CN101050605A - Heat-resistance type transfer aluminum plated paper and its producing process - Google Patents
Heat-resistance type transfer aluminum plated paper and its producing process Download PDFInfo
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- CN101050605A CN101050605A CN 200710074065 CN200710074065A CN101050605A CN 101050605 A CN101050605 A CN 101050605A CN 200710074065 CN200710074065 CN 200710074065 CN 200710074065 A CN200710074065 A CN 200710074065A CN 101050605 A CN101050605 A CN 101050605A
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Abstract
The present invention relates to a temperature-resistant type transfer aluminized paper and its production process. Said process successively includes the following steps: coating release layer on the film; coating anchoring layer on release layer; vacuum aluminizing on the anchoring layer; coating adhesive on the aluminized layer; then making them be combined with paper; stripping film from release layer so as to obtain the invented temperature-resistant type transfer aluminized paper.
Description
Technical field
The present invention relates to a kind of composite, more particularly, the present invention relates to a kind of paper substrate composite and production technology thereof of aluminizing.
Background technology
The aluminium paper composite that vacuum aluminum-coated transfer method is produced though it is few with the aluminium amount, has very strong metal-like; Its shading, thermal insulation, moisture barrier property are strong, composite products such as alternative pure aluminum foil, aluminizer, and be suitable for carrying out following process with machines such as printing machine, embossing machine, high-speed crosscutting machines, therefore, at home and abroad packaging industry is employed as the novel environment friendly packaging material in recent years, as is widely used in packaging fields such as cigarette, food, medicine.
Existing vacuum aluminum-coated transfer method is produced the aluminium paper composite, be on film such as PET film, to be coated with release layer, binder course, again vacuum aluminum-coated on the coating, on aluminium coated coating adhesive, compound with paper then, at last the PET film is peeled off, obtain heat-resistance type transfer aluminum plated paper.And as the packing of some product such as cigarette the time, need outside wrapping paper, seal the OPP film again.And common heat-resistance type transfer aluminum plated paper is because the heatproof limitation of selected coating, through heat-sealing OPP film the time, the heat of heat-seal land can see through the coating that release layer, binder course etc. are formed, make the molecular configuration of coating change, thereby rheology, destruction are taken place, and then make air, heat infiltrate resin bed, and cause light reflective deterioration, variable color, influenced the attractive in appearance of the packings of product such as tobacco bale greatly.
Summary of the invention
Above-mentioned shortcoming at prior art, the objective of the invention is to provide a kind of heat-resistance type transfer aluminum plated paper and production technology thereof, it has following advantage: the heat resistance of transfer paper and printing adaptability all can improve greatly, and are beneficial to environmental protection, and production cost is lower.
For this reason, one of technical solution of the present invention is a kind of production technology of heat-resistance type transfer aluminum plated paper, and it comprises the steps: A in regular turn) on film, be coated with release layer; B) on release layer, be coated with binder course; C) vacuum aluminum-coated on binder course; D) coating binder on the binder course of aluminizing, compound with paper then; E) film is peeled off from release layer, obtained heat-resistance type transfer aluminum plated paper; And described release layer and binder course are to adopt resin to disperse through dissolution with solvents, are modulated into releasing layer coating/binder course coating, and coating forms respectively again; Described resin comprises cellaburate resin and Nitro cellulose resin, and described solvent comprises one or more in ethyl acetate, butanone, DAA and the isopropyl alcohol.
Described releasing layer coating proportioning is a cellaburate resin 60%～98%, Nitro cellulose resin 2%～40%; Described binder course coating formula is a cellaburate resin 5%～65%, Nitro cellulose resin 35%～95%.
According to coating is poor owing to temperature tolerance, vitrification point is on the low side, high temperature can cause breakdown of coating, and make the original analysis of coating loss of gloss, recognize that the steric configuration of molecular resin and the relation of temperature are the important microcosmic essence of coating loss of gloss deepening, technology of the present invention is choose reasonable resin and solvent on a large amount of experimental basis, utilize selected resin that higher softening point and suitable molecular weight are arranged, thereby make it have high temperature resistant, heat insulation performance, optimize proportioning, form the good coating of temperature tolerance at film surface.Experimental results show that: technology of the present invention can make coating smooth, even, index such as adhesive force and pliability is good, suitable vacuum evaporating aluminium lamination thereon, make the aluminium spraying layer thickness of goods of the present invention can be thinned to 0.02 μ m～0.05 μ m, thereby cut down the consumption of raw materials and production cost, and be convenient to natural degradation, free from environmental pollution; And its product temperature tolerance can reach 140 ℃～170 ℃, the heat-sealing temperature when being enough to bear cigarette pack, and can allow total dry-coated amount at 0.9～2.0g/m
2, reduce the coating cost greatly, more help environmental protection.Glossiness can descend greatly after tradition transfer paper coating was heated, and glossiness is 30Gs even lower only, and technology of the present invention makes the goods glossiness reach 50Gs even higher, attractive packages, and product specification improves.In addition, the smoothness of goods of the present invention, folding resistance, ABRASION RESISTANCE, printing adaptability all improve significantly.
The concrete improvement of the present invention also comprises:
As preferable enforcement prescription, described release layer and binder course resin also comprise acrylic resin, alkyd resins wherein one or more, described binder course coating also comprises colorant or dyestuff.
The proportion optimization of described release layer each component is as follows: cellaburate resin 60%～95%, Nitro cellulose resin 2%～40%, acrylic resin 0%～10%; The proportion optimization of described binder course each component is as follows: cellaburate resin 5%～65%, Nitro cellulose resin 35%～95%, acrylic resin 0%～20%, alkyd resins 0%～20%; To account for the percentage by weight of coating be 5%～15% to resin in releasing layer coating and/or the binder course coating; Colorant or dyestuff are with respect to binder course coating, and its percentage by weight is 0～2.0%.
In order to adapt to follow-up false proof and attractive in appearance needs, between described step B, C, also comprise mold pressing step B1, molding temperature is promptly controlled 130 ℃～180 ℃ of floral axis temperature, makes pattern in described binder course surface pressure.
In order to reach good coating effect, in the described steps A, 60～120 meters/minute of the control coating machine speeds of service adopt 120～220 order knurled belt material, releasing layer coating is uniformly coated on the film, dries through 80 ℃～160 ℃ temperature of baking oven, and its dry-coated amount is 0.4～1.2g/m
2Among the described step B, 60～120 meters/minute of the control coating machine speeds of service adopt 175～300 order knurled belt material, and binder course coating is uniformly coated on the release layer, dries through 80 ℃～160 ℃ temperature of baking oven, and its total dry-coated amount is 0.9～2.0g/m
2Control suitable dry-coated amount, can not only keep bigger adhesive force and intensity, simultaneously but also keep lower production cost.
Among the described step C, control vacuum aluminum-coated machine vacuum and be not less than 2.0 * 10
-2Mbar, under the condition that the vacuum aluminum-coated machine speed of service is 200～900 meters/minute, with the aluminium of high temperature melting evaporation, evenly spraying plating forms the transfer membrane of aluminizing of band aluminium lamination on described binder course.
For cooperate release layer and binder course and with the combined strength bination of paper substrate, described adhesive is a carboxylic styrene butadiene latex, among the described step D, adopt 60～175 order knurled belt glue, carboxylic styrene butadiene latex is uniformly coated on the aluminium coated, compound with paper, through 60 ℃～150 ℃ temperature oven dry of baking oven, make aluminium coated and paper reach certain combined strength bination and bond strength.
In order to satisfy additional requirement such as non-web feed printing, to alleviate water evaporates/minimizing that baking causes paper substrate to goods, the too dry and curling problem of paper appears, between described step D and the E, comprise that also the back of the body is coated with step D1, under 60～120 meters/minute conditions of the control compounding machine speed of service, adopt 120～220 order knurled belt material, the compo that will comprise humectant, acrylic resin and solvent, be uniformly coated on the described sheet paper products back side, dry under 60～130 ℃ of temperature of baking oven, the dry-coated amount that the back of the body is coated with is 0.3～1.0g/m
2
Another technical solution of the present invention is a kind of heat-resistance type transfer aluminum plated paper, and it comprises ply of paper, coating, aluminium coated, and described ply of paper density is 30～400g/m
2, the coating of described coating comprises cellaburate resin and Nitro cellulose resin, described aluminum layer thickness 0.02 μ m～0.05 μ m.
The heatproof of described heat-resistance type transfer aluminum plated paper reaches 140 ℃～170 ℃.
As described above as can be known: heat-resistance type transfer aluminum plated paper of the present invention satisfies the requirement of client's high-temperature resistant with lower dry-coated amount, and product temperature tolerance, adhesive force also have bigger room for promotion with the increase of dry-coated amount.Relatively mention in the Chinese patent 03139780.8 its secondary coating dry-coated amount be 2～15g/m
2, the total coating weight of coating of the present invention is 0.9～2.0g/m
2, its production cost is well below correlation technique.
The present invention will be further described below in conjunction with specific embodiment.
The specific embodiment
Embodiment 1:
Release layer, press the coating of column weight amount than the preparation coating:
Resin: cellaburate resin 85%
Nitro cellulose resin 15%
Solvent: butanone 48%
DAA 20%
Ethyl acetate 22%
Isopropyl alcohol 10%
The percentage by weight that resin accounts for coating is 10%;
Binder course, press the coating of column weight amount than the preparation coating:
Resin: cellaburate resin 25%
Nitro cellulose resin 65%
Acrylic resin 5%
Alkyd resins 5%
Solvent: butanone 48%
DAA 20%
Ethyl acetate 22%
Isopropyl alcohol 10%
The percentage by weight that resin accounts for coating is 13%;
It is evenly standby to add percentage by weight with respect to binder course coating again and be 1% coloring material for mixing;
Once be coated with (comprising levelling, oven dry), dry-coated amount 0.7g/m for the PET film with releasing layer coating
2, on release layer, carry out secondary coating (comprising levelling, oven dry), total dry-coated amount 1.8g/m with binder course coating
2, with vacuum aluminum-coated machine at coat side spraying plating aluminium lamination 0.03 μ m, with compounding machine with aluminizer and body paper (90g/m
2Two-sided art paper) compound, adhesive adopts carboxylic styrene butadiene latex, then the PET film is peeled off.
Above-mentioned once coating is, under 95 meters/minute conditions of the coating machine speed of service, adopt 120 order knurled belt material, releasing layer coating is uniformly coated on the PET film, be followed successively by 90 ℃, 125 ℃, 140 ℃, 130 ℃, 120 ℃ (deviation ± 5 ℃) in five joint oven for drying temperature;
Above-mentioned secondary coating, be under 95 meters/minute conditions of the coating machine speed of service, adopt 200 order knurled belt material, binder course coating, be uniformly coated on coated film one time, be followed successively by 90 ℃, 125 ℃, 140 ℃, 130 ℃, 120 ℃ (deviation ± 5 ℃) in five joint oven for drying temperature;
Above-mentioned vacuum evaporating aluminium lamination is to be not less than 2.0 * 10 in vacuum aluminum-coated machine vacuum
-2Mbar, under 450 meters/minute conditions of the vacuum aluminum-coated machine speed of service, with the aluminium of high temperature melting evaporation, evenly spraying plating forms the spraying plating aluminium lamination through being coated with on the base material of binder course operation, also is aluminizer;
Above-mentioned compound working procedure is, in 100 ℃ of oven for drying temperature, 115 ℃, 125 ℃, 120 ℃, 110 ℃ (deviation ± 5 ℃), under 90 meters/minute conditions of the compounding machine speed of service, adopt 90 order knurled belt material, aluminizer and paper base material are combined with each other with carboxylic styrene butadiene latex;
Its heat resistance reaches 160 ℃, and the heat-resistance type transfer aluminum plated paper glossiness reaches more than the 50Gs.Wherein heat resistance is a simulation heat sealed package condition, adopt the heat-sealing instrument to seal a second (surpassing the actual heat sealed package time) down as 160 ℃ at 104kpa pressure and certain heat-sealing temperature, the variable color situation of visual observations paper surface is if no obvious variable color illustrates that then the heat resistance of this product reaches 165 ℃; Glossiness is at 45, detects (down together) with vancometer.
Embodiment 2:
Release layer, press the coating that the column weight amount once is coated with than preparation:
Coating: cellaburate resin 75%
Nitro cellulose resin 22%
Acrylic resin 3%
Solvent: butanone 48%
DAA 20%
Ethyl acetate 22%
Isopropyl alcohol 10%
The percentage by weight that resin accounts for coating is 9%;
Binder course, press the coating of column weight amount than the preparation coating:
Resin: cellaburate resin 25%
Nitro cellulose resin 75%
Solvent: butanone 48%
DAA 20%
Ethyl acetate 22%
Isopropyl alcohol 10%
The percentage by weight that resin accounts for coating is 12%;
The PET film once is coated with (comprising levelling, oven dry), dry-coated amount 0.6g/m with above-mentioned releasing layer coating
2, on release layer, carry out secondary coating (comprising levelling, oven dry), total dry-coated amount 1.2g/m with binder course coating
2, with vacuum aluminum-coated machine at coat side spraying plating aluminium lamination 0.035 μ m, with compounding machine with aluminizer and body paper (90g/m
2Two-sided art paper) compound, adhesive adopts carboxylic styrene butadiene latex, then the PET film is peeled off.
Above-mentioned once coating, be under 95 meters/minute conditions of the coating machine speed of service, adopt 160 order knurled belt material, releasing layer coating is uniformly coated on the PET film, be followed successively by 90 ℃, 125 ℃, 140 ℃, 130 ℃, 120 ℃ (deviation ± 5 ℃) in five joint oven for drying temperature;
Above-mentioned secondary coating is under 95 meters/minute conditions of the coating machine speed of service, adopts 240 order knurled belt material, with binder course coating, be uniformly coated on the release layer, be followed successively by 90 ℃, 120 ℃, 145 ℃, 135 ℃, 120 ℃ (deviation ± 5 ℃) in five joint oven for drying temperature
Other process conditions are basic identical in embodiment 1.Its heatproof reaches 165 ℃, and the heat-resistance type transfer aluminum plated paper glossiness reaches 70Gs.
Claims (10)
1, a kind of production technology of heat-resistance type transfer aluminum plated paper, it comprises the steps: A in regular turn) on film, be coated with release layer; B) on release layer, be coated with binder course; C) vacuum aluminum-coated on binder course; D) coating binder on aluminium coated, compound with paper then; E) film is peeled off from release layer, obtained heat-resistance type transfer aluminum plated paper; It is characterized in that: described release layer and binder course are to adopt resin to disperse through dissolution with solvents, are modulated into releasing layer coating/binder course coating, and coating forms respectively again; Described resin comprises cellaburate resin and Nitro cellulose resin, and described solvent comprises one or more in ethyl acetate, butanone, DAA and the isopropyl alcohol.
2, the production technology of heat-resistance type transfer aluminum plated paper according to claim 1, it is characterized in that: the weight proportion of resin is a cellaburate resin 60%～98% in the described releasing layer coating, Nitro cellulose resin 2%～40%; The weight proportion of resin is a cellaburate resin 5%～65% in the described binder course coating, Nitro cellulose resin 35%～95%.
3, the production technology of heat-resistance type transfer aluminum plated paper according to claim 1, it is characterized in that: described releasing layer coating also comprises acrylic resin; Binder course coating also comprise acrylic resin, alkyd resins wherein one or more, described binder course coating also comprises colorant or dyestuff.
4, as the production technology of heat-resistance type transfer aluminum plated paper as described in the claim 3, it is characterized in that: the weight proportion of the each component of resin is as follows in the described releasing layer coating: cellaburate resin 60%～95%, 2%～36% part of Nitro cellulose resin, acrylic resin 0%～10%; The weight proportion of the each component of resin is as follows in the described binder course coating: cellaburate resin 5%～65%, Nitro cellulose resin 35%～95%, acrylic resin 0%～20%, alkyd resins 0%～20%; To account for the percentage by weight of coating be 5%～15% to resin in releasing layer coating and/or the binder course coating; Colorant or dyestuff are with respect to binder course coating, and its percentage by weight is 0～2.0%.
5, as the production technology of heat-resistance type transfer aluminum plated paper as described in one of claim 1-4, it is characterized in that: between described step B, C, also comprise mold pressing step B1, molding temperature is promptly controlled under 130 ℃～180 ℃ conditions of floral axis temperature, makes pattern in described binder course surface pressure.
6, as the production technology of heat-resistance type transfer aluminum plated paper as described in one of claim 1-4, it is characterized in that: in the described steps A, 60～120 meters/minute of the control coating machine speeds of service, adopt 120～220 order knurled belt material, releasing layer coating is coated on the film, dries through 80 ℃～160 ℃ temperature of baking oven, and its dry-coated amount is 0.4～1.2g/m
2Among the described step B, 60～120 meters/minute of the control coating machine speeds of service adopt 175～300 order knurled belt material, and binder course coating is coated on the release layer, dries through 80 ℃～160 ℃ temperature of baking oven, and its total dry-coated amount reaches 0.9～2.0g/m
2
7, as the production technology of heat-resistance type transfer aluminum plated paper as described in one of claim 1-4, it is characterized in that: among the described step C, control vacuum aluminum-coated machine vacuum and be not less than 2.0 * 10
-2Mbar, under the condition that the vacuum aluminum-coated machine speed of service is 200～900 meters/minute, with the aluminium of high temperature melting evaporation, spraying plating forms the transfer membrane of aluminizing of band aluminium lamination on described binder course; Described adhesive is a carboxylic styrene butadiene latex, among the described step D, adopts 60～175 order knurled belt glue, carboxylic styrene butadiene latex is uniformly coated on the binder course of aluminizing compound with paper, through 60 ℃～150 ℃ temperature oven dry of baking oven.
8, as the production technology of heat-resistance type transfer aluminum plated paper as described in one of claim 1～4, it is characterized in that: between described step D and the E, comprise that also the back of the body is coated with step D1, promptly control under the condition of 60～120 meters/minute of the compounding machine speeds of service, adopt 120～220 order knurled belt material, will comprise the compo of humectant, acrylic resin and solvent, be coated on the described sheet paper products back side, dry under 60 ℃～130 ℃ temperature of baking oven, the dry-coated amount that the back of the body is coated with is 0.3～1.0g/m
2
9, a kind of heat-resistance type transfer aluminum plated paper, it comprises ply of paper, coating, aluminium coated, it is characterized in that: described ply of paper density is 30～400g/m
2, the coating of described coating comprises cellaburate resin and Nitro cellulose resin, described aluminum layer thickness 0.02 μ m～0.05 μ m.
10, as heat-resistance type transfer aluminum plated paper as described in the claim 9, it is characterized in that: the heatproof of described heat-resistance type transfer aluminum plated paper reaches 140 ℃～170 ℃.
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