45 minutes, add additive at last, stirred 15 minutes, stir and finish, be cooled to about 30 ℃, blowing filters, and it is promptly good to pack.
According to percentage of the present invention when the Xanthochromia-resistance dacron afterprocessing oil solution produced of manufacture method can reach following quality index:
1, outward appearance (25 ℃): colourless to faint yellow transparent oily liquid
2, pH value (1% aqueous solution, 25 ℃): 6.0 to 8.0
3, active constituent content (%, 〉=): 98.5
4, kinematic viscosity (40 ± 0.1 ℃, m
2/ s): (8～15) * 10
-6
Claims (5)
1, a kind of Xanthochromia-resistance dacron afterprocessing oil solution, mainly form, it is characterized in that the percentage by weight of each component is: smooth agent 85% to 90%, emulsifying agent 5% to 10% by smooth agent, emulsifying agent, detergent, additive, detergent 2% to 4%, additive 1% to 1.5%.
2, a kind of Xanthochromia-resistance dacron afterprocessing oil solution according to claim 1 is characterized in that described smooth agent is one or more the mixture in technical white oil, the unit alcohol aliphatic alcohol ester of three hydrogenation; Described emulsifying agent is polyoxyethylene nonylphenol ether, oleic acid polyoxyethylene, C
12-14One or more mixtures of alcohol polyoxyethylene ether, sorbitan fatty acid ester; Described detergent is one or more the mixture in coconut oil alkanolamide, the polyoxyethylene nonylphenol ether; Described additive be methyl-silicone oil and prevent splash agent, one or more the mixture in the organic acid.
3, a kind of Xanthochromia-resistance dacron afterprocessing oil solution according to claim 1 and 2 is characterized in that smooth agent 88%: wherein 15 of three hydrogenation
#White oil 80%, the different monooctyl ester 8% of stearic acid; Emulsifying agent 8%: wherein polyoxyethylene nonylphenol ether 6%, C
12-14Alcohol polyoxyethylene ether 2%; Detergent 2%: wherein the coconut oil alkanolamide 2%; Additive 2%: methyl-silicone oil 0.5% prevents splash agent 1.5%.
4, a kind of Xanthochromia-resistance dacron afterprocessing oil solution according to claim 1 and 2 is characterized in that smooth agent 90%: select 10 of three hydrogenation for use
#White oil; Emulsifying agent 6%: select sorbitan fatty acid ester 4% for use, polyoxyethylene nonylphenol ether 2%; Detergent 2%: select Nonyl pheno-10 ether for use; Additive 2%: select methyl-silicone oil 1% for use, prevent splash agent 1%.
5, a kind of manufacture method of Xanthochromia-resistance dacron afterprocessing oil solution, after it is characterized in that percentage by weight by each component takes by weighing, elder generation is with emulsifying agent, the detergent suction reactor of accurate measurement, be heated to 50 ℃ to 80 ℃ and stir,, stir after 40 minutes to 60 minutes again with in the smooth agent suction reactor, add additive, cooling after stirring is filtered, packing.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810061144 CN101250812B (en) | 2008-03-12 | 2008-03-12 | Xanthochromia-resistance dacron afterprocessing oil solution and manufacturing method thereof |
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|---|---|---|---|
| CN 200810061144 CN101250812B (en) | 2008-03-12 | 2008-03-12 | Xanthochromia-resistance dacron afterprocessing oil solution and manufacturing method thereof |
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| CN101250812A true CN101250812A (en) | 2008-08-27 |
| CN101250812B CN101250812B (en) | 2013-02-20 |
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| CN 200810061144 Expired - Fee Related CN101250812B (en) | 2008-03-12 | 2008-03-12 | Xanthochromia-resistance dacron afterprocessing oil solution and manufacturing method thereof |
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| CN101949093A (en) * | 2010-09-17 | 2011-01-19 | 嘉兴高科新纤维有限公司 | Finish for nylon FDY and preparation method |
| CN102767075A (en) * | 2012-06-25 | 2012-11-07 | 桐乡市恒隆化工有限公司 | Oiling agent for producing high-F terylene DTY and production method thereof |
| CN103015183A (en) * | 2012-11-29 | 2013-04-03 | 桐乡市恒隆化工有限公司 | Compound type emulsifier for DTY (drawn twisted yarn) oil agent compounding |
| CN103806268A (en) * | 2014-03-04 | 2014-05-21 | 天津工业大学 | Polyester DTY (draw texturing yarn) oil agent and preparation method thereof |
| CN104358114A (en) * | 2014-11-27 | 2015-02-18 | 何庆堃 | Deformation oiling agent for alginate fiber high-stretch yarn |
| CN104499098A (en) * | 2014-12-11 | 2015-04-08 | 桐乡市恒隆化工有限公司 | Filament finish emulsifier |
| CN104975496A (en) * | 2015-06-30 | 2015-10-14 | 盐城工学院 | Complex oil agent for textile and preparation method thereof |
| CN105088772A (en) * | 2015-08-13 | 2015-11-25 | 太仓市隆纺油剂有限公司 | Environmentally-friendly anti-yellowing polyester DTY oiling agent and preparation method thereof |
| CN105671964A (en) * | 2016-02-25 | 2016-06-15 | 苏州三和开泰花线织造有限公司 | Preparation method of oiling agent for polyester spinning |
| CN105839393A (en) * | 2015-09-09 | 2016-08-10 | 杨恩弟 | Multifunctional multielement textile finishing agent |
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| CN106120343A (en) * | 2016-07-08 | 2016-11-16 | 苏州夏尔植物油脂科技有限公司 | A kind of terylene, cotton synthetic fibre silk oil preparation, preparation method and applications |
| CN108930159A (en) * | 2018-08-06 | 2018-12-04 | 江苏悦孚油品有限公司 | A kind of DTY texturing oil and preparation method thereof |
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| CN111945426A (en) * | 2020-08-18 | 2020-11-17 | 江苏双江能源科技股份有限公司 | Terylene DTY oiling agent and preparation method thereof |
| CN112626851A (en) * | 2020-12-22 | 2021-04-09 | 太仓市隆纺油剂有限公司 | Anti-yellowing stable DTY textile oil and preparation method thereof |
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| CN101949093A (en) * | 2010-09-17 | 2011-01-19 | 嘉兴高科新纤维有限公司 | Finish for nylon FDY and preparation method |
| CN101949093B (en) * | 2010-09-17 | 2012-05-02 | 嘉兴高科新纤维有限公司 | Finish for nylon FDY and preparation method |
| CN102767075A (en) * | 2012-06-25 | 2012-11-07 | 桐乡市恒隆化工有限公司 | Oiling agent for producing high-F terylene DTY and production method thereof |
| CN103015183A (en) * | 2012-11-29 | 2013-04-03 | 桐乡市恒隆化工有限公司 | Compound type emulsifier for DTY (drawn twisted yarn) oil agent compounding |
| CN103806268A (en) * | 2014-03-04 | 2014-05-21 | 天津工业大学 | Polyester DTY (draw texturing yarn) oil agent and preparation method thereof |
| CN104358114A (en) * | 2014-11-27 | 2015-02-18 | 何庆堃 | Deformation oiling agent for alginate fiber high-stretch yarn |
| CN104499098A (en) * | 2014-12-11 | 2015-04-08 | 桐乡市恒隆化工有限公司 | Filament finish emulsifier |
| CN104975496A (en) * | 2015-06-30 | 2015-10-14 | 盐城工学院 | Complex oil agent for textile and preparation method thereof |
| CN105088772A (en) * | 2015-08-13 | 2015-11-25 | 太仓市隆纺油剂有限公司 | Environmentally-friendly anti-yellowing polyester DTY oiling agent and preparation method thereof |
| WO2017024423A1 (en) * | 2015-08-13 | 2017-02-16 | 太仓市隆纺油剂有限公司 | Environmentally-friendly anti-yellowing dacron dty oiling agent and preparation method therefor |
| CN105839393A (en) * | 2015-09-09 | 2016-08-10 | 杨恩弟 | Multifunctional multielement textile finishing agent |
| CN105671964A (en) * | 2016-02-25 | 2016-06-15 | 苏州三和开泰花线织造有限公司 | Preparation method of oiling agent for polyester spinning |
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| CN106120343A (en) * | 2016-07-08 | 2016-11-16 | 苏州夏尔植物油脂科技有限公司 | A kind of terylene, cotton synthetic fibre silk oil preparation, preparation method and applications |
| CN108930159A (en) * | 2018-08-06 | 2018-12-04 | 江苏悦孚油品有限公司 | A kind of DTY texturing oil and preparation method thereof |
| CN109722889A (en) * | 2019-01-02 | 2019-05-07 | 上海中孚特种油品有限公司 | A kind of environment-friendly type spinning oil and preparation method thereof |
| CN109957861A (en) * | 2019-02-28 | 2019-07-02 | 常州凯途纺织品有限公司 | A kind of heat-resisting oxidation-resistance spinning oil |
| CN111945426A (en) * | 2020-08-18 | 2020-11-17 | 江苏双江能源科技股份有限公司 | Terylene DTY oiling agent and preparation method thereof |
| CN112626851A (en) * | 2020-12-22 | 2021-04-09 | 太仓市隆纺油剂有限公司 | Anti-yellowing stable DTY textile oil and preparation method thereof |
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| CN113969436A (en) * | 2021-12-10 | 2022-01-25 | 江苏悦孚油品有限公司 | Chinlon spinning oil and preparation method thereof |
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Inventor after: Zhu Jiancheng Inventor after: Sun Yanlin Inventor before: Zhu Jiancheng |
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