CN100408584C - 二乙基锌的制备方法 - Google Patents
二乙基锌的制备方法 Download PDFInfo
- Publication number
- CN100408584C CN100408584C CNB2006100468676A CN200610046867A CN100408584C CN 100408584 C CN100408584 C CN 100408584C CN B2006100468676 A CNB2006100468676 A CN B2006100468676A CN 200610046867 A CN200610046867 A CN 200610046867A CN 100408584 C CN100408584 C CN 100408584C
- Authority
- CN
- China
- Prior art keywords
- reaction
- zinc
- temperature
- added
- iodoethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2006100468676A CN100408584C (zh) | 2006-06-06 | 2006-06-06 | 二乙基锌的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2006100468676A CN100408584C (zh) | 2006-06-06 | 2006-06-06 | 二乙基锌的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1861609A CN1861609A (zh) | 2006-11-15 |
CN100408584C true CN100408584C (zh) | 2008-08-06 |
Family
ID=37389151
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2006100468676A Expired - Fee Related CN100408584C (zh) | 2006-06-06 | 2006-06-06 | 二乙基锌的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN100408584C (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2018019291A1 (en) * | 2016-07-29 | 2018-02-01 | The Hong Kong University Of Science And Technology | C(sp3)-c(sp2) cross-coupling reaction of organozinc reagents and heterocyclic (pseudo)halides |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4385003A (en) * | 1981-10-30 | 1983-05-24 | Stauffer Chemical Company | Dialkylzinc composition having improved thermal stability |
US4402880A (en) * | 1981-10-30 | 1983-09-06 | Stauffer Chemical Company | Dialkylzinc compositions having improved thermal stability |
US4407758A (en) * | 1981-10-30 | 1983-10-04 | Stauffer Chemical Company | Dialkylzinc compositions having improved thermal stability |
US4732992A (en) * | 1986-12-22 | 1988-03-22 | Stauffer Chemical Company | Method for recovery of alkylaluminum halides |
US4841082A (en) * | 1988-08-19 | 1989-06-20 | Texas Alkyls, Inc. | Preparation of dimethylzinc |
JPH04221389A (ja) * | 1990-12-25 | 1992-08-11 | Mitsui Toatsu Chem Inc | ジアルキル亜鉛の製造方法 |
RU1775403C (ru) * | 1990-07-23 | 1992-11-15 | Нижегородский политехнический институт | Способ получени диэтилцинка высокой чистоты |
US6184404B1 (en) * | 1998-03-05 | 2001-02-06 | Metallgesellschaft Aktiengesellschaft | Process for the selective alkylation of aldehydes by means of organozinc compounds |
-
2006
- 2006-06-06 CN CNB2006100468676A patent/CN100408584C/zh not_active Expired - Fee Related
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4385003A (en) * | 1981-10-30 | 1983-05-24 | Stauffer Chemical Company | Dialkylzinc composition having improved thermal stability |
US4402880A (en) * | 1981-10-30 | 1983-09-06 | Stauffer Chemical Company | Dialkylzinc compositions having improved thermal stability |
US4407758A (en) * | 1981-10-30 | 1983-10-04 | Stauffer Chemical Company | Dialkylzinc compositions having improved thermal stability |
US4732992A (en) * | 1986-12-22 | 1988-03-22 | Stauffer Chemical Company | Method for recovery of alkylaluminum halides |
US4841082A (en) * | 1988-08-19 | 1989-06-20 | Texas Alkyls, Inc. | Preparation of dimethylzinc |
RU1775403C (ru) * | 1990-07-23 | 1992-11-15 | Нижегородский политехнический институт | Способ получени диэтилцинка высокой чистоты |
JPH04221389A (ja) * | 1990-12-25 | 1992-08-11 | Mitsui Toatsu Chem Inc | ジアルキル亜鉛の製造方法 |
US6184404B1 (en) * | 1998-03-05 | 2001-02-06 | Metallgesellschaft Aktiengesellschaft | Process for the selective alkylation of aldehydes by means of organozinc compounds |
Non-Patent Citations (2)
Title |
---|
制备高纯二乙基锌的改进方法. 陈玉英,赵晨阳,陈晓惠.稀有金属,第5期. 1992 |
制备高纯二乙基锌的改进方法. 陈玉英,赵晨阳,陈晓惠.稀有金属,第5期. 1992 * |
Also Published As
Publication number | Publication date |
---|---|
CN1861609A (zh) | 2006-11-15 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN108191621A (zh) | 一种频哪酮的制备工艺 | |
CN107827947A (zh) | 从含甾醇酯的渣油中提取高纯度甾醇的方法 | |
CN104387234B (zh) | 一种3-甲基-3-丁烯-1-醇的合成方法 | |
CN106588735A (zh) | 一种双(叔丁基过氧化异丙基)苯的生产方法 | |
CN101284783B (zh) | 一种硝基苯醚类化合物的合成方法 | |
CN100408584C (zh) | 二乙基锌的制备方法 | |
CN102976897A (zh) | 一种四氟丙醇的提纯方法 | |
CN109369328A (zh) | 一种简单安全合成丙炔醇的制备方法 | |
CN103193636B (zh) | 一种合成2,3-丁二醇酯的方法 | |
CN102030625B (zh) | 一种香兰素合成的方法 | |
CN104447672A (zh) | 一种活性炭固载杂多酸用于合成ε-己内酯的方法 | |
CN107235937A (zh) | 一种(s)‑3‑羟基四氢呋喃的合成方法 | |
CN106349139A (zh) | 一种高纯度过氧苯甲酰的制备方法 | |
CN113582824B (zh) | 一种高纯度环丙基甲基酮的制备方法 | |
CN103102369B (zh) | 一种乙基膦酸二乙酯的生产方法 | |
CN102442933B (zh) | 溶剂型过氧化新癸酸特丁酯(bnp)的制备方法 | |
CN106809887A (zh) | 一种制备氯铱酸的方法 | |
CN111825705A (zh) | 一种三氟化硼二甲基硫醚络合物的制备方法 | |
CN102464633A (zh) | (甲基)丙烯酸缩水甘油酯的合成方法 | |
CN114920642A (zh) | 一种获得高纯度脂肪酸单甘油酯和脂肪酸二甘油酯的分离工艺 | |
CN114716358A (zh) | 一种利用微反应器连续合成过氧乙酸的方法 | |
CN108299197B (zh) | 一种3-烷氧基丙烯酸酯合成方法 | |
CN112430197A (zh) | 一种3-氧代-5-羟基-6-氰基己酸叔丁酯的合成方法 | |
KR20200131065A (ko) | 연속식 반응공정을 사용하는 알킬 3-알콕시프로피오네이트의 제조방법 | |
CN115466255B (zh) | 一种托品醇及其合成方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: KELIDE CHEMICAL TECH DEVELOPMENT CO., LTD., DALIAN Free format text: FORMER OWNER: JINGYUAN ELECTRONIC GASEOUS RESEARCH CENTER CO., LTD., DALIAN Effective date: 20111213 |
|
C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20111213 Address after: 116600 storage processing zone IE-33, Dalian Free Trade Zone, Liaoning Patentee after: Dalian Free Trade Zone Credit Chemical Technology Development Co., Ltd. Address before: 116600 storage processing zone IE-33, Dalian Free Trade Zone, Dalian, Liaoning Patentee before: Jingyuan Electronic Gaseous Research Center Co., Ltd., Dalian |
|
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080806 Termination date: 20150606 |
|
EXPY | Termination of patent right or utility model |