CN101082560A - Vacuum apparatus including a particle monitoring unit, particle monitoring method and program, and window member for use in the particle monitoring - Google Patents
Vacuum apparatus including a particle monitoring unit, particle monitoring method and program, and window member for use in the particle monitoring Download PDFInfo
- Publication number
- CN101082560A CN101082560A CN 200710139134 CN200710139134A CN101082560A CN 101082560 A CN101082560 A CN 101082560A CN 200710139134 CN200710139134 CN 200710139134 CN 200710139134 A CN200710139134 A CN 200710139134A CN 101082560 A CN101082560 A CN 101082560A
- Authority
- CN
- China
- Prior art keywords
- particle
- particle monitoring
- gas
- window member
- process chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Abstract
The present invention provides a particle which can practically monitor the particle including the deposit that is easily stripped, and a particle monitoring used window component which can accurately evaluate the cleaning degree of the vacuum apparatus. The particle monitoring used window component is composed of the transparent base component arranged between the frame body which forms the scheduled space and the particle monitoring apparatus which monitors the particle in the frame body, and the base component is composed of a transparent base and a surface treating layer which actuates scheduled treatment to the opposite surface of the gas in the frame body of the base.
Description
(the application is that the application number that proposed on March 29th, 2005 is dividing an application of 2005100601714 application of the same name)
Technical field
The present invention relates to be provided with vacuum plant and particle monitoring method, program and the window part for particle monitoring of particle monitoring.
Background technology
For to goods processing such as semiconductor wafer (hereinafter referred to as " wafer ") enforcement etch processes, use the semiconductor-fabricating device (Figure 10) of using plasma.When the goods processing, because being attached on the wafer of goodsization, the particle that produces causes pollution, yield rate reduces, and therefore, requires the cleanliness of height for semiconductor-fabricating device.
Figure 10 is an organigram of roughly representing semiconductor-fabricating device in the past.
Among Figure 10, semiconductor-fabricating device 800 possesses the process chamber of the cylindrical vessel of wafer enforcement goods processing being made by being used for 810.In process chamber 810 inside, be provided with the wafer station of having buried the electrode that can apply high voltage (HV:High Voltage) underground, the wafer mounting is on this wafer station.On the top of process chamber 800, dispose the shower nozzle 811a that is provided with a plurality of through holes, shower nozzle 811a imports employed corrosive processing in the process chamber 810 with gas (processing gas) when the goods processing by these through holes.
In addition, on the process chamber 810, its top is connected with the suction line of being made by the tubular part that is used to import purge gas, and this suction line is provided with the valve 811 of the purge gas flow that restriction will supply with to process chamber 810.Be connected with the main vacuum lines of making by the thin tube-like parts 830 of taking out pipeline 820 in advance and making in the bottom, take out pipeline 820 in advance and main vacuum lines 830 is collaborated on exhaust line by extra heavy pipe shape parts.
Taking out pipeline 820 in advance is provided with: the dry pump (DP:Dry Pump) 822 and the valve 821 of restriction by the gas flow of dry pump 822 discharges of discharging the gas in the process chamber 810 by exhaust line.
On the main vacuum lines 830 from process chamber 810 1 sides be disposed with automatic pressure adjusting gear (APC:Auto Pressure Controller) 831, as the isolation valve (ISO:Isolation Valve) 832 of gate valve, the turbomolecular pump (TMP:Turbo-Molecular Pump) 833 that air capacity is also bigger than dry pump 822.
In semiconductor-fabricating device 800, in order to carry out the goods processing, during pressure in reducing process chamber 810, the gases in the process chamber 810 are discharged by taking out pipeline 820 in advance, after the valve-off 821, make process chamber 810 reach required vacuum tightness by main vacuum lines 830.When carrying out the goods processing,, require high vacuum if carry out etch processes.In carrying out the goods processing,, continue exhaust by main vacuum lines 830 in order to keep vacuum tightness.
After the goods processing finishes, by suction line purge gas is supplied with process chamber 810, carry out exhaust by exhaust line, like this, discharge the particle that swims in process chamber 810 from process chamber 810 with purge gas, with purge gas clean process chamber 810 (such as, with reference to patent documentation 1).
In addition, in order to estimate the cleanliness of process chamber 810, be provided with the optical profile type particle monitoring device of selling on the market (PM:particle monitoring device) (not shown), attempt monitor particles.
In order to monitor the particle that is discharged from when the goods processing in real time, the particle monitoring device many between the automatic pressure adjusting gear 831 and process chamber 810 on the main vacuum lines 830, between automatic pressure adjusting gear 831 and isolation valve 832 or, on process chamber 810, be provided with.
In addition, in the particle monitoring device, the parts such as lens of the glass processing gas etch of being corroded property easily particularly, for example, bring into use a week after, glass parts generation albefaction.Therefore, need to change these parts or keep in repair, not only the cost of semiconductor-fabricating device 800 is ascended to heaven, and reduce service time.In contrast, take out in advance on the pipeline 820, can prevent that the glass parts of particle monitoring device from corroding by the particle monitoring device is arranged on.
The particle monitoring device is owing to be difficult to monitor under high vacuum with the particle such as the high-speed mobile of 20m/sec, so, in order to improve the particle detection accuracy rate, propose a kind of like this technical scheme: the gas flow area of the exhaust line of main vacuum lines 830 grades that restricted passage is made by extra heavy pipe shape parts comes monitor particles.(such as, with reference to patent documentation 2).
In addition, the semiconductor-fabricating device among Figure 10 800 possess with process chamber 810 opposite faces be provided with by quartz glass (SiO
2) the transparent window member (not shown) made, this window member is such as playing a role as the window that is used for importing microwave to process chamber 810 in.
Be in the environment that fluorine is a plasma if constitute the quartz glass of window member, then (Si) atom of the silicon in the quartz glass and fluorine are that the bioactive molecule of the fluoro free radical that contains of plasma etc. reacts, as silicon fluoride (SiF
4) volatilization, thereby pollute wafer, perhaps window member is corroded from the surface, produces scared (deterioration).
In order to suppress this deterioration, heat quartz glass usually.In addition, in order to suppress the deterioration of window member, aluminium oxide (Al has been proposed
2O
3) and quartzy second window member of making of making by the parts that are dispersed with first phase of making by quartz in mutually (such as, with reference to patent documentation 3).In addition, though be not window member, the material that is in following state is come out by motion: the parts that use in process chamber as glass bell jar, focusing ring etc. make silicon dioxide (SiO
2) in contain aluminium (Al) and carry out fusion, become silicon dioxide and aluminium dioxide amorphous material (such as, with reference to patent documentation 4).No matter which kind of technology contains aluminium by making in the predetermined components, and improving for fluorine is the tolerance of plasma or bioactive molecule.
(patent documentation 1) opens flat 06-056999 communique in fact
(patent documentation 2) spy opens flat 11-304688 communique
(patent documentation 3) spy opens the 2001-261364 communique
(patent documentation 4) spy opens the 2003-292337 communique
,, only monitor the particle that moves with the gas of discharging, therefore, can't monitor attached to the sediment on the inwall of process chamber 810 (deposit) from process chamber 810 according to the technology of above-mentioned patent documentation 1,2 records.
Sediment strips down from this inwall in the goods processing, becomes the reason of polluting wafer, therefore, requires more correctly to estimate the cleanliness of process chamber 810 by sediment is monitored energetically as particle.
In addition, if for the deterioration that suppresses window member heats, unfavorable condition can take place in the circuit that then is arranged on the inside of semiconductor-fabricating device 800, has perhaps promoted the deterioration of laser aid.
Moreover, according to the above-mentioned technology that contains aluminium in the predetermined parts that makes, the aluminium atom is in the state of dispersion in silicon dioxide or quartz, therefore, can not bring into play plasma-resistance efficiently on the surface or for the tolerance of bioactive molecule, the replacing frequency of these predetermined parts increases.Its result, it is elongated to change required time, and the productive capacity of semiconductor-fabricating device 800 reduces, and simultaneously, renewal cost rises, and the cost of semiconductor-fabricating device 800 improves.In addition, reduce or the viewpoint that suppresses cost is considered from the productive capacity that prevents semiconductor-fabricating device 800, also require to reduce the replacing frequency such as the window part for particle monitoring that possesses the particle monitoring device that connects main vacuum lines of semiconductor-fabricating device 800.
Summary of the invention
First purpose of the present invention is: provide a kind of can the monitoring effectively to comprise the sedimental particle of easily peeling off, correctly estimate vacuum plant and the particle monitoring method and the program of the cleanliness of vacuum plant.
Second purpose of the present invention is: a kind of tolerance that can bring into play efficiently for bioactive molecule is provided, makes and change the window part for particle monitoring that frequency reduces.
In order to realize above-mentioned first purpose, the vacuum plant of the present invention the 1st aspect possesses: the container that forms predetermined space; Discharge the exhaust gear of gas in the described container by predetermined gas outlet; At least one is arranged on the described gas outlet, limits the exhaust limiting mechanism of the described gas flow that is discharged from; Between described at least one exhaust limiting mechanism and described exhaust gear, be arranged on the described gas outlet, monitor the particle monitoring mechanism of the particle in the described gas outlet, it is characterized in that: have the wiper mechanism of in described container, supplying with purge gas by predetermined supply pipe; And between described wiper mechanism and described container, be arranged on the described supply pipe, limit the supply limiting mechanism of the described purge gas flow that is supplied to; When described supply limiting mechanism allows to discharge described gas at described at least one exhaust limiting mechanism, begin to supply with described purge gas; Described monitored particle contains supply by described purge gas and is free on particle in the described container.
The vacuum plant of the present invention the 2nd aspect is the described vacuum plant in the 1st aspect according to the present invention, it is characterized in that:
Possess: in described container, supply with corrosive processing with the processing of gas with gas supply mechanism with discharge other exhaust gears of described processing usefulness gas;
Described at least one exhaust limiting mechanism forbids discharging described gas discharging described processing by described other exhaust gears when using gas.
The vacuum plant of the present invention the 3rd aspect is the described vacuum plant in the 1st or 2 aspects according to the present invention, it is characterized in that: the flow of the described purge gas that is supplied to of described supply limiting mechanism restriction makes the force value of described purge gas reach interior more than 2 times of force value of described container.
The vacuum plant of the present invention the 4th aspect is each described vacuum plant in the 1st～3 aspect according to the present invention, it is characterized in that:
Possesses the electric power feed mechanism that in described container, discharges;
When described electric power feed mechanism allows to discharge described gas at described at least one exhaust limiting mechanism, begin to carry out described discharge;
Described monitored particle contains by described discharge particle free in described container.
In order to realize above-mentioned first purpose, the vacuum plant of the present invention the 5th aspect possesses: the container that forms predetermined space; Discharge the exhaust gear of gas in the described container by predetermined gas outlet; Be arranged on the described gas outlet, limit at least one exhaust limiting mechanism of the described gas flow that is discharged from; Between described at least one exhaust limiting mechanism and described exhaust gear, be arranged on the described gas outlet, monitor the particle monitoring mechanism of the particle in the described gas outlet, it is characterized in that:
Possesses the electric power feed mechanism that in described container, discharges;
When described electric power feed mechanism allows to discharge described gas at described at least one exhaust limiting mechanism, begin to carry out described discharge;
Described monitored particle contains by described discharge particle free in described container.
The described vacuum plant in the present invention the 6th aspect is the described vacuum plant in the 5th aspect according to the present invention, it is characterized in that: described electric power feed mechanism produces electromagnetic stress by described discharge in described container.
The described vacuum plant in the present invention the 7th aspect is the described vacuum plant in the 5th or 6 aspects according to the present invention, it is characterized in that:
Possess: the wiper mechanism of in described container, supplying with purge gas by predetermined supply pipe; Between described wiper mechanism and described container, be arranged on the described supply pipe, limit the supply limiting mechanism of the described purge gas flow that is supplied to;
When described supply limiting mechanism allows to discharge described gas at described at least one exhaust limiting mechanism, begin to supply with described purge gas;
Described monitored particle contains by the supply of described purge gas particle free in described container.
In order to realize above-mentioned first purpose, the present invention the 8th aspect is a kind of particle monitoring method that possesses the vacuum tank of the container that forms predetermined space, it is characterized in that having:
By the steps of exhausting of predetermined gas outlet with the discharge of the gas in the described container;
Monitor the particle monitoring step of the particle in the described gas outlet;
Limit the exhaust conditioning step of the described gas flow that is discharged from;
In described container, supply with the cleaning step of purge gas by predetermined supply pipe; With
Limit the supply conditioning step of the described purge gas flow that is supplied to,
In described supply conditioning step, when allowing to discharge described gas, described exhaust conditioning step begins to supply with described purge gas;
Described monitored particle contains by the supply of described purge gas particle free in described container.
The particle monitoring method of the present invention the 9th aspect is the described particle monitoring method in the 8th aspect according to the present invention, it is characterized in that:
Have: in described container, supply with corrosive processing and use the gas supplying step with the processing of gas and discharge described processing other steps of exhausting with gas,
In the described exhaust conditioning step, discharge described processing when using gas, forbid discharging described gas in described other steps of exhausting.
The described particle monitoring method in the present invention the 10th aspect is the described particle monitoring method in the 8th or 9 aspects according to the present invention, it is characterized in that:
In described supply conditioning step, limit the flow of the described purge gas that is supplied to, make the force value of described purge gas reach interior more than 2 times of force value of described container.
The described particle monitoring method in the present invention the 11st aspect is each described particle monitoring method in the 8th～10 aspect according to the present invention, it is characterized in that:
Has the discharge step of in described container, discharging;
In described discharge step, when described exhaust conditioning step allows to discharge described gas, begin to carry out described discharge;
Described monitored particle contains by described discharge particle free in described container.
In order to realize above-mentioned first purpose, the present invention the 12nd aspect is a kind of particle monitoring method that possesses the vacuum tank of the container that forms predetermined space, has: by the steps of exhausting of predetermined gas outlet with the discharge of the gas in the described container;
Limit the exhaust conditioning step of the described gas flow that is discharged from;
Monitor the particle monitoring step of the particle in the described gas outlet; It is characterized in that,
Has the discharge step of in described container, discharging;
In described discharge step, when described exhaust conditioning step allows to discharge described gas, begin to carry out described discharge;
Described monitored particle contains by described discharge particle free in described container.
The described particle monitoring method in the present invention the 13rd aspect is the described particle monitoring method in the 12nd aspect according to the present invention, it is characterized in that:
In described discharge step, in described container, produce electromagnetic stress by described discharge.
The described particle monitoring method in the present invention the 14th aspect is the described particle monitoring method in the 12nd or 13 aspects according to the present invention, it is characterized in that:
Have: in described container, supply with the cleaning step of purge gas and the supply conditioning step of the described purge gas flow that is supplied to of restriction by predetermined supply pipe;
In described supply conditioning step, when described exhaust conditioning step allows to discharge described gas, begin to supply with described purge gas;
Described monitored particle contains by the supply of described purge gas particle free in described container.
In order to realize above-mentioned first purpose, the present invention the 15th aspect is a kind of to make the program of the particle monitoring method of the vacuum tank that computer run possesses the container that forms predetermined space, it is characterized in that:
Possess: the particle monitoring program element of the vent sequence unit of the gas in the described container being discharged by predetermined gas outlet, the particle in the described gas outlet of monitoring, the exhaust limiting program unit of the described gas flow that is discharged from of restriction, in described container, supply with the cleaning procedure unit of purge gas and limit the supply limiting program unit of the described purge gas flow that is supplied to by predetermined supply pipe
Described supply limiting program unit begins to supply with described purge gas when allowing to discharge described gas in described exhaust limiting program unit;
Described monitored particle contains by the supply of described purge gas particle free in described container.
In order to realize above-mentioned first purpose, the present invention the 16th aspect is described to be a kind of program of particle monitoring method of vacuum tank of the container that computer run is possessed form predetermined space, it is characterized in that:
Possess: the vent sequence unit of the gas in the described container being discharged by predetermined gas outlet, the exhaust limiting program unit of the described gas flow that is discharged from of restriction, the particle monitoring program element of the particle in the described gas outlet of monitoring and the discharge procedures unit that in described container, discharges;
Described discharge procedures unit when allowing to discharge described gas in described exhaust limiting program unit, begins to carry out described discharge;
Described monitored particle contains by described discharge particle free in described container.
In order to realize above-mentioned second purpose, the present invention the 17th aspect is described to be a kind of window part for particle monitoring, by in the framework that forms predetermined space with monitor the transparent substrate that is provided with between the particle monitoring device of the particle in this framework and make, it is characterized in that:
Described substrate by transparent pedestal and with this pedestal on described framework in the face of gas opposite face on implement predetermined process surface-treated layer constitute.
The described window member in the present invention the 18th aspect is the described window member in the 17th aspect according to the present invention, it is characterized in that:
Described surface-treated layer contains a kind of material that is selected from carbon, yttrium, yttria and the calcium fluoride.
The described window member in the present invention the 19th aspect is the described window member in the 18th aspect according to the present invention, it is characterized in that:
Described carbon is made by crystalloid adamas or diamond-like-carbon.
The described window member in the present invention the 20th aspect is the described window member in the 18th or 19 aspects according to the present invention, it is characterized in that:
Described a kind of material, its amount is in the whole quality of described surface-treated layer, in the scope of 10～100 quality %.
The described window member in the present invention the 21st aspect is the described window member in the 17th aspect according to the present invention, it is characterized in that:
Described surface-treated layer contains aluminium or aluminium oxide.
The described window member in the present invention the 22nd aspect is the described window member in the present invention the 21st aspect, it is characterized in that:
Described aluminium or aluminium oxide, its amount is in the whole quality of described surface-treated layer, in the scope of 10～100 quality %.
The described window member in the present invention the 23rd aspect is each described window member in the 17th～22 aspect according to the present invention, it is characterized in that:
Described predetermined process is handled for coating.
The described window member in the present invention the 24th aspect is each described window member in the 17th～22 aspect according to the present invention, it is characterized in that:
Described predetermined process is a doping treatment.
The described window member in the present invention the 25th aspect is each described window member in the 17th～24 aspect according to the present invention, it is characterized in that:
Described surface-treated layer, its thickness is in the scope of 100nm～10 μ m.
The described window member in the present invention the 26th aspect is each described window member in the 17th～25 aspect according to the present invention, it is characterized in that:
Described pedestal is made by the glass that with silicon is major component;
Described surface-treated layer is in the interior bioactive molecule that gas contained of described framework.
In order to realize above-mentioned second purpose, the present invention the 27th aspect is described to be a kind of window part for particle monitoring, by in the framework that forms predetermined space with monitor the transparent substrate that is provided with between the particle monitoring device of the particle in this container and make, it is characterized in that:
Described substrate is made by calcium fluoride.
The described window member in the present invention the 28th aspect is each described window member in the 17th～27 aspect according to the present invention, it is characterized in that:
Described framework is made by container or pipe arrangement.
The effect of invention
The described program of particle monitoring method or the present invention the 15th aspect of the described vacuum plant in the 1st aspect, the described vacuum plant in the present invention the 8th aspect according to the present invention, since when allow discharging gas by beginning to supply with purge gas, free particle obtains monitoring in described container, therefore, can monitor effectively and contain the sedimental particle of easily peeling off, correctly estimate the cleanliness of vacuum plant.
The particle monitoring method of the described vacuum plant of the described vacuum plant in the 2nd aspect or the present invention the 9th aspect according to the present invention, can be in the discharge of the gas of the gas outlet of discharging by other gas outlets that no thoroughfare when handling with gases, prevent that the particle monitoring device is corroded, and prolongs its life-span.
The particle monitoring method of the described vacuum plant of the described vacuum plant in the 3rd aspect or the present invention the 10th aspect according to the present invention, limit the flow of the described purge gas that is supplied to, make the force value of purge gas reach interior more than 2 times of force value of container, therefore, can make to produce shock wave in the container conscientiously, sediment is stripped down.
The particle monitoring method of the described vacuum plant of the described vacuum plant in the 4th aspect or the present invention the 11st aspect according to the present invention, except that the particle free by supplying with purge gas, the particle that enters in the container by the discharge that begins when allowing to discharge gas obtains monitoring, therefore, can monitor more effectively and contain the sedimental particle of easily peeling off, more correctly estimate the cleanliness of vacuum plant.
The described program of particle monitoring method or the present invention the 16th aspect of the described vacuum plant in the 5th aspect, the described vacuum plant in the present invention the 12nd aspect according to the present invention, free particle obtains monitoring in container by the discharge that begins when allowing to discharge gas, therefore, can monitor more effectively and contain the sedimental particle of easily peeling off, more correctly estimate the cleanliness of vacuum plant.
The particle monitoring method of the described vacuum plant of the described vacuum plant in the 6th aspect or the present invention the 13rd aspect according to the present invention owing to produce electromagnetic stress by discharge in container, therefore, can make sediment strip down effectively.
The particle monitoring method of the described vacuum plant of the described vacuum plant in the 7th aspect or the present invention the 14th aspect according to the present invention, except that the particle that in container, dissociates by the discharge that when allowing to discharge gas, begins, free particle obtains monitoring by supplying with purge gas, therefore, can monitor more effectively and contain the sedimental particle of easily peeling off, more correctly estimate the cleanliness of vacuum plant.
The described window part for particle monitoring in the 17th aspect according to the present invention, transparent substrate by transparent pedestal and with this pedestal on container in the face of gas opposite face on implemented predetermined process surface-treated layer constitute, therefore, can bring into play tolerance efficiently, reduce and change frequency for bioactive molecule.
The described window part for particle monitoring in the 18th aspect according to the present invention, described surface-treated layer contains a kind of material that is selected from carbon, yttrium, yttria and the calcium fluoride, therefore, on surface-treated layer, can bring into play tolerance more efficiently, reduce effectively and change frequency for bioactive molecule.
The described window part for particle monitoring in the 20th aspect according to the present invention, the amount of the material of formation surface-treated layer in the scope of 10～100 quality %, therefore, can improve the tolerance for bioactive molecule in the whole quality of surface-treated layer.
The described window part for particle monitoring in the 21st aspect according to the present invention, surface-treated layer contains aluminium or aluminium oxide, therefore, can bring into play the tolerance for bioactive molecule more efficiently on surface-treated layer, reduces effectively and changes frequency.
The described window part for particle monitoring in the 22nd aspect according to the present invention, the amount of aluminium or aluminium oxide in the scope of 10～100 quality %, therefore, can improve the tolerance for bioactive molecule in the whole quality of surface-treated layer.
The described window part for particle monitoring in the 23rd aspect according to the present invention, predetermined process is handled for coating, therefore, surface-treated layer can be set on pedestal easily.
The described window part for particle monitoring in the 24th aspect according to the present invention, predetermined process is a doping treatment, therefore, surface-treated layer can be set on pedestal effectively.
Therefore the described window part for particle monitoring in the 25th aspect according to the present invention, the thickness of surface-treated layer, can improve the tolerance for bioactive molecule in the scope of 100nm～10 μ m.
The described window part for particle monitoring in the 26th aspect according to the present invention, pedestal is made by the glass that with silicon is major component, surface-treated layer is in the plasma environment that generates in the container, therefore, can prevent that silicon is in the plasma environment, simultaneously, bring into play tolerance efficiently, reduce effectively and change frequency for bioactive molecule at surface-treated layer.
The described window part for particle monitoring in the 27th aspect according to the present invention, transparent substrate is made by calcium fluoride, therefore, can bring into play the tolerance for bioactive molecule efficiently, reduces and changes frequency.
Description of drawings
Fig. 1 possesses the synoptic diagram of the semiconductor-fabricating device structure of the vacuum plant that relates to first embodiment of the invention for expression roughly.
Fig. 2 is the synoptic diagram of particle monitoring device construction in the presentation graphs 1 roughly.
The curve map of the intensity of the detection signal that Fig. 3 is measured by the photo detector of particle monitoring device among Fig. 2 for expression.
Fig. 4 is the time diagram of expression by the order of the particle monitoring method of semiconductor-fabricating device execution among Fig. 1.
Fig. 5 is in the order of presentation graphs 4, the curve map of the amounts of particles of being measured by the particle monitoring device.
Fig. 6 possesses the synoptic diagram of the semiconductor processing device structure of the vacuum plant that relates to the 3rd embodiment of the present invention for expression roughly.
Fig. 7 is the time diagram of expression by the order of the particle monitoring method of the vacuum carrying device execution of Fig. 6.
Fig. 8 relates to the sectional view of the structure of the window part for particle monitoring of four embodiment of the invention for expression at length.
Fig. 9 is the partial cross section figure of the structure of semiconductor-fabricating device in the presentation graphs 1 at length.
Figure 10 is an organigram of roughly representing semiconductor-fabricating device in the past.
Symbol description: 100 process chambers, 110 chamber walls, 111 wafer station, 112 high-voltage power supplies, 120 valves, 200 take out pipeline in advance, 210 particle monitoring devices (PM), 219,340 window part for particle monitoring, 219a pedestal, the 219b surface-treated layer, 220 dry pump (DP), 300 main vacuum lines, 310 automatic pressure adjusting gears (APC), 320 isolation valves (ISO), 1000 semiconductor-fabricating devices.
Embodiment
Below, explain embodiments of the present invention with reference to accompanying drawing.
Fig. 1 possesses the synoptic diagram of the semiconductor-fabricating device structure of the vacuum plant that relates to first embodiment of the invention for expression roughly.
Among Fig. 1, semiconductor-fabricating device 1000 possesses the process chamber of being made by cylindrical vessel 100 (vacuum plant), and its commercialization that has been used for to the employing of having implemented etching or sputter, CVD (chemical vapor deposition) etc. as the semiconductor wafer (hereinafter referred to as " wafer ") of handled object plasma is handled.Process chamber 100 is connected on the load locking room of the carrying arm that possesses the conveyance wafer, and by the carrying arm of this load locking room, wafer is moved into process chamber 100.
In addition, on process chamber 100 tops, connecting the suction line of being made by tubular part that is used to import purge gas, suction line is provided with restriction should be supplied with valve 120 from the flow of purge gas to process chamber 100.
As purge gas, can use corrosivity low, obtain and low-cost gas easily, this gas has nitrogen (N
2), helium (He), argon gas (Ar), dry air, oxygen (O
2) etc.In addition, halogen gas is because the parts of the glass of corrosion aftermentioned particle monitoring device, so, use improper as purge gas.
In process chamber 100 bottoms, be connected with the main vacuum lines of making such as the thin tube-like parts that by diameter are 25mm 300 of taking out pipeline 200 in advance and making, take out pipeline 200 in advance and main vacuum lines 300 is collaborated at exhaust line such as the extra heavy pipe shape parts that by diameter are 150mm.Exhaust line will be discharged to the outside of semiconductor-fabricating device 1000 from the gas of taking out pipeline 200 and/or main vacuum lines 300 in advance.
Taking out pipeline 200 in advance is provided with: discharge valve a, the b of the gas flow that the dry pump (DP) 220 of the gas in the process chamber 100, gas flow that restricted passage dry pump 220 is discharged promptly flow into to exhaust line from process chamber 100 and the optical profile type particle monitoring device (PM) 210 of monitor particles between valve a, b by exhaust line.
Be provided with in order from process chamber 100 1 sides on the main vacuum lines 300: the automatic pressure adjusting gear (APC) 310 of the pressure in the monitoring process chamber 100, as the isolation valve (ISO) 320 of gate valve, the turbomolecular pump (TMP) 330 that is connected with above-mentioned dry pump 220.The exhaust of the process chamber 100 that isolation valve 320 restriction turbomolecular pumps 330 are controlled.Automatic pressure adjusting gear 310 is monitored the pressure of process chamber 100 on one side, Yi Bian adjust the limited degree of isolation valve 320.Turbomolecular pump 330 is compared with dry pump 220, and air capacity is bigger.
In the semiconductor-fabricating device 1000, in order to carry out the goods processing, when reducing the pressure of process chamber 100, by taking out pipeline 200 in advance, the pressure exhaust of process chamber 100 is to predetermined pressure, after valve-off a, the b, by main vacuum lines 300, monitor the pressure of process chambers 100 on one side by automatic pressure adjusting gear 310, Yi Bian make it to reach required pressure or vacuum.When the goods processing is carried out, owing to be fed in the process chamber 100 by the corrosive processing gas of above-mentioned shower nozzle 120a, so the exhaust of being undertaken by main vacuum lines 300 is continued.
Fig. 2 is the synoptic diagram of particle monitoring device construction in the presentation graphs 1 roughly.
Among Fig. 2, particle monitoring device 210 possesses: the framework 211 that surrounds the periphery configuration of taking out pipeline 200 in advance, irradiation is such as the LASER Light Source 212 of the laser of the wavelength in visible light zone, to in framework 211, take out catoptron 213 on the pipeline 200 in advance from the laser leaded light of LASER Light Source 212 irradiation, the beam baffle plate (damper) 214 of the light institute incident by taking out pipeline 200 in advance, accept by the photo detector 215 of the laser at random of the particle by taking out pipeline 200 in advance by being arranged on the window part for particle monitoring of making by quartz 219 on the framework 211, the lens 216 of the laser polymerization at random on the photo detector 215 will be incident on.As with Fig. 3 aftermentioned, will measure as detection signal by the laser that photo detector 215 is accepted.Above-mentioned window part for particle monitoring 219 disposes at a predetermined angle for the incident direction of laser.
Take out pipeline 200 in advance at least in the part that laser shone, for passing through by magnesium fluoride (MgF
2) quartz glass that waits the antireflection film of making to apply one part surface or whole surface makes.
The curve map of the intensity of the detection signal that Fig. 3 is measured by the photo detector 215 of particle monitoring device 210 among Fig. 2 for expression.
As shown in Figure 3, in the signal of measuring by photo detector 215, contain the undesired signal that produces because of the scattering of loosing regularly.This undesired signal is owing to having the predetermined interference wide cut, so be set with the threshold value that applies the signal intensity of predetermined edge value on the higher limit of disturbing wide cut in particle monitoring device 210.
Fig. 4 is the time diagram of expression by the instruction sequences of the particle monitoring method of 1000 execution of semiconductor-fabricating device among Fig. 1.
As shown in Figure 4, finishing the goods processing takes out of after the wafer, when monitor particles, at first, in the power supply of connecting particle monitoring device 210, open valve a, the b of process chamber 100 1 sides, simultaneously, in the power supply of closing automatic pressure adjusting gear 310, close isolation valve 320 (not shown).Like this, the exhaust of process chamber 100 switches to from main vacuum lines 300 and to take out pipeline 200 in advance.
Then, open valve 120, purge gas is supplied with process chamber 100 with the higher flow value of cleaning than the purge gas that is used in the past of flow value such as 70L/min (70000SCCM) by suction line.Process chamber 100 is usually such as 10
-1-10
-4Carry out the goods processing under the high vacuum environment of Pa, so purge gas rises the force value in the process chamber 100 to flow into hastily in the process chamber 100 than the higher force value of force value in the process chamber 100.Rise the final stable arrival force value that reached preferably more than 133.3Pa (1Torr) by this force value.By making the stable force value that arrives more than 133.3Pa, give and discharge gas with bigger viscous force, can easily discharge particle with this gas.
Therefore, the storewide in the process chamber 100 is given in the inflow rapidly of purge gas, i.e. chamber wall 110 and the wafer station 120 physical property vibration to produce because of shock wave.
For the force value that makes purge gas reaches more than 2 times of force value in the process chamber 100, purge gas is preferably supplied with by suction line.Like this, can give object in the process chamber 100 effectively with vibration.
Under state that valve 120 open, from high-voltage power supply 112 to electrode 113 apply 3 time high voltage HV thereafter.About applying of these high voltages HV, as the second embodiment aftermentioned of the present invention it.
When finishing the monitoring of particle, valve-off 120 and valve a, b open isolation valve 320 in order, turn back to the state after the goods processing finishes.
This order is because execution after finishing the goods processing and taking out of wafer, so, can prevent the pollution of wafer.In addition, preferably when not using processing gas, carry out.Like this, the glass parts that can prevent particle monitoring device 210 corrode.
According to Fig. 4, when monitor particles, the object in the process chamber 100 is given in the physical property vibration (shock wave) that will be produced by purge gas.
Fig. 5 is in the order of presentation graphs 4, the curve map of the amounts of particles of being measured by particle monitoring device 210.In addition, Fig. 5 represents one of the measurement result example by the front and back that produce based on the vibration of purge gas.
As shown in Figure 5, between the several seconds after valve 120 is opened, a large amount of particles such as amounting to 9000 are counted out.This is because also be counted out as particle by the sediment of peeling off from chamber wall 110 and wafer station 111 etc. based on the vibration of purge gas.Like this, can monitor the particle that comprises the sediment of peeling off easily effectively, thereby correctly estimate the cleanliness factor of process chamber 100.In addition, opening the time of valve 120 as shown in Figure 4, is 1～5 second, preferably 2～5 seconds, that is, preferably can fully guarantee to vibrate the time of diffusion required time in process chamber 100.
According to Fig. 4 and Fig. 5, open valve 120, by the vibration of physical property that purge gas carried out is given in the process chamber 100 object at least once, sediment is peeled off energetically, therefore monitor particles, can correctly estimate the cleanliness of process chamber 100 effectively.
In addition, because monitor particles after the goods processing, so by valve-off a in advance when the goods processing, can prevent the inflow of purge gas, prevent the corrosion of the glass parts of particle monitoring device 210 effectively, prolong the life-span of particle monitoring device 210, thereby can improve the productive capacity of semiconductor-fabricating device 1000.
In the above-mentioned embodiment, be the physical property vibration that has utilized by the supply generation of purge gas, but the vibration that will utilize is the passable of what form.Such as, in order to produce vibration, also can in process chamber 100, apply the ultrasound wave of tens of kHz.In addition, owing to utilize the physical property vibration, suction line does not preferably have aperture (orifice) structure in the place that is connected with process chamber 100 or vacuum transfer chamber 100 '.
In addition, the preferred several physical property that produces is vibrated.In the case, produce the physical property vibration, sedimental peeling off is inhibited at every turn, and therefore, there is the tendency that reduces in granule number.Like this, the cleanliness of process chamber 100 can be carried out goods processing next time after obtaining higher evaluation.
Above-mentioned embodiment as shown in Figure 4, is preferably carried out with following second embodiment combination of the present invention that will illustrate.
The structure that possesses the semiconductor-fabricating device of the vacuum plant that relates to second embodiment of the present invention because therefore identical with above-mentioned first embodiment, omit its explanation, about the particle monitoring method of semiconductor-fabricating device 1000, only illustrates different part.
The semiconductor-fabricating device 1000 that relates to present embodiment, as shown in Figure 4, when being in the state that valve a, b open, from high-voltage power supply 112 to electrode 113 such as applying high voltage HV intermittently 3 times.The high voltage HV that applies preferably+more than the 1kV or-below the 1kV.
In addition, preferably alternatively apply ± 1kV voltage.Like this, can produce electromagnetic stress described later (electromagnetic stress) efficiently.
When applying high voltage HV, moment ground generation DC (DirectCurrent) discharge is followed with it in process chamber 100, tilts the generation electromagnetic stress at chamber wall 110 or wafer station 111 last moments ground formation current potential.Electromagnetic stress is peeled off sediment from chamber wall 110 or wafer station 111 etc., and the sediment under peeling off is discharged from purge gas as particle, by particle monitoring device 210 is monitored.
The grain count result of the particle monitoring device 210 when applying a high voltage HV comes to the same thing with shown in Figure 5., when applying the number of times increase of high voltage HV intermittently, be suppressed owing to peeling off, so there is the tendency that reduces in amounts of particles by the sediment of electromagnetic stress generation.Therefore, high voltage HV applies, and preferably carries out 1～10 time, and even more ideal is to carry out in 2～5 times number of times scope.
According to present embodiment, by carrying out applying of a high voltage HV at least, can peel off sediment energetically, therefore monitor particles, can correctly estimate the cleanliness of process chamber 100 effectively.
In addition owing to carry out repeatedly applying of high voltage HV intermittently, therefore, can be evaluated as in the cleanliness of process chamber 100 higher after, carry out the goods processing of next time.
In addition, in the present embodiment, as shown in Figure 4, under the state that valve 120 is opened, carry out applying of high voltage HV, but also can under valve 120 closing state, carry out.Like this, can prevent the wafer vibration by the purge gas that comes from suction line.
In addition, for chamber wall 110 or 111 last moments of wafer station ground form current potential and tilt and apply high voltage HV, but also can apply high-frequency RF (Radio Frequency).Produce the RF discharge by applying RF, and apply high voltage HV and similarly can produce electromagnetic stress.Apply RF, preferably do not continue the RF discharge for a long time, get final product such as carrying out about 1 second.
Above-mentioned embodiment is preferably carried out with above-mentioned first embodiment combination as shown in Figure 4.
In above-mentioned first and second embodiment, be connected exhaust line on the process chamber 100 and be arranged to take out in advance the such two system of pipeline 200 and main vacuum lines 300, but be arranged to more than three systems also passable.In addition, under the situation of exhaust line that is a system, as the 3rd embodiment aftermentioned of the present invention it.
Fig. 6 possesses the synoptic diagram of the semiconductor processing device structure of the vacuum plant that relates to third embodiment of the invention for expression roughly.
Among Fig. 6, possesses vacuum transfer chamber 100 ' with a system exhaust pipeline as the vacuum carrying device 1000 ' of vacuum plant.Vacuum transfer chamber 100 ' is applicable to such as the load locking room on the process chamber 100 that is connected semiconductor-fabricating device 1000 among Fig. 1, load locking room possess the conveyance wafer carrying arm.Vacuum carrying device 1000 ' is by the wafer station 120 conveyance wafers of carrying arm to process chamber 100.
Vacuum transfer chamber 100 ' is being connected with the suction line that possesses valve 120 ', and is being connected with the exhaust line 200 ' of the particle monitoring device (PM) 210 ' that possesses dry pump (DP) 220 ', valve a ', b ' and be provided with between valve a ', b '.
That is, omitted the structure of main vacuum lines 300 in the structure that is configured to above-mentioned first embodiment of present embodiment, therefore,, omitted their explanation, only described with regard to different piece about giving the member of same symbol.
Omitted the turbomolecular pump 330 of main vacuum lines 300 on the vacuum transfer chamber 100 ', therefore, vacuum transfer chamber 100 ' is not limited to high vacuum when monitor particles.Under the sort of situation, reach to a certain degree high vacuum in advance by dry pump 220 ', carry out order shown in Figure 7.In addition, therefore order shown in Figure 7 omits its explanation as first embodiment with Fig. 4 explanation.
According to Fig. 6 and Fig. 7,, the physical property that purge gas produces is vibrated the object of giving in the vacuum transfer chamber 100 ' by opening valve 120 ', sediment is peeled off energetically, therefore monitor particles, can correctly estimate the cleanliness of vacuum transfer chamber 100 ' effectively.
In addition, in above-mentioned the 3rd embodiment, vacuum transfer chamber 1000 ' is arranged to possess a system exhaust pipeline, but also can possess the exhaust line of multisystem.Under the situation of the exhaust line that possesses multisystem, the induction coefficient of the exhaust line of the coefficient of the mobile difficulty of the fluids such as gas that are discharged from as expression is different mutually usually, and no matter the exhaust line of which kind of induction coefficient can be suitable for present embodiment.
In addition, above-mentioned embodiment preferably with the execution that combines of above-mentioned second embodiment.In the case, connect the high-voltage power supply identical on the object in the vacuum transfer chamber 100 ' with high-voltage power supply 112.
In above-mentioned the first～three embodiment, estimated the process chamber 100 when not having wafer or the cleanliness of vacuum transfer chamber 100 ', but also can estimate process chamber 100 or vacuum transfer chamber 100 ' object in addition, such as the cleanliness of wafer.
Such as, at first, the cleanliness that are evaluated as process chamber 100 are very high, do not have peeling off of particle, then, move into wafer, estimate the cleanliness of the process chamber 100 when having wafer.Afterwards, two cleanliness relatively being estimated.In view of the above, can estimate the cleanliness of wafer.Similarly, connect airtight the situation of wafer station 111 and the situation of not connecting airtight, also can estimate the cleanliness of chip back surface by the back side of wafer.
In above-mentioned the first～three embodiment, monitor particles after the goods processing, but also can be before the goods processing finishes or in the goods processing monitor particles.
In addition, suction line is set to preferably do not have orifice structure in the place that is connected with process chamber 100 or vacuum transfer chamber 100 ', but exists in process chamber 100 or vacuum transfer chamber 100 ' under the situation of wafer etc., also orifice structure can be arranged.Like this, give the vibration of physical property such as wafer by purge gas, can suppress wafer etc. and sustain damage.
In the above-mentioned embodiment, window part for particle monitoring among Fig. 2 219 is made by quartz, but if made by transparent matrix material, what can.
In addition, purpose of the present invention, also can reach like this: the medium that will write down the program coding (program coding corresponding with the order of Fig. 4 or Fig. 7) of the software of realizing above-mentioned embodiment function is supplied with computing machine such as the PC600 among Fig. 9 described later, and the program coding that this computing machine (perhaps CPU, MPU etc.) is read the income medium moves.
In addition, move the program coding of reading such as PC600 by computing machine, not only the aforementioned embodiments function is accomplished, and according to the indication of this program coding, the operating system of working on PC600 (OS) etc. is carried out part or all actual treatment, much less also comprises the situation that realizes the function of aforementioned embodiments by this processing.
In addition, the program coding of reading from medium is after writing the function expansion card that inserts PC600 or having the reservoir of the work expanding element that connects computing machine, indication according to this program coding, this function expansion card or the CPU etc. with the work expanding element that connects computing machine carry out part or all actual treatment, much less also comprise the situation by the function of this processings realization aforementioned embodiments.
In addition, said procedure realizes that with PC600 the function of above-mentioned embodiment gets final product, and its mode also can have the modes such as script (script) data to the program of moving by target code, decoding, supply OS.
As program recording medium is provided, be to store getting final product of said procedure, such as: RAM, NV-RAM, soft (registered trade mark) dish, CD, photomagneto disk, CD-ROM, MO, CD-R, CD-RW, DVD (DVD-ROM, DVD-RAM, DVD-RW, DVD+RW), tape, Nonvolatile memory card, ROM etc.Perhaps, other computing machines or the download such as data bank of said procedure by being connected in internet, commercial network or LAN (Local Area Network) etc. provides.
Below, describe about the window part for particle monitoring that relates to the 4th embodiment of the present invention.
Fig. 8 relates to the sectional view of the structure of the window part for particle monitoring of four embodiment of the invention for expression at length.
The window part for particle monitoring that relates to four embodiment of the invention, the window part for particle monitoring 219 that replaces being made by quartz in above-mentioned first embodiment uses.In addition, in this 4th embodiment,, omit its explanation to giving prosign with semiconductor-fabricating device 1000 identical construction and the element that relate to first embodiment.
Among Fig. 8, window part for particle monitoring 219 has the generally cylindrical body shape respectively, is arranged on to take out in advance between pipeline 200 and the particle monitoring device 210, more particularly, inserts to be embedded in to have and is taking out the hole portion of mending shape mutually that pipeline 200 forms in advance.In addition, window part for particle monitoring 219 is not limited to insert the generally cylindrical body that is embedded in the hole portion of taking out pipeline 200 in advance, such as, also can have and the roughly cylindrical shape of taking out the hollow of pipeline 200 roughly the same diameters in advance, partly constitute and take out pipeline 200 in advance.
In addition, window part for particle monitoring 219 is made of transparent pedestal 219a and the surface-treated layer 219b that is arranged on the pedestal 219a.Pedestal 219a has gas surface of contact that joins with the gas opposite of taking out in advance in the pipeline 200 and the control surface that is connected on the particle monitoring device 210, and surface-treated layer 219b makes by implement surface-treated material described later on the gas surface of contact of pedestal 219a.
Surface-treated layer 219b contains a kind of material of selecting in the following material: carbon (C), yttrium (Y), yttria (Y
2O
3), calcium fluoride (CaF
2), aluminium (Al) and aluminium oxide (Al
2O
3).In addition, be under the situation of carbon at material, preferably make by crystalloid adamas or diamond-like-carbon (DLC:diamond-like carbon).By using these materials, can fully improve for halogen is the tolerance (hereinafter referred to as " plasma-resistance ") of plasma or for the tolerance of bioactive molecule.
In the above-mentioned material group, calcium fluoride not only has such physical property: water insoluble, fusing point is that 1373 ℃, spendable maximum temperature are 900 ℃, the hardness shown with the Knoop numerical table is 158.3, permeable light wavelength zone (seeing through wavelength region may) is 0.2～9.0 μ m and be 1000cm for wavelength
-1The refractive index of light be 1.39, and have high corrosion-resistant, because the hardness height also has high resistance to pressure for halogen.In addition, about calcium fluoride, can be easily and obtain the high product of purity cheaply.In addition, compared with quartz, also more be difficult to be dissolved in hydrofluorite as hydrofluoric aqueous solution.
As mentioned above, calcium fluoride is owing to have higher resistance to pressure, so it is just in time suitable as window member, in addition, because spendable maximum temperature is 900 ℃, thus the process chamber 100 of the hot environment that also just in time is fit to reach about 900 ℃, in addition, because it is bigger than quartz to see through wavelength region may, just in time be fit to optical detecting.Therefore, use calcium fluoride the most preferred.
In addition, aluminium atom in monomer aluminium and the aluminium and the reaction of the fluorine in the plasma generate aluminum fluoride (AlF
3).The aluminum fluoride that generates is owing to remaining in surface-treated layer 219b, and is therefore, high especially for the plasma-resistance of fluorine.
In addition, halogen is that plasma contains halogen or its compound that corrodes quartz glass, such as the CF of containing is arranged
4/ Ar/O
2/ CO plasma, F
2Plasma, CF
4, C
4F
8, C
5F
8Deng fluorocarbons be that the fluorine of plasma etc. or the fluorine of its compound are plasma or chlorine (Cl
2) plasma.These halogens are the bioactive molecule that plasma contains halogen free radical etc., and the silicon atom reaction with as the composition of glass etc. makes deteriorations such as glass.
In addition, constitute the material of surface-treated layer 219b, its amount is preferably in the scope of 10～100 quality % of the whole quality that accounts for surface-treated layer 219b.This be because, if amount less than 10 quality %, so just can not fully improve the tolerance for plasma-resistance or bioactive molecule of surface-treated layer 219b.
In addition, the thickness of surface-treated layer 219b is preferably in the scope of 100nm～100 μ m.This be because, if thickness less than 100nm, surface-treated layer 219b peels off from pedestal 219a under situation about being made by coated film described later easily so, is plasma etching by halogen easily under situation about being made by doped layer.On the other hand, this is because if thickness just is difficult to form on pedestal 219a above 100 μ m, when production cost rose, the transparency of surface-treated layer 219b reduced, and became difficult by the particle in the particle monitoring device 210 monitoring exhaust lines 200.
Below, the surface treatment of carrying out about the gas surface of contact to pedestal 219a describes.
As surface treatment, such method is arranged: on the gas surface of contact of pedestal 219a, make the coated film of making by the material that constitutes surface-treated layer 219b coating process, constitute the material of surface-treated layer 219b by mixing to predetermined depth from the surface of the gas surface of contact of pedestal 219a, on pedestal 219a, form the doping method of doped layer, but also can be other arbitrary method.
As above-mentioned coating process, following method is arranged: the potpourri that above-mentioned materials such as silicon dioxide and aluminium oxide are made blows meltallizing method on the gas surface of contact that is attached to pedestal 219a, sputter above-mentioned material or with method of PVD film forming etc. in the method for carrying out fusion, cooling on the gas surface of contact of pedestal 219a, with the material behind this potpourri of fusion.By coating, can easily on pedestal 219a, form surface-treated layer 219b.
As above-mentioned doping method, by following method: ion implantation, make the partly fusion of gas surface of contact of pedestal 219a, mix the method for above-mentioned material etc.In addition, on pedestal 219a, after the doping above-mentioned material, preferably fire (baking).In addition, under by the situation that is entrained in the surface-treated layer 219b that formation is made by doped layer on the pedestal 219a, their formation border becomes indeterminate, still, at least from the gas surface of contact of surface-treated layer 219b to predetermined depth, the amount that is doped material is preferably in above-mentioned scope.By mixing, the surface-treated layer 219b that forms on pedestal 219a can not peel off, so, can on pedestal 219a, form surface-treated layer 219b effectively.
Window part for particle monitoring 219 according to Fig. 8, owing on pedestal 219a, form surface-treated layer 219b, therefore, on surface-treated layer 219b as the new gas surface of contact that constitutes, can bring into play plasma-resistance efficiently or, reduce it and change frequency for the tolerance of bioactive molecule.In addition, owing to reduced the replacing frequency,, can improve the productive capacity of semiconductor-fabricating device 1000 so can guarantee for a long time to keep the time of the vacuum pressure of exhaust line 200.
In addition, window part for particle monitoring 219 has plasma-resistance or for the tolerance of bioactive molecule, its deterioration is inhibited, therefore, particle monitoring device 210 can be monitored effectively and contain the sedimental particle of peeling off, and correctly estimates the cleanliness of semiconductor-fabricating device 1000.
In addition, in the above-mentioned embodiment, the window part for particle monitoring 219 of Fig. 8 preferably has enough hardness, with as transparency height, use with the window member on the opposite, space of vacuum for the wavelength in the visible light zone of the laser of LASER Light Source 212 irradiation.
In addition, also can on the control surface of pedestal 219a, form the film of making by magnesium fluoride.Like this, can prevent the reflection of light of incident window part for particle monitoring 219.
In addition, in above-mentioned the 4th embodiment, the window part for particle monitoring 219 of Fig. 8 is made of pedestal 219a and surface-treated layer 219b, but also can be made by the single global facility that calcium fluoride is made.
In addition, above-mentioned window part for particle monitoring 219 also goes for other vacuum tank, such as the framework of particle monitoring device 210 ' among the process chamber among Fig. 1 100, Fig. 6 or pipe arrangement etc.In addition, also can be used for particle monitoring device miscellaneous part in addition.Adopt Fig. 9 that their concrete use-case is described.
Fig. 9 is the partial cross section figure of the structure of semiconductor-fabricating device 1000 in the presentation graphs 1 at length.
Among Fig. 9, semiconductor-fabricating device 1000 removes inscape shown in Figure 1, also possesses: CCD (the charge coupled device) camera 500 of object such as the laser that sends from particle monitoring device 400 of taking pictures in the scene of the particle in its monitoring position process chamber 100 (in situ) particle monitoring device (ISPM) 400 and the photographing process chamber 100.Particle monitoring device 400 and CCD camera 500 are connected on the PC (PC) 600.On the PC600, be connected with CVD instrument control part 620 in addition by signal processing part 610.
In addition, the CCD camera of the chamber wall 110 of CCD camera 500 by being arranged on process chamber 100 is with the laser in window member (not shown) the photographing process chamber 100, with the portrait input PC600 that takes.Like this, in the umber of pulse of metering laser, the sensor that can be used as the laser that calculates the particle scattering in the processed chamber 100 plays a role.This CCD camera by constituting with same structure and the material of the window part for particle monitoring 219 of Fig. 8, like this, can suppress the corrosion on surface with window member, reduces it and changes frequency, and simultaneously, the sensitivity that can suppress sensor reduces.In addition, play a role, also can use photomultiplier replaced C CD camera 500 as sensor.
In addition, semiconductor-fabricating device 1000 possesses the focusing ring 117 on the wafer station of being disposed at 111 tops, this focusing ring 117 is also by making such as calcium fluoride with same structure and the material of the window part for particle monitoring 219 of Fig. 8, like this, when can realize insulating, can suppress the corrosion on surface, reduce it and change frequency.
According to Fig. 9, window member 440, CCD camera with window member, and process chamber 100 such as focusing ring 117 in parts by making with same structure and the material of the window part for particle monitoring 219 of Fig. 8, therefore, can suppress the corrosion on their surfaces, reduce their replacing frequency.In addition, owing to surperficial corrosion is suppressed, so, can suppress the wafer contaminations that take place in the process chamber 100.
The vacuum plant, its particle monitoring method and the program that relate to embodiment of the present invention are not limited to the process chamber or the load locking room of semiconductor-fabricating device, but go for forming the container of the predetermined space of exhaust, such as liquid crystal manufacturing installation, other substrate board treatments of flat-panel monitor etc.
In addition, the window part for particle monitoring that relates to embodiment of the present invention goes in the framework that forms predetermined space and monitors the transparent window part for particle monitoring that is provided with between the particle monitoring of the particle in this framework.
Claims (12)
1. window part for particle monitoring by in the framework that forms predetermined space with monitor the transparent substrate that is provided with between the particle monitoring device of the particle in this framework and make, is characterized in that:
Described substrate by transparent pedestal and with this pedestal on described framework in the face of gas opposite face on implement predetermined process surface-treated layer constitute.
2. window member according to claim 1 is characterized in that:
Described surface-treated layer contains a kind of material that is selected from carbon, yttrium, yttria and the calcium fluoride.
3. window member according to claim 2 is characterized in that:
Described carbon is made by crystalloid adamas or diamond-like-carbon.
4. according to claim 2 or 3 described window members, it is characterized in that:
Described a kind of material, its amount is in the whole quality of described surface-treated layer, in the scope of 10～100 quality %.
5. window member according to claim 1 is characterized in that:
Described surface-treated layer contains aluminium or aluminium oxide.
6. the described window member of claim 5 is characterized in that:
Described aluminium or aluminium oxide, its amount is in the whole quality of described surface-treated layer, in the scope of 10～100 quality %.
7. according to each described window member in the claim 1～6, it is characterized in that:
Described predetermined process is handled for coating.
8. according to each described window member in the claim 1～6, it is characterized in that:
Described predetermined process is a doping treatment.
9. according to each described window member in the claim 1～8, it is characterized in that:
Described surface-treated layer, its thickness is in the scope of 100nm～10 μ m.
10. according to each described window member in the claim 1～9, it is characterized in that:
Described pedestal is made by the glass that with silicon is major component;
Described surface-treated layer is in the interior bioactive molecule that gas contained of described framework.
11. a window part for particle monitoring by in the framework that forms predetermined space with monitor the transparent substrate that is provided with between the particle monitoring device of the particle in this container and make, is characterized in that:
Described substrate is made by calcium fluoride.
12., it is characterized in that according to each described window member in the claim 1～11:
Described framework is made by container or pipe arrangement.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP200496456 | 2004-03-29 | ||
| JP2004096456 | 2004-03-29 | ||
| JP2004329675 | 2004-11-12 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100601714A Division CN100378925C (en) | 2004-03-29 | 2005-03-29 | Vacuum device, its particle monitoring method,program and window part for particle monitoring |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101082560A true CN101082560A (en) | 2007-12-05 |
Family
ID=38912245
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200710139134 Pending CN101082560A (en) | 2004-03-29 | 2005-03-29 | Vacuum apparatus including a particle monitoring unit, particle monitoring method and program, and window member for use in the particle monitoring |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JP2009296006A (en) |
| CN (1) | CN101082560A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103954537A (en) * | 2014-05-09 | 2014-07-30 | 河北大学 | Dry type particle granularity measuring method |
| CN109937470A (en) * | 2016-11-07 | 2019-06-25 | 应用材料公司 | The method and apparatus of nano particle of the detection and analysis from semiconductor chamber component |
| CN111524841A (en) * | 2020-07-06 | 2020-08-11 | 上海陛通半导体能源科技股份有限公司 | Semiconductor process equipment and method capable of detecting mechanical microparticles in real time |
| CN111826632A (en) * | 2019-04-22 | 2020-10-27 | 上海新微技术研发中心有限公司 | Deposition method and deposition equipment for amorphous silicon film |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5876248B2 (en) * | 2011-08-09 | 2016-03-02 | 東京エレクトロン株式会社 | Particle monitoring method and particle monitoring apparatus |
| JP2019168310A (en) * | 2018-03-23 | 2019-10-03 | 栗田工業株式会社 | Aggregation state monitoring sensor |
| KR102404654B1 (en) * | 2021-02-04 | 2022-05-31 | 이재훈 | Apparatus for monitoring state of powder deposition in gas exhausting line for semiconductor production facility |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04136172A (en) * | 1990-09-26 | 1992-05-11 | Showa Denko Kk | Method for coating inside with diamond |
| US5250098A (en) * | 1992-07-27 | 1993-10-05 | Ford Motor Company | Thermally durable anti-reflective glass |
| JPH0827566A (en) * | 1994-07-14 | 1996-01-30 | Sumitomo Metal Mining Co Ltd | Production of observation window of vacuum device |
| JP2003115478A (en) * | 2001-10-05 | 2003-04-18 | Toshiba Ceramics Co Ltd | Window member for plasma processor |
| JP3891848B2 (en) * | 2002-01-17 | 2007-03-14 | 東京エレクトロン株式会社 | Processing apparatus and processing method |
-
2005
- 2005-03-29 CN CN 200710139134 patent/CN101082560A/en active Pending
-
2009
- 2009-09-16 JP JP2009214301A patent/JP2009296006A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103954537A (en) * | 2014-05-09 | 2014-07-30 | 河北大学 | Dry type particle granularity measuring method |
| CN109937470A (en) * | 2016-11-07 | 2019-06-25 | 应用材料公司 | The method and apparatus of nano particle of the detection and analysis from semiconductor chamber component |
| CN109937470B (en) * | 2016-11-07 | 2023-05-16 | 应用材料公司 | Method and apparatus for detecting and analyzing nanoparticles from semiconductor chamber components |
| CN111826632A (en) * | 2019-04-22 | 2020-10-27 | 上海新微技术研发中心有限公司 | Deposition method and deposition equipment for amorphous silicon film |
| CN111524841A (en) * | 2020-07-06 | 2020-08-11 | 上海陛通半导体能源科技股份有限公司 | Semiconductor process equipment and method capable of detecting mechanical microparticles in real time |
| CN111524841B (en) * | 2020-07-06 | 2020-10-23 | 上海陛通半导体能源科技股份有限公司 | Semiconductor process equipment and method capable of detecting mechanical microparticles in real time |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2009296006A (en) | 2009-12-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100378925C (en) | Vacuum device, its particle monitoring method,program and window part for particle monitoring | |
| US8854625B2 (en) | Vacuum apparatus including a particle monitoring unit, particle monitoring method and program, and window member for use in the particle monitoring | |
| CN101082560A (en) | Vacuum apparatus including a particle monitoring unit, particle monitoring method and program, and window member for use in the particle monitoring | |
| US6734388B2 (en) | Dry surface cleaning apparatus | |
| CN100390938C (en) | Removal of material by polarized radiation and back side application of radiation | |
| US5821175A (en) | Removal of surface contaminants by irradiation using various methods to achieve desired inert gas flow over treated surface | |
| CN101268346A (en) | Apparatus for determining a temperature of a substrate and methods therefor | |
| EP0693978B1 (en) | Removal of surface contaminants by irradiation | |
| CN109791900B (en) | Method and apparatus for process chamber cleaning endpoint detection | |
| JP2006287228A (en) | Semiconductor processor capable of self-cleaning | |
| Pryatel et al. | Cleaning practices and facilities for the National Ignition Facility (NIF) | |
| KR100452927B1 (en) | Storage box for preventing physical and chemical pollution | |
| CN102024683A (en) | Method for judging whether to start processing | |
| WO2013186008A1 (en) | A self-cleaning optical system | |
| Hein et al. | Lithography-free glass surface modification by self-masking during dry etching | |
| Elg | Removal of tin from exterme ultraviolet collector optics by an in-situ hydrogen plasma | |
| CN103730315B (en) | A kind of method improving plasma etch process | |
| JPH08304614A (en) | Synthetic resin reflection mirror, its production and producing device | |
| US11715628B2 (en) | Method of forming plasma processing apparatus, related apparatus, and method of forming semiconductor device using the same | |
| Gischkat et al. | Influence of substrate cleaning on the laser resistance of antireflective coatings | |
| JPH09263936A (en) | Production of thin film and thin film | |
| US20210035767A1 (en) | Methods for repairing a recess of a chamber component | |
| JP2003037058A (en) | Method of manufacturing x-ray mask | |
| JPH10183332A (en) | Production of optical thin film and device therefor | |
| Hägglund | Maskmaterial för djupets avborosilikatglas |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20071205 |