CN101249059A - Moisture-keeping face pack and method of preparing the same - Google Patents
Moisture-keeping face pack and method of preparing the same Download PDFInfo
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- CN101249059A CN101249059A CNA2008100605511A CN200810060551A CN101249059A CN 101249059 A CN101249059 A CN 101249059A CN A2008100605511 A CNA2008100605511 A CN A2008100605511A CN 200810060551 A CN200810060551 A CN 200810060551A CN 101249059 A CN101249059 A CN 101249059A
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- sargassum fusiforme
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Abstract
The invention relates to a moisturizing facial mask and a preparation method thereof. The facial mask contains extract A and B derived from Sargassum fusiforme by special process and additives such as vitamin E beneficial for skin care; and has anti-skin aging, blood vessel beautification, anti-acne, skin repairing, whitening and moisturizing effects; and integrates functions of polysaccharides, such as anticoagulant, antioxidant, anti-wrinkle, freckle-removing and antiaging effects. The preparation method of the facial mask is simple.
Description
Technical field
The present invention relates to the cosmetic skincare product field, specifically refer to a kind of moisture saver mask and preparation method thereof.
Background technology
The people who payes attention to skin nursing knows the importance of frequent face mask film, and the facial film of various functions can allow skin well be nursed, as cleaning, preserve moisture, whiten, the exfoliation reparation, nutrition or the like, everyone can find corresponding facial film at the skin situation of oneself, has healthy moist skin.And the suitable facial film of opening and closing can help you to improve facial skin.
Along with the raising that development of science and technology and people require operational maintenance, the useful composition that the manufacturer begins to extract in the plant prepares the skin care item that satisfy people's requirement.Sargassum fusiforme (Harv.) Setch is a kind of seaweed plant, its extract has plurality of health care functions, effects such as the blood fat reducing that it had, blood glucose, antitumor, antiviral, defying age, antiinflammatory for example, its extract has been applied in the multiple field, and the crude polysaccharides that extracts from Sargassum fusiforme (Harv.) Setch has more excellent antioxidant activity.And according to the difference of extraction process, the effective ingredient in the Sargassum fusiforme (Harv.) Setch extract is also different, so the effect that it had is also different.
Currently marketed facial film is of a great variety, according to the function of facial film cleaning pack is arranged, moisture saver mask, and the facial film of releiving, regenerating mask, extra firming facial mask and cleawhite pack, moisture saver mask wherein adopts vaseline class and polyalcohols as preserving moisture composition mostly.General winter or the utmost point dry skin of only being suitable for of vaseline series products, young crowd then is not suitable for to inclined to one side oiliness, and feels greasy, can block pore, not easy cleaning; The many products of polyalcohols only are applicable to the season that relative humidity is bigger, and it is unfavorable to skin on the contrary that the autumn and winter use.
Summary of the invention
Technical problem to be solved by this invention is the situation at prior art, and a kind of good in oxidation resistance, moisture saver mask that moisture retention is strong are provided.
Another technical problem to be solved by this invention is the situation at prior art, and the preparation method of a kind of good in oxidation resistance, moisture saver mask that moisture retention is strong is provided.
The present invention solves the problems of the technologies described above the technical scheme that is adopted: this moisture saver mask is characterized in that comprising following ingredients: (each component content is the quality percentage composition except that specifying)
Sargassum fusiforme (Harv.) Setch extract A 1.5-3%
Sargassum fusiforme (Harv.) Setch extract B 10-20%
Vitamin E 1-2%
Glycerol 3-5%
Polyvinylpyrrolidone 2-2%
Ethanol 1-2%
Carboxymethyl cellulose (CMC) 3-5%
Tween-60 0.5-0.8%
Polyethylene Glycol 10-15%
Methyl parahydroxybenzoate 0.05-0.10%
Quintessence oil 0.01-0.05%
Sterilization deionized water 44-68%
The preparation method of wherein said Sargassum fusiforme (Harv.) Setch extract A is as follows: after using the clear water rinsing clean Sargassum fusiforme (Harv.) Setch, 50-60 ℃ of oven dry, pulverized 80 mesh sieves then and obtain dry powder, dry powder is added flooding 2-3 hour, wherein the mass ratio of dry powder and water is 1: 30-40; With 800-1200W ultrasonic Treatment 10-15 minute, with said extracted thing centrifugal 10-15min under the speed of 4000-5000r/min, precipitate water under 70-80 ℃ of temperature is carried 1-2h, the same then method is centrifugal, precipitation reuse 2% carbonic acid soda is carried 1-2h, centrifugal with method, merge the above-mentioned gained supernatant that respectively goes on foot, regulate supernatant pH value to 7.0,0.1Mpa, 55-60 ℃ of reduced vacuum concentrates, concentrated solution Sevage method Deproteinization 2-4 time, the supernatant ethanol precipitation of volume fraction 65%, precipitate is successively used 1: 5-10 (quality: acetone volume), absolute ethanol washing, precipitate is through 0.1MPa, 55-60 ℃ of vacuum decompression drying obtains Sargassum fusiforme (Harv.) Setch extract A crude product.With 1: 5-10 (mass ratio) Rhizoma Zingiberis Recens removes raw meat, 1: after the absorption of 10-15 granular active carbon, through the centrifugal 10-15min of 4000-5000r/min, behind the supernatant liquid filtering, with 1: 2-4 (volume: quality) AB-8 macroporous adsorbent resin decolouring, filter and obtain the Sargassum fusiforme (Harv.) Setch extract A;
The preparation method of Sargassum fusiforme (Harv.) Setch extract B is as follows: after fresh Sargassum fusiforme (Harv.) Setch is used the clear water rinsing; add distilled water with the ratio of expecting solid ratio 1: 30-40; place ice bath to handle 10-15 minute with ultrasound wave 800-1200W; 4 ℃ of lixiviate 2-3h; centrifugal 10-15min under 4000-5000 rev/min the speed; behind the supernatant liquid filtering; with 1: the 5-10 Rhizoma Zingiberis Recens removes raw meat; reuse 1: 10-15 granular active carbon absorption; centrifugal 10-15min under 4000-5000 rev/min the speed; behind the supernatant liquid filtering, with 1: after the decolouring of 2-4 AB-8 macroporous adsorbent resin, filter and obtain Sargassum fusiforme (Harv.) Setch extract B (aforesaid operations carries out) under 4 ℃ of conditions.
The main component of the Sargassum fusiforme (Harv.) Setch extract A of extracting through this technology is a bioactive polysaccharide, it has slow down aging, blood vessel beauty treatment, anti-acne, repairing skin tissue, whitens and moisture-keeping function, and this is relevant with absorptive physicochemical property with biological function such as antibacterial with the anticoagulation of polysaccharide, antioxidation, promotion hyperplasia; The main component of Sargassum fusiforme (Harv.) Setch extract B is Vc and SOD, and Vc has antioxidation, whitening effect.SOD has very strong antioxidation, brightens, crease-resistant, speckle dispelling, the anti-ageing effect of waiting for a long time.
The preparation method of aforesaid moisture saver mask is as follows:
A) prepare Sargassum fusiforme (Harv.) Setch extract A and Sargassum fusiforme (Harv.) Setch extract B respectively according to the above-mentioned method for preparing Sargassum fusiforme (Harv.) Setch extract A and Sargassum fusiforme (Harv.) Setch extract B;
B) get Sargassum fusiforme (Harv.) Setch extract A fully dissolving under 50-60 ℃ of water bath condition that 1.5-3% prepares, 400-500 commentaries on classics/min is stirred to cooling in magnetic stirring apparatus, adds the Sargassum fusiforme (Harv.) Setch extract B that 10-20% prepares, and stirs;
C) the 0.05-0.10% methyl parahydroxybenzoate is dissolved in the 1-2% ethanol, adds the quintessence oil of 0.01-0.05% and the aquesterilisa of 44-68%;
D) Polyethylene Glycol of limit adding 10-15% and the polyvinylpyrrolidone of 2-3% are slowly stirred in the carboxymethyl cellulose limit of getting 3-5%, be stirred to the mucus shape, add the mixed Sargassum fusiforme (Harv.) Setch extract A of step a and the mixture of Sargassum fusiforme (Harv.) Setch extract B, the glycerol of 3-5%, the vitamin E of 1-2% and the mixture of steps d, the Tween-60 that adds 0.5-0.8% while stirring makes it to be emulsified into even paste;
E) with after the emulsifying of the resulting paste usefulness of steps d vacuum colloidal mill, be packaged as required specification.
Adopt said components and the prepared moisture saver mask of preparation method, through clinical trial, compared with prior art, owing to wherein contain Sargassum fusiforme (Harv.) Setch extract A and Sargassum fusiforme (Harv.) Setch extract B, cooperate the VE that adds simultaneously, contain rich in amino acid, vitamin and polysaccharide, the energy skin nutrition, has good affinity and stability with memebrane protein, increase dermal osmosis, played fine moistening effect with other composition compatibility in the prescription, and surfactant is a kind of natural moisture preserving agent to the skin pessimal stimulation in the elimination prescription; Product uses the back easy cleaning in addition, is not subject to seasonal restrictions, and the effect of protection cell membrane has the moistening effect of asking than long time, compares with like product, and performance of keeping humidity improves 10-15%; It also has the external free radical ability of very strong removing, and the active polysaccharide that is contained in the Sargassum fusiforme (Harv.) Setch extract simultaneously has strong anti-oxidation, brightens, crease-resistant, speckle dispelling, the anti-ageing effect of waiting for a long time; This facial film stable performance did not occur denaturalization phenomenon at 40 ℃ in 5～7 days with-5 ℃ of placements; Because Sargassum fusiforme (Harv.) Setch is cheap and easy to get, extraction process is simple, so moisture saver mask production cost provided by the present invention is low simultaneously.
Description of drawings
Fig. 1 is the percentage of water loss test result of several moisture saver mask when RH40%5 in the embodiment of the invention 1.
The specific embodiment
Below in conjunction with embodiment the present invention is described in further detail.If no special instructions, described ratio is mass percent.
A) prepare the Sargassum fusiforme (Harv.) Setch extract A: after using the clear water rinsing clean Sargassum fusiforme (Harv.) Setch, 58 ℃ of oven dry, pulverized 80 mesh sieves then and obtain dry powder, dry powder was added flooding 2.5 hours, wherein the mass ratio of dry powder and water is 1: 33; With 1000W ultrasonic Treatment 12 minutes, 4500 rev/mins of said extracted things is centrifugal 10 minutes, precipitate water under 77 ℃ of temperature is carried 1.5h, the same then method is centrifugal, precipitation reuse 2% carbonic acid soda is carried 1.5h, centrifugal with method, merge the above-mentioned gained supernatant that respectively goes on foot, regulate supernatant pH value to 7.0,0.1Mpa, 56 ℃ of reduced vacuum concentrate, concentrated solution Sevage method Deproteinization 3 times, the supernatant ethanol precipitation of volume fraction 65%, precipitate successively used 1: 8 acetone, absolute ethanol washing, 0.1Mpa, precipitate obtains Sargassum fusiforme (Harv.) Setch extract A crude product through the vacuum decompression drying in the time of 60 ℃.After going raw meat, granular active carbon absorption in 1: 12 with 1: 8 Rhizoma Zingiberis Recens, through 4000 rev/mins centrifugal 15 minutes, behind the supernatant liquid filtering,, filter and obtain the Sargassum fusiforme (Harv.) Setch extract A with AB-8 macroporous adsorbent resin decolouring in 4: 1;
B) prepare the Sargassum fusiforme (Harv.) Setch extract B: after fresh Sargassum fusiforme (Harv.) Setch is used the clear water rinsing; to expect that 1: 30 ratio of solid ratio adds distilled water; place ice bath to handle 12 minutes with ultrasound wave 800W; 4 ℃ of lixiviate 2h; under 4000 rev/mins the speed centrifugal 10 minutes; behind the supernatant liquid filtering; remove raw meat with 1: 10 Rhizoma Zingiberis Recens; reuse granular active carbon absorption in 1: 10; under 4000 rev/mins the speed centrifugal 10 minutes; behind the supernatant liquid filtering, with 4: 1 (volumes: quality) after the decolouring of AB-8 macroporous adsorbent resin, filter and obtain the Sargassum fusiforme (Harv.) Setch extract B.
C) 2% the Sargassum fusiforme (Harv.) Setch extract A that step a is obtained is fully dissolving under 50 ℃ of water bath condition, and 400 rev/mins are stirred 40 minutes to cooling in magnetic stirring apparatus, add the 15% Sargassum fusiforme (Harv.) Setch extract B that is made by step b and are stirred to evenly;
D) 0.05% methyl parahydroxybenzoate is dissolved in 2% ethanol, adds the aquesterilisa of 0.01% quintessence oil and 54.44%, stir;
E) getting 3% carboxymethyl cellulose limit slowly stirs the limit and adds 15% Polyethylene Glycol and 2% polyvinylpyrrolidone, be stirred to the mucus shape, the mixture that adds mixture, 5% glycerol, vitamin E 1% and the steps d of resulting Sargassum fusiforme (Harv.) Setch extract A of step c and Sargassum fusiforme (Harv.) Setch extract B, add Tween-60 0.5% while stirring, make it to be emulsified into even paste;
F) with after the emulsifying of the resulting paste usefulness of step e vacuum colloidal mill, be packaged as required specification.
The prepared moisture saver mask of test said method:
1, the Sargassum fusiforme (Harv.) Setch facial film effect test of preserving moisture
Weight method:
Take by weighing each 5.0g of facial film sample in the following table 1 respectively, evenly be applied to and be stained with 3cm adhesive plaster, size in the weighing botle of Φ 40 * 25, do not add a cover, be placed on 29 ℃, relative humidity (RH) and be in 40% ± 5% the constant temperature and humidity plant incubator, took out weighing every 2 hours.Parallel test 3 times, calculate average percentage of water loss:
Percentage of water loss %=W1-W2/W1-W * 100%
The weighing botle weight of sample before the W1-experiment, gram;
Sample and weighing botle weight behind the W2-specific time interval, gram;
W-weighing botle weight, gram.
Experimental result sees Table 1 and Fig. 1.
By table 1 and Fig. 1 as can be known, under identical test condition, moisture saver mask percentage of water loss of the present invention is minimum,
Table 1: different moisture saver mask percentage of water loss test effect tables
The in vitro tests of Sargassum fusiforme (Harv.) Setch facial film oxidisability
DPPH non-oxidizability detection side is with reference to " biochemistry and biophysics progress " 2006 the 6th phases of periodical " estimating the plant oxidation resistance with removing organic free radical DPPH method " method improvement. utilize the absworption peak of the feature aubergine group of DPPH solution, with spectrophotometry, add OD514 absorbs behind antioxidant or the plant extraction liquid decline and represent that it eliminates ability to organic free radical.
DPPH earlier with the small amount of ethanol dissolving, and is mixed with the solution of 1 * 10-4mol/L concentration with 10% ethanol, keeps in Dark Place.Get 2mLDPPH solution, add 2mL facial film extraction solution and fully mix.Measure its OD at 514nm (maximum absorption wave strong point) behind the 30min
514To remove DPPH50% is IC
50Required facial film amount is the non-oxidizability index.Clearance rate P calculates available following formula:
P＝[A
0-(A
i-A
j)]/A
0
A in the formula
0The absorbance of=2mL DPPH solution+2mL solvent; A
i=2mL DPPH solution+2mL Sargassum fusiforme (Harv.) Setch solution absorbency; A
jThe absorbance of=2mL Sargassum fusiforme (Harv.) Setch solution+2mL solvent.
Result of the test shows do not find to have external radical scavenging activity in Fructus Cucumidis sativi, the aloe face pack test, and the every gram of facial film of the present invention has the external 0.05mg organic free radical (DPPH) of removing function, has obvious antioxidative advantage.
Claims (2)
1, a kind of moisture saver mask is characterized in that comprising following ingredients: (each component content is the quality percentage composition except that specifying)
Sargassum fusiforme (Harv.) Setch extract A 1.5～3%
Sargassum fusiforme (Harv.) Setch extract B 10-20%
Vitamin E 1-2%
Glycerol 3-5%
Polyvinylpyrrolidone 2-3%
Ethanol 1-2%
Carboxymethyl cellulose (CMC) 3-5%
Tween-60 0.5-0.8%
Polyethylene Glycol 10-15%
Methyl parahydroxybenzoate 0.05-0.10%
Quintessence oil 0.01-0.05
Sterilization deionized water 44-68%
Wherein, the preparation method of described Sargassum fusiforme (Harv.) Setch extract A is:
After the rinsing totally of Sargassum fusiforme (Harv.) Setch usefulness clear water, 50-60 ℃ of oven dry, pulverized 80 mesh sieves then and obtained dry powder, dry powder is added flooding 2～3h, wherein the mass ratio of dry powder and water is 1: 30-40; With 800-1200W ultrasonic Treatment 10-15 minute, the said extracted thing is centrifugal, collect supernatant, precipitate water under 70-80 ℃ of temperature is carried 1-2hr, and then the centrifugal 10-15min of 4000-5000r/min, collect supernatant, precipitate reuse 2% carbonic acid soda is carried 1-2 hour, centrifugal with method, merge and collect the above-mentioned gained supernatant that respectively goes on foot, regulate supernatant pH value to 7.0,0.1Mpa 55-60 ℃ of reduced vacuum concentrates, concentrated solution Sevage method Deproteinization 2-4 time, the supernatant ethanol precipitation of volume fraction 65%, precipitate is successively used 1: 5-10 (quality: acetone volume), absolute ethanol washing, precipitate is through vacuum 0.1Mpa, 55-60 ℃ of drying under reduced pressure obtains Sargassum fusiforme (Harv.) Setch extract A crude product.With 1: 6-10 (mass ratio) Rhizoma Zingiberis Recens removes raw meat, 1: after the absorption of 10-15 granular active carbon, through the centrifugal 10-15min of 4000-5000r/min, behind the supernatant liquid filtering, with 4: 1 (volume: quality) AB-8 macroporous adsorbent resin decolouring, filter and obtain the Sargassum fusiforme (Harv.) Setch extract A;
The preparation method of described Sargassum fusiforme (Harv.) Setch extract B is:
Indispensable Sargassum fusiforme (Harv.) Setch extract B: after the rinsing of fresh Sargassum fusiforme (Harv.) Setch usefulness clear water; add distilled water with the ratio of expecting solid ratio 1: 30-40; place ice bath to handle 10-15 minute with ultrasound wave 800-1200W; 4 ℃ of lixiviate 2-3h; centrifugal 10-15min under the 4000-5000r/min speed; behind the supernatant liquid filtering; with 1: the 5-10 Rhizoma Zingiberis Recens removes raw meat; reuse 1: 10-15 granular active carbon absorption; centrifugal 10-15min under the 4000-5000r/min speed; behind the supernatant liquid filtering, use 1-2: after the decolouring of 4 AB-8 macroporous adsorbent resins, filter and obtain Sargassum fusiforme (Harv.) Setch extract B (aforesaid operations carries out) under 4 ℃ of conditions
2, a kind of preparation method of moisture saver mask as claimed in claim 1 comprises the steps:
A) at first prepare Sargassum fusiforme (Harv.) Setch extract A and Sargassum fusiforme (Harv.) Setch extract B according to the method that such scheme provided;
B) with the Sargassum fusiforme (Harv.) Setch extract A 1.5-3% fully dissolving under 50-60 ℃ of water bath condition that obtains, in magnetic stirring apparatus, be stirred to cooling under 400-500 rev/min the speed, add 10-20% Sargassum fusiforme (Harv.) Setch extract B;
C) the 0.05-0.10% methyl parahydroxybenzoate is dissolved in the 1-2% ethanol, adds 0.01-0.05% quintessence oil and 44-68% aquesterilisa;
E) get 3-5 part carboxymethyl cellulose limit and slowly stir Polyethylene Glycol that the limit adds 10-15% and the polyvinylpyrrolidone of 2-3%, be stirred to the mucus shape, add the resulting Sargassum fusiforme (Harv.) Setch extract A of step b and the mixture of Sargassum fusiforme (Harv.) Setch extract B, the glycerol of 3-5%, the vitamin E of 1-2% and the mixture of step c, the Tween-60 that adds 0.5-0.8% while stirring makes it to be emulsified into even paste;
F) with after the emulsifying of the resulting paste usefulness of step e vacuum colloidal mill, be packaged as required specification.
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| Application Number | Priority Date | Filing Date | Title |
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| CNA2008100605511A CN101249059A (en) | 2008-03-27 | 2008-03-27 | Moisture-keeping face pack and method of preparing the same |
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| CNA2008100605511A CN101249059A (en) | 2008-03-27 | 2008-03-27 | Moisture-keeping face pack and method of preparing the same |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100152286A1 (en) * | 2008-11-17 | 2010-06-17 | Beijing Gingko Group Biological Technology Co., Ltd. | Method for Producing Fucoxanthin |
| CN102871851A (en) * | 2012-09-07 | 2013-01-16 | 浙江万里学院 | Application of acetylsalicylic acid as tyrosinase inhibitor |
| CN104940109A (en) * | 2015-07-01 | 2015-09-30 | 浙江海洋学院 | Natural marine facial mask based on shell and preparation method of natural marine facial mask |
| CN106063773A (en) * | 2015-04-22 | 2016-11-02 | 江陵原州大学校产学协力团 | The ultraviolet isolation compositions contained as effective ingredient using Sargassum fusiforme (Harv.) Setch extract |
| CN106691951A (en) * | 2017-03-08 | 2017-05-24 | 张仕英 | Method for preparing herba agrimoniae extracting solution for facial mask through ultrasonic-assisted extraction |
| CN107411998A (en) * | 2017-07-03 | 2017-12-01 | 浙江海洋大学 | A kind of anti-oxidant face mask of the active peptide containing hairtail |
| CN109908058A (en) * | 2019-04-01 | 2019-06-21 | 浙江万里学院 | A kind of moisture saver mask and preparation method thereof |
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2008
- 2008-03-27 CN CNA2008100605511A patent/CN101249059A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100152286A1 (en) * | 2008-11-17 | 2010-06-17 | Beijing Gingko Group Biological Technology Co., Ltd. | Method for Producing Fucoxanthin |
| US8871217B2 (en) * | 2008-11-17 | 2014-10-28 | Beijing Gingko Group Biological Technology Co., Ltd. | Method for producing fucoxanthin |
| CN102871851A (en) * | 2012-09-07 | 2013-01-16 | 浙江万里学院 | Application of acetylsalicylic acid as tyrosinase inhibitor |
| CN106063773A (en) * | 2015-04-22 | 2016-11-02 | 江陵原州大学校产学协力团 | The ultraviolet isolation compositions contained as effective ingredient using Sargassum fusiforme (Harv.) Setch extract |
| CN106063773B (en) * | 2015-04-22 | 2019-09-10 | 江陵原州大学校产学协力团 | The ultraviolet light isolation composition contained using sargassum fusifome extract as effective component |
| CN104940109A (en) * | 2015-07-01 | 2015-09-30 | 浙江海洋学院 | Natural marine facial mask based on shell and preparation method of natural marine facial mask |
| CN106691951A (en) * | 2017-03-08 | 2017-05-24 | 张仕英 | Method for preparing herba agrimoniae extracting solution for facial mask through ultrasonic-assisted extraction |
| CN107411998A (en) * | 2017-07-03 | 2017-12-01 | 浙江海洋大学 | A kind of anti-oxidant face mask of the active peptide containing hairtail |
| CN107411998B (en) * | 2017-07-03 | 2020-11-06 | 浙江海洋大学 | Antioxidant mask containing active peptide of hairtail |
| CN109908058A (en) * | 2019-04-01 | 2019-06-21 | 浙江万里学院 | A kind of moisture saver mask and preparation method thereof |
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Open date: 20080827 |