CN101108257A - Method of preparing liquid antibiotic deodorizer and application thereof - Google Patents
Method of preparing liquid antibiotic deodorizer and application thereof Download PDFInfo
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- CN101108257A CN101108257A CNA2007100178930A CN200710017893A CN101108257A CN 101108257 A CN101108257 A CN 101108257A CN A2007100178930 A CNA2007100178930 A CN A2007100178930A CN 200710017893 A CN200710017893 A CN 200710017893A CN 101108257 A CN101108257 A CN 101108257A
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Abstract
The invention relates to a preparation and application of a liquid antibacterial deodorant. The liquid antibacterial deodorant is excellent in antibacterial, safe and reliable, convenient in use, and suitable for all kinds of air disinfection environment to eliminate the bad smell. The product has no negative effects on human body in the preparation and application process. The invention consists of the following materials: citric acid with the weight ratio no less than 1, malic acid with the weight ratio no less than 1, lactic acid with the weight ratio no less than 3, essence with the weight ratio no less than 1, chelating agent with the weight ratio no less than 1, stabilizer with the weight ratio no less than 1 and water with the weight ratio no more than 92. The preparation is done under room temperature, as is specified in the followings. Firstly dissolve the materials in water respectively, secondly mix, lay the materials still and filter, thirdly mix and filter the dissolved solution and dispose the insoluble; then add the chelating agents, stabilizers and essence to be uniformly dispersed.
Description
One, technical field:
The present invention relates to a kind of deodorizer of health field, especially relate to a kind of preparation method and application of liquid antibiotic deodorizer.
Two, background technology:
Stench be abnormal flavour in the materials such as atmosphere, water, garbage by air dielectric, act on people's olfactory sensation thinking and perceived a kind of perception is polluted.Odorant distributes wide, and the source is many, and coverage is big, people's health is caused serious harm, even become some national public hazards.Thereby, how to remove the stench in the environment safely and efficiently, ensure the quality of environment for human survival, become the focus in the current environment improvement.
At present, the removal method for stink mainly contains:
(1) chemical deodorizing method (oxidizing process, absorption process, absorption method) comprises firing method (flame combustion, catalytic combustion);
(2) physical deodorization method, as cover the method for keeping away, dilution diffusion method etc.;
(3) biological deodorizing method mainly is to utilize microbial deodorant, and the material that physiology and the biochemical metabolism by microorganism will have stink is transformed.
The scope of application of table 1 deodorizing method
| Deodorizing method | The scope of application | Remarks | |
| The physics method | Cover the method for keeping away, | Stench intensity is in uncontrollable discharge source, 2.5 grades of left and right sides | |
| The dilution diffusion method | In, low stench formidable opponent emission source in a organized way | Need build chimney | |
| Firing method | Flame combustion, | The industrial source that the high concentration odorant discharges in a organized way | Fuel consumption is many |
| Catalytic combustion | The industrial source that the high concentration odorant discharges in a organized way | Need catalyst | |
| Chemical oxidization method | The ozone oxidation method | In, low concentration odorant emission source in a organized way | The disposal cost height |
| Catalytic oxidation | In, low concentration odorant emission source in a organized way | Need catalyst | |
| Other oxidizing process | In, low concentration odorant emission source in a organized way | Need the consumption oxidant | |
| Absorption process | The wood absorption process | The industrial source that the water solublity odorant discharges in a organized way | Produce secondary pollution |
| The acid absorption process | The industrial source that acid odorant discharges in a organized way | Need to handle absorption liquid | |
| Alkali absorb method | The alkalescence odorant is emission source in a organized way | Need to handle absorption liquid | |
| The digested sludge absorption process | In, low odorant emission source in a organized way | ||
| Absorption method | In, low odorant emission source in a organized way | Adsorbent need be regenerated | |
| The biological decomposition method | The soil method | High, medium and low odorant is emission source in a organized way | |
| Composting process | |||
| Combination method | The foul smell of complicated component is emission source in a organized way |
Above-mentioned processing method respectively has its pluses and minuses.For the volatile organic waste gas and the foul gas of big flow, low concentration, use that physics and chemical Treatment exist that investment is big, complicated operation, problem that operating cost is high.Along with expanding economy, people are to the raising of environmental quality requirement, good anti-bacterial effect, safe and reliable, easy to use, be fit to the sterilization of various air place, can eliminate stink, and the research of the antibacterial deodorant that in preparation and use human body had no adverse effect of product is significant.
Three, summary of the invention:
The object of the present invention is to provide a kind of preparation method and application of liquid antibiotic deodorizer, its good anti-bacterial effect, safe and reliable, easy to use, be fit to the sterilization of various air place, can eliminate stink, and product has no adverse effect to human body in preparation and use.
For achieving the above object, the technical solution used in the present invention is:
A kind of preparation method of liquid antibiotic deodorizer is characterized in that being being made by the raw material of following weight parts:
Citric acid 〉=1 weight portion
Malic acid 〉=1 weight portion
Lactic acid 〉=3 weight portions
Essence 〉=1 weight portion
Chelating agen 〉=1 weight portion
Stabilizing agent 〉=1 weight portion
Water≤92 weight portions
Preparation process is carried out at normal temperatures, and each component is used water dissolution respectively, and is miscible then, leaves standstill and filters, and the solution after then these being dissolved mixes and filters, and discards insoluble matter, adds chelating agen and stabilizing agent, adds essence at last, is uniformly dispersed.
Above-mentioned preparation method may further comprise the steps:
(1) citric acid is dissolved with deionized water (with the pure water of ion exchange preparation), filter then, discard insoluble matter;
(2) with the malic acid deionized water dissolving, filter then, discard insoluble matter;
(3) with the lactic acid deionized water dissolving;
(4) above-mentioned three part solution are mixed under stirring condition and filter, discard insoluble matter;
(5) chelating agen and stabilizing agent are dissolved in water;
(6) add 0.5-5 ‰ essence, be uniformly dispersed.
Above-mentioned preparation method may further comprise the steps:
(1) take by weighing 1 weight portion citric acid, 1 weight portion malic acid, measuring 3 weight portion content is 90% lactic acid, spends the small amount of deionized water dissolving respectively, filters then, discards insoluble matter;
(2) take by weighing the stabilizing agent Sodium Tvlose or xanthan gum 1.5 weight portions are dissolved in water;
(3) take by weighing chelating agen sodium citrate 1.5 weight portions and be dissolved in water;
(4) above-mentioned solution is mixed, by the proportioning water amount of being settled to;
(5) add 1-5 weight portion essence, being uniformly dispersed promptly gets product.
A kind of application of liquid antibiotic deodorizer is characterized in that: described deodorizer uses for spraying, both can be used as the disinfectant of air or body surface, can be used as foot odor deodorizer again.
Compared with prior art, the advantage and the effect that have of the present invention is as follows:
Four, description of drawings:
Fig. 1 is a process chart of the present invention.
Five, the specific embodiment:
Preparation method of the present invention is that organic acid dissolving back is added chelating agen and stabilizing agent, adds essence at last, and being uniformly dispersed gets product.
Embodiment:
At room temperature take by weighing citric acid, each 1g of malic acid, measure lactic acid (concentration is 90%) 3ml and add fully dissolving in the 1000ml deionized water (with the pure water of ion exchange preparation), filter, discard insoluble matter, take by weighing the stabilizing agent Sodium Tvlose or xanthan gum 1.5g is dissolved in water, take by weighing chelating agen sodium citrate 1.5g and be dissolved in water, add 3g essence then, be uniformly dispersed, promptly obtain finished product, packing.
That deodorizer has is liquid, spraying, roll (roll-on), aerosol, solid, shaped, dosage form such as Powdered.Wherein, the liquid spray type is convenient aspect practical with respect to other dosage form.Therefore, the using method of liquid antibiotic deodorizer of the present invention is the liquid spray method, and it both can be used as the disinfectant of air or body surface, can be used as foot odor deodorizer again.
The indoor rubbish deodorizing test of antibacterial and deodouring spray
In the room of a sealing, put the malodorous rubbish of the highly septic generation of a pile (mainly being house refuse), about 0.5m place evenly establishes 4 sampled points around rubbish, sampled point overhead highly is respectively 1.0m, 1.2m, 1.4m, 1.6m, and each measures before the spray medicine and the NH in the 5min stench behind the spray medicine
3, H
2S concentration.During mensuration, the room atmosphere condition: atmospheric temperature is 28 ℃, and atmospheric pressure is 1 atmospheric pressure.Deodorizing effect sees Table 2:
Odorant NH in the rubbish before and after table 2 microbial deodorant sprays
3, H
2The comparison of S concentration
| Test event | Sampling position (height overhead: m) | Analysis result (mg/m3) | Clearance (%) | |
| Before the spray medicine | Spray medicine (5min) | |||
| NH 3 | 1.0 1.2 1.4 1.6 | 0.8234 0.7832 0.6572 0.6370 | 0.2810 0.2000 0.1423 0.1084 | 65.87 74.46 78.35 82.98 |
| H 2S | 1.0 1.2 1.4 1.6 | 0.112 0.098 0.060 0.058 | 0.037 0.024 0.013 0.018 | 66.96 75.51 78.33 68.97 |
Deodorizer has tangible deodorizing effect, NH to house refuse as shown in Table 2
3The highest clearance can reach 82.98%, H
2The highest clearance of S can reach 78.33%.
Antibacterial deodorant of the present invention purifies the test of animal house air effect
Livestock products public hazards such as the foul smell that produces in the scale animal and poultry cultivation, dust, water pollution, inorganic pollution, pathogen and parasitic ovum cause the concern of the whole society day by day, their control have been become the focus of countries in the world environmental conservation.In these livestock products public hazards, the stink that is caused by fecaluria and other garbages is the problem of a ten minutes headache during herding is produced, and also is one of emphasis in the livestock products public hazards prevention field.The feces in scale chicken farm and stench that is produced and harmful gas cause severe contamination to water quality, soil, air and the crop of surrounding, become the route of infection of infectious disease, parasitic disease and the infecting both domestic animals and human disease of chicken.Particularly ammonia has intensive volatility, the fertility performance of chicken is descended, and be detrimental to health.Evaporate into the H2S in the atmosphere, also can cause acid rain, damage crop.Studies show that harmful gass such as the ammonia of pungent odour and cacodorous hydrogen sulfide are arranged, concentration can make the fertility performance of chicken descend when low, can cause then when concentration is high that chickling is poisoned to death.
It is reported certain laying hen group when 23～26 ages in week, and under no ammonia condition, its laying rate is 70.2%; When ammonia concentration was 52.6 * 10-6, laying rate dropped to 51.5%; When ammonia concentration was 78.3 * 10-6, laying rate dropped to 42.2%.Ammonia and other harmful gass can also make the resistance of chickling reduce, and contacts Avian pneumo-encephalitis virus as chickling in the environment of no ammonia and have only 40% infectedly, and 3 days chickling of raising in the house that contains 20.0 * 10-6 ammonia contacts Avian pneumo-encephalitis virus and infected with regard to 100%.Therefore, adopting an effective measure and eliminate stench and harmful gas in the hen house, is a very important important process guaranteeing chicken group health and improve fertility performance.
Moreover, these malodorant mass-energy influence people and animals' physiological function, stimulate olfactory nerves and nervi trigeminus, and respiratory center is had an effect, and influence people and animals' breathing function, and H2S and NH3 also have intensive toxicity.Therefore, people are utilizing various technology to destroy foul odors to atmospheric pollution at present.
We use antibacterial deodorant that hen house has been carried out deodorizing test, and concrete operations are as follows:
The utilization spraying is pressed every m with deodorizer
3Space even dispenser liquid deodorant on the ground is measured the concentration of ammonia and hydrogen sulfide; Gas sampling CD-1 type portable type air sampler.5 point samplings in the hurdle house are averaged repeated experiments 5 times.Deodorizer is to the degradation effect such as the table 3 of hen house ammonia and hydrogen sulfide:
Table 3 deodorizer is to the degradation effect of ammonia in the hen house and hydrogen sulfide
| Test number (TN) | 1 | 2 | 3 | 4 | 5 | Meansigma methods |
| Before ammonia concentration/mgm-3 throws in before and after ammonia concentration/mgm-3 throws in the house behind the deodorizer ammonia degradation rate in the house/(%) and throws in the house before throwing in the house concentration of hydrogen sulfide/mgm-3 throw in before and after concentration of hydrogen sulfide/mgm-3 throws in the house behind the deodorizer hydrogen sulfide degradation rate in the house/(%) | 67.8 18.0 73.5 21.7 4.0 81.6 | 66.5 17.8 73.2 20.3 3.8 81.3 | 58.2 15.7 73.0 23.4 4.2 82.1 | 48.8 14.7 69.6 19.6 3.6 81.6 | 62.8 17.6 72.0 20.5 3.8 81.5 | 16.8 72.2 3.9 81.8 |
The result shows that this deodorizer can make ammonia and the average respectively degraded 72.5% and 81.8% of hydrogen sulfide in the hen house, and air ammonia and hydrogen sulfide on average drop to 16.8mgm respectively in the house
-3And 3.9mgm
-3, can obviously reduce the stink in the hen house.Studies show that this deodorizer is to purify animal house air cleanser preferably at present.
Claims (4)
1. the preparation method of a liquid antibiotic deodorizer is characterized in that being being made by the raw material of following weight parts:
Citric acid 〉=1 weight portion
Malic acid 〉=1 weight portion
Lactic acid 〉=3 weight portions
Essence 〉=1 weight portion
Chelating agen 〉=1 weight portion
Stabilizing agent 〉=1 weight portion
Water≤92 weight portions
Preparation process is carried out at normal temperatures, and each component is used water dissolution respectively, and is miscible then, leaves standstill and filters, and the solution after then these being dissolved mixes and filters, and discards insoluble matter, adds chelating agen and stabilizing agent, adds essence at last, is uniformly dispersed.
2. the preparation method of a kind of liquid antibiotic deodorizer according to claim 1, it is characterized in that: described preparation method may further comprise the steps:
(1) citric acid is dissolved with deionized water (with the pure water of ion exchange preparation), filter then, discard insoluble matter;
(2) with the malic acid deionized water dissolving, filter then, discard insoluble matter;
(3) with the lactic acid deionized water dissolving;
(4) above-mentioned three part solution are mixed under stirring condition and filter, discard insoluble matter;
(5) chelating agen and stabilizing agent are dissolved in water;
(6) add 0.5-5 ‰ essence, be uniformly dispersed.
3. the preparation method of a kind of liquid antibiotic deodorizer according to claim 1 and 2, it is characterized in that: described preparation method may further comprise the steps:
(1) take by weighing 1 weight portion citric acid, 1 weight portion malic acid is measured 3 weight portion content and is 90% lactic acid, spends the small amount of deionized water dissolving respectively, filters then, discards insoluble matter;
(2) take by weighing the stabilizing agent Sodium Tvlose or xanthan gum 1.5 weight portions are dissolved in water;
(3) take by weighing chelating agen sodium citrate 1.5 weight portions and be dissolved in water;
(4) above-mentioned solution is mixed, by the proportioning water amount of being settled to;
(5) add 1-5 weight portion essence, being uniformly dispersed promptly gets product.
4. the application of a kind of liquid antibiotic deodorizer according to claim 1 is characterized in that: described deodorizer uses for spraying, both can be used as the disinfectant of air or body surface, can be used as foot odor deodorizer again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100178930A CN101108257A (en) | 2007-05-18 | 2007-05-18 | Method of preparing liquid antibiotic deodorizer and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100178930A CN101108257A (en) | 2007-05-18 | 2007-05-18 | Method of preparing liquid antibiotic deodorizer and application thereof |
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| Publication Number | Publication Date |
|---|---|
| CN101108257A true CN101108257A (en) | 2008-01-23 |
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|---|---|---|---|
| CNA2007100178930A Pending CN101108257A (en) | 2007-05-18 | 2007-05-18 | Method of preparing liquid antibiotic deodorizer and application thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101843244A (en) * | 2010-05-05 | 2010-09-29 | 刘思波 | Thermochemical sterilizing liquid for haemodialysis machine |
| US20120045525A1 (en) * | 2008-11-20 | 2012-02-23 | Zhejiang Forestry College | Mosquito repellent solution, preparation method and use thereof |
| CN103239741A (en) * | 2013-05-30 | 2013-08-14 | 唐煦轮 | Three-acid deodorant |
| CN103800928A (en) * | 2014-03-06 | 2014-05-21 | 苏州爱德芬生物科技有限公司 | Antibiotic deodorant |
| CN103861138A (en) * | 2014-03-24 | 2014-06-18 | 王镭 | Efficient deodorant with surface absorption function and use method of deodorant |
| CN109876621A (en) * | 2019-03-07 | 2019-06-14 | 湖北省农业科学院畜牧兽医研究所 | A kind of end removing means and deodorizing methods for livestock manure fermented foul smell |
| CN110787132A (en) * | 2019-12-17 | 2020-02-14 | 河南牧翔动物药业有限公司 | Veterinary disinfectant citric acid and malic acid powder and preparation method thereof |
| CN111202067A (en) * | 2020-03-06 | 2020-05-29 | 吉林云飞医药有限公司 | Citric acid disinfectant and preparation method and application thereof |
| CN112755231A (en) * | 2020-12-29 | 2021-05-07 | 南京凯创微锌环境技术有限公司 | Preparation method of chicken farm deodorant |
-
2007
- 2007-05-18 CN CNA2007100178930A patent/CN101108257A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120045525A1 (en) * | 2008-11-20 | 2012-02-23 | Zhejiang Forestry College | Mosquito repellent solution, preparation method and use thereof |
| CN101843244A (en) * | 2010-05-05 | 2010-09-29 | 刘思波 | Thermochemical sterilizing liquid for haemodialysis machine |
| CN103239741A (en) * | 2013-05-30 | 2013-08-14 | 唐煦轮 | Three-acid deodorant |
| CN103800928A (en) * | 2014-03-06 | 2014-05-21 | 苏州爱德芬生物科技有限公司 | Antibiotic deodorant |
| CN103861138A (en) * | 2014-03-24 | 2014-06-18 | 王镭 | Efficient deodorant with surface absorption function and use method of deodorant |
| CN109876621A (en) * | 2019-03-07 | 2019-06-14 | 湖北省农业科学院畜牧兽医研究所 | A kind of end removing means and deodorizing methods for livestock manure fermented foul smell |
| CN110787132A (en) * | 2019-12-17 | 2020-02-14 | 河南牧翔动物药业有限公司 | Veterinary disinfectant citric acid and malic acid powder and preparation method thereof |
| CN111202067A (en) * | 2020-03-06 | 2020-05-29 | 吉林云飞医药有限公司 | Citric acid disinfectant and preparation method and application thereof |
| CN112755231A (en) * | 2020-12-29 | 2021-05-07 | 南京凯创微锌环境技术有限公司 | Preparation method of chicken farm deodorant |
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Open date: 20080123 |