CN100510705C - Method for confirming no applying glue region of perforated tipping paper on ventilated cigarette filter tip - Google Patents

Method for confirming no applying glue region of perforated tipping paper on ventilated cigarette filter tip Download PDF

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Publication number
CN100510705C
CN100510705C CNB2007101930949A CN200710193094A CN100510705C CN 100510705 C CN100510705 C CN 100510705C CN B2007101930949 A CNB2007101930949 A CN B2007101930949A CN 200710193094 A CN200710193094 A CN 200710193094A CN 100510705 C CN100510705 C CN 100510705C
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China
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tipping paper
applying glue
color
perforated
glue zone
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CN101178354A (en
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邢军
李晓辉
唐纲岭
侯宏卫
周明珠
周德成
胡清源
刘锋
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Zhengzhou Tobacco Research Institute of CNTC
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Zhengzhou Tobacco Research Institute of CNTC
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Abstract

The invention relates to a method for determining an area of a perforated tipping paper which is not applied with adhesive and is arranged on a ventilation cigarette filter, and the invention is characterized in that: the method includes the following steps: a. a coloring agent is prepared, the ethanol solution of iodine with the concentration of (3 to 60g/L) and the ethanol solution of potassium iodide with the concentration of (1 to 30g/L) are taken according to a volume ratio of 1:1 for full and even mixing; b. the distilled water or purified water is taken for standby; c. the perforated tipping paper is arranged in the coloring agent for coloring, when the color of the tipping paper turns to coffee, the tipping paper is taken out; d. the tipping paper after the coloring is placed in the water for dilution, when the color of the area of the tipping paper which is applied with the adhesive and the color of the tipping paper which is not applied with the adhesive have the significant difference, the tipping paper is taken out for drying; e. the area of the perforated tipping paper which is not applied with the adhesive can be determined by the significant boundary between the two areas. The method provides an effective and rapid means, which can not only determine the area of the perforated tipping paper which is not applied with the adhesive on the finished cigarette product, but also not affect the actual size of the area which is not applied with the adhesive, so the invention can be used for the evaluation of the cigarette manufacturers to the requirements and effects of the ventilation technology of the ventilation cigarette filters.

Description

The perforated tipping paper method in applying glue zone not on a kind of definite ventilated cigarette filter tip
Technical field
The present invention relates to the tobacco field, relate on a kind of definite ventilation cigarette the not method in applying glue zone of perforated tipping paper specifically, by this method, can understand, grasp and evaluating cigarette manufacturing enterprise be to the designing requirement of filter tip aeration technology and the effect of ventilation cigarette.
Background technology
Fall in the burnt technology various, adopt filter tip aeration technology the most generally, promptly effectively cooperate with high saturating shaping paper and finish by perforated tipping paper.We know, the filter tip of cigarette partly is to be rolled by tipping paper parcel filter stick to form, filter stick then is wrapped in tow by shaping paper and makes, generally, be to adopt a certain amount of white glue with vinyl that tipping paper and shaping paper are clung fully in the middle of cigarette cigarette process, guarantee the wide degree and the presentation quality of whole cigarette, but for the cigarette (hereinafter to be referred as the ventilation cigarette) that adopts the filter tip aeration technology, mean and to adopt perforated tipping paper and high saturating shaping paper, if also to adopt use the same method carries out bondingly, that has just lost the effect that filter tip ventilates.Therefore want to make the filter tip aeration technology to reach good effect, it is bonding just need to carry out part between perforated tipping paper and high saturating shaping paper, the perforated tape (zone) of reserving perforated tipping paper does not carry out bonding, so both guaranteed good filter tip ventilation effect, guaranteed the wide degree and the presentation quality of whole cigarette again, this part not adhesion area be referred to as not applying glue district.
Design for traditional cigarette process, people adopt the perforated tipping paper of known air permeability design load, high saturating shaping paper to cooperatively interact and carry out the filter tip ventilation often, but the ventilation effect of actual cigarette also will be subjected to the influence in the not applying glue district of perforated tipping paper.If reality can not meet the demands in the applying glue district, then cause the imagination of actual ventilation rate and expection to differ far away.Moreover for the cigarette finished product an of the unknown, classic method but has no way of learning the perforated tipping paper actual size in applying glue zone not on the ventilation cigarette.
Summary of the invention
Purpose of the present invention just be based on the zone of applying glue on the perforated tipping paper that separates in the ventilated cigarette filter tip and the process characteristic in applying glue zone not and at present still not from known finished cigarettes determine on its filter tip perforated tipping paper not the applying glue zone method and the not method in applying glue zone of perforated tipping paper is provided on a kind of definite effectively ventilated cigarette filter tip, thereby understanding, grasp and evaluating cigarette manufacturing enterprise are to the designing requirement of filter tip aeration technology and the effect of ventilation cigarette.
The objective of the invention is to be achieved through the following technical solutions: on definite ventilated cigarette filter tip of the present invention perforated tipping paper not the method in applying glue zone may further comprise the steps: a. prepares colorant, get concentration for (ethanolic solution of 3~60g/L) iodine and concentration are the (ethanolic solution of 1~30g/L) potassium iodide, volume ratio by 1: 1 fully mixes it; B. it is standby to get a certain amount of water, and described water is distilled water or pure water; C. will be from ventilated cigarette filter tip isolated perforated tipping paper to put into colorant painted, treat to take out after the tipping paper color becomes dark brown; D. will put into water through painted tipping paper and dilute, treat that taking out after the marked difference appears in the color in tipping paper applying glue zone and the color in applying glue zone not, dries; E. can determine on the ventilated cigarette filter tip not applying glue zone of perforated tipping paper by two interregional obvious boundaries.
In the present invention, the dilution of described d step comprises twice, to put into water through painted tipping paper earlier and carry out the dilution first time, the color in applying glue zone and the obviously difference back taking-up of color appearance in applying glue zone at least 15 seconds time or the tipping paper, to put into water once more through the tipping paper of dilution for the first time then and carry out dilution second time, the time be at least 30 seconds or the color in tipping paper applying glue zone and not the color in applying glue zone occur taking out after the marked difference.
The dry process of tipping paper can be to be placed on the mode of drying in the shade naturally on the filter paper in the above-mentioned d step, also can be that other is used always or the mode of similarly drying in the shade.
Colorant among the present invention is specially formulated at the characteristic of the process characteristic of perforated tipping paper on the filter tip in the ventilation cigarette cigarette production run and bonding agent, is used for distinguishing applying glue zone and applying glue zone not on the perforated tipping paper.The cigarette of ventilation cigarette need apply a certain amount of mouth tackifier that connects when propping up with the actual cigarette of filter tip, with perforated tipping paper with two parts integrator, but because the designing requirement of ventilation cigarette, the perforated area that needs to reserve perforated tipping paper is not carried out applying glue, play a role with high saturating shaping paper with the punching district that guarantees perforated tipping paper, play corresponding ventilation effect.The chief component of perforated tipping paper is a fiber, and the tackifier that tipping paper uses is commonly called as white glue with vinyl as the polyvinyl acetate emulsion adhesive, after soon VAM carries out emulsion polymerization in aqueous medium, at mixed emulsion adhesives that gets such as inserts.Usually this class tackifier is to add gelatinized corn starch etc. after the emulsion adhesive that will make suitably dilutes again to carry out thickening, colorant is made up of the ethanolic solution of certain density iodine and the ethanolic solution of potassium iodide, utilize iodine to meet the principle of starch variable color, the applying glue zone and the not applying glue area region of perforated tipping paper are separated.Because in pure medium, iodine is separated from the inclusion compound that it and starch form easily, and the sensitivity of the colour developing effect of starch and iodine decreases, each iodide ion in the colorant in the ethanolic solution of potassium iodide, can follow an iodine molecule combination, generate triiodide ion I 3The I that generates 3 -Ion can be dissociated into iodine and iodide ion.When reaction needed iodine, above-mentioned balance promptly moves to left, and making has the iodine supply in the solution.On the other hand, the sensitivity of colour developing is increased.In addition, in to painted back tipping paper dilution, because unnecessary iodine is insoluble in water, iodide ion is combination with it, forms the teriodide of solubility, makes chromogenic reaction lasting.This method provide a kind of effectively, means efficiently, can determine the not applying glue zone of perforated tipping paper from finished cigarettes, do not influence its not physical size in applying glue zone again, therefore, can be used for filter tip aeration technology designing requirement and the effect of evaluating cigarette manufacturing enterprise the ventilation cigarette.
Specific embodiments
The present invention does description in a second once in conjunction with the embodiments, but does not limit the present invention.
Embodiment 1
Present embodiment is determined perforated tipping paper on the ventilated cigarette filter tip, and the method step in applying glue zone is not as follows:
(1), the preparation colorant: getting ethanolic solution and the concentration that concentration is 6.35g/L iodine is the ethanolic solution of 15g/L potassium iodide, packs in the beaker by 1: 1 volume, it is fully mixed, liquor capacity 3ml, stand-by;
(2), prepare sample: perforated tipping paper and height are shaped after paper separates thoroughly, reject high saturating shaping paper, perforated tipping paper is stand-by.
(3), painted: clip tipping paper with tweezers and put into iodine solution, 15 seconds time, make tipping paper painted, the tipping paper color becomes dark brown, takes out.
(4), dilution for the first time: get a beaker, the 3ml distilled water of packing into clips tipping paper with tweezers and puts into distilled water and dilute, and 15 seconds time, the applying glue field color on the tipping paper bigger difference occurs with not applying glue field color, takes out.
(5), dilution for the second time: get another beaker, the 3ml distilled water of packing into clips tipping paper with tweezers and puts into distilled water and carry out secondary dilution, and the time is 30 seconds, and the applying glue field color on the tipping paper marked difference occurs with not applying glue field color, takes out.
(6), will be placed on the filter paper through the perforated tipping paper of secondary dilution and dry in the shade naturally, to be measured.
(7), a tangible rectangle that presents on the tipping paper is not applying glue zone of perforated tipping paper.
Embodiment 2
Present embodiment is determined perforated tipping paper on the ventilated cigarette filter tip, and the method step in applying glue zone is not as follows:
(1), the preparation colorant: getting ethanolic solution and the concentration that concentration is 20.1g/L iodine is the ethanolic solution of 5g/L potassium iodide, packs in the beaker by 1: 1 volume, it is fully mixed, liquor capacity 3ml, stand-by;
(2), prepare sample: perforated tipping paper and height are shaped after paper separates thoroughly, reject high saturating shaping paper, perforated tipping paper is stand-by.
(3), painted: clip tipping paper with tweezers and put into iodine solution, 15 seconds time, make tipping paper painted, the tipping paper color becomes dark brown, takes out.
(4), dilution for the first time: get a beaker, the 3ml pure water water of packing into clips tipping paper with tweezers and puts into distilled water and dilute, and 15 seconds time, the applying glue field color on the tipping paper bigger difference occurs with not applying glue field color, takes out.
(5), dilution for the second time: get another beaker, the 3ml pure water of packing into clips tipping paper with tweezers and puts into distilled water and carry out secondary dilution, and the time is 30 seconds, and the applying glue field color on the tipping paper marked difference occurs with not applying glue field color, takes out.
(6), will be placed on the filter paper through the perforated tipping paper of secondary dilution and dry in the shade naturally, to be measured.
(7), a tangible rectangle that presents on the tipping paper is not applying glue zone of perforated tipping paper.

Claims (3)

1, the perforated tipping paper method in applying glue zone not on a kind of definite ventilated cigarette filter tip, it is characterized in that: it may further comprise the steps: a. prepares colorant, get that to contain iodine concentration be the ethanolic solution of 3~60g/L and contain the ethanolic solution that potassium iodide concentration is 1~30g/L, volume ratio by 1: 1 fully mixes it; B. it is standby to get a certain amount of water, and described water is distilled water or pure water; C. will be from ventilated cigarette filter tip isolated perforated tipping paper to put into colorant painted, treat to take out after the tipping paper color becomes dark brown; D. will put into water through painted tipping paper and dilute, treat that taking out after the marked difference appears in the color in tipping paper applying glue zone and the color in applying glue zone not, dries; E. can determine on the ventilated cigarette filter tip not applying glue zone of perforated tipping paper by two interregional obvious boundaries.
2, the perforated tipping paper method in applying glue zone not on definite ventilated cigarette filter tip according to claim 1, it is characterized in that: the dilution in the described d step comprises twice, to put into water through painted tipping paper earlier and carry out the dilution first time, the color in applying glue zone and the obviously difference back taking-up of color appearance in applying glue zone at least 15 seconds time or the tipping paper, to put into water once more through the tipping paper of dilution for the first time then and carry out dilution second time, the time be at least 30 seconds or the color in tipping paper applying glue zone and not the color in applying glue zone occur taking out after the marked difference.
3, the perforated tipping paper method in applying glue zone not on definite ventilated cigarette filter tip according to claim 1, it is characterized in that: the dry process of tipping paper is the mode of drying in the shade naturally on filter paper in the above-mentioned d step.
CNB2007101930949A 2007-12-12 2007-12-12 Method for confirming no applying glue region of perforated tipping paper on ventilated cigarette filter tip Active CN100510705C (en)

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CNB2007101930949A CN100510705C (en) 2007-12-12 2007-12-12 Method for confirming no applying glue region of perforated tipping paper on ventilated cigarette filter tip

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Application Number Priority Date Filing Date Title
CNB2007101930949A CN100510705C (en) 2007-12-12 2007-12-12 Method for confirming no applying glue region of perforated tipping paper on ventilated cigarette filter tip

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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101666921B1 (en) * 2015-01-26 2016-10-17 류일영 Personal information leakage prevention functional ink method
CN109527647B (en) * 2018-12-10 2021-04-16 河南中烟工业有限责任公司 Tipping paper gluing area form detection method based on image detection method
CN109527648B (en) * 2018-12-10 2021-04-20 河南中烟工业有限责任公司 Cigarette non-glue area symbol rate detection method based on image detection method
CN111780692A (en) * 2019-12-09 2020-10-16 红塔烟草(集团)有限责任公司 Method for quantitatively measuring non-glue area of tipping paper of cigarette filter
CN112697785A (en) * 2020-11-10 2021-04-23 红云红河烟草(集团)有限责任公司 Method for testing and evaluating gluing uniformity of cigarette roll joint lap

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