CN100471818C - Method for preparing color vertical line enamelled pattern ceramics - Google Patents
Method for preparing color vertical line enamelled pattern ceramics Download PDFInfo
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- CN100471818C CN100471818C CNB2006101020718A CN200610102071A CN100471818C CN 100471818 C CN100471818 C CN 100471818C CN B2006101020718 A CNB2006101020718 A CN B2006101020718A CN 200610102071 A CN200610102071 A CN 200610102071A CN 100471818 C CN100471818 C CN 100471818C
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Abstract
The present invention relates to pottery making technology, and is especially one kind of color enameled pottery with vertical pattern and its making process. The making process of the color enameled pottery with vertical pattern includes the following steps: 1. making sintered biscuit with feldspar, quartz, clay, glass powder, sodium carbonate, sodium silicate and water, and through crushing, molding, sintering and other steps; 2. compounding clinkers; 3. compounding color mud for vertical lines; and 4. compounding glaze material with the clinkers, pigment, water and CMC; coating glaze material for several times and final sintering.
Description
Technical field
The invention belongs to the enamelled pattern ceramics production technical field, be specifically related to a kind of color vertical line enamelled pattern ceramics and preparation method thereof.
Background technology
Vertical line enamelled pattern ceramics be a kind of in warm colored glaze.According to " drink stream vegetarian is said porcelain " record, the enamel flower is created in the Yuan Dynasty, prevails in the Ming Dynasty.Pottery tire enamel flower mostly is Shanxi one band and burns.Decorative pattern on this puckery tire, adopt found the powder technology more, sketches the contours of convex line or embossed decoration decorative pattern profile, fills out bottom and figure colour with required color material respectively then, goes into klining.Enamelled pattern ceramics was unearthed some in Shanxi Jin Nan, grave, the southeast, Shanxi, but burnt the kilneye and the technology division of history into periods of making the enamel flower, did not find yet so far.In addition, the upright line of existing pottery is to adopt blank mud attached to the enamel floral organ that bakes on the mold, and upright line mass of the enamelled pattern ceramics that burns out and color and luster are relatively poor.
Summary of the invention
The present invention overcomes problems of the prior art, and a kind of clay preparation method who makes color vertical line enamelled pattern ceramics of color vertical line who makes of frit and photoghraphic coupler is provided.
The present invention realizes by following technical proposal, the preparation method of color vertical line enamelled pattern ceramics,
1), blank preparation: select feldspar 20-25 part for use, quartzy 10-15 part, clay 60-65 part, the raw material of glass powder 8-10 part; Add water and the yellow soda ash 0.2% of 33-35%, water glass 0.3% is ground into 200 purpose mud shape things, makes mold with plaster mold slip casting; Carry out the making of color vertical line after the moulding, base substrate biscuiting temperature is 1150 ℃, flat burning 30 minutes, biscuiting water-intake rate 10-15%.
2), the preparation of enamel flower frit, form by the preparation of raw material of following weight ratio,
Frit A number: saltpetre 50-55 part, scoria English fine powder 45-50 part, 1 part of Quilonum Retard is fired through 1200-1250 ℃, is aqueous, and shrend is used.
Frit B number: salt of wormwood 28-32 part, red lead 18-25 part, scoria English fine powder 40-50 part is fired through 1200-1250 ℃, is aqueous, and shrend is used.
3), the preparation of color vertical line mud, form by the preparation of raw material of following weight ratio,
Frit A 85-88 part, clay 5-8 part, color vertical line mud photoghraphic coupler 7-10%, scoria English fine powder 15-18 part; Levigate by the various upright line mud of prescription to 10000-hole sieve surplus＜0.01% fineness, add suitable quantity of water and 3-4% carboxymethyl cellulose after the drying, be rolled into the clay shape through three roller ink grinding mills, standby.
4), the preparation of glaze, be to utilize the enamel flower frit for preparing to add photoghraphic coupler ferric oxide or cupric oxide or Manganse Dioxide or tindioxide and contain cobalt black look ceramic pigment formulated again according to the glaze colours needs, during batching, by expecting than water=1:0.8 water distribution, the 1.5-2.0% carboxymethyl cellulose that adds dosage, mesh-of-grind is 10000-hole sieve surplus＜0.01%, and in order to repeatedly being coated with glaze, temperature of glaze firing is 1050-1150 ℃.
Color vertical line mud photoghraphic coupler of the present invention has ceramic black developing agent or ceramic praseodymium cerium yellow pigment or Victoria Green WPB beramic color or extra large dark blue beramic color or ceramic red pigment or zirconium dioxide or tindioxide.The proportioning of its color vertical line mud and color vertical line mud photoghraphic coupler is:
1), the upright line mud prescription of black:
Frit A 85-88 part, clay 3-5 part, 15 parts of scoria English fine powders, ceramic black developing agent 7-10 part;
2), yellow upright line mud prescription
Frit B 75-80 part, clay 3-5 part, 15 parts of scoria English fine powders, ceramic praseodymium cerium yellow pigment 8-10 part;
3), green upright line mud prescription
Frit A 85-88 part, clay 3-5 part, 15 parts of scoria English fine powders, Victoria Green WPB beramic color 7-9 part;
4), blue upright line mud
Frit B 83-86 part, clay 3-5 part, 15 parts of scoria English fine powders, extra large dark blue beramic color 7-9 part;
5), red upright line mud prescription:
Frit A 34-35 part, frit B 35-40 part, clay 3-5 part, 15 parts of scoria English fine powders, ceramic red pigment 8-10 part;
6), the upright line mud prescription of white:
Frit A 30-35 part, frit B 35-40 part, clay 3-5 part, zirconium dioxide 5-10 part, tindioxide 5-10 part.
The preparation of glaze of the present invention:
1, the preparation of the brightly yellowish glaze of enamel
Frit A number 50 parts, 47 parts of B frits, 13 parts of ferric oxide.
2, enamel flower purple glaze
Frit A number 43 parts, 47 parts of B frits, 5 parts of manganese oxide.
4, enamel flower black glaze
Frit B number 93 parts, contain 7 parts of cobalt black look ceramic pigments.
5, the grey color glaze of enamel
Frit B number 86 parts, 14 parts of tindioxide.
6, peacock blue glaze
B frit 26-30 part, A frit 50-60 part, cupric oxide 6-13 part.
More than Pei Fang oxide compound is selected the first grade of chemical materials for use, when preparing burden by various prescriptions, by expecting: water=1:0.8 water distribution, 2% carboxymethyl cellulose that adds dosage, mesh-of-grind are 10000-hole sieve surplus＜0.01%, in order to repeatedly being coated with glaze, temperature of glaze firing is 1050-1150 ℃, can suitably adjust.
Color vertical line mud of the present invention is to add photoghraphic coupler and form preparing on the basis of frit, and it is colored gorgeous to use this color vertical line mud that the upright line of enamelled pattern ceramics is presented, the special-effect that texture is sparkling and crystal-clear.Make the decoration of traditional enamelled pattern ceramics improve artistic value.
Embodiment
Embodiment 1 is an example to make color vertical line enamelled pattern ceramics Dragon Lord figure jar;
(1), blank preparation: select 25 parts of feldspars for use, quartzy 10 parts, 65 parts of clays, the raw material that glass powder is 10 parts; Add water and the yellow soda ash 0.2% of 33-35%, water glass 0.3% is ground into 200 purpose mud shape things, makes a jar parison tire with plaster mold slip casting; Pass through repaired biscuit, wash base, drying process, carry out the making of color vertical line mud then, at first carry out the preparation of enamel flower frit, preparation of raw material by following weight ratio forms, frit A number: 50 parts in saltpetre, 45 parts of scoria English fine powders, 1 part of Quilonum Retard, fire through 1200-1250 ℃, be aqueous, shrend is used.Frit B number: 28 parts in salt of wormwood, 28 parts of red leads, 40 parts of scoria English fine powders are fired through 1200-1250 ℃, are aqueous, and shrend is used.Then make color vertical line mud, the preparation of green upright line mud by frit A number 88 parts, 3 parts of clays, 8 parts of Victoria Green WPB beramic colors, 15 parts of scoria English fine powders.After batching, mesh-of-grind is 10000-hole sieve surplus＜0.01%, after levigate, drying adds suitable quantity of water and 3-4% carboxymethyl cellulose, is rolled into the clay shape through three roller ink grinding mills, the upright line mud that makes in the tubulose poly-bag, the mud bar that manually squeezes out sticks on the mold by the figure line.Through the base substrate biscuiting, the biscuiting temperature is 1150 ℃, the flat burning 30 minutes.
(2), preparation enamel brightly yellowish glaze, its prescription is 50 parts of A frits, 47 parts of B frits, 13 parts of ferric oxide.During batching, by material: water=1:0.8 water distribution, add 2% carboxymethyl cellulose of dosage, mesh-of-grind is 10000-hole sieve surplus＜0.01%, in order to repeatedly being coated with glaze, temperature of glaze firing is 1050-1150 ℃, can suitably adjust.
Embodiment 2 is an example to make color vertical line enamelled pattern ceramics four-quadrant figure hemisphere bottle;
(1), blank preparation: select 20 parts of feldspars for use, quartzy 15 parts, 60 parts of clays, the raw material that glass powder is 8 parts; Add water and the yellow soda ash 0.2% of 33-35%, water glass 0.3% is ground into 200 purpose mud shape things, makes a bottle parison tire with plaster mold slip casting; Pass through repaired biscuit, wash base, drying process, carry out the making of color vertical line mud then, at first carry out the preparation of enamel flower frit, preparation of raw material by following weight ratio forms, frit A number: 55 parts in saltpetre, 48 parts of scoria English fine powders, 1 part of Quilonum Retard, fire through 1200-1250 ℃, be aqueous, shrend is used.Frit B number: 32 parts in salt of wormwood, 25 parts of red leads, 40 parts of scoria English fine powders are fired through 1200-1250 ℃, are aqueous, and shrend is used.Then make color vertical line mud, the upright line mud preparation of black, frit A number 88 parts, 4 parts of clays, 9 parts of ceramic black developing agents, 15 parts of scoria English fine powders.The preparation of green upright line mud by frit A number 85 parts, 3 parts of clays, 15 parts of scoria English fine powders.9 parts of Victoria Green WPB beramic colors.The preparation of the upright line mud of white, frit A number 35 parts, frit B number 40 parts, 5 parts of clays, 8 parts of zirconium dioxides, 10 parts of tindioxide.The preparation of red upright line mud, frit A number 34 parts, frit B number 39 parts, 3 parts of clays, 15 parts of scoria English fine powders, 10 parts of ceramic red pigments.Above-mentioned color vertical line mud is after batching, mesh-of-grind is 10000-hole sieve surplus＜0.01%, add suitable quantity of water and 3-4% carboxymethyl cellulose after the drying, be rolled into the clay shape through three roller ink grinding mills, the upright line mud that makes is contained in the tubulose poly-bag, the mud bar that manually squeezes out sticks on the mold by the figure line.Through the base substrate biscuiting, the biscuiting temperature is 1150 ℃, the flat burning 30 minutes.
(2), preparation enamel Blossom Peacock blue glaze, its prescription is 30 parts of B frits, 60 parts of A frits, 10 parts of cupric oxide.During batching, by material: water=1:0.8 water distribution, add 2% carboxymethyl cellulose of dosage, mesh-of-grind is 10000-hole sieve surplus＜0.01%, in order to repeatedly being coated with glaze, temperature of glaze firing is 1050-1150 ℃, can suitably adjust.
Embodiment 3 is an example to make color vertical line enamelled pattern ceramics prosperity brought by the dragon and the phoenix figure pin;
(1), blank preparation: select 23 parts of feldspars for use, quartzy 15 parts, 62 parts of clays, the raw material that glass powder is 9 parts; Add water and the yellow soda ash 0.2% of 33-35%, water glass 0.3% is ground into 200 purpose mud shape things, makes a bottle parison tire with plaster mold slip casting; Pass through repaired biscuit, wash base, drying process, carry out the making of color vertical line mud then, at first carry out the preparation of enamel flower frit, preparation of raw material by following weight ratio forms, frit A number: 55 parts in saltpetre, 48 parts of scoria English fine powders, 1 part of Quilonum Retard, fire through 1200-1250 ℃, be aqueous, shrend is used.Frit B number: 32 parts in salt of wormwood, 25 parts of red leads, 40 parts of scoria English fine powders are fired through 1200-1250 ℃, are aqueous, and shrend is used.Then make color vertical line mud, the preparation of green upright line mud by frit A number 84 parts, 4 parts of clays, 8 parts of Victoria Green WPB beramic colors, 15 parts of scoria English fine powders.The preparation of the upright line mud of white, frit A number 35 parts, frit B number 40 parts, 5 parts of clays, 10 parts of zirconium dioxides, 8 parts of tindioxide.The preparation of yellow upright line mud, frit B number 75 parts, 5 parts of clays, 15 parts of scoria English fine powders, 10 parts of ceramic praseodymium cerium yellow pigments.
Above-mentioned color vertical line mud is after batching, mesh-of-grind is 10000-hole sieve surplus＜0.01%, after oven dry, add suitable quantity of water and 3-4% carboxymethyl cellulose, be rolled into the clay shape through three roller ink grinding mills, the upright line mud that makes in the tubulose poly-bag, the mud bar that manually squeezes out sticks on the mold by the figure line.Through the base substrate biscuiting, the biscuiting temperature is 1150 ℃, flat burning 30 minutes, biscuiting water-intake rate 10-15%.
(2), the preparation enamel spends purple eggplant color glaze, its prescription is 43 parts of A frits, 47 parts of B frits, Manganse Dioxide 5%.During batching, by material: water=1:0.8 water distribution, add 2% carboxymethyl cellulose of dosage, mesh-of-grind is 10000-hole sieve surplus＜0.01%, in order to repeatedly being coated with glaze, temperature of glaze firing is 1050-1150 ℃, can suitably adjust.
Claims (3)
1, a kind of preparation method of color vertical line enamelled pattern ceramics is characterized in that:
1), the preparation of blank: select feldspar 20-25 part for use, quartzy 10-15 part, clay 60-65 part, the raw material of glass powder 8-10 part, water and the yellow soda ash 0.2% of adding 33-35%, water glass 0.3%, be ground into 200 purpose mud shape things, make mold with plaster mold slip casting; Carry out the making of color vertical line after the moulding, the base substrate biscuiting, the biscuiting temperature is 1150 ℃, flat burning 30 minutes, biscuiting water-intake rate 10-15%;
2), the preparation of enamel flower frit, form by the preparation of raw material of following weight ratio,
Frit A number: saltpetre 50-55 part, scoria English fine powder 45-50 part, 1 part of Quilonum Retard is fired through 1200-1250 ℃, is aqueous, and shrend is used;
Frit B number: salt of wormwood 28-32 part, red lead 18-25 part, scoria English fine powder 40-50 part is fired through 1200-1250 ℃, is aqueous, and shrend is used;
3), the preparation of color vertical line mud, form by the preparation of raw material of following weight ratio,
Frit 75-88 part, clay 3-5 part, scoria English fine powder 15-18 part, color vertical line mud photoghraphic coupler 5-10 part, levigate by the various upright line mud of prescription to 10000-hole sieve surplus＜0.01% fineness, add suitable quantity of water and 3-4% carboxymethyl cellulose after the drying, be rolled into the clay shape through three roller ink grinding mills, standby;
4), the preparation of glaze, be to utilize the enamel flower frit for preparing to add photoghraphic coupler ferric oxide or cupric oxide or Manganse Dioxide or tindioxide and contain cobalt black look ceramic pigment formulated again according to the glaze colours needs, during batching, by expecting than water=1:0.8 water distribution, the 1.5-2.0% carboxymethyl cellulose that adds dosage, mesh-of-grind is 10000-hole sieve surplus＜0.01%, and in order to repeatedly being coated with glaze, temperature of glaze firing is 1050-1150 ℃.
2, the preparation method of color vertical line enamelled pattern ceramics according to claim 1 is characterized in that described color vertical line mud photoghraphic coupler has ceramic black developing agent or ceramic praseodymium cerium yellow pigment or Victoria Green WPB beramic color or extra large dark blue beramic color or ceramic red pigment or zirconium dioxide or tindioxide.
3, the preparation method of color vertical line enamelled pattern ceramics according to claim 2 is characterized in that the proportioning of color vertical line mud and color vertical line mud photoghraphic coupler, makes by the raw material of following weight ratio,
1), the upright line mud prescription of black:
Frit A 85-88 part, clay 3-5 part, 15 parts of scoria English fine powders, ceramic black developing agent 7-10 part;
2), yellow upright line mud prescription:
Frit B 75-80 part, clay 3-5 part, 15 parts of scoria English fine powders, ceramic praseodymium cerium yellow pigment 8-10 part;
3), green upright line mud prescription:
Frit A 85-88 part, clay 3-5 part, 15 parts of scoria English fine powders, Victoria Green WPB beramic color 7-9 part;
4), blue upright line mud prescription:
Frit B 83-86 part, clay 3-5 part, 15 parts of scoria English fine powders, extra large dark blue beramic color 7-9 part;
5), red upright line mud prescription:
Frit A 34-35 part, frit B 35-40 part, clay 3-5 part, 15 parts of scoria English fine powders, ceramic red pigment 8-10 part;
6), the upright line mud prescription of white:
Frit A 30-35 part, frit B 35-40 part, clay 3-5 part, zirconium dioxide 5-10 part, tindioxide 5-10 part.
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| CN101891502A (en) * | 2010-08-12 | 2010-11-24 | 醴陵陶润实业发展有限公司 | Method for manufacturing peacock glaze |
| CN102491733B (en) * | 2011-11-28 | 2013-01-30 | 白银陇烨陶瓷有限公司 | Method for firing art ceramic products |
| CN102765967A (en) * | 2012-07-11 | 2012-11-07 | 卢群山 | Painted pottery glaze composition and preparation process for composition-containing painted pottery |
| CN103204705B (en) * | 2013-01-09 | 2015-05-13 | 唐山工业职业技术学院 | Manufacturing process for medium-temperature vitreous crystal glaze of bone china |
| CN103951385A (en) * | 2014-04-14 | 2014-07-30 | 阳城县侨枫瓷业有限公司 | Fahua chinaware and production method thereof |
| CN106187326B (en) * | 2016-06-29 | 2018-10-30 | 刘欣 | A kind of bright-colored color manufacture craft |
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| Title |
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| 明代景德镇陶瓷雕塑. 余祖球.陶瓷科学与艺术，第4期. 2003 |
| 明代景德镇陶瓷雕塑. 余祖球.陶瓷科学与艺术，第4期. 2003 * |
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