CN101224409A - 一种高吸附值微粉硅胶生产方法 - Google Patents
一种高吸附值微粉硅胶生产方法 Download PDFInfo
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- CN101224409A CN101224409A CNA2007101134520A CN200710113452A CN101224409A CN 101224409 A CN101224409 A CN 101224409A CN A2007101134520 A CNA2007101134520 A CN A2007101134520A CN 200710113452 A CN200710113452 A CN 200710113452A CN 101224409 A CN101224409 A CN 101224409A
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- silica gel
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- washing
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 77
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 26
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 15
- 238000001179 sorption measurement Methods 0.000 title claims abstract description 15
- 239000000843 powder Substances 0.000 title abstract description 25
- 239000000741 silica gel Substances 0.000 claims abstract description 46
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 46
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000017 hydrogel Substances 0.000 claims abstract description 24
- 238000005406 washing Methods 0.000 claims abstract description 22
- 239000000499 gel Substances 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 11
- 238000000227 grinding Methods 0.000 claims abstract description 11
- 238000012545 processing Methods 0.000 claims abstract description 10
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 9
- 230000032683 aging Effects 0.000 claims abstract description 9
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000004806 packaging method and process Methods 0.000 claims abstract description 7
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 6
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 6
- 238000005303 weighing Methods 0.000 claims abstract description 6
- 239000003292 glue Substances 0.000 claims description 15
- 239000000443 aerosol Substances 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 10
- 238000007654 immersion Methods 0.000 claims description 10
- 239000011148 porous material Substances 0.000 claims description 10
- 238000012856 packing Methods 0.000 claims description 9
- 238000000465 moulding Methods 0.000 claims description 8
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 8
- 230000008676 import Effects 0.000 claims description 4
- 239000008188 pellet Substances 0.000 claims description 4
- 239000000428 dust Substances 0.000 claims description 3
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 238000001033 granulometry Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000009423 ventilation Methods 0.000 claims description 3
- 238000004804 winding Methods 0.000 claims description 3
- 238000001514 detection method Methods 0.000 abstract description 3
- 238000000926 separation method Methods 0.000 abstract 2
- 238000002791 soaking Methods 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 39
- 235000013405 beer Nutrition 0.000 description 10
- 238000005516 engineering process Methods 0.000 description 8
- 239000003795 chemical substances by application Substances 0.000 description 5
- 230000000274 adsorptive effect Effects 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 3
- 229910001424 calcium ion Inorganic materials 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- -1 iron ion Chemical class 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000012372 quality testing Methods 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
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- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Silicon Compounds (AREA)
Abstract
Description
指标 | 单位 | 啤酒湿胶 | 啤酒干胶 | 食用油湿胶 |
孔容 | Cc/ml | 1.0-1.1 | 1.0-1.1 | 0.7-1.0 |
比表面积 | m2/ml | 500-600 | 500-600 | --- |
堆积密度 | g/l | --- | --- | 500 |
PH值 | --- | 3.5-5.5 | 6-7 | 3.5-5.5 |
含水量 | % | 60-65 | ≤5 | 60-65 |
二氧化硅含量 | % | ≥98.5 | ≥98.5 | ≥98.5 |
可溶铁离子 | ppm | ≤20 | ≤20 | ≤20 |
可溶钙离子 | ppm | ≤20 | ≤20 | ≤20 |
颗粒粒径要求 | cm | ≤2 | ≤1 | ≤2 |
项目 | 单位 | 指标 |
孔容 | Cc/ml | 1.0-1.1 |
比表面积 | m2/ml | 500-600 |
堆积密度 | g/l | --- |
PH值 | --- | 3.5-5.5 |
含水量 | % | 60-65 |
二氧化硅含量 | % | ≥98.5 |
可溶铁离子 | ppm | ≤20 |
可溶钙离子 | ppm | ≤20 |
颗粒粒径要求 | cm | ≤2 |
项目 | 单位 | 指标 | 检测方法 |
烘干失重(160℃) | % | ≤6 | GB |
二氧化硅含量 | % | ≥98.0 | DIN55921 |
PH值(5%水份散液) | --- | 6.0-8.0 | DINENIS0787-9 |
平均颗粒直径 | um | 15 | GB |
可溶铁离子 | mg/100g | ≤2.0 | GB |
可溶钙离子 | mg/100g | ≤5.0 | GB |
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2007101134520A CN101224409B (zh) | 2007-10-18 | 2007-10-18 | 一种高吸附值微粉硅胶生产方法 |
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CN2007101134520A CN101224409B (zh) | 2007-10-18 | 2007-10-18 | 一种高吸附值微粉硅胶生产方法 |
Publications (2)
Publication Number | Publication Date |
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CN101224409A true CN101224409A (zh) | 2008-07-23 |
CN101224409B CN101224409B (zh) | 2011-06-15 |
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CN2007101134520A Expired - Fee Related CN101224409B (zh) | 2007-10-18 | 2007-10-18 | 一种高吸附值微粉硅胶生产方法 |
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CN (1) | CN101224409B (zh) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102311987A (zh) * | 2011-07-05 | 2012-01-11 | 贾晓斌 | 一种含有微粉硅胶的生物转化方法 |
CN102328933A (zh) * | 2011-06-30 | 2012-01-25 | 青岛美高集团有限公司 | 一种啤酒硅胶及其制备方法 |
CN103043674A (zh) * | 2012-12-26 | 2013-04-17 | 青岛中能集团有限公司 | 一种微粉硅胶 |
CN104014300A (zh) * | 2013-07-29 | 2014-09-03 | 吉林省临江天元催化剂有限公司 | 硅藻土制备带有助滤功能啤酒稳定剂的方法 |
CN106276926A (zh) * | 2016-08-12 | 2017-01-04 | 乳山市大洋硅胶厂 | 改性变压吸附硅胶的生产方法 |
CN108196020A (zh) * | 2017-12-19 | 2018-06-22 | 浙江省海洋水产研究所 | 一种水产品中持久性有机污染物的分离方法 |
CN108195982A (zh) * | 2017-12-19 | 2018-06-22 | 浙江省海洋水产研究所 | 一种水产品中持久性有机污染物的检测方法 |
US10525448B2 (en) | 2015-07-22 | 2020-01-07 | Basf Corporation | High geometric surface area catalysts for vinyl acetate monomer production |
-
2007
- 2007-10-18 CN CN2007101134520A patent/CN101224409B/zh not_active Expired - Fee Related
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102328933A (zh) * | 2011-06-30 | 2012-01-25 | 青岛美高集团有限公司 | 一种啤酒硅胶及其制备方法 |
CN102328933B (zh) * | 2011-06-30 | 2013-04-17 | 青岛美高集团有限公司 | 一种啤酒硅胶的制备方法 |
CN102311987A (zh) * | 2011-07-05 | 2012-01-11 | 贾晓斌 | 一种含有微粉硅胶的生物转化方法 |
CN102311987B (zh) * | 2011-07-05 | 2014-03-26 | 贾晓斌 | 一种含有微粉硅胶的生物转化方法 |
CN103043674A (zh) * | 2012-12-26 | 2013-04-17 | 青岛中能集团有限公司 | 一种微粉硅胶 |
CN104014300B (zh) * | 2013-07-29 | 2016-02-17 | 吉林省临江天元催化剂有限公司 | 硅藻土制备带有助滤功能啤酒稳定剂的方法 |
CN104014300A (zh) * | 2013-07-29 | 2014-09-03 | 吉林省临江天元催化剂有限公司 | 硅藻土制备带有助滤功能啤酒稳定剂的方法 |
US10525448B2 (en) | 2015-07-22 | 2020-01-07 | Basf Corporation | High geometric surface area catalysts for vinyl acetate monomer production |
US10864500B2 (en) | 2015-07-22 | 2020-12-15 | Basf Corporation | High geometric surface area catalysts for vinyl acetate monomer production |
CN106276926A (zh) * | 2016-08-12 | 2017-01-04 | 乳山市大洋硅胶厂 | 改性变压吸附硅胶的生产方法 |
CN106276926B (zh) * | 2016-08-12 | 2018-01-30 | 乳山市大洋硅胶厂 | 改性变压吸附硅胶的生产方法 |
CN108196020A (zh) * | 2017-12-19 | 2018-06-22 | 浙江省海洋水产研究所 | 一种水产品中持久性有机污染物的分离方法 |
CN108195982A (zh) * | 2017-12-19 | 2018-06-22 | 浙江省海洋水产研究所 | 一种水产品中持久性有机污染物的检测方法 |
Also Published As
Publication number | Publication date |
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CN101224409B (zh) | 2011-06-15 |
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Owner name: SHANDONG ZHONGDA BIO-PHARMACEUTICAL CO., LTD. Free format text: FORMER OWNER: YANTAI BORUITE FINE CHEMICAL INDUSTRY CO., LTD. Effective date: 20120326 |
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Free format text: CORRECT: ADDRESS; FROM: 264000 YANTAI, SHANDONG PROVINCE TO: 264006 YANTAI, SHANDONG PROVINCE |
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Effective date of registration: 20120326 Address after: 264006 Taishan Road, Yantai economic and Technological Development Zone, Shandong 67-4, China Patentee after: Shandong Zhongda Biological Pharmaceutical Co., Ltd. Address before: 264000 No. 087, Kunlun mountain road, Yantai economic and Technological Development Zone, Shandong Patentee before: Yantai Boruite Fine Chemical Industry Co., Ltd. |
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Owner name: QINGDAO MINTAI HIGH-TECH MATERIAL CO., LTD. Free format text: FORMER OWNER: SHANDONG ZHONGDA BIO-PHARMACEUTICAL CO., LTD. Effective date: 20130524 |
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Free format text: CORRECT: ADDRESS; FROM: 264006 YANTAI, SHANDONG PROVINCE TO: 266209 QINGDAO, SHANDONG PROVINCE |
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TR01 | Transfer of patent right |
Effective date of registration: 20130524 Address after: 266209 Shandong city of Qingdao province Jimo City Heng Town Government 20 St. Patentee after: Qingdao people Thai hi tech materials Co., Ltd. Address before: 264006 Taishan Road, Yantai economic and Technological Development Zone, Shandong 67-4, China Patentee before: Shandong Zhongda Biological Pharmaceutical Co., Ltd. |
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Granted publication date: 20110615 Termination date: 20131018 |