CN100575428C - The preparation method of low temperature solidifying environment protection type cathode electrophoresis coating - Google Patents
The preparation method of low temperature solidifying environment protection type cathode electrophoresis coating Download PDFInfo
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- CN100575428C CN100575428C CN200710027826A CN200710027826A CN100575428C CN 100575428 C CN100575428 C CN 100575428C CN 200710027826 A CN200710027826 A CN 200710027826A CN 200710027826 A CN200710027826 A CN 200710027826A CN 100575428 C CN100575428 C CN 100575428C
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- 238000002360 preparation method Methods 0.000 title claims abstract description 34
- 238000001962 electrophoresis Methods 0.000 title claims abstract description 22
- 238000000576 coating method Methods 0.000 title claims abstract description 19
- 239000011248 coating agent Substances 0.000 title claims abstract description 18
- 229920005989 resin Polymers 0.000 claims abstract description 45
- 239000011347 resin Substances 0.000 claims abstract description 45
- 238000006243 chemical reaction Methods 0.000 claims abstract description 28
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 27
- 150000002148 esters Chemical class 0.000 claims abstract description 24
- 239000004593 Epoxy Substances 0.000 claims abstract description 23
- 239000002904 solvent Substances 0.000 claims abstract description 22
- 238000001723 curing Methods 0.000 claims abstract description 21
- 239000000839 emulsion Substances 0.000 claims abstract description 20
- 239000002002 slurry Substances 0.000 claims abstract description 14
- 230000003197 catalytic effect Effects 0.000 claims abstract description 12
- 150000001412 amines Chemical class 0.000 claims abstract description 11
- 239000011159 matrix material Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 9
- 238000012986 modification Methods 0.000 claims abstract description 8
- 230000004048 modification Effects 0.000 claims abstract description 8
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims abstract description 7
- 150000001408 amides Chemical class 0.000 claims abstract description 7
- 239000012948 isocyanate Substances 0.000 claims abstract description 7
- 150000002513 isocyanates Chemical class 0.000 claims abstract description 7
- 238000007142 ring opening reaction Methods 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000008367 deionised water Substances 0.000 claims description 16
- 229910021641 deionized water Inorganic materials 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 14
- 239000003822 epoxy resin Substances 0.000 claims description 10
- 229920000647 polyepoxide Polymers 0.000 claims description 10
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 8
- 239000006185 dispersion Substances 0.000 claims description 8
- 230000035484 reaction time Effects 0.000 claims description 8
- 239000000049 pigment Substances 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- 239000004576 sand Substances 0.000 claims description 6
- 239000003054 catalyst Substances 0.000 claims description 5
- 239000003995 emulsifying agent Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 229940106691 bisphenol a Drugs 0.000 claims description 4
- -1 catalyzer Substances 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 238000000227 grinding Methods 0.000 claims description 4
- 238000009413 insulation Methods 0.000 claims description 4
- 238000004945 emulsification Methods 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- MNAHQWDCXOHBHK-UHFFFAOYSA-N 1-phenylpropane-1,1-diol Chemical compound CCC(O)(O)C1=CC=CC=C1 MNAHQWDCXOHBHK-UHFFFAOYSA-N 0.000 claims description 2
- 229940049676 bismuth hydroxide Drugs 0.000 claims description 2
- TZSXPYWRDWEXHG-UHFFFAOYSA-K bismuth;trihydroxide Chemical compound [OH-].[OH-].[OH-].[Bi+3] TZSXPYWRDWEXHG-UHFFFAOYSA-K 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 abstract description 8
- 230000004580 weight loss Effects 0.000 abstract description 8
- 238000013035 low temperature curing Methods 0.000 abstract description 7
- 238000007711 solidification Methods 0.000 abstract description 6
- 230000008023 solidification Effects 0.000 abstract description 6
- 238000012545 processing Methods 0.000 abstract description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 14
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 14
- 229940043265 methyl isobutyl ketone Drugs 0.000 description 14
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 8
- 238000009835 boiling Methods 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 238000010992 reflux Methods 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 238000010792 warming Methods 0.000 description 6
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- WHIVNJATOVLWBW-UHFFFAOYSA-N n-butan-2-ylidenehydroxylamine Chemical compound CCC(C)=NO WHIVNJATOVLWBW-UHFFFAOYSA-N 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- 239000003973 paint Substances 0.000 description 3
- 229920000768 polyamine Polymers 0.000 description 3
- 229920000570 polyether Polymers 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 3
- ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 235000019628 coolness Nutrition 0.000 description 2
- 229960002887 deanol Drugs 0.000 description 2
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 239000012972 dimethylethanolamine Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 230000035939 shock Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 239000005058 Isophorone diisocyanate Substances 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
- 229910000416 bismuth oxide Inorganic materials 0.000 description 1
- 150000001868 cobalt Chemical class 0.000 description 1
- TYIXMATWDRGMPF-UHFFFAOYSA-N dibismuth;oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Bi+3].[Bi+3] TYIXMATWDRGMPF-UHFFFAOYSA-N 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 description 1
- JEHCHYAKAXDFKV-UHFFFAOYSA-J lead tetraacetate Chemical compound CC(=O)O[Pb](OC(C)=O)(OC(C)=O)OC(C)=O JEHCHYAKAXDFKV-UHFFFAOYSA-J 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000005056 polyisocyanate Substances 0.000 description 1
- 229920001228 polyisocyanate Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
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CN200710027826A CN100575428C (en) | 2007-04-30 | 2007-04-30 | The preparation method of low temperature solidifying environment protection type cathode electrophoresis coating |
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CN200710027826A CN100575428C (en) | 2007-04-30 | 2007-04-30 | The preparation method of low temperature solidifying environment protection type cathode electrophoresis coating |
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CN101054487A CN101054487A (en) | 2007-10-17 |
CN100575428C true CN100575428C (en) | 2009-12-30 |
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CN200710027826A Expired - Fee Related CN100575428C (en) | 2007-04-30 | 2007-04-30 | The preparation method of low temperature solidifying environment protection type cathode electrophoresis coating |
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Families Citing this family (35)
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ATE552314T1 (en) * | 2007-12-14 | 2012-04-15 | Du Pont | ORGANIC SOLVENT-FREE PIGMENT DISPERSANT FOR WATER-BASED ELECTRICAL COATING |
DE102008012085A1 (en) * | 2008-02-29 | 2009-09-10 | Basf Coatings Ag | Cathodic electrodeposition paint containing organometallic compound |
CN102153729B (en) * | 2011-03-04 | 2013-06-12 | 重庆三峡油漆股份有限公司 | Semi-enclosed organic amine curing agent and application thereof to anti-corrosive coating |
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CN103031038B (en) * | 2012-12-25 | 2016-01-06 | 广东科德化工实业有限公司 | Cathode electrophoresis dope of a kind of low-temperature curing and preparation method thereof and using method |
CN103146295B (en) * | 2013-03-01 | 2015-06-03 | 广东科德化工实业有限公司 | Matte cathode electrophoresis coating as well as preparation method and use method for same |
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CN103305110B (en) * | 2013-06-24 | 2016-03-02 | 浩力森涂料(上海)有限公司 | A kind of low-temperature curing cathode electrophoresis coating and preparation method thereof |
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CN108929427B (en) * | 2018-06-12 | 2020-12-22 | 湖南大学 | Preparation method of blocked isocyanate for improving film-forming property of cathode electrophoretic coating |
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-
2007
- 2007-04-30 CN CN200710027826A patent/CN100575428C/en not_active Expired - Fee Related
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CN101054487A (en) | 2007-10-17 |
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Effective date of registration: 20120523 Address after: 528200, Guangdong, Foshan, Nanhai District, Guicheng street, No. 17 deep sea road, Han Tian science and technology city A District No. 7 building, building six Patentee after: Foshan Kefoo Technology Co., Ltd. Address before: 528000 Science Museum, three South Xing Road, Nanhai District, Foshan City, Guangdong province (mailbox ninth, Nanhai City, Guangdong province), Guicheng Patentee before: Yuan Xing |
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Address after: 528200, Guangdong, Foshan, Nanhai District, Guicheng street, No. 17 deep sea road, Han Tian science and technology city A District No. 7 building, building six Patentee after: Guangdong customer service Polytron Technologies Inc Address before: 528200, Guangdong, Foshan, Nanhai District, Guicheng street, No. 17 deep sea road, Han Tian science and technology city A District No. 7 building, building six Patentee before: Foshan Kefoo Technology Co., Ltd. |
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Correction item: Patentee Correct: Guangdong Kefoo Technology Co., Ltd.|528200, Guangdong, Foshan, Nanhai District, Guicheng street, No. 17 deep sea road, Han Tian science and technology city A District No. 7 building, building six False: Guangdong customer service Polytron Technologies Inc|528200, Guangdong, Foshan, Nanhai District, Guicheng street, No. 17 deep sea road, Han Tian science and technology city A District No. 7 building, building six Number: 29 Volume: 30 |
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Free format text: CORRECT: PATENTEE; FROM: GUANGDONG CUSTOMER SERVICE TECHNOLOGY CO., LTD.:528200 FOSHAN, GUANGDONG PROVINCE TO: GUANGDONG KEFOO TECHNOLOGY CO., LTD.:528200 FOSHAN, GUANGDONG PROVINCE |
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Application publication date: 20071017 Assignee: Foshan Kefoo Technology Co., Ltd. Assignor: Yuan Xing Contract record no.: 2011440000464 Denomination of invention: Method of preparing low temperature solidifying environment protection type cathode electrophoresis coating Granted publication date: 20091230 License type: Exclusive License Record date: 20110527 |
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Effective date of registration: 20161018 Address after: Six, Guangdong, Foshan, Nanhai District, Guicheng street, 17 deep sea road, 602 days, 7 building, No. 528200, A District, Han Tian science and Technology City Patentee after: Foshan rich Technology Co., Ltd. Address before: 528200, Guangdong, Foshan, Nanhai District, Guicheng street, No. 17 deep sea road, Han Tian science and technology city A District No. 7 building, building six Patentee before: Guangdong Kefoo Technology Co., Ltd. |
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