CA2646867A1 - Hair dyes comprising 3-amin0-2,6-dimethylphenol - Google Patents

Abstract

The present invention relates to a composition comprising as coupler compound 3-amino-2,6-dimethylphenol and/or its inorganic or organic salt; as well as a method of dyeing keratin fibers using the above dye composition.

Description

HAIR DYES COMPRISING 3-AMINO-2,6-DIMETHYLPHENOL
FIELD OF THE INVENTION
The subject matter of the present application are compositions and methods for dyeing keratin fibers containing the 3-amino-2,6-dimethylphenol and physiologically compatible salts thereof.
BACKGROUND OF THE INVENTION
In the field of dyeing keratin fibers, in particular hair coloring, oxidation dyes have achieved significant importance. The coloration arises here as a result of the reaction of certain developer substances with certain coupler substances in the presence of a suitable oxidizing agent. The developer substances used here are, in particular, unsubstituted or substituted 1,4-diaminobenzenes.
Besides dyeing to the desired intensity, numerous additional demands are made on oxidation dyes which are used for coloring human hair. For example, the dyes must be acceptable from a toxicological and dermatological point of view and the hair colorations achieved must have good light fastness, permanent wave fastness, acid fastness and rubbing fastness.
However, in any case, such colorations must remain stable over a period of at least 4 to 6 weeks without being affected by light, rubbing and chemical agents. Furthermore, it is required that the suitable dyes possess a good physiological compatibility.

The currently used colorants, however, do not satisfy the above mentioned requirements in all respects. Therefore there is still a need for novel coupler substances which satisfy the above mentioned requirements to a better degree.

SUMMARY OF THE INVENTION
Therefore there is a need for new o-aminophenol derivatives with improved properties, especially with regard to improved physiological compatibility.
DETAILED DESCRIPTION OF THE INVENTION
It has now been found that 3-amino-2,6-dimethylphenol and its salts have improved properties, especially they are non-sensitizing.

The present invention therefore relates to compositions and methods for dyeing keratin fibers, especially wool, silk or hair, particularly human hair, using the 3-amino-2,6-dimethylphenol and/or its inorganic or organic salt.

Although the 3-amino-2,6-dimethylphenol and/or its inorganic or organic salt are especially suitable for dyeing kertain fibers, in principle it would also be possible to dye other natural or synthetic fibers, especially cotton or nylon 66, with the 3-amino-2,6-dimethylphenol.

The 3-amino-2,6-dimethylphenol and/or its inorganic or organic salt may be used alone or in combination with known developer substances and/or coupler substances.

Suitable developers for use in the compositions described herein include, but are not limited to:
p-phenylenediamine derivatives, e.g. benzene-1,4-diamine (commonly known as p-phenylenediamine), 2-methyl-benzene-1,4-diamine, 2-chloro-benzene-1,4-diamine, N-phenyl-benzene-l,4-diamine, N-(2-ethoxyethyl)benzene-1,4-diamine, 2-[(4-amino-phenyl)-(2-hydroxy-ethyl)-amino]-ethanol, (commonly known as N,N-bis(2-hydroxyethyl)-p-phenylenediamine) (2,5-diamino-phenyl)-methanol, 1-(2'-Hydroxyethyl)-2,5-diaminobenzene, 2-(2,5-diamino-phenyl)-ethanol, N-(4-aminophenyl)benzene-1,4-diamine, 2,6-dimethyl-benzene-1,4-diamine, 2-isopropyl-benzene-1,4-diamine, 1-[(4-aminophenyl)amino]-propan-2-ol, 2-propyl-benzene-1,4-diamine, 1,3-bis[(4-aminophenyl)(2-hydroxyethyl)amino]propan-2-ol, N4,N4,2-trimethylbenzene-1,4-diamine, 2-methoxy-benzene-1,4-diamine, 1-(2,5-diaminophenyl)ethane-1,2-diol, 2,3-dimethyl-benzene-1,4-diamine, N-(4-amino-3-hydroxy-phenyl)-acetamide, 2,6-diethylbenzene-1,4-diamine, 1,4-diamino-2-methoxymethylbenzene, 2,5-dimethylbenzene-1,4-diamine, 2-thien-2-ylbenzene-1,4-diamine, 2-thien-3-ylbenzene-1,4-diamine, 2-pyridin-3-ylbenzene-1,4-diamine, 1,1'-biphenyl-2,5-diamine, 2-(methoxymethyl)-benzene-1,4-diamine, 2-(aminomethyl)benzene-1,4-diamine, 2-(2,5-diaminophenoxy)ethanol, N-[2-(2,5-diaminophenoxy)ethyl]-acetamide, N,N-dimethylbenzene-1,4-diamine, N,N-diethylbenzene-1,4-diamine, N,N-dipropylbenzene-1,4-diamine, 2-[(4-aminophenyl)-(ethyl)amino]ethanol, 2-[(4-amino-3-methyl-phenyl)-(2-hydroxy-ethyl)-amino]-ethanol, N-(2-methoxyethyl)-benzene-1,4-diamine, 3-[(4-aminophenyl)amino]propan-l-ol, 3-[(4-aminophenyl)-amino]propane-1,2-diol, N-(4-[(4-aminophenyl)amino]butyl}benzene-1,4-diamine, and 2-[2-(2-{2-[(2,5-diaminophenyl)-oxy]ethoxy}ethoxy)ethoxy]benzene-1,4-diamine;
1,3-Bis(N(2-Hydroxyethyl)-N-(4-amino-phenyl)amino)-2-propanol; 2,2'-[1,2-Ethanediyl-bis-(oxy-2,l-ethanediyloxy)]-bis-benzene-1,4-diamine; N,N-Bis(2-hydroxyethyl)-p-phenylinediamine; p-aminophenol derivatives such as: 4-amino-phenol (commonly known as p-aminophenol), 4-methylamino-phenol, 4-amino-3-methyl-phenol, 4-amino-2-hydroxymethyl-phenol, 4-amino-2-methyl-phenol, 4-amino-l-hydroxy-2-(2'-hydroxyethylaminomethyl)benzene, 4-amino-2-methoxymethyl-phenol, 5-amino-2-hydroxy-benzoic acid, 1-(5-amino-2-hydroxy-phenyl)-ethane-1,2-diol, 4-amino-2-(2-hydroxy-ethyl)-phenol, 4-amino-3-(hydroxymethyl)-phenol, 4-amino-3-fluoro-phenol, 4-amino-2-(aminomethyl)-phenol, 4-amino-2-fluoro-phenol;
1-Hydroxy-2,4-diaminobenzene; 1-(2'-Hydroxyethyloxy)-2,4-diaminobenzene; 2,4-Diamino-5-methylphenetol; o-phenylenediamine derivatives such as: 3,4-Diaminobenzoic acid and salts thereof; o-aminophenol derivatives such as: 2-amino-phenol (commonly known as o-aminophenol), 2,4-diaminophenol, 2-amino-5-methyl-phenol, 2-amino-6-methyl-phenol, N-(4-amino-3-hydroxy-phenyl)-acetamide, and 2-amino-4-methyl-phenol; and heterocyclic derivatives such as: pyrimidine-2,4,5,6-tetramine (commonly known as 2,4,5,6-tetraamino-pyridine), 1-methyl-lH-pyrazole-4,5-diamine, 2-(4,5-diamino-lH-pyrazol-1-yl)ethanol, NZ,N2-dimethyl-pyridine-2,5-diamine, 2-[(3-amino-6-methoxypyridin-2-yl)amino]ethanol, 6-methoxy-N2-methyl-pyridine-2,3-diamine, 2,5,6-triaminopyrimidin-4(1H)-one, pyridine-2,5-diamine, 1-isopropyl-lH-pyrazole-4,5-diamine, 1-(4-methylbenzyl)-1H-pyrazole-4,5-diamine, 1-(benzyl)-1H-pyrazole-4,5-diamine, 1-(4-chlorobenzyl)-1H-pyrazole-4,5-diamine, pyrazolo[1,5-a]-pyrimidine-3,7-diamine, 5,6,7-trimethylpyrazolo[1,5-a]pyrimidin-3-ylamine hydrochloride, 7-methylpyrazolo[1,5-a]pyrimidin-3-ylamine hydrochloride, 2,5,6,7-teramethyl-pyrazolo[1,5-a]pyrimidin-3-ylamine hydrochloride, 5,7-di-tert-butylpyrazolo[1,5-a]pyrimidin-3-ylamine hydrochloride, 5,7-di-trifluoromethyl-pyrazolo[ 1,5-a]pyrimidin-3-ylamine hydrochloride, 2-methylpyrazolo[1,5-a]pyrimidin-3,7-diamine hydrochloride; 4-hydroxy-2,5,6-triaminopyrimidine; 1-(2'hydroxyethyl)-amino-3,4-methylene dioxybenzene; and 1-hydroxyethyl-4,5-diaminopyrazole sulphate.
Additional developers include: N-(3-furylmethyl)benzene-1,4-diamine; N-Thiophen-3-ylmethyl-benzene- 1,4-diamine; N-(2-furylmethyl)benzene-1,4-diamine; N-Thiophen-2-ylmethyl-benzene-1,4-diamine; 4-Hydroxy-benzoic acid (2,5-diamino-benzylidene)-hydrazide; 3-(2,5-Diamino-phenyl)-N-ethyl-acrylamide; 2-[3 -(3 -Amino-phenylamino)-propenyl] -benzene-1,4-diam ine;
2-[3-(4-Amino-phenylamino)-propenyl]-benzene-1,4-diamine; 2-(6-Methyl-pyridin-2-yl)-benzene-1,4-diamine; 2-Pyridin-2-yl-benzene-1,4-diamine; 2-[3-(4-Amino-phenylamino)-propenylj-benzene-1,4-diamine; 2-[3-(3-Amino-phenylamino)-propenyl]-benzene-1,4-diamine;
3-(2,5-Diamino-phenyl)-N-ethyl-acrylamide; 2-Thiazol-2-yl-benzene-1,4-diamine;

4-Hydroxy-benzoic acid (2,5-diamino-benzylidene)-hydrazide; 3'-Fluoro-biphenyl-2,5-diamine; 2-Propenyl-benzene- 1,4-diamine; 2'-Chloro-biphenyl-2,5-diamine; N-Thiophen-3-ylmethyl-benzene-1,4-diamine; N-(3-furylmethyl)benzene-1,4-diamine; 4'-Methoxy-biphenyl-2,5-diamine; N-(4-Amino-benzyl)-benzene-1,4-diamine; 2-Methyl-5-[(1-H-pyrrol-2-ylmethyl)-amino]-phenol;

5-[(Furan-2-ylmethyl)-amino]-2-methyl-phenol; 5-Isopropylamino-2-methyl-phenol; Biphenyl-2,4,4'-triamine hydrochloride; 5-(4-Amino-phenyl)aminomethyl-benzene-1,3-diamine hydrochloride; 5-Phenylaminomethyl-benzene-1,3-diamine hydrochloride; 2-[4-Amino-2-(3,5-diamino-benzylamino)-phenoxy]-ethanol hydrochloride; 5-(3-Amino-phenyl)aminomethyl-benzene-1,3-diamine hydrochloride; N-(2-Amino-benzyl)-benzene-1,3-diamine hydrochloride;
N-Furan-2-ylmethyl-benzene-1,3-diamine hydrochloride; 2-[(3-Amino-phenylamino)-methyl]-phenol hydrochloride; 4-Amino-2-propylaminomethyl-phenol; hydrochloride;
N-Benzo[1,3]dioxol-5-ylmethyl-benzene-1,3-diamine hydrochloride; N-[4-Amino-2-(2-hydroxy-ethyl)-2H-pyrazol-3-yl]-3-(5-amino-2-hydroxy-phenyl)-acrylamide;
hydrochloride; 4-Amino-2-(isopropylamino-methyl)-phenol; hydrochloride; 4-Thiophen-3-yl-benzene-1,3-diamine;
hydrochloride hydrochloride; 5-Phenylaminomethyl-benzene-1,3-diamine hydrochloride;
5-(3-Amino-phenyl)aminomethyl-benzene-1,3-diamine hydrochloride; 4-Thiophen-3-yl-benzene-1,3-diamine; hydrochloride; 2',4'-Diamino-biphenyl-4-ol; hydrochloride;
5-Cyclobutylamino-2-methyl-phenol; 5-Cyclobutylamino-2-methyl-phenol; 4-Amino-2-(pyridin-3-ylaminomethyl)-phenol; 5-(3-Amino-phenyl)aminomethyl-benzene-1,3-diamine hydrochloride;
5-Allylaminomethyl-benzene-1,3-diamine hydrochloride; N-(4-Amino-benzyl)-benzene-1,3-diamine hydrochloride; N-Benzyl-benzene-1,3-diamine hydrochloride;
3-[(3-Amino-phenylamino)-methyl]-phenol hydrochloride; N-(4-Methoxy-benzyl)-benzene-1,3-diamine hydrochloride; N-Thiophen-2-ylmethyl-benzene-1,3-diamine hydrochloride; 4-Amino-2-[(2-hydroxy-5-nitro-phenylamino)-methyl]-phenol; hydrochloride; 2',4'-Diamino-biphenyl-4-ol hydrochloride; Biphenyl-2,4,4'-triamine; 5-(4-Amino-phenyl)aminomethyl-benzene-1,3-diamine hydrochloride; 2-[4-Amino-2-(3,5-diamino-benzylamino)-phenoxy]-ethanol hydrochloride;
5-Allylaminomethyl-benzene-1,3-diamine hydrochloride; 5-(3-Amino-phenyl)aminomethyl-benzene- 1,3-diamine hydrochloride; N-(4-Amino-benzyl)-benzene-1,3-diamine hydrochloride;
N-Benzyl-benzene-1,3-diamine hydrochloride; 3-[(3-Amino-phenylamino)-methyl]-phenol hydrochloride; N-(2-Amino-benzyl)-benzene-1,3-diamine hydrochloride; N-(4-Methoxy-benzyl)-benzene- 1,3-diamine hydrochloride; N-Furan-2-ylmethyl-benzene-1,3-diamine hydrochloride; 2-[(3-Amino-phenylamino)-methyl]-phenol hydrochloride; N-Thiophen-2-ylmethyl-benzene-1,3-diamine hydrochloride; N-Benzo[1,3]dioxol-5-ylmethyl-benzene-1,3-diamine hydrochloride; N-[4-Amino-2-(2-hydroxy-ethyl)-2H-pyrazol-3 -yl]-3-(5-amino-2-hydroxy-phenyl)-acrylamide hydrochloride; 4-Amino-2-propylaminomethyl-phenol; hydrochloride; 4-Amino-2-(isopropylamino-methyl)-phenol hydrochloride; 4-Amino-2-[(2-hydroxy-5-nitro-phenylamino)-methyl]-phenol hydrochloride; 2-Methyl-5-[(1-H-pyrrol-2-ylmethyl)-amino]-phenol; 5-[(Furan-2-ylmethyl)-amino]-2-methyl-phenol; 5-Isopropylamino-2-methyl-phenol; 5-Cyclobutylamino-2-methyl-phenol; 4-Amino-2-(pyridin-3-ylaminomethyl)-phenol; and 5-Cyclobutylamino-2-methyl-phenol.
The following compounds are especially suitable as developer compounds: 1,4-diamino-2,6-dimethylbenzene, 1,4-diamino-2-methoxymethylbenzene,1,4-diamino-2,5-dimethylbenzene, 1,4-diamino-2,3-dimethylbenzene, 2-chloro-1,4-diaminobenzene, 4-phenylaminoaniline, 4-dimethylaminoaniline, 4-diethylamino-aniline, 4-[di(2-hydroxyethyl)amino]aniline, 4-[(2-methoxyethyl)amino]-aniline, 4-[(3-hydroxypropyl)amino]aniline, 1,4-diamino-2-(2-hydroxyethyl)benzene, 1,4-diamino-2-(1-methylethyl)benzene, 1,3-bis-[(4-aminophenyl)-(2-hydroxyethyl)amino]-2-propanol, 1,8-bis-(2,5-diaminophenoxy)-3,6-dioxaoctane, aminophenol, 4-amino-3-methylphenol, 4-methyl-aminophenol, 4-amino-2-(aminomethyl)phenol, 4-amino-2-[(2-hydroxyethyl)amino]-methylphenol, 4-amino-2-(methoxymethyl)phenol, 4-amino-2-(2-hydroxyethyl)phenol, 5-amino-salicylic acid, 2,5-diaminopyridine, 2,4,5,6-tetraamino-pyrimidine, 2,5,6-triamino-4-(1H)-pyrimidone, 4,5-diamino-1-(2-hydroxyethyl)-1H-pyrazole, 4,5-diamino-l-(1-methylethyl)-1H-pyrazole, 4,5-diamino-l-[(4-methylphenyl)-methyl]-1H-pyrazole, 1-[(4-chlorophenyl)methyl]-4,5-diamino-lH-pyrazole, 4,5-diamino-l-methyl-lH-pyrazole, 4,5-diamino-3-methyl-l-phenyl-lH-pyrazole, 4,5-diamino-1-(2-hydroxyethyl)-3-methyl-lH-pyrazole, 2-amino-phenol and 2-amino-6-methylphenol, or their salts.

To produce special shades it is advantageous to use the 3-amino-2,6-dimethylphenol ot its salts in combination with additional coupler substances, such as phenols, resorcinol and naphthol derivatives such as: naphthalene- 1,7-diol, benzene- 1,3-diol, 4-chlorobenzene-1,3-diol, naphthalen-l-ol, 2-methyl-naphthalen-l-ol, naphthalene-1,5-diol, naphthalene-2,7-diol, benzene-1,4-diol, 2-methyl-benzene-1,3-diol, 7-amino-4-hydroxy-naphthalene-2-sulfonic acid, 2-isopropyl-5-methylphenol, 1,2,3,4-tetrahydro-naphthalene-1,5-diol, 2-chloro-benzene-1,3-diol, 4-hydroxy-naphthalene-l-sulfonic acid, benzene- 1,2,3-triol,naphthalene-2,3-diol, 5-dichloro-2-methylbenzene-1,3-diol, 4,6-dichlorobenzene-1,3-diol, 2,3-dihydroxy-[1,4]naphthoquinone; and 1-Acetoxy-2-methylnaphthalene; m-phenylenediamines such as: 2,4-diaminophenol, benzene-1,3-diamine, 2-(2,4-diamino-phenoxy)-ethanol, 2-[(3-amino-phenyl)-(2-hydroxy-ethyl)-amino]-ethanol, 2-mehyl-benzene-1,3-diamine, 2-[[2-(2,4-diamino-phenoxy)-ethyl]-(2-hydroxy-ethyl)-amino]-ethanol, 4-{3-[(2,4-diaminophenyl)oxy]-propoxy}benzene-1,3-diamine, 2-(2,4-diamino-phenyl)-ethanol, 2-(3-amino-4-methoxy-phenylamino)-ethanol, 4-(2-amino-ethoxy)-benzene-1,3-diamine, (2,4-diamino-phenoxy)-acetic acid, 2-[2,4-diamino-5-(2-hydroxy-ethoxy)-phenoxy]-ethanol, 4-ethoxy-6-methyl-benzene-1,3-diamine, 2-(2,4-diamino-5-methyl-phenoxy)-ethanol, 4,6-dimethoxy-benzene-1,3-diamine, 2-[3-(2-hydroxy-ethylamino)-2-methyl-phenylamino]-ethanol, 3-(2,4-diamino-phenoxy)-propan-l-ol, N-[3-(dimethylamino)phenyl]urea, 4-methoxy-6-methylbenzene-1,3-diamine, 4-fluoro-6-methylbenzene-1,3-diamine, 2-({3-[(2-hydroxyethyl)amino]-4,6-dimethoxyphenyl}-amino)ethanol, 3-(2,4-diaminophenoxy)-propane-1,2-diol, 2-[2-amino-4-(methylamino)-phenoxy]ethanol, 2-[(5-amino-2-ethoxy-phenyl)-(2-hydroxy-ethyl)-amino]-ethanol, 2-[(3-aminophenyl)amino]ethanol, 2,4-Diamino-5-(2'-hydroxyethyloxy)toluene; N,N-Dimethyl-3-ureidoaniline; N-(2-aminoethyl)benzene-1,3-diamine, 4- {[(2,4-diamino-phenyl)oxy]methoxy}-benzene-1,3-diamine, 1-methyl-2,6-bis(2-hydroxyethylamino)benzene; and 2,4-dimethoxy-benzene-1,3-diamine; m-aminophenols such as:
3-amino-phenol, 2-(3-hydroxy-4-methyl-phenylamino)-acetamide, 2-(3-hydroxy-phenylamino)-acetamide, 5-amino-2-methyl-phenol, 5-(2-hydroxyethylamino)-2-methyl-phenol, 5-amino-2,4-dichloro-phenol, 3-amino-2-methyl-phenol, 3-amino-2-chloro-6-methyl-phenol, 5-amino-2-(2-hydroxy-ethoxy)-phenol, 2-chloro-5-(2,2,2-trifluoro-ethylamino)-phenol, 5-amino-4-chloro-2-methyl-phenol, 3-cyclopentylamino-phenol, 5-[(2-hydroxyethyl)amino]-4-methoxy-methylphenol, 5-amino-4-methoxy-2-methylphenol, 3-(dimethylamino)phenol, 3-(diethylamino)phenol, 5-amino-4-fluoro-2-methylphenol, 5-amino-4-ethoxy-2-methylphenol, 3-amino-2,4-dichloro-phenol, 3-[(2-methoxyethyl)amino]phenol, 3-[(2-hydroxyethyl)amino]phenol, 5-amino-2-ethyl-phenol, 5-amino-2-methoxyphenol, 5-[(3-hydroxy-propyl)amino]-2-methylphenol, 3-[(3-hydroxy-2-methylphenyl)-amino]propane-1,2-diol, 3-[(2-hydroxyethyl)amino]-2-methylphenol; 1-Methyl-2-hydroxy-4-(2'-hydroxyethyl)amino-benzene;
1,3-Bis-(2,4-Diaminophenoxy)propane; 1-Hydroxy-2-methyl-5-amino-6-chlorobenzene; and heterocyclic derivatives such as: 3,4-dihydro-2H-1,4-benzoxazin-6-ol, 4-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one, 6-methoxyquinolin-8-amine, 4-methylpyridine-2,6-diol, 2,3-dihydro-1,4-benzodioxin-5-ol, 1,3-benzodioxol-5-ol, 2-(1,3-benzodioxol-5-ylamino)ethanol, 3,4-dimethylpyridine-2,6-diol, 5-chloropyridine-2,3-diol, 2,6-dimethoxypyridine-3,5-diamine, 1,3-benzodioxol-5-amine, 2-{[3,5-diamino-6-(2-hydroxy-ethoxy)-pyridin-2-yl]oxy}-ethanol, 1H-indol-4-ol, 5-amino-2,6-dimethoxypyridin-3-ol, 1H-indole-5,6-diol, IH-indol-7-ol, IH-indol-5-ol, 1H-indol-6-ol, 6-bromo-1,3-benzodioxol-5-ol, 2-aminopyridin-3-ol, pyridine-2,6-diamine, 3-[(3,5-diaminopyridin-2-yl)oxy]propane-1,2-diol, 5-[(3,5-diaminopyridin-2-yl)oxy]pentane-1,3-diol, 1H-indole-2,3-dione, indoline-5,6-diol, 3,5-dimethoxypyridine-2,6-diamine, 6-methoxypyridine-2,3-diamine; 3,4-dihydro-2H-1,4-benzoxazin-6-amine; 4-hydroxy-N-methylindole, 1H-5-methylpyrazol-5-one, 1-phenyl-3-methylpyrazol-5-one, 2,6-dimethylpyrazolo[1,5-b]-1,2,4-triazole, 2,6-dimethyl[3,2-c]-1,2,4-triazole, 6-methylpyrazolo-[1,5-a]benzimidazole, 2,6-dihydroxypyridine, 2,6-dihydroxy-3,4-dimethylpyridine, 5-methylpyrazolo[5,1-e]-1,2,3-triazole, 5-methyl-6-chloropyrazolo[5,1-e]-1,2,3,-triazole, 5-phenylpyrazolo[5,1-e]-1,2,3-triazole and its addition salts, 1H-2,6-dimethylpyrazolo[1,5-b]-1,2,4-triazole tosylate, 7,8-dicyano-4-methylimidazolo-[3,2-a]imidazole, 2,7-dimethylpyrazolo[1,5-a]pyrimidin-5-one, 2,5-dimethylpyrazolo[1,5-a]pyrimidin-7-one, and 2-methyl-5-methoxymethyl-pyrazolo[1,5-a]pyrimidin-7-one; 6-Hydroxybenzomorpholine; and 3-Amino-2-methylamino-6-methoxypyridine; 1-Phenyl-3-methyl-5-pyrazolone-2,4-dihydro-5,2-phenyl-3H-pyrazole-3-one, 2-amino-5-ethyl-phenol and 2-amino-5-methyl-phenol.
Preferred coupler substances include: N-(3-dimethylaminophenyl)urea, 2,6-diaminopyridine, 2-amino-4-[(2-hydroxyethyl)amino]anisole, 2,4-diamino-l-fluoro-5-methylbenzene, 2,4-diamino-l-methoxy-5-methylbenzene, 2,4-diamino-l-ethoxy-5-methylbenzene, 2,4-diamino-1-(2-hydroxyethoxy)-5-methylbenzene, 2,4-di-[(2-hydroxyethyl)amino]-1,5-dimethoxybenzene, 2,3-diamino-6-methoxypyridine, 3-amino-6-methoxy-2-(methylamino)-pyridine, 2,6-diamino-3,5-dimethoxypyridine, 3,5-diamino-2,6-dimethoxypyridine, 1,3-diaminobenzene, 2,4-diamino-1-(2-hydroxyethoxy)benzene, 2,4-diamino-l-(3-hydroxypropoxy)benzene, 1-(2-aminoethoxy)-2,4-diaminobenzene, 2-amiono-l-(2-hydroxyethoxy)-4-methylaminobenzene, 2,4-diaminophenoxyacetic acid, 3-[di(2-hydroxyethyl)-amino]aniline, 4-amino-2-di[(2-hydroxyethyl)amino]-1-ethoxybenzene, 5-methyl-2-(1-methylethyl)phenol, 3-[(2-hydroxyethyl)amino]aniline, 3-[(2-aminoethyl)amino]aniline, 1,3-di(2,4-diaminophenoxy)propane, di-(2,4-diaminophenoxy)methane, 1,3-diamino-2,4-dimethoxybenzene, 2,6-bis-(2-hydroxyethyl)aminotoluene, 4-hydroxyindol, 3-dimethylaminophenol, 3-diethylaminophenol, 5-amino-2-methylphenol, 5-amino-4-fluoro-2-methylphenol, 5-amino-4-methoxy-2-methylphenol, 5-amino-4-ethoxy-2-methylphenol, 3-amino-2,4-dichlorophenol, 5-amino-2,4-dichlorophenol, 3-amino-2-methylphenol, 3-amino-2-chloro-6-methyl-phenol, 3-amino-phenol, 2-[(3-hydroxyphenyl)amino]acetamide, 5-[(2-hydroxyethyl)amino]-2-methylphenol, 3-[(2-hydroxyethyl)amino]-phenol, 3-[(2-methoxy-ethyl)amino]-phenol, 5-amino-2-ethylphenol, 2-amino-5-ethyl-phenol, 2-(4-amino-hydroxyphenoxy)-ethanol, 5-[(3-hydroxypropyl)amino]-2-methylphenol, 3-[(2,3-dihydroxypropyl)-amino]-2-methyl-phenol, 3-[(2-hydroxyethyl)amino]-2-methylphenol, 2-amino-3-hydroxypyridine, 5-amino-4-chloro-2-methylphenol, 1-naphthol, 1,5-dihydroxy-naphthalene, 1,7-dihydroxy-naphthalene, 2,3-dihydroxynaphthalene, 2,7-dihydroxynaphthalene, 2-methyl-l-naphthol acetate, 1,3-dihydroxy-benzene, 1-chloro-2,4-dihydroxybenzene, 2-chloro-1,3-dihydroxybenzene, 1,2-dichloro-3,5-dihydroxy-4-methylbenzene, 1,5-dichloro-2,4-dihydroxybenzene, 1,3-dihydroxy-2-methylbenzene, 3,4-methylenedioxyphenol, 3,4-methylenedioxy-aniline, 5-[(2-hydroxyethyl)amino]-1,3-benzodioxole, 6-bromo-l-hydroxy-3,4-methylendioxybenzene, 3,4-diaminobenzoic acid, 3,4-dihydro-6-hydroxy-1,4(2H)-benzoxazine, 6-amino-3,4-dihydro-1,4(2H)-benzoxazine, 3-methyl-l-phenyl-5-pyrazolone, 5,6-dihydroxyindole, 5,6-dihydroxyindoline, 5-hydroxy-indole, 6-hydroxyindole, 7-hydroxy-indole and 2,3-indolindione, or their salts.

The hair dye compositions of the present invention will generally comprise from about 0.001 /a to about 15% by weight of dye precursors. For example compositions providing low intensity dyeing such as natural blond to light brown hair shades generally comprise from about 0.001% to about 7% by weight, preferably from about 0.1% to about 5% by weight, more preferably from about 0.2% to about 2% by weight of dyeing composition of precursors and couplers. Darker shades such as browns and black typically comprise from 0.001% to about 15% by weight, preferably from about 0.05% to about 10% by weight, more preferably form about 1% to about 5% by weight of precursors and couplers.
The developer substances and coupler substances are generally used in approximately equimolar amounts; however, it is not disadvantageous if the developer substances are present in this regard in a certain excess or deficit, for example a coupler:developer ratio of 1:3 to 1:0.3.
The hair colouring compositions of the present invention are preferably hair colouring compositions which comprise oxidative dyeing compositions. Such compositions comprise oxidative hair dye precursors (also known as primary intermediates) that will deliver a variety of hair colors to the hair. These small molecules are activated by the oxidizing agent and react with further molecules to form a larger colored complex in the hair shaft. The precursors may be used alone or in combination with other precursors, and one or more may be used in combination with one or more couplers. Couplers (also known as color modifiers or secondary intermediates) are generally colorless molecules that can form colors in the presence of activated precursors, and are used with other precursors or couplers to generate specific color effects or to stabilize the color.
The choice of precursors and couplers will be determined by the color, shade and intensity of coloration that is desired. The precursors and couplers may be used herein, singly or in combination, to provide dyes having a variety of shades ranging from ash blonde to black.

Nevertheless the hair colouring compositions of the present invention comprising at least one compound of formula (I) may also include non-oxidative hair dyes (i.e. direct dyes) which may be used alone or in combination with the above described oxidative dyes.
Suitable direct dyes include: direct-dyeing anionic, cationic or non-ionic dye compounds.
The following are preferred examples of anionic direct-dyeing dye compounds for use in the compositions of the invention: 6-hydroxy-5-[(4-sulfophenyl)azo]-2-naphthalene sulfonic acid disodium salt (C.I. 15985; Food Yellow No. 3; FD&C Yellow No. 6), 2,4-dinitro-l-naphthol-7-sulfonic acid disodium salt (C.I. 10316; Acid Yellow No. 1; Food Yellow No.
1), 2-(indan-l,3-dion-2-yl)quinoline-x,x-sulfonic acid (mixture of mono- and disolfuonic acid) (C.I.47005;D&C
Yellow No. 10; Food Yellow No. 13, Acid Yellow No. 3), 5-hydroxy-1-(4-sulfophenyl)-4-[(4-sulfophenyl)azo]pyrazole-3-carboxylic acid sodium salt (C.I. 19140; Food Yellow No. 4; Acid Yellow No. 23), 9-(2-carboxyphenyl)-6-hydroxy-3H-xanthen-3-one (C.I.45350;
Acid Yellow No. 73; D&C Yellow No. 8), 5-[(2,4-dinitrophenyl)amino]-2-phenylaminobenzenesulfonic acid sodium salt (C.1.10385; Acid Orange No. 3), 4-[(2,4-dihydroxyphenyl)azo]-benzene sulfonic acid monosodium salt (C.I.14270; Acid Orange No. 6), 4-[(2-hydroxynaphth-l-yl)azo]benzenesulfonic acid sodium salt (C.I. 15510; Acid Orange No. 7), 4-[(2,4-dihydroxy-3-[(2,4-dimethylphenyl)azo]phenyl)azo]-benzene sulfonic acid sodium salt (C.I.20170; Acid Orange No. 24), 4-hydroxy-3-[(4-sulfonaphth-l-yl)azo]-1-naphthalene sulfonic acid disodium salt (C.I. 14720; Acid Red No. 14), 6-hydroxy-5-[(4-sulfonaphth-l-yl)azo]-2,4-naphthalene-disulfonic acid trisodium salt (C.I. 16255; Ponceau 4R; Acid Red No. 18), 3-hydroxy-4-[(4-sulfonaphth-l-yl)azo]-2,7-naphthalene-disulfonic acid trisodium salt (C.I.
16185; Acid Red No.
27), 8-amino-l-hydroxy-2-(phenylazo)-3,6-naphthalene disulfonic acid disodium salt (C.I.17200;
Acid Red No. 33), 5-(acetylamino)-4-hydroxy-3-[(2-methylphenyl)azo]-2,7-naphthalene disulfonic acid disodium salt (C.I.18065; Acid Red No. 35), 2-(3-hydroxy-2,4,5,7-tetraiodo-dibenzopyran-6-on-9-yl)-benzene sulfonic acid disodium salt (C.I. 45430; Acid Red No. 51), N-[6-(diethylamino)-9-(2,4-disulfophenyl)-3H-xanthen-3-yliden]-N-ethylethanaminium hydroxide, inner Salt, sodium salt (C.1.45100; Acid Red No. 52), 8-[(4-(phenylazo)phenyl)azo]-7-naphthol-1,3-disulfonic acid disodium salt (C.I. 27290; Acid Red No. 73), 2',4',5',7'-tetrabromo-3',6'-dihydroxyspiro[isobenzofuran-l-(3H),9'-[9H]xanthen]-3-one disodium salt (C.1.45380; Acid Red No. 87), 2',4',5',7'-tetrabromo-4,5,6,7-tetrachloro-3',6'-dihydroxyspiro[isobenzofuran-1(3H),9'[9H]xanthen]-3-one disodium salt (C.I.
45410; Acid Red No. 92), 3',6'-dihydroxy-4',5'-diiodospiro[isobenzofuran-1(3H),9'(9H)-xanthen)-3-one disodium salt (C.I. 45425; Acid Red No. 95), (2-sulfophenyl)-di-[4-(ethyl-((4-sulfophenyl)methyl)-amino)phenyl]carbenium disodium salt, betaine (C.I. 42090; Acid Blue No.9;
FD&C Blue No.1), 1,4-bis-[(2-sulfo-4-methyl-phenyl)amino]-9,10-anthraquinone disodium salt (C.I. 61570; Acid Green No. 25), bis-[4-(dimethylamino)phenyl]-(3,7-disulfo-2-hydroxynaphth-1-yl)carbenium inner salt, monosodium salt (C.I. 44090; Food Green No. 4; Acid Green No. 50), bis-[4-(diethylamino)phenyl](2,4-disulfophenyl)carbenium inner salt, sodium salt (2:1) (C.I. 42045;
Food Blue No. 3; Acid Blue No. 1), bis[4-(diethylamino)phenyl]-(5-hydroxy-2,4-disulfophenyl)carbenium inner salt, calcium salt (2:1) (C.I. 42051; Acid Blue No. 3), 1-amino-4-(cyclohexylamino)-9,10-anthraquinone-2-sulfonic acid sodium salt (C.I. 62045;
Acid Blue No.
62), 2-(1,3-dihydro-3-oxo-5-sulfo-2H-indol-2-yliden)-2,3-dihydro-3-oxo-lH-indol-5-sulfonic acid disodium salt (C.I. 73015; Acid Blue No. 74), 9-(2-carboxyphenyl)-3-[(2-methylphenyl)-amino] 6-[(2-methyl-4-sulfophenyl)amino]xanthylium inner salt, monosodium salt (C.I. 45190;
Acid Violet No. 9), 1-hydroxy-4-[(4-methyl-2-sulfophenyl)amino]-9,10-anthraquinone sodium salt (C.I. 60730; D&C Violet No. 2; Acid Violet No. 43), bis-[3-nitro-4-[(4-phenylamino)-3-sulfophenylami no]phenyl]-sulfone (C.I. 10410; Acid Brown No. 13), 5-amino-4-hydroxy-6-[(4-nitrophenyl)azo]3-(phenylazo)-2,7-naphthalene disulfonic acid disodium salt (C.1.20470; Acid Black No. 1), 3-hydroxy-4-[(2-hydroxynaphth-1-yl)azo]-7-nitronaphthalenesulfonic acid chromium complex (3:2) (C.I. 15711; Acid Black No. 52), 3-[(2,4-dimethyl-5-sulfophenyl)azo]-4-hydroxy-l-naphthalene-sulfonic acid disodium salt (C.I. 14700; Food Red No.
1; Ponceau SX;
FD&C Red No. 4), 4-(acetylamino)-5-hydroxy-6-[(7-sulfo-4-[(4-sulfophenyl)azo]naphth-1 yl)azo]-1,7-naphthalene disulfonic acid tetrasodium salt (C.I. 28440; Food Black No. 1), 3-hydroxy-4-(3-methyl-5-oxo-l-phenyl-4,5-dihydro-1 H-pyrazole-4-yl-azo)-naphthalene-l-sulfonic acid sodium salt chromium complex (Acid Red No. 195), 6-hydroxy-5-((2-methoxy-5-methyl-4-sulfophenyl)azo)-2-naphthalene sulfonic acid disodium salt (FD&C Red No.40; Red 40; C.I.16035), 3-hydroxy-4-[(4-methyl-2-sulfophenyl)azo]-2-naphthalenecarboxylic acid Disodium salt (Pigment Red 57; C.I.15850) and 4,4'-(4,5,6,7-tetrabromo-l, 1-dioxido-3H-2, 1-benzoxathiol-3-ylidene)bis[2,6-dibromophenol] (Tetrabromophenol Blue).

The following are preferred cationic direct-dyeing dye compounds: 9-(dimethylamino)-benzo[a]phenoxazin-7-ium chloride (C.I. 51175; Basic Blue No. 6), di[4-(diethylamino)phenyl]-[4-(ethylamino)naphthyl]carbenium chloride (C.I. 42595; Basic Blue No. 7), 3,7-di(dimethylamino)phenothiazin-5-ium chloride (C.I. 52015; Basic Blue No.
9), di[4-dimethylamino)phenyl][4(phenylamino)naphthyl]carbenium chloride (C.I. 44045;
Basic Blue No. 26), 2-[(4-(ethyl(2-hydroxyethyl )amino)phenyl )azo]-6-methoxy-3-methylbenzothiazol ium methylsulfate (C.I. 11154; Basic Blue No. 41), 8-amino-2-bromo-5-hydroxy-4-imino-6-[(3-(trimethylammonio)phenyl)amino]-1 (4H)naphthalenone chloride (C.I.56059; Basic Blue No.
99), bis-[4-(dimethylamino)phenyl][4-(methylamino)phenyl]carbenium chloride (C.I. 42535;
Basic Violet No. 1), tris-(4-amino-3-methylphenyl)carbenium chloride (C.I.
42520; Basic Violet No. 2), tris-[4-(dimethylamino)phenyl]carbenium chloride (C.I. 42555; Basic Violet No. 3), 2-[3,6-(diethylamino)dibenzopyranium-9-yl]benzoic acid chloride (C.I. 45170;
Basic Violet No.
10), di(4-aminophenyl)(4-amino-3-methylphenyl)carbenium chloride (C.I. 42510;
Basic Violet No. 14), 1,3-bis[(2,4-diamino-5-methylphenyl)azo]-3-methylbenzene (C.I.
21010;Basic Brown No. 4), 1-[(4-aminophenyl)azo]-7-(trimethylammonio)-2-naphthol chloride (C.I.
12250; Basic Brown No. 16), 1-[(4-amino-2-nitrophenyl)azo]-7-(trimethylammonio)-2-naphthol chloride (C.I.
12251; Basic Brown No.l7), 1-[(4-amino-3-nitrophenyl)azo]-7-(trimethylammonio)-2-naphthol chloride (C.I. 12251; Basic Brown No. 17), 2-[(4-aminophenyl)azo]-1,3-dimethyl-IH-imidazolium chloride (Basic Orange No. 31), 3-[(4-amino-2,5-dimethoxyphenyl)azo]-N,N,N-trimethyl-benzeneaminium chloride (Basic Orange No. 69), 3,7-diamino-2,8-dimethyl-5-phenylphenazinium chloride (C.I. 50240; Basic Red No. 2), 1,4-dimethyl-5-[(4(dimethylamino)phenyl)azo]-1,2,4-triazolium chloride (C.I. 11055; Basic Red No. 22), 2-((4-(Dimethylamino)-phenyl)azo)-1,3-dimethyl-IH-imidazolium chloride (Basic Red No. 51), 2-hydroxy-l-[(2-methoxyphenyl)azo]-7-(trimethylammonio)naphthalene chloride (C.I. 12245;
Basic Red No. 76), 2-[2-((2,4-dimethoxyphenyl)amino)ethenyl]-1,3,3-trimethyl-3H-indol-l-ium-chloride (C.I. 48055; Basic Yellow No. 11), 3-methyl-l-phenyl-4-[(3-(trimethylammonio)phenyl)azo]-pyrazole-5-one chloride (C.I. 12719; Basic Yellow No. 57), 4-Methyl-(phenyl-hydrazonomethyl)-pyridinium-methylsulfate (Basic Yellow No.
87), bis-[4-(diethylamino)phenyl]phenylcarbenium hydrogen sulfate(1:1) (C.I. 42040; Basic Green No. 1), 4-[(2,6-dichlorphenyl)(4-imino-3,5-dimethyl-2,5-cyclohexadien-l-ylidene)methyl]-2,6-dimethyl-benzeneamine phosphate (HC Blue No. 15; Basic Blue No. 77) and N,N-dimethyl-3-{[4-(methylamino)-9,10-dioxo-9,10-dihydro-l-anthracenyl]amino) -N-propyl-l-propanamin.ium bromide (HC Blue No. 16).

To improve the color balance and to produce special shades the following nonionic direct-dyeing dye compounds have proven to be useful in the compositions according to the invention:
1-amino-2-[(2-hydroxyethyl)amino]-5-nitrobenzene (HC Yellow No. 5), 1-(2-hydroxyethoxy)-2-[(2-hydroxyethyl)amino]-5-nitrobenzene (HC Yellow No. 4), 1-[(2-hydroxyethyl)amino]-2-nitrobenzene (HC Yellow No. 2), 2-[(2-hydroxyethyl)amino]-1-methoxy-5-nitrobenzene, 2-nitro-p-phenylenediamine, 4-nitro-p-phenylenediamine, N,N'-bis(2-hydroxyethyl)-2-nitro-p-phenylenediamine, 2-hydroxyethylamino-5-nitroanisole, 3-methylamino-4-nitrophenoxyethanol, 2-nitro-5-glyceryl-methylaniline, N-(2-nitro-4-aminophenyl)-allylamine, 2-amino-3-nitrophenol, 1-(2-hydroxyethoxy)-3-methylamino-4-nitrobenzene, 2,3-(dihydroxy-propoxy)-3-methylamino-4-nitrobenzene, 2-[(2-hydroxyethyl)amino]-5-nitrophenol (HC Yellow No. 11), 3-[(2-aminoethyl)amino]-1-methoxy-4-nitrobenzene hydrochloride (HC Yellow No.9), 1-[(2-ureidoethyl)amino]-4-nitrobenzene, 4-[(2,3-dihydroxypropyl )amino]-3-nitro-l-trifluoromethylbenzene (HC Yellow No. 6), 1-chloro-2,4-bis-[(2-hydroxyethyl)amino]-5-nitrobenzene (HC Yellow No. 10), 4-[(2-hydroxyethyl)amino]-3-nitro-l-methylbenzene, 1-chloro-4-[(2-hydroxyethyl)amino]-3-nitrobenzene (HC Yellow No. 12), 4-[(2-hydroxyethyl)-amino]-3-nitro-l-trifluoromethylbenzene (HC Yellow No. 13), 4-[(2-hydroxyethyl)amino]-3-nitrobenzonitrile (HC Yellow No. 14), 4-[(2-hydroxyethyl)amino]-3-nitrobenzamide (HC Yellow No. 15), 1-amino-4-[(2-hydroxyethyl)amino]-2-nitrobenzene (HC Red No. 7), 2-amino-4,6-dinitrophenol, 2-ethylamino-4,6-dinitrophenol, 4-amino-2-nitrodiphenylamine (HC Red No. 1), 1-amino-4-[di(2-hydroxyethyl)amino]-2-nitrobenzene hydrochloride (HC Red No.
13), 1-amino-5-chloro-4-[(2hydroxyethyl)amino]-2-nitrobenzene, 4-amino-l-[(2-hydroxyethyl)-amino]-2-nitrobenzene (HC Red No. 3), 4-amino-3-nitrophenol, 4-[(2-hydroxyethyl)amino]-3-nitrophenol, 1-[(2-aminoethyl)amino]4-(2-hydroxyethoxy)-2-nitrobenzene (HC
Orange No. 2), 4-(2,3-dihydroxypropoxy)-1-[(2-hydroxyethyl)amino]-2-nitrobenzene (HC Orange No. 3), 1 -amino-5-chloro-4-[(2,3-dihydroxypropyl)amino]-2-nitrobenzene (HC Red No.
10), 5-chloro-1,4-[di(2,3-dihydroxypropyl)amino]-2-nitrobenzene (HC Red No. 11), 2-[(2-hydroxyethyl)-amino]4,6-dinitrophenol, 4-ethylamino-3-nitrobenzoic acid, 2-[(4-amino-2-nitrophenyl)amino]-benzoic acid, 2-chloro-6-methylamino-4-nitrophenol2-chloro-6-[(2-hydroxyethyl)amino]4-nitrophenol, 2-chloro-6-ethylamino-4-nitrophenol, 2-amino-6-chloro-4-nitrophenol, 4-[(3-hydroxypropyl )-amino]-3-nitrophenol, 2,5-diamino-6-nitropyridine, 1,2,3,4-tetrahydro-6-nitrochinoxalin, 7-amino-3,4-dihydro-6-nitro-2H-1,4-benzoxazine (HC Red No.
14),1,4-bis-[(2-hydroxyethyl )-amino]-2-nitrobenzene, 1-(2-hydroxyethyl )ami no-2-nitro-4-[di(2-hydroxyethyl)amino]benzene (HC Blue No. 2), 1-amino-3-methyl-4-[(2-hydroxyethyl)amino]-6-nitrobenzene (HC Violet No. 1), 4-[ethyl-(2-hydroxyethyl)amino]-1-[(2-hydroxyethyl)amino]-2-nitrobenzene hydrochloride (HC Blue No. 12), 4-[di(2-hydroxyethyl)amino]-1-[(2-methoxyethyl )amino] -2-nitrobenzene (HC Blue No. 11), 1-[(2,3-dihydroxy-propyl)amino]4-[methyl-(2-hydroxyethyl)amino]-2-nitrobenzene (HC Blue No. 10), 1-[(2,3-dihydroxypropyl)amino]4-[ethyl-(2-hydroxyethyl)amino]-2-nitrobenzene hydrochloride (HC Blue No. 9), hydroxyethyl-2-nitro-p-toluidine, 1-(3-hydroxypropylamino)-4-[di(2-hydroxyethyl)amino]-2-nitrobenzene (HC
Violet No. 2), 1-methylamino-4-[methyl-(2,3-dihydroxypropyl)amino]-2nitrobenzene (HC Blue No. 6), 3-nitro-p-hydroxyethylaminophenol, 2-((4-amino-2-nitrophenyl)amino)-5-dimethylamino-benzoic acid (HC Blue No. 13), 1,4-Bis[2,3-Dihydroxypropylamino]-9,10-anthracenedione (HC Blue No. 14), 2-nitro-4'-hydroxy-diphenylamine (HC Orange No. 1), 1-[(2-hydroxyethyl)amino]4-methylamino-9,10-anthraquinone (C.I. 61505, Disperse Blue No. 3), 2,2'-[[4-[(4-aminophenyl)azo]phenyl]-imino]-bisethanol (Disperse Black No. 9), 2-[(2-aminoethyl)amino]-9,10-anthraquinone (HC Orange No. 5), 1 -hydroxy-4-[(4-methyl-2-sulfophenyl)amino]-9,10-anthraquinone, 1-[(3-aminopropyl)amino]-4-methylamino-9,10-anthraquinone (HC Blue No. 8), 1,4-diamino-anthraquinone (Disperse Violet No.
1), 1-[(3-aminopropyl)amino]-9,10-anthraquinone (HC Red No. 8), 1,4-diamino-2-methoxy-9,10-anthraquinone (C.I.62015, disperse Red No. 11, Solvent Violet No. 26), 1,4-dihydroxy-5,8-bis[(2-hydroxyethyl)amino-9,10-anthraquinone (C.I. 62500, disperse Blue No. 7, Solvent Blue No. 69), 1-[di-(2-hydroxyethyl)amino]-3-methyl-4-[(4-nitrophenyl)azo]benzene (C.I. 11210, disperse Red No. 17), 4-amino-2-nitrophenylamine-2'-carboxylic acid, 4-[(4-aminophenyl)azo]-1-[di(2-hydroxyethyl)amino]-3-methylbenzene (HC Yellow No. 7), 2,6-diamino-3-[(pyridine-3-yl)azo]pyridine, hydroxyanthraquinone-aminopropylmethyl-morpholinium-methosulfate, 2,5-dihydroxy-3-methoxy-6-methyl-1,4-benzoquinone, 2-((4-(acetylamino)phenyl)-azo)-methylphenol (C.I. 11855; disperse Yellow No. 3), 2-hydroxy-1,4-naphthoquinone (Lawsone), 4-nitrophenyl-aminoethylurea, picramic acid, 2-hydroxyethyl-picramic acid, 1,4-di((2-hydroxyethyl)amino)-9,10-anthracendione, 1,4-di((3-hydroxypropyl)amino)-9,10-anthracendione and 1-((2-hydroxyethyl)amino)-4-((3-hydroxypropyl)amino)-9,10-anthracendione (Disperse Blue 377; C.I.615061).

The following compounds may also be used as direct-dyeing dye compounds:
natural dyes like Indigofera Tinctoria and Henna (Lawsonia lnermis) or nitrophenols like 2-amino-4,6-dinitrophenol, 2-ethylamino-4,6-dinitrophenol, 2-[(2-hydroxyethyl)-amino]4,6-dinitrophenol and dye compounds of the following general formula (VII):
H
CI NHR

NO2 formula (VII) wherein R represents hydrogen, methyl, ethyl or hydroxyethyl.

The hair dye compositions of the present invention will generally comprise from about 0.001% to about 10% by weight of direct dyes, preferably from about 0.1 % to about 5% by weight, more preferably from about 0.2% to about 2% by weight.
The composition of the present invention comprising at least one compound of formula (I) and optionally additional oxidation dye precursor compounds and/or direct-dyeing dye compounds is applied to the fibers to be dyed in a suitable dye-carrying composition.

The present invention also relates to ready-to-apply hair dye mixtures for the oxidative dyeing of hair, which are each made by mixing an oxidation dye precursor composition with an oxidizing agent immediately prior to application. They are characterized by a content of at least one compound of formula (I) as well as additional oxidation dye precursor compounds and/or direct-dyeing dye compounds as needed.
Any oxidizing agent known in the art (including air-oxgen and enzyme-based oxidizing systems) may be utilized in the present invention. Preferred water-soluble oxidizing agents are inorganic peroxygen materials capable of yielding hydrogen peroxide in an aqueous solution. Water-soluble peroxygen oxidizing agents are well known in the art and include hydrogen peroxide, inorganic alkali metal peroxides such as sodium periodate and sodium peroxide and organic peroxides such as urea peroxide, melamine peroxide, and inorganic perhydrate salt bleaching compounds, such as the alkali metal salts of perborates, percarbonates, perphosphates, persilicates, persulphates and the like. These inorganic perhydrate salts may be incorporated as monohydrates, tetrahydrates etc. Alkyl and aryl peroxides, and or peroxidases may also be used.
Mixtures of two or more such oxidizing agents may also be used if desired. The oxidizing agents may be provided in aqueous solution or as a powder which is dissolved prior to use. Preferred for use in the compositions according to the present invention are hydrogen peroxide, percarbonate, persulphates and combinations thereof.

According to the present invention the compositions comprise from 0.1% to about 15% by weight, preferably from 1% to 10% by weight, and most preferably from 2% to 7%
by weight of an oxidizing agent.

Another preferred oxidizing agent for use herein is a source of peroxymonocarbonate ions.
Preferably such a source is formed in situ from a source of hydrogen peroxide and a hydrogen carbonate ion source. Such an oxidizing agent has been found to be particularly effective at a pH
of up to and including 9.5, preferably 7.5 to 9.5 more preferably pH 9.
Moreover, this system is also particularly effective in combination with a source of ammonia or ammonium ions. It has been found that this oxidizing agent can deliver improvements to the desired hair colour results particularly with regard to the delivery of high lift, whilst considerably reducing the odour, skin and scalp irritation and damage to the hair fibres.

Accordingly, any source of these ions may be utilized. Suitable sources for use herein include sodium, potassium, guanidine, arginine, lithium, calcium, magnesium, barium, ammonium salts of carbonate, carbamate and hydrocarbonate ions and mixtures thereof such as sodium carbonate, sodium hydrogen carbonate, potassium carbonate, potassium hydrogen carbonate, guanidine carbonate, guanidine hydrogen carbonate, lithium carbonate, calcium carbonate, magnesium carbonate, barium carbonate, ammonium carbonate, ammonium hydrogen carbonate and mixtures thereof. Percarbonate salts may also be utilized to provide both the source of carbonate ions and oxidizing agent. Preferred sources of carbonate ions, carbamate and hydrocarbonate ions are sodium hydrogen carbonate, potassium hydrogen carbonate, ammonium carbamate, and mixtures thereof.
According to the present invention the compositions comprise from 0.1% to about 15% by weight, preferably from 1% to 10% by weight, and most preferably from 1% to 8%
by weight of a hydrogencarbonate ion and from 0.1% to 10% by weight, preferably from 1% to 7% by weight, and most preferably from 2% to 5% by weight of a source of hydrogen peroxide.
According to the present invention the composition may further optionally comprise at least one source of alkalizing agent, preferably a source of ammonium ions and or ammonia. Any agent known in the art may be used such as alkanolamides for example monoethanolamine, diethanolamine, triethanolamine, monopropanolamine, dipropanolamine, tripropanolamine, 2-amino-2-methyl-1, 3-propanediol, 2-amino-2-methyl-l-propanol, and 2-amino-2-hydroxymethyl-1,3-propanediol and guanidium salts. Particularly, preferred alkalizing agents are those which provide a source of ammonium ions. Any source of ammonium ions is suitable for use herein. Preferred sources include ammonium chloride, ammonium sulphate, ammonium nitrate, ammonium phosphate, ammonium acetate, ammonium carbonate, ammonium hydrogen carbonate, ammonium carbamate, ammonium hydroxide, percarbonate salts, ammonia and mixtures thereof. Particularly preferred are ammonium carbonate, ammonium carbamate, ammonium hydrogen carbonate, ammonia and mixtures thereof. The compositions of the present invention may comprise from 0.1% to 10% by weight, preferably from 0.5% to 5%
by weight, most preferably from 1% to 3% by weight, of an alkalizing agent, preferably ammonium ions.
According to the present invention the compositions may further comprise a source of radical scavenger. As used herein the term radical scavenger refers to a species that can react with a reactive radical, preferably carbonate radicals, to convert the reactive radical by a series of fast reactions to a less reactive species.

Suitable radical scavengers for use herein include compounds according to the general formula (RSI):
R''-Y-C(H)(R3 )-R4 -(C(H)(RS )-Y-R6')n (RSI) wherein Y is NRZ', 0, or S, preferably NR2', n is 0 to 2, and wherein R4' is monovalent or divalent and is selected from: (a) substituted or unsubstituted, straight or branched, alkyl, mono-or polyunsaturated alkyl, heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic systems, (b) substituted or unsubstituted, mono- or polycyclic aliphatic, aryl, or heterocyclic systems, or (c) substituted or unsubstituted, mono-, poly-, or perfluoro alkyl systems; the systems of (a), (b) and (c) comprising from 1 to 12 carbon atoms and 0 to 5 heteroatoms selected from 0, S, N, P, and Si; and wherein R4' may be connected to R3' or RS' to create a 5, 6 or 7-membered ring; and wherein R'', R2', R3', RS', and R6' are monovalent and are selected independently from: (a), (b) and (c) described herein above, or H.
Preferably, R4' is selected from: (a) substituted or unsubstituted, straight or branched, alkyl, heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic systems, (b) substituted or unsubstituted, mono- or polycyclic aliphatic, aryl, or heterocyclic systems, or (c) substituted or unsubstituted, mono-, poly-, or perfluoro alkyl systems; more preferably R4' is selected from (a) substituted or unsubstituted, straight or branched, alkyl, heteroalkyl, aliphatic, or heteroaliphatic systems, (b) substituted or unsubstituted, aryl, or heterocyclic systems, or (c) substituted or unsubstituted, mono-, poly-, or perfluoro alkyl systems; more preferably substituted or unsubstituted, straight or branched, alkyl, or heteroalkyl systems.

Preferably, the R4' systems of (a), (b), and (c), described herein above, comprise from 1 to 8 carbon atoms, preferably from 1 to 6, more preferably from 1 to 4 carbon atoms and from 0 to 3 heteroatoms; preferably from 0 to 2 heteroatoms; most preferably from 0 to I
heteroatoms.
Where the systems contain heteroatoms, preferably they contain 1 heteroatom.
Preferred heteroatoms include 0, S, and N; more preferred are 0, and N; and most preferred is O.
Preferably, R", R2', R3', R5', and R6' are selected independently from any of the systems defined for R4 above, and H.

In alternative embodiments, any of R'', R2', R3', R4', R5', and R6' groups are substituted.
Preferably, the substituent(s) is selected from: (a) the group of C-linked monovalent substituents consisting of: (i) substituted or unsubstituted, straight or branched, alkyl, mono- or poly-unsaturated alkyl, heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic systems, (ii) substituted or unsubstituted, mono- or polycyclic aliphatic, aryl, or heterocyclic systems, or (iii) substituted or unsubstituted, mono-, poly-, or perfluoro alkyl systems; said systems of (i), (ii) and (iii) comprising from I to 10 carbon atoms and 0 to 5 heteroatoms selected from 0, S, N, P, and Si;
(b) the group of S-linked monovalent substituents consisting of SA1, SCN, SO2A', SO3A', SSA', SOA', SO2NA'A2, SNA'AZ, and SONA'A2; (c) the group of 0-linked monovalent substituents consisting of OAI, OCN and ONAlA2; (d) the group of N-linked monovalent substituents consisting ofNA'AZ, (NA'A2A 3 )+, NC, NA'OA2, NA'SA2, NCO, NCS, NOZ, N NA', N=NOA', NA'CN, NA'NA2A3; (e) the group of monovalent substituents consisting of COOAi, CON3, CONA'2, CONA'COA2, C(=NA')NA'A2, CHO, CHS, CN, NC, and X; and (f) the group consisting fluoroalkyl monovalent substituents consisting of mono-, poly-, or per-fluoro alkyl systems comprising from 1 to 12 carbon atoms and 0 to 4 heteroatoms.
For the groups (b) to (e), described above, A', AZ, and A3 are monovalent and are independently selected from: (1) H, (2) substituted or unsubstituted, straight or branched, alkyl, mono- or poly-unsaturated alkyl, heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic systems, (3) substituted or unsubstituted, mono- or polycyclic aliphatic, aryl, or heterocyclic systems, or (4) substituted or unsubstituted, mono-, poly-, or perfluoro alkyl systems; said systems of (2), (3) and (4) comprising from 1 to 10 carbon atoms and 0 to 5 heteroatoms selected from 0, S, N, P, and Si;
and wherein X is a halogen selected from the group consisting of F, Cl, Br, and I.

Preferred substituents for use herein include those having a Hammett Sigma Para (ap) Value from -0.65 to +0.75, preferably from -0.4 to +0.5. Hammett Sigma Values are described in Advanced Organic Chemistry - Reactions, Mechanisms and Structure (Jerry March, 5`h ed.
(2001) at pages 368-375).

Alternative suitable radical scavengers for use herein are compounds according to the general formula (RSII) H
R" R"
5 ~ 1 I /
R4" R
2"
R

(RSII) wherein Rl >, RZ==, R3 , R4,=, and R5 are each independently selected from H, COO-M+, Cl, Br, SO3"M}, NO2, OCH3, OH or a C1 to C10 primary or secondary alkyl and M is either H or alkali metal. Preferably, the above-described radical scavengers have a pKa of more than 8.5 to ensure protonation of the hydroxy goup.

Other suitable radical scavengers for use herein include those selected from group (III) benzylamine, imidazole, di-tert-butylhydroxytoluene, hydroquinone, guanine, pyrazine, piperidine, morpholine, methylmorpholine, 2-methyoxyethylamine, and mixtures thereof.
Preferred radical scavengers according to the present invention are selected from the classes of alkanolamines, amino sugars, amino acids, esters of amino acids and mixtures thereof.
Particularly preferred compounds are: monoethanolamine, 3-amino-l-propanol, 4-amino-l-butanol,5-amino-l-pentanol, 1-amino-2-propanol, 1-amino-2-butanol, 1-amino-2-pentanol, 1-amino-3-pentanol, 1-amino-4-pentanol, 3-amino-2-methylpropan-l-ol, 1-amino-2-methylpropan-2-ol, 3-aminopropane-1,2-diol, glucosamine, N-acetylglucosamine, glycine, arginine, lysine, proline, glutamine, histidine, sarcosine, serine, glutamic acid, tryptophan, and mixtures thereof, and the salts such as the potassium, sodium and ammonium salts thereof and mixtures thereof. Especially preferred compounds are glycine, sarcosine, lysine, serine, 2 methoxyethylamine, glucosamine, glutamic acid, morpholine, piperdine, ethylamine, 3 amino-1-propanol and mixtures thereof.

The radical scavengers according to the present invention preferably have a molecular weight of less than 500, preferably less than 300, more preferably less than 250 in order to facilitate penetration of the radical scavenger into the hair fibre. The compositions of the present invention preferably comprise from 0.1% to 10% by weight, preferably from 1% to 7% by weight of radical scavenger. The radical scavenger is also preferably selected such that it is not an identical species as the alkalizing agent. According to one embodiment of the present invention the radical scavenger may be formed insitu in the hair dyeing compositions prior to application to the hair fibres.

The compositions of the present invention may further comprise additional ingredients which include, but are not limited to, thickeners, solvents, enzymes, surfactants, conditioning agents, carriers, antioxidants or.reducing agents, stabilizers, chelants, perfumes, hair swelling agents and/or polymers. Some of these additional components are detailed hereafter.

Thickeners: The composition of the present invention may optionally further comprise at least about 0.0 1% by weight, especially from 0.05 to 25% by weight, of thickeners.
Thickeners are preferably comprised in amount sufficient to provide the composition with a viscosity of from about 1 Pa.s to 40 Pa.s (1,000 to 40,000 cP) at 26 C in order to provide a composition that can be readily applied to the hair without dripping.
The at least one thickener is chosen, for example, from:
(i) associative thickeners;
(ii) crosslinked acrylic acid homopolymers;
(iii) crosslinked copolymers of (meth)acrylic acid and of (C1-C6)alkyl acrylate;
(iv) nonionic homopolymers and copolymers containing ethylenically unsaturated monomers of ester and amide type;
(v) ammonium acrylate homopolymers and copolymers of ammonium acrylate and of acrylamide;
(vi) polysaccharides;
(vii) C12-C30 fatty alcohols and (viii) particulate or crystalline thickeners.

(i) As used herein, the expression "associative thickener" means an amphiphilic thickener comprising both hydrophilic units and hydrophobic units, for example, at least one C8-C30 fatty chain and at least one hydrophilic unit. Representative associative thickeners that may be used are associative polymers chosen from:
(a) nonionic amphiphilic polymers comprising at least one fatty chain and at least one hydrophilic unit;
(b) anionic amphiphilic polymers comprising at least one hydrophilic unit and at least one fatty-chain unit;
(c) cationic amphiphilic polymers comprising at least one hydrophilic unit and at least one fatty-chain unit; and (d) amphoteric amphiphilic polymers comprising at least one hydrophilic unit and at least one fatty-chain unit;
The nonionic amphiphilic polymers comprising at least one fatty chain and at least one hydrophilic unit may, for example, be chosen from:
(1) celluloses modified with groups comprising at least one fatty chain; for example:
hydroxyethylcelluloses modified with groups comprising at least one fatty chain chosen from alkyl, arylalkyl and alkylaryl groups, and in which the alkyl groups are, for example, C8-C22, such as the product Natrosol Plus Grade 330 CS(C 16 alkyls) sold by the company Aqualon, and the product Bermocoll EHM 100 sold by the company Berol Nobel, and celluloses modified with polyalkylene glycol alkylphenyl ether groups, such as the product Amercell Polymer HM-1500 (polyethylene glycol (15) nonylphenyl ether) sold by the company Amerchol;
(2) hydroxypropyl guars modified with groups comprising at least one fatty chain, such as the product Esaflor HM 22 (C22 alkyl chain) sold by the company Lamberti, and the products Miracare XC95-3 (C14 alkyl chain) and RE205-1 (C20 alkyl chain) sold by the company Rhodia Chimie;
(3) polyether urethanes comprising at least one fatty chain, such as C10-C30 alkyl or alkenyl groups, for instance the products Elfacos T 210 and Elfacos T 212 sold by the company Akzo or the products Aculyn 44 and Aculyn 46 and Aculyn 48 sold by the company Rohm &
Haas;
(4) copolymers of vinylpyrrolidone and of fatty-chain hydrophobic monomers;
examples that may be mentioned include: the products Antaron V216 and Ganex V216 (vinylpyrrolidone/hexadecene copolymer) sold by the company I.S.P., the products Antaron V220 and Ganex V220 (vinylpyrrolidone/eicosene copolymer) sold by the company I.S.P. ;
(5) copolymers of C1-C6 alkyl acrylates or methacrylates and of amphiphilic monomers comprising at least one fatty chain, such as the oxyethylenated methyl methacrylate/stearyl acrylate copolymer sold by the company Goldschmidt under the name Anti1208;

(6) copolymers of hydrophilic acrylates or methacrylates and of hydrophobic monomers comprising at least one fatty chain, such as polyethylene glycol methacrylate/lauryl methacrylate copolymer; and (7) polymers as described in WO 96/40815 comprising at least one hydrophobbic group and at least one hydrophilic group, such as the following polymers according INCI
designation:
Polyether-1, PEG-180/Laureth-50/TMMG Copolymer and PEG-180/Octoxynol-40/TMMG
Copolymer (sold by the company United Catalysts under the name Pure-Thix 1442, Pure-Thix 1450, Pure-Thix HH, Pure-Thix L and Pure-Thix M).
The anionic amphiphilic polymers comprising at least one hydrophilic unit and at least one fatty-chain unit, may, for example, be chosen from those comprising at least one fatty-chain allyl ether unit and at least one hydrophilic unit comprising an ethylenic unsaturated anionic monomeric unit, for example, a vinylcarboxylic acid unit and further, for example, chosen from units derived from acrylic acids, methacrylic acids and mixtures thereof, wherein the fatty-chain allyl ether unit corresponds to the monomer of formula below:
CHZ=C(Rl)CH2OBõR (I) in which R1 is chosen from H and CH3, B is an ethyleneoxy radical, n is chosen from zero and integers ranging from 1 to 100, R is chosen from hydrocarbon-based radicals chosen from alkyl, arylalkyl, aryl, alkylaryl and cycloalkyl radicals, comprising from 10 to 30 carbon atoms, and, further, for example, from 10 to 24 carbon atoms and even further, for example, from 12 to 18 carbon atoms.
In one embodiment, a unit of formula (I) is, for example, a unit in which Rl may be H, n may be equal to 10 and R may be a stearyl (C 18) radical.
Anionic amphiphilic polymers of this type are described and prepared, according to an emulsion polymerization process, in patent EP-0 216 479 B2.
In one embodiment, anionic amphiphilic polymers are, for example, polymers formed from 20%
to 60% by weight of acrylic acid and/or of methacrylic acid, from 5% to 60% by weight of lower alkyl (meth)acrylates, from 2% to 50% by weight of fatty-chain allyl ether of formula (I), and from 0% to 1% by weight of a crosslinking agent which is a well-known copolymerizable unsaturated polyethylenic monomer, for example, diallyl phthalate, allyl (meth)acrylate, divinylbenzene, (poly)ethylene glycol dimethacrylate and methylenebisacrylamide.
Examples of such polymers are crosslinked terpolymers of methacrylic acid, of ethyl acrylate and of polyethylene glycol (10 EO) stearyl ether (Steareth- 10), such as those sold by the company Ciba under the names Salcare SC 80 and Salcare SC 90, which are aqueous 30%
emulsions of a crosslinked terpolymer of methacrylic acid, of ethyl acrylate and of steareth-10 allyl ether (40/50/10).
The anionic amphiphilic polymers may further be chosen, for example, from those comprising at least one hydrophilic unit of unsaturated olefinic carboxylic acid type, and at least one hydrophobic unit of the type such as a (C 10-C30) alkyl ester of an unsaturated carboxylic acid. The hydrophilic unit of unsaturated olefinic carboxylic acid type corresponds to, for example, the monomer of formula (II) below:
CH2=CR'-COOH (II) in which R' is chosen from H, CH3, and C2H5, i.e. acrylic acid, methacrylic acid and ethacrylic acid units. And the hydrophobic unit of the type such as a (C 10-C30) alkyl ester of an unsaturated carboxylic acid corresponds to, for example, the monomer of formula (III) below:
CH2=CR' -COORZ (III) in which R' is chosen from H, CH3, and C2H5 (i.e. acrylate, methacrylate and ethacrylate units) and is, for example, chosen from, for example, H (acrylate units) and CH3 (methacrylate units), R2 is chosen from C 10-C30 alkyl radicals, for example, C 12-C22 alkyl radical.
Examples of (C10-C30)alkyl esters of unsaturated carboxylic acids include lauryl acrylate, stearyl acrylate, decyl acrylate, isodecyl acrylate, and dodecyl acrylate, and the corresponding methacrylates, lauryl methacrylate, stearyl methacrylate, decyl methacrylate, isodecyl methacrylate and dodecyl methacrylate.
Anionic amphiphilic polymers of this type are disclosed and prepared, for example, according to U.S. Pat. Nos. 3,915,921 and 4,509,949.
Representative anionic amphiphilic polymers that may be used may further be chosen from polymers formed from a mixture of monomers comprising:
(1) acrylic acid, an ester of formula (IV) below:
CH2=CR'-COOR2 (N) in which R' is chosen from H and CH3, RZ is chosen from C10-C30 alkyl radicals, such as alkyl radicals comprising from 12 to 22 carbon atoms, and a crosslinking agent; such as polymers derived from 95% to 60% by weight of the acrylic acid (hydrophilic unit), 4%
to 40% by weight of C10-C30 alkyl acrylate (hydrophobic unit), and 0% to 6% by weight of crosslinking polymerizable monomer, or polymers derived from 98% to 96% by weight of the acrylic acid (hydrophilic unit), 1% to 4% by weight of C 10-C30 alkyl acrylate (hydrophobic unit) and 0.1 %
to 0.6% by weight of crosslinking polymerizable monomer; or (2) acrylic acid and lauryl methacrylate, such as the polymers formed from 66%
by weight of acrylic acid and 34% by weight of lauryl methacrylate.

The crosslinking agent may be a monomer comprising a group (V) I
CH2=C (V) with at least one other polymerizable group whose unsaturated bonds are not conjugated with respect to one another. Mention may be made, for example, of polyallyl ethers such as polyallylsucrose and polyallyl pentaerythritol.
Among said polymers above mention may be made, for example, of the products sold by the company Noveon under the trade names Pemulen TR 1, Pemulen TR2, Carbopol 1382, and further, for example, Pemulen TRI, and the product sold by the company S.E.P.C. under the name Coatex SX.
Suitable anionic amphiphilic fatty-chain polymers, include for example the methacrylic acid/methyl acrylate/ethoxylated alkyl dimethyl-meta-isopropenylbenzylisocyanate copolymer sold under the name Viscophobe DB 1000 by the company Amerchol.
Further suitable anionic amphiphilic fatty-chain polymers, include polymers having the INCI
designation Acrylates/Ceteth-20 Itaconate Copolymer (sold by the company National Starch under the name Structure 3001) and Acrylates/Steareth-20 Itaconate Copolymer (sold by the company National Starch under the name Structure 2001).
The cationic amphiphilic polymers used are, for example, chosen from quaternized cellulose derivatives and polyacrylates comprising amino side groups.
The quaternized cellulose derivatives are, for example, chosen from;
quaternized celluloses modified with groups comprising at least one fatty chain, such as alkyl, arylalkyl and alkylaryl groups comprising at least 8 carbon atoms, and mixtures thereof, quaternized hydroxyethylcelluloses modified with groups comprising at least one fatty chain, such as alkyl, arylalkyl and alkylaryl groups comprising at least 8 carbon atoms, and mixtures thereof.
Quaternized and non-quaternized polyacrylates comprising amino side groups having for example, hydrophobic groups, such as Steareth 20 (polyoxy-ethylenated(20) stearyl alcohol) and (C10-C30)alkyl PEG-20 itaconate.
The alkyl radicals borne by the above quaternized celluloses and hydroxyethylcelluloses, for example, contain from 8 to 30 carbon atoms. The aryl radicals, for example, are chosen from phenyl, benzyl, naphthyl and anthryl groups.
Examples of quaternized alkylhydroxyethyl-celluloses comprising C8-C30 fatty chains are the products Quatrisoft LM 200, Quatrisoft LM-X 529-18-A, Quatrisoft LM-X 529-18B
(C12 alkyl) and Quatrisoft LM-X 529-8 (C 18 alkyl) sold by the company Amerchol, and the products Crodacel QM, Crodacel QL (C12 alkyl), Crodacel QS (C18 alkyl) sold by the company Croda, Softcat Polymer SL-5, Softcat Polymer SL-30, Softcat Polymer SL-60 and Softcat SL-100 sold by the company Amerchol.
Examples of polyacrylates comprising amino side chains is Structure Plus from the company National Starch.
Among amphoteric amphiphilic polymers comprising at least one hydrophilic unit and at least one fatty-chain unit, mention may be made, for example, of methacrylamidopropyltrimethylammonium chloride/acrylic acid/C10-C30 alkyl methacrylate copolymers, wherein the alkyl radical is, for example, a stearyl radical.
(ii) Among the crosslinked acrylic acid homopolymers that may be mentioned are those crosslinked with an allylic alcohol ether of the sugar series, such as the products sold under the names Carbopol 980, 981, 954, 2984 and 5984 by the company Noveon or the products sold under the names Synthalen M, Synthalen L and Synthalen K by the company 3V
Sigma.
(iii) Crosslinked copolymers of (meth)acrylic acid and of C 1-C6 alkyl acrylate may be chosen from crosslinked copolymers of methacrylic acid and of ethyl acrylate as an aqueous dispersion comprising 38% active material sold, for example, under the name Viscoatex 538C by the company Coatex, and crosslinked copolymers of acrylic acid and of ethyl acrylate as an aqueous dispersion comprising 28% active material sold under the name Aculyn 33 by the company Rohm & Haas. Crosslinked copolymers of methacrylic acid and of ethyl acrylate include an aqueous dispersion comprising 30% active material manufactured and sold under the name Carbopol Aqua SF-1 by the company Noveon.
(iv) Among the nonionic homopolymers or copolymers comprising ethylenically unsaturated monomers of ester and/or amide type, mention may be made of the products sold under the names: Cyanamer P250 by the company Cytec (polyacrylamide); PMMA MBX-8C by the company US Cosmetics (methyl methacrylate/ethylene glycol dimethacrylate copolymer);
Acryloid B66 by the company Rohm & Haas (butyl methacrylate/methyl methacrylate copolymer); BPA 500 by the company Kobo (polymethyl methacrylate).
(v) Ammonium acrylate homopolymers that may be mentioned include the product sold under the name Microsap PAS 5193 by the company Hoechst.
Copolymers of ammonium acrylate and of acrylamide include the product sold under the name Bozepol C Nouveau or the product PAS 5193 sold by the company Hoechst (which are described and prepared in documents FR-2 416 723, U.S. Pat. Nos. 2,798,053 and 2,923,692).
(vi) The polysaccharides are, for example, chosen from glucans, modified and unmodified starches (such as those derived, for example, from cereals, for instance wheat, corn or rice, from vegetables, for instance yellow pea, and tubers, for instance potato or cassaya), amylose, amylopectin, glycogen, dextrans, celluloses and derivatives thereof (methylcelluloses, hydroxyalkylcelluloses, ethyl hydroxyethylcellu loses, and carboxymethylcelluloses), mannans, xylans, lignins, arabans, galactans, galacturonans, chitin, chitosans, glucuronoxylans, arabinoxylans, xyloglucans, glucomannans, pectic acids and pectins, alginic acid and alginates, arabinogalactans, carrageenans, agars, glycosaminoglucans, succinoglucans, gum arabics, gum tragacanths, ghatti gums, karaya gums, carob gums, galactomannans, such as guar gums, and nonionic derivatives thereof (hydroxypropyl guar) and xanthan gums, and mixtures thereof.
For example, suitable polysaccharides are described in "Encyclopedia of Chemical Technology", Kirk-Othmer, Third Edition, 1982, volume 3, pp. 896-900, and volume 15, pp.
439-458, in "Polymers in Nature" by E. A. MacGregor and C. T. Greenwood, published by John Wiley &
Sons, Chapter 6, pp. 240-328,1980, and in "Industrial Gums-Polysaccharides and their Derivatives", edited by Roy L. Whistler, Second Edition, published by Academic Press Inc., the content of these three publications being entirely incorporated by reference.
For example, starches, guar gums and celluloses and derivatives thereof may be used. Suitable starches include for example, of macromolecules in the form of polymers comprising elemental moieties that are anhydroglucose units. The number of these moieties and their assembly make it possible to distinguish between amylose (linear polymer) and amylopectin (branched polymer).
The relative proportions of amylose and of amylopectin, and also their degree of polymerization, may vary as a function of the botanical origin of the starches. The botanical origin of the starch molecules used may be cereals or tubers. Thus, the starches may be, for example, chosen from corn starch, rice starch, cassaya starch, tapioca starch, barley starch, potato starch, wheat starch, sorghum starch and pea starch. Starches are generally in the form of a white powder, which is insoluble in cold water and which has an elementary particle size ranging from 3 to 100 microns.
The starches may optionally be C1-C6 hydroxyalkylated or C1-C6 acylated (such as acetylated).
The starches may also have undergone heat treatments. Distarch phosphates or of compounds rich in distarch phosphate, for instance the products sold under the references Prejel VA-70-T AGGL
(gelatinized hydroxypropylated cassaya distarch phosphate) or Prejel TKl (gelatinized cassaya distarch phosphate) or Prejel 200 (gelatinized acetylated cassaya distarch phosphate) by the company Avebe, or Structure ZEA from National Starch (hydroxypropylated corn distarch phosphate), Structure XL from National Starch (hydroxypropylated starch phosphate) may also be used.
The guar gums may be modified or unmodified. The unmodified guar gums are, for example, the products sold under the name Vidogum GH 175 by the company Unipectine and under the names Meyro-Guar 50 and Jaguar C by the company Meyhall. The modified nonionic guar gums are, for example, modified with C1-C6 hydroxyalkyl groups. Among hydroxyalkyl groups, mention may be made, for example, of hydroxymethyl, hydroxyethyl, hydroxypropyl and hydroxybutyl groups.
These guar gums are well known in the state of the art and may be prepared, for example, by reacting corresponding alkene oxides, such aspropylene oxides, with guar gum so as to obtain a guar gum modified with hydroxypropyl groups. The degree of hydroxyalkylation, which corresponds to the number of alkylene oxide molecules consumed by the number of free hydroxyl functions present on the guar gum, may, for example, range from 0.4 to 1.2.
Such nonionic guar gums optionally modified with hydroxyalkyl groups are sold, for example, under the trade names Jaguar HP8, Jaguar HP60 and Jaguar HP 120, Jaguar DC 293 and Jaguar HP 105 by the company Rhodia Chimie (Meyhall) or under the name Galactasol 4H4FD2 by the company Aqualon.
Suitable celluloses include for example, hydroxyethylcellulose and hydroxypropylcelluloses, such as the products sold under the names Klucel EF, Klucel H, Klucel LHF, Klucel MF and Klucel G by the company Aqualon.
(vii) The C12 - C30 fatty alcohols are, for example, chosen from myristyl alcohol, cetyl alcohol, stearyl alcohol, behenyl alcohol or mixture thereof. When fatty alcohols are used as thickeners, at least one additional surfactant with HLB value above about 6 is commonly included to form bi-layers with fatty alcohols. The most useful bi-layer structures include gel network phase where parallel bi-layers of fatty alcohols are swollen by water forming semi-solid creams, and vesicle dispersions where fatty alcohols bi-layers are curved into approximately spherical uni-lamellar or multi-lamellar aggregates.
(viii) The particulate and crystalline thickeners are for example, clays, fumed silica, microcrystalline cellulose, trihydroxystearin (ThixcinR), ethyleneglycol mono-and di-stearate or mixture thereof. The particulate or crystalline thickeners work via mechanisms well known in the art, for example particle aggregation, "house of card" particle arrangement or crystalline fiber formation.

In addition the dye compositions can be thickend by adding prior to use anionic acrylic polymers as described in WO 0 1/97772, which are sold by Arch Personal Care Products, South Plainfield, USA under the tradename ViscUp EZ.

Conditioning agent: The compositions of the present invention may comprise or are used in combination with a composition comprising a conditioning agent in an amount of at least about 0.0 1% by weight, especially from 0.1 % to 10% by weight. Conditioning agents suitable for use herein are selected from silicone materials, amino silicones, fatty alcohols, polymeric resins, polyol carboxylic acid esters, cationic polymers, cationic surfactants, insoluble oils and oil derived materials and mixtures thereof. Additional materials include mineral oils and other oils such as glycerin and sorbitol.
The conditioning agent will generally be used at levels of from about 0.05% to about 20% by weight of the composition, preferably of from about 0.1 % to about 15% by weight, more preferably of from about 0.2% to about 10% by weight, even more preferably of from about 0.2%
to about 2% by weight.
Particularly useful conditioning materials are cationic polymers. Conditioners of cationic polymer type may be chosen from those already know by those skilled in the art as improving at least one cosmetic properties of keratin fibres treated with a cosmetic composition.
Cationic polymers may be chosen from those comprising units of at least one amine group chosen from primary, secondary, tertiary and quaternary amine groups that may either form part of the main polymer chain, or be borne by a side substituant that is directly attached to the main polymer chain. Such cationic polymers generally have a number average molecular mass ranging from 500 to 5,000,000, or more preferably from 1000 to 3,000,000. Polymers of the polyamine, polyamino amide and polyquaternary ammonium type that may be used include but are not limited to:
(1) homopolymers and copolymers derived from acrylic or methacrylic esters or amides.
Copolymers of these polymers may also comprise at least one unit derived from comonomers which may be chosen from the family of acrylamides, methacrylamides, diacetone acylamides, acrylamides and methacrylicamides substituted on the nitrogen with at least one group chosen from lower (C1-C4) alkyls, acrylic and methacrylic acids and esters thereof, vinlylactams such as vinlypyrrolidone and vinylcaprolactam, and vinyl esters. Examples of such polymers include:
Copolymers of acrylamide and of methacryloyloxyethyltrimethylammonium methosulfate, examples of which include polymers known via the INCI nomenclature as Polquaternium-5, such as the products sold under the names Reten 210, Reten 220, Reten 230, Reten 240, Reten 1104, Reten 1105, Reten 1006 by the company Hercules and Merquat 5, Merquat 5 SF by the company Nalco.
Copolymers of vinylpyrrolidone and dimethylaminopropyl methacrylamide, examples of which include polymers known via the INCI nomenclature as Polyquaternium-28, such as the products sold under the name Gafquat HS- 100 by the company International Speciality Products (ISP).
Copolymers of vinyl pyrrolidone and dialkyaminoalkyl acrylates or methactylates, examples of which include polymers known via the INCI nomenclature as Polquaternium-11, such as the products sold under the name Gafquat 440, Gafquat 734, Gafquat 755, Gafquat 755N by the company International Speciality Products (ISP), and Luviquat PQ11 PM by the company BASF
and Polyquat-11 SL by the company Sino Lion.
Copolymers vinylpyrrolidone, dimethylaminopropyl methacrylamide and methacryloylaminopropyl lauryldimonium chloride, examples of which include polymers known via the INCI nomenclature as polyquatemium-55, such as the products sold under the name Styleze W-20 by the company International Speciality Products (ISP).
Copolymers of acrylic acid, acrylamide and methacrylamidopropyltrimonium chloride, examples of which include polymers known via the INCI nomenclature as Polyquaternium-53, such as the products sold under the name Merquat 2003 by the company Nalco.
Copolymers of dimethyaminopropylacrylate (DMAPA), acrylic acid and acrylonitrogens and diethyl sulfate, examples of which include polymers known via the INCI
nomenclature as Polyquaternium-31, such as the products sold under the name Hypan QT 100 by the company Lipo.
Copolymers of acrylamide, acrylamidopropyltrimonium chloride, 2-amidopropylacrylamide sulfonate, and dimethyaminopropylacrylate (DMAPA), examples of which include polymers known via the INCI nomenclature as polyquaternium-43, such as the products sold under the name Bozequat 4000 by the company Clairant.
Copolymers of acrylic acid, methylacrylate and methacrylamidopropyltrimonium chloride, examples of which include polymers known via the INCI nomenclature as Polyquaternium-47, such as the products sold under the name Merquat 2001 and Merquat 2001N sold commercially by Nalco.
Copolymes of methacryloyl ethyl betaine, 2-hydroxyethyl methacrylate and methacryloyl ethyl trimethyl ammonium chloride, examples of which include polymers known via the INCI
nomenclature as Polyquaternium-48, such as the products sold under the name Plascize L-450 by the company Goo Chemcial.
Copolymers of acrylic acid diallyl dimethyl ammonium chloride and acrylamide, examples of which include polymers known via the INCI nomenclature as polyquaternium 39, such as the products sold under the name Merquat 3330 and Merquat 3331 by the company Nalco.
Further examples include copolymers of methacrylamide methacrylamido-propyltrimonium and methacryloylethyltrimethyl ammonium chloride and their derivatives, either homo or copolymerised with other monomers, examples of which include polymers known via the INCI
nomenclature as: Polyquaternium-8, Polyquatemium-9, Polyquaternium-12, Polyquaternium-13 Polyquaternium-14, Polyquaternium-15, such as the products sold under the name Rohagit KF
720 F by the company Rohm, Polyquatemium-30, such as the products sold under the name Mexomere PX by the company Chimex, Polyquaternium-33, Polyquatemium-35, Polyquaternium-36, such as the products sold under the name Plex 3074 L by the company Rhon, Polyquaternium 45, such as the products sold under the name Plex 3073L
by the company Rohn, Polyquaternium 49, such as the products sold under the name Plascize L-440 by the company Goo Chemicals, Polyquaternium 50 such as the products sold under the name Plascize L-441 by the company Goo Chemicals, Polyquatemium-52.
(2) Cationic polysaccharides, such as cationic celluloses and cationic galactomannan gums.
Among the cationic polysaccharides that maybe mentioned, for example, are cellulose ether derivatives comprising quaternary ammonium groups and cationic cellulose copolymers or cellulose derivatives grafted with a water-soluble quaternary ammonium monomer and cationic galactomannan gums. Examples include but are not limited to:
Copolymers of hydroxyethylcelluloses and diallyldimethyl ammonium chlorides, examples of which include polymers known via the INCI nomenclature as Polyquaternium-4, such as the products sold under the name Celquat L 200 and Celquat H 100 by the company National Starch.
Copolymers of hydroxyethylcelluloses and a trimethyl ammonium substituted epoxide, examples of which include polymers known via the INCI nomenclature as Polyquaternium-10, such as the products sold under the name AEC Polyquaternium-10 by the company A&E Connock, Catinal C-100 Catinal HC-35 Catinal HC-100 Catinal HC-200 Catinal LC-100 Catinal LC-200 by the company Toho, Celquat SC-240C Celquat SC-230M, by the company National Starch, Dekaquat 400, Dekaquat 3000 by the company Dekker, Leogard GP by the company Akzo Nobel, RITA Polyquta 400 RITA, Polyquta 3000 by the company RITA, UCARE
Polymer JR-125 UCARE Polymer JR-400 UCARE Polymer JR-30M UCARE Polymer LK UCARE Polymer LR 400 UCARE Polymer LR 30M by the company Amerchol.
Copolymers of hydroxyethylcelluloses and lauryl dimethyl ammonium substituted epoxides, examples of which include polymers known via the INCI nomenclature as Polyquaternium-24, such as the products sold under the name Quatrisoft polymer LM-200 by the company Amerchol.
Derivatives of Hydroxypropyl Guar, examples of which include polymers known via the INCI
nomenclature as Guar Hydroxypropyltrimonium Chloride, such as the products sold under the name Catinal CG-100, Catinal CG-200 by the company Toho, Cosmedia Guar C-261N, Cosmedia Guar C-261N, Cosmedia Guar C-261N by the company Cognis, DiaGum P
5070 by the company Freedom Chemical Diamalt, N-Hance Cationic Guar by the company Hercules/Aqualon, Hi-Care 1000, Jaguar C-17, Jaguar C-2000, Jaguar C-13S, Jaguar C-14S, Jaguar Excel by the company Rhodia, Kiprogum CW, Kiprogum NGK by the company Nippon Starch.
Hydroxypropyl derivatives of Guar Hydroxypropyltrimonium Chloride, examples of which include polymers known via the INCI nomenclature as Hydroxypropyl Guar Hydroxypropyltrimonium Chloride, such as the products sold under the name Jagaur C- 162 by the company Rhodia.
(3) Polyamino amide derivatives resulting from the condensation of polyalkylene polyamines with polycarboxylic acids followed by alkylation with difunctional agents.
Among the derivative, mention may be made for example to adipic acid /
dimethylaminohydroxypropyl /
diethylenetriamine.
(4) Polymers obtained by reaction of a polyalkylene polyamine comprising two primary amines groups and at last one secondary amine group with a decarboxylic acid chosen from diglycolic acids and saturated aliphatic dicarboxylic acids comprising from 3 to 8 carbon atoms. Non-limiting examples of such derivatives include the adipic acid / epxoypropyl /
diethylenetriamine.
(5) Cyclopolymers of dialkdiallylamine or of dialkyldiallyammonium, among which polymers mention may be made of:
Dimethyldiallyammonium chloride polymers, examples of which include polymers known via the INCI nomenclature as Polyquaternium-6, such as the products sold under the name Merquat 100 by the company Nalco, Mirapol 100 by the company Rhodia, Rheocare CC6 by the company Cosmetic Rheologies, AEC polyquaternium-6 by the company A&E Connock, Agequat 400 by the company CPS, Conditioner P6 by the company 3 V Inc., Flocare C 106 by the company SNF, Genamin PDAC by the company Clariant, Mackernium 006 by the company McIntyre.
Copolymers of acrylamides and dimethyldiallylammonium chlorides monomers, examples of 25, which include polymers known via the INCI nomenclature as Polyquatemium-7, such as the products sold under the name AEC Polyquatemium-7 by the company A&E Connock, Agequat-5008, Agequat C-505 by the company CPS, Conditioner P7 by the company 3V Inc.
Flocare C
107 by the company SNF Mackernium 007, Mackernium 007S by the company McIntyre, ME
Polymer 09W by the company Toho, Merquat 550, Merquat 2200, Merquat S by the company Nalco, Mirapo1550 by the company Rhodia, Rheocare CC7, Rheocare CCP7 by the company Cosmetic Rheologies, Salcare HSP-7, Salcare SC 10, Salcare Super 7 by the company Ciba.
Copolymers of dimethyldiallylammoniumchlorides and acrylic acids, examples of which include polymers known via the INCI nomenclature as polyquaternary-22, such as the products sold under the name Merquat 280 and Merquat 295 by the company Nalco.

(6) Quaternary diammonium polymers comprising repeating units of formula [-N+(R')(R2) -AN
' ' (R3)(R4)-B'-] [2X"], in which R', R2, R3 and R4, which may be identical or different, are chosen from aliphatic, alicyclic and arylaliphatic radicals comprising from 1 to 20 carbon atoms and from lower hydroxyalkylaliphatic radicals, or R', R2, R3 and R4, together or separately, constitute, with the nitrogen atoms to which they are attached, heterocycles optionally comprising a second heteroatom other then nitrogen, or R', R2, R3 and R4, are choen from liner or branched C1-C6 alkyl radicals substituted with at least one group chosen from nitrile, ester, acyl and amide groups and groups of -CO-O-R5-D and -CO-NH-R5-D wherein R5 is chosen from alkylene groups and D is chosen from quaternary ammonium groups. A' and B', which may be identical or different, are chosen from linear and branched, saturated or unsaturated polymethylene groups comprising 2 to 20 carbon atoms. The polymethylene groups may comprise, linked to or intercalated in the main ring, at least one entity chosen from aromatic rings, oxygen and sulphur atoms and sulphoxide, sulphone, disulphide, amino, alkylamino, hydroxyl, quaternary, ammonium, ureido, amide and ester groups, and X" is an anion derived from inorganic and organic acids. D is chosen from a glycol residue, a bis-secondary diamine residue, a bis-primary diamine residue or a ureylene group. An examples of which include polymers known via the INCI nomenclature as Hexadimethrine chloride, where R', R2, R3 and R4 are each methyl radicals, A' is (CH2)3 and B' is (CH2)6 and X = Cl. Further examples of which include polymers known via the INCI nomenclature as polyquatemium-34 where R'and R2 are ethyl radicals and R3 and R4 are methyl radicals and A' is (CH2)3 and B' is (CH2)3 and X
= Br, such as the products sold under the name Mexomere PAX by the company Chimax.
(7) Polyquaternary ammonium polymers comprising repeating units of formula [-N+(R6)(R')-(CH2)r-NH-CO-(CH2)q-(CO)t-NH-(CH2)s-N+(Rg)(R9)-A-] [2X-], in which R6, R', R8 and R9 which may be identical or different, are chosen from a hydrogen atom and a methyl, ethyl, propyl, hydroxyethyl, hydroxypropyl, and -CH2CH2(OCH2CH2)pOH
radicals, wherein p is equal to 0 or an integer ranging from 1 to 6, wherein R6, R7, R8 and R9 do not all simultaneously represent a hydrogen atom. R and s which maybe identical or different are each an integer ranging from 1 to 6, q is equal to 0 or an integer ranging from 1 to 34 and X- is an anion such as a halide. T is an integer chosen to be equal to 0 or 1. A is chosen from divalent radicals such as -CH2-CH2-O-CH2-CH2-. Examples of which include Polymers known via the INCI nomenclature as polyquatemium-2, where r=s=3, q=0,t=0, R6, R', R8 and R9 are methyl groups, and A is -CH2-CH2-O-CH2-CH2, such as the products sold under the name Ethpol PQ-2 from Ethox and Mirapol A- 15 by the company Rhodia.

Polymers known via the INCI nomenclature as polyquaternium-17 where 1=s=3, q=4, t=1, R6, R', R8 and R9 are methyl groups, and A is -CH2-CH2-O-CH2-CH2.
Polymers known via the INCI nomenclature as Polyquaternium 18, where r=s=3, q=7, t=1, R6, R', R8 and R9 are methyl groups, and A is -CH2-CH2-O-CH2-CH2 Polymers known via the INCI nomenclature as the block copolymer formed by the reaction of Polyquaternium-2 with Polyquaternium-17, known as Polyquaternium 27, such as the products sold under the name Mirapol 175 by the company Rhodia.

(8) Copolymers of vinylpyrrolidones and of vinylimidazoles and optionally vinylcaprolactums, examples of which include polymers known via the INCI nomenclature as Polyquaternary-16 formed from methylvinylimidazolium chlorides and vinylpyrrolidones, such as the products sold under the name Luviquat FC370, Luviquat FC550, Luviquat FC905, Luviquat HM-552 by the company BASF. Or copolymers of vinylcaprolactams and vinylpyrrolidones with methylvinylimidazolium methosulfates, examples of which include polymers known via the INCI nomenclature as Polyquaternium-46, such as the products sold under the name Luviquat Hold by the company BASF. Or copolymers of vinylpyrrolidones and quaternized imidazolines, examples of which include polymers known via the INCI nomenclature poylquaterary 44, such as the products sold under the name Luviquat Care by the company BASF

(9) Polyamines such as the product Polyquart H sold by Cognis under the reference name polyethylene glycol (15) tallow polyamine in the CTFA dictionary.

(10) Cross linked methacryloyloxy(C1-C4)alkyltri(Cl-C4)alkylammonium salt polymers such as the polymers obtained by homopolymerisation of dimethylaminoethyl methacrylates quaternized with methyl chloride, or by copolymerisation of acrylamides with dimethylaminoethyl methacrylates quatemized with methyl chloride, the homo or copolymerisation being followed by crosslinking with a compound comprising olefinic unsaturation, such as methylenebisacrylamides, examples of which include polymers known via the INCI
nomenclature as Polyquaternium-37, such as the products sold under the name Synthalen, CN
Synthalen CR, Synthalen CU, sold by 3V sigma, or as a dispersion in another media such as the products sold under the name Salcare SC95 and Salcare SC96 by the company Ciba or Rheocare CTH(E) by the company Cosmetic Rheologies. Or in another example of which include polymers known via the INCI nomenclature as Polyquaternium-32, or when sold as a dispersion in mineral oil such as the products sold under the name Salcare SC92 by the company Ciba.

(11) Further examples of cationic polymers include polymers known via the INCI
nomenclature as Polyquaternium 51, such as the products sold under the name Lipidure-PMB by the company NOF, via the INCI nomenclature as Polyquatemium 54, such as the products sold under the name Qualty-Hy by the company Mitsui, and via the INCI nomenclature as Polyquatemium 56 such as the products sold under the name Hairrol UC-4 by the company Sanyo chemicals.

(12) silicone polymers comprising cationic groups and/or groups which may be ionised into cationic groups. For example: cationic silicones of the general formula (R10-N+(CH3)2)-R"-(Si(CH3)2-0)x-R"-(N+(CH3)2)-R'0), where Rl0 is an alkyl derived from coconut oil, and R" is (CH2CHOCH2O(CH2)3 and x is a number between 20 and 2000, examples of which include polymers known by the INCI nomenclature as Quatemium 80, such as the products sold under the name as Abil Quat 3272 and Abil Quat 3474 sold commercially by Goldschmidt.
Silicones containing groups which may be ionised into cationic groups, for example aminosilicones containing at least 10 repeating siloxane -(Si(CH3)2-O) units within the polymer chain, with either terminal, graft or a mixture of terminal and graft aminofunctional groups.
Example functional groups are not limited to aminoethylaminopropyl, aminoethylaminoisobutly, aminopropyl. In the case of graft polymers, the terminal siloxane units may either be (CH3)3Si-0 or RIZ(CH3)2Si-0, where R12 may be either OH or OR13, where R13 is a C1-C8 alky group, or a mixture of both functional terminal groups. These silicones are also available as preformed emulsions. Polymer with terminal siloxane units of (CH3)3Si-O examples of which include polymers known by the 1NCI nomenclature as trimethylsilylamodimethicone, such as the products sold under the name as DC-2-8566, DC 7224 and DC-2-8220 sold commercially by Dow Corning and SF1708 and SM 2125 sold commercially by GE Silicones and Wacker Belsil ADM 653 sold commercially by Wacker silicones. Further examples include polymers with terminal siloxane units of (R12O)(CH3)2Si-O where R12 may be either OH or OR'3, where R13 is a Cl-C8 alky group, or a mixture of both functional terminal groups, known by the INCI
nomenclature as amodimethicone, such as the products sold under the name as Wacker Belsil ADM 1100, Wacker Belsil ADM 1600, Wacker Belsil ADM 652, Wacker Belsil ADM
6057E, Wacker Belsil ADM 8020 sold commercial by Wacker Silicones, DC929, DC939 and sold commercially by Dow Corning and SM2059 sold commercially by GE silicones.
Silicones containing groups which may be ionised into cationic groups - for example silicones containing at least 10 repeating siloxane -(Si(CH3)2-0) units within the polymer chain, with either terminal, graft or a mixture of terminal and graft aminofunctional groups, together with additional functional groups. Additional functional groups may include polyoxyalkylene, the reaction product of amines and carbinols, alky chains. For example products know by the INCI
nomenclature as methoxy PEG/PPG-7/3 Aminopropyl Dimethicone, such as the product sold under the name of Abil Soft AF 100 sold commercially by Degussa. For example products know by the INCI nomenclature as Bis (C 13-15 Alkoxy) PG Amodimethicone, such as the product sold under the name of DC 8500 sold commercially by Dow Coming.

Surfactants: The compositions according to the present invention may further comprise one or more surfactants. Surfactants suitable for use herein generally have a lipophilic chain length of from about 8 to about 30 carbon atoms and may be selected from anionic, nonionic, amphoteric and cationic surfactants and mixtures thereof. The total level of surfactant is from about 0.5% to about 60% by weight, preferably from about 2% to about 30% by weight, more preferably from about 8% to about 25% by weight and especially from about 10% to about 20% by weight.
The compositions of the invention preferably comprise a mixture of anionic and amphoteric surfactants with one or more nonionic surfactants. Anionic components, where may be present in the range of from about 0.1% to about 20% by weight, preferably from about 0.1% to about 15%
by weight, and more preferably from about 5% to about 15% by weight of the composition;
amphoteric or nonionic components, may independently be present is in the range from about 0.1 % to about 15% by weight, preferably from about 0.5% to about 10% by weight, more preferably from about 1% to about 8% by weight.
As examples of anionic surfactants, which may be used, alone or as mixtures, mention may be made, for example, of salts (such as alkaline salts, for example, sodium salts, ammonium salts, amine salts, amino alcohol salts and magnesium salts) of the following compounds: alkyl sulphates, alkyl ether sulphates, alkylamido ether sulphates, alkylarylpolyether sulphates, monoglyceride sulphates; alkyl sulphonates, alkyl phosphates, alkylamide sulphonates, alkylaryl sulphonates, a-olefin sulphonates, paraffin sulphonates; alkyl sulphosuccinates, alkyl ether sulphosuccinates, alkylamide sulphosuccinates; alkyl sulphosuccinamates; alkyl sulphoacetates;
alkyl ether phosphates; acyl sarcosinates; acyl isethionates and N-acyltaurates. The alkyl or acyl radical of all of these various compounds, for example, comprises from 8 to 24 carbon atoms, and the aryl radical, for example, is chosen from phenyl and benzyl groups.
Among the anionic surfactants, which may also be used, mention may also be made of fatty acid salts such as the salts of oleic, ricinoleic, palmitic and stearic acids, coconut oil acid or hydrogenated coconut oil acid; acyl lactylates in which the acyl radical comprises from 8 to 20 carbon atoms. Weakly anionic surfactants may also be used, such as alkyl-D-galactosiduronic acids and their salts, as well as polyoxyalkylenated (C6-C24) alkyl ether carboxylic acids, polyoxyalkylenated (C6-C24) alkylaryl ether carboxylic acids, polyoxyalkylenated (C6-C24) alkylamido ether carboxylic acids and their salts, for example, those comprising from 2 to 50 ethylene oxide groups, and mixtures thereof. Anionic derivatives of polysaccharides, for example carboxyalkyl ether of alkyl polyglucosides, may be also used.
The nonionic surfactants are compounds that are well known (see, for example, in this respect "Handbook of Surfactants" by M. R. Porter, published by Blackie & Son (Glasgow and London), 1991, pp. 116-178). They may be chosen, for example, from polyethoxylated, polypropoxylated and polyglycerolated fatty acids, alkyl phenols, a-diols and alcohols comprising a fatty chain comprising, for example, from 8 to 18 carbon atoms, it being possible for the number of ethylene oxide or propylene oxide groups to range, for example, from 2 to 200 and for the number of glycerol groups to range, for example, from 2 to 30. Mention may also be made of copolymers of ethylene oxide and of propylene oxide, condensates of ethylene oxide and of propylene oxide with fatty alcohols; polyethoxylated fatty amides preferably having from 2 to 30 mol of ethylene oxide and their momoethanolamine and diethanolamine derivatives, polyglycerolated fatty amides, for example, comprising on average from 1 to 5, and such as from 1.5 to 4, glycerol groups; polyethoxylated fatty amines such as those containing from 2 to 30 mol of ethylene oxide; oxyethylenated fatty acid esters of sorbitan having from 2 to 30 mol of ethylene oxide;
fatty acid esters of sucrose, fatty acid esters of polyethylene glycol, alkylpolyglycosides, N-alkylglucamine derivatives, amine oxides such as (Clo-C]4)alkylamine oxides or N-acylaminopropylmorpholine oxides.
The amphoteric surfactants may be chosen, for example, from aliphatic secondary and tertiary amine derivatives in which the aliphatic radical is chosen from linear and branched chains comprising from 8 to 22 carbon atoms and comprising at least one water-soluble anionic group (for example carboxylate, sulphonate, sulphate, phosphate or phosphonate); mention may also be made of (C8-C20)alkylbetaines, sulphobetaines, (Cg-CZo)alkylamido(CI-C6)alkylbetaines or (C8-C2o)alkylamido(C1-C6)alkylsulphobetaines.
Among the amine derivatives, mention may be made of the products sold under the name Miranol, as described, for example, in U.S. Pat. Nos. 2,528,378 and 2,781,354 and having the structures of: RZ-CON HCHZCH2-N+(R3)(R4)(CH2COO-) (VI) in which: R2 is chosen from alkyl radicals derived from an acid R2-COOH
present in hydrolysed coconut oil, and heptyl, nonyl and undecyl radicals, R3 is a(3-hydroxyethyl group and R4 is a carboxymethyl group; and of R5-CONHCHZCHZ-N(B)(C) (VII) wherein B represents -CH2CH2OX', C represents -(CHZ)Z Y', with z=1 or 2, X' is chosen from the -CH2CH2-COOH group and a hydrogen atom, Y' is chosen from -COOH and -CH2-CHOH-SO3H radicals, R5 is chosen from alkyl radicals of an acid RS-COOH
present in coconut oil or in hydrolysed linseed oil, alkyl radicals, such as C7, C9, CII and C13 alkyl radicals, a C 17 alkyl radical and its iso form, and unsaturated C 17 radical.
These compounds are classified in the CTFA dictionary, 5th edition, 1993, under the names disodium cocoamphodiacetate, disodium lauroamphodiacetate, disodium caprylamphodiacetate, disodium capryloamphodiacetate, disodium cocoamphodipropionate, disodium lauroamphodipropionate, disodium caprylamphodipropionate, disodium capryloamphodipropionate, lauroamphodipropionic acid, and cocoamphodipropionic acid. Salts of diethyl aminopropyl cocoaspartamid may be also used.
The cationic surfactants may be chosen from: A) the quaternary ammonium salts of general formula (VIII): [NR'R2R3R4]+ X" (VIII) wherein X- is an anion chosen from halides (chloride, bromide and iodide), (C2-C6)alkyl sulphates, such as methyl sulphate, phosphates, alkyl and alkylaryl sulphonates, and anions derived from organic acids, such as acetate and lactate, and (i) the radicals R' to R3, which may be identical or different, are chosen from linear and branched aliphatic radicals comprising from 1 to 4 carbon atoms, and aromatic radicals such as aryl and alkylaryl. The aliphatic radicals may comprise at least one hetero atom such as oxygen, nitrogen, sulphur and halogens. The aliphatic radicals are chosen, for example, from alkyl, alkoxy and alkylamide radicals, R4 is chosen from linear and branched alkyl radicals comprising from 16 to 30 carbon atoms.
The cationic surfactant is, for example, a behenyltrimethylammonium salt (for example a chloride or bromide).
(ii) the radicals Rl and R2, which may be identical or different, are chosen from linear and branched aliphatic radicals comprising from 1 to 4 carbon atoms, and aromatic radicals such as aryl and alkylaryl. The aliphatic radicals may comprise at least one hetero atom such as oxygen, nitrogen, sulphur and halogens. The aliphatic radicals are chosen, for example, from alkyl, alkoxy, alkylamide and hydroxyalkyl radicals comprising from about 1 to 4 carbon atoms;
R3 and R4, which may be identical or different, are chosen from linear and branched alkyl radicals comprising from 12 to 30 carbon atoms, the said alkyl radicals comprise at least one function chosen from ester and amide functions.
R3 and R4 are chosen, for example, from (C12-C22)alkylamido(CZ-C6)alkyl and (C12-C22)alkylacetate radicals.
The cationic surfactant is, for example, a dicetyldimethyl ammonium salt (for example chloride);
B) the quaternary ammonium salts of imidazolinium, such as that of formula (IX) below:

+
Re CH2-CH2-N(R8)-CO-R5 X
N / N\ /

(IX) in which R5 is chosen from alkenyl and alkyl radicals comprising from 8 to 30 carbon atoms, for example fatty acid derivatives of tallow, R6 is chosen from a hydrogen atom, C1-C4 alkyl radicals and alkenyl and alkyl radicals comprising from 8 to 30 carbon atoms, R7 is chosen from CI -C4 alkyl radicals, R8 is chosen from a hydrogen atom and CI-C4 alkyl radicals, and X- is an anion chosen from halides, phosphates, acetates, lactates, alkyl sulphates, alkyl sulphonates and alkylaryl sulphonates.
In one embodiment, R5 and R6 are, for example, a mixture of radicals chosen from alkenyl and alkyl radicals comprising from 12 to 21 carbon atoms, such as fatty acid derivatives of tallow, R7 is methyl and R8 is hydrogen. Such a product is, for example, Quaternium-27 (CTFA 1997) or Quaternium-83 (CTFA 1997), which are sold under the names "Rewoquat " W75, W90, W75PG and W75HPG by the company Witco, C) the diquaternary ammonium salts of formula (X):

[(R9)(R10)(Rl l)-N-(CH2)3-N(R12)(R13)(R14)]++ 2X" (X) in which R9 is chosen from aliphatic radicals comprising from about 16 to 30 carbon atoms, R10, R1 l, R12, R13 and R14, which may be identical or different, are chosen from hydrogen and alkyl radicals comprising from 1 to 4 carbon atoms, and X- is an anion chosen from halides, acetates, phosphates, nitrates and methyl sulphates. Such diquatemary ammonium salts, for example, include propanetallowdiammonium dichloride; and D) the quatemary ammonium salts comprising at least one ester function, of formula (XI) below:
(CrH2rO)z-R 18 R17-CO-(OCnH20y- i +-(CpH2pO)XR16 X-R 15 (XI) in which:
R15 is chosen from C1-C6 alkyl radicals and Cl-C6 hydroxyalkyl and dihydroxyalkyl radicals;
R16 is chosen from: a radical R19C(O)-, linear and branched, saturated and unsaturated C1-C22 hydrocarbon-based radicals R20, and a hydrogen atom, R18 is chosen from: a radical R21C(O)-, linear and branched, saturated and unsaturated Ci-C6 hydrocarbon-based radicals R22, and a hydrogen atom, R17, R19 and R21, which may be identical or different, are chosen from linear and branched, saturated and unsaturated C7-C21 hydrocarbon-based radicals; n, p and r, which may be identical or different, are chosen from integers ranging from 2 to 6; y is chosen from integers ranging from 1 to 10; x and z, which may be identical or different, are chosen from integers ranging from 0 to 10; X- is an anion chosen from simple and complex, organic and inorganic anions; with the proviso that the sum x+y+z is from I to 15, that when x is 0, then R16 is R20 and that when z is 0, then R18 is R22.
In one embodiment, the ammonium salts of formula (XI) may be used, in which:
R15 is chosen from methyl and ethyl radicals, x and y are equal to 1; z is equal to 0 or 1; n, p and r are equal to 2; R16 is chosen from: a radical R19C(O)-,methyl, ethyl and C14-hydrocarbon-based radicals, and a hydrogen atom; R17, R19 and R21, which may be identical or different, are chosen from linear and branched, saturated and unsaturated C7-C2 1, hydrocarbon-based radicals; R18 is chosen from: a radical R21C(O)- and a hydrogen atom.
Such compounds are sold, for example, under the names Dehyquart by the company Cognis, Stepanquat by the company Stepan, Noxamium by the company Ceca, and Rewoquat WE 18 by the company Rewo-Witco.

Chelants: According to the present invention the compositions may comprise chelants.
Chelants are well known in the art and refer to a molecule or a mixture of different molecules each capable of forming a chelate with a metal ion. Chelants are well known in the art and a non-exhaustive list thereof can be found in AE Martell & RM Smith, Critical Stability Constants, Vol.
1, Plenum Press, New York & London (1974) and AE Martell & RD Hancock, Metal Complexes in Aqueous Solution, Plenum Press, New York & London (1996) both incorporated herein by reference.
Chelants suitable for use herein are carboxylic acids (in particular aminocarboxylic acids), polyamines, phosphonic acids (in particular aminophosphonic acids) and polyphosphoric acids (in particular linear polyphosphoric acids), their salts and derivatives.
Examples of preferred chelants include ethylenediaminotetraacetic acid (EDTA), nitrilotriacetic acid, diethylenetriamine pentaacetic acid (DTPA), ethylenediamine disuccinic acid (EDDS), ethylenediamine diglutaric acid (EDGA), 2-hydroxypropylenediamine disuccinic acid (HPDS), glycinamide-N,N'-disuccinic acid (GADS), ethylenediamine-N-N'-diglutaric acid (EDDG), 2-hydroxypropylenediamine-N-N'-disuccinic acid (HPDDS), salts thereof and derivatives thereof.

Chelants may be incorporated into the composition of the present invention as stabilizers and or preservatives. In addition it has also been found that chelants provide hair fibre damage benefits and thus they may be utilized in order to further improve the hair damage profile of the present invention. Levels of chelants in the present invention may be as low as about 0.1% by weight, preferably at least about 0.25% by weight, more preferably about 0.5% by weight, for the most effective chelants such as diamine-N,N'-dipolyacid chelants and monoamine monoamide-N,N'-dipolyacid chelants (for example EDDS). Less effective chelants will be more preferably used at levels of at least about 1% by weight, even more preferably above about 2% by weight of the composition, depending of the efficiency of the chelant. Levels as high as about 10% by weight may be used, but above this level significant formulation issues may arise.

Solvents: Suitable solvents for use in the compositions of the present invention include, but are not limited to, water, butoxydiglycol, 1,2-propylene glycol, glycerol, lower aliphatic alcohols (e.g. ethanol, n-propanol or isoproanol), ethoxydiglycol, isopropylalcohol, hexylene glycol, benzyl alcohol and dipropylene glycol.

Antioxidants or reducing a eg nts: Suitable antioxidants or reducing agents for use in the compositions of the present invention include, but are not limited to, ascorbic acid, thioglycolic acid and sodium sulfite.
The form of the oxidation dye precursor composition and also for the ready-to-apply dye mixture may be, for example, a solution, especially an aqueous or aqueous-alcoholic solution. However a particularly preferred form of the composition according to the invention is a cream, a gel or an emulsion. Its composition comprises a mixture of the dye ingredients with the conventional additive ingredients usually used in this type of preparation.

According to a preferred embodiment of the present invention dye powders, granules or pellets are mixed with an appropriate dye carrier mass prior to use to form the oxidation dye precursor composition. Particularly preferred is the use of the dye-containing granules/pellets according to WO 2005/044208 which are mixed with an appropriate dye carrier mass prior to use to form the oxidation dye precursor composition. WO 2005/044208 herewith is explicitly incorporated herein by reference.

The ready-to-apply hair dye mixture according to the invention is preferably made by a method comprising mixing the oxidation dye precursor composition with a liquid oxidizing agent immediately prior to application.

Hydrogen peroxide, or its addition compounds with urea, melamine or sodium bromate, in the form of a 1 to 12 percent by weight, preferably 6 percent by weight, aqueous solution, is preferred as the oxidizing agent. Hydrogen peroxide is especially preferred.

The oxidation dye precursor composition and the oxidizing agent are mixed with each other in a weight ratio of from 5:1 to 1:3. A weight ratio of 1:1 to 1:2 is especially preferred.

The pH of the ready-to-apply hair dye mixture according to the invention is adjusted during the mixing of the preferred alkaline oxidation dye precursor composition with the mostly acidic oxidizing agent. The resulting pH value of the mixture is determined by the alkali content of the dye-carrying or oxidation dye precursor composition, the acid content of the oxidizing agent and the mixing ratio. The pH of the ready-to-apply hair dye composition amounts to 3 to 11, preferably from 6 to 10.5.

The pH values of both the oxidation dye precursor composition and the oxidizing agent-containing composition may both be adjusted by adding dilute organic or inorganic acids, such as phosphoric acid, ascorbic acid and lactic acid, or bases, such as monoethanolamine, triethanolamine, 2-amino-2-methyl-l-propanol, ammonia, sodium hydroxide, potassium hydroxide or tris(hydroxymethyl)aminomethane.

After mixing the above-described oxidation dye precursor composition with an oxidizing agent, an amount of the ready-to-apply hair dye mixture sufficient for dyeing the hair, generally from 60 to 200 grams, is applied to the hair.

The hair dye mixture is allowed to act on the hair after application for 10 to 45 minutes at 15 to 50 C, preferably for 30 to 40 minutes at 30 C to 40 C. It is subsequently rinsed from the hair with water. If necessary the hair is washed with a shampoo after rinsing with water and perhaps with a dilute weak organic acid, for example citric or tartaric acid.
Subsequently the hair is dried.

The new p-phenylenediamine derivatives of formula (I) allow the creation of non-sensitizing oxidative hair dyes with good dyeing properties.

The examples below are intended to illustrate the subject-matter of the invention in more detail without limiting it thereto.

EXAMPLES
Example lA to 3100A: Hair Dye Solution Dye carrier mass A: 10.0 g Sodium lauryl ether sulfate (28 % strength aqueous solution) 7.8 g Ethanol 0.3 g Ascorbic acid 0.3 g Sodium sulfite, anhydrous 0.3 g Ethylenediaminetetraacetic acid disodium salt hydrate 9.0 g Ammonium hydroxide (22 % strength aqueous solution) X g Dyes (according to the below-mentioned table 2) ad 100.0 g Water, demineralized The pH of the solution was between 10 and 10.5.

Immediately prior to application 50 g of the above-described dye carrier mass A are mixed with 50 grams of a 6% by weight aqueous hydrogen peroxide solution. The resulting ready-to-apply hair dye mixture is applied to the hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1 B to 3100B; Hair Dye Cream Dye carrier mass B: 15.00 g Cetylstearylalcohol 2.30 g Glycerinmonostearate 0.80 g Lanolin 3,80 g Lanolinalcohol 3.50 g Sodium lauryl diglykolether sulfate (28 % strength aqueous solution) 1.42 g Steareth-20 7.80 g Ethanol 0.30 g Ascorbic acid 0.30 g Sodium sulfite, anhydrous 0.30 g ethylenediaminetetraacetic acid disodium salt hydrate 10.00 g Ammonium hydroxide (22 % strength aqueous solution) 0.20 g Perfume X g Dyes (according to the below-mentioned table 2) ad 100.00 g Water, demineralized The pH of the cream was between 9.5 and 10.5.

Immediately prior to application 75 g of the above-described dye carrier mass B are mixed with 50 grams of a 9% by weight aqueous hydrogen peroxide solution. The resulting ready-to-use hair dye mixture is applied to the hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1C to 3100C: Hair Dye Gel Dye carrier mass C: 15,00 g Oleic acid 3,00 g Glycerol 7,00 g Isopropanol 0,50 g Ascorbic acid 0,40 g Sodium sulfite, anhydrous 0,40 g Sodium hydroxide 10,00 g Ammonium hydroxide (25 % strength aqueous solution) X g Dyes (according to the below-mentioned table 2) ad 100,00 g Water, demineralized Immediately prior to application 100 g of the above-described dye carrier mass C are mixed with 100 grams of a 6% by weight aqueous hydrogen peroxide solution. The resulting ready-to-apply hair dye mixture is applied to the hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1D to 3100D: Hair Dye Dye carrier mass D: 9.500 g Propylene glycol 5.000 g Ammonium hydroxide 4.000 g Ethoxydiglycol 4.500 g Ethanolamine 1.000 g Oleic acid 6.000 g Hexylene glycol 3.500 g Cocamidopropyl betaine 0.300 g Oleth-10 0.300 g Oleth-2 1.500 g Dilinoleic acid 0.500 g C 12-C 15 Pareth-3 7.000 g Soytrimonium chloride 0.005 g Sodium metasilicate 0.500 g Erythorbic acid 0.300 g Ethylenediaminetetraacetic acid disodium salt 0.300 g Sodium sulfite X g Dyes (according to the below-mentioned table 2) ad 100.000 g Water, demineralized Immediately prior to application 75 g of the above-described dye carrier mass D are mixed with 50 grams of a 9% by weight aqueous hydrogen peroxide solution. The resulting ready-to-use hair dye mixture is applied to bleached hair in the required amount. After an acting time of 40 minutes at 30 C the hair is washed with a shampoo, rinsed with water and dried.

Example lE to 3100E: Nonionic Hair Dye Dye carrier mass E: 7.00 g Cetylstearyl alcohol 2.00 g Glyceryl oleate 13.00 g Polysorbate 40 6.00 g Ceteareth-50 0.50 g Sodium sulfite, anhydrous 0.10 g Ethylenediaminetetraacetic acid disodium salt 8.00 g Ammonia (25% strength aqueous solution) X g Dyes (according to the below-mentioned table 2) ad 100.00 g Water Hydrogen peroxide emulsion 3.0 g Cetylstearyl alcohol 0.8 g PEG-25 cetyl/stearyl ether 0.3 g Lanolin alcohol 6.0 g Hydrogen peroxide 0.1 g Phosphoric acid (85% strength aqueous solution) ad 100.0 g Water 60 g of the above non-ionic dye carrier mass E are mixed prior to application with 60 g of the above hydrogen peroxide emulsion (pH = 2.5). The pH of the resulting ready-to-use hair dye composition is about 10. The resulting ready-to-use hair dye mixture is applied to bleached hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1F to 3100F: Hair Dye Dye carrier mass F: 0.100 g Sodium sulphite 0.200 g Ascorbic Acid 0.003 g Ethylenediaminetetraacetic acid disodium salt 0.200 g Citric Acid 4.000 g Ammonia (30% strength aqueous solution) 1.000 g Acrylates Copolymer (Aculyn 33A) 0.500 g Oleth 5 1.000 g Oleth 2 0.900 g Oleic Acid 3.000 g Cocamidopropyl betaine 0.050 g Etidronic Acid 1.000 g Trisodium Ethylenediamine disuccinate 2.500 g Isopropyl alcohol 8.600 g Hydrogen Peroxide (35% aqueous solution) 3.000 g Soytrimonium Chloride and propylene glycol 0.003 g Simethicone 1.000 g Steareth-21 0.500 g PEG-50 Hydrogenated Palmamide 0.200 g Oleyl Alcohol 0.500 g Acrylates Steareth-20 Methacrylate Copolymer (Aculyn(V 22) 2.000 g Propylene Glycol 4.200 g Ethoxy Diglycol 0.500 g C 11-15 Pareth-9 0.800 g C12-15 Pareth-3 X g Dyes (according to the below-mentioned table 2) ad 100.000 g Water The pH of the ready-to-use hair dye composition is about 10. The ready-to-use hair dye mixture is applied to bleached hair in the required amount. After an acting time of 40 minutes at 30 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1 G to 3100G: Hair Dye Dye carrier mass G: 0.100 g Sodium sulphite 0.200 g Ascorbic Acid 0.003 g Ethylenediaminetetraacetic acid disodium salt 0.200 g Citric Acid 4.000 g Ammonia (30% strength aqueous solution) 1.000 g Acrylates Copolymer (Aculyn(V 33A) 0.500 g Oleth 5 1.000 g Oleth 2 0.900 g Oleic Acid 3.000 g Cocamidopropyl betaine 0.050 g Etidronic Acid 1.000 g Trisodium Ethylenediamine disuccinate 2.500 g Isopropyl alcohol 13.000 g Hydrogen Peroxide (35% aqueous solution) 3.000 g Soytrimonium Chloride and propylene glycol 0.003 g Simethicone 1.000 g Steareth-21 0.500 g PEG-50 Hydrogenated Palmamide 0.200 g Oleyl Alcohol 1.000 g Acrylates Steareth-20 Methacrylate Copolymer (Aculyn 22) 2.000 g Propylene Glycol 4.200 g Ethoxy Diglycol 0.500 g C 11-15 Pareth-9 0.800 g C12-15 Pareth-3 X g Dyes (according to the below-mentioned table 2) ad 100.000 g Water The pH of the ready-to-use hair dye composition is about 10. The ready-to-use hair dye mixture is applied to bleached hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1H to 3100H: Hair Dye Dye carrier mass H: 0.1 g Sodium sulphite 0.1 g Ascorbic Acid 5.0 g Ammonium Carbonate 0.1 g Potassium Hydrogen Carbonate 0.2 g Ammonium Acetate 2.0 g Cetearyl Alcohol (and) Dicetyl Phosphate (and) Ceteth-10 Phosphate (Crodafos(V CES) 1.0 g Ceteareth-25 (Volpo(I CS25) 2,0 g Sodium Glycinate 2.0 g Stearyl Alcohol 0.3 g Sodium Hydroxide (50% aqueous solution) 0.1 g Ethylenediaminetetraacetic acid tetrasodium salt 0.5 g Etidronic Acid 8.6 g Hydrogen Peroxide (35% aqueous solution) 0.2 g Polyquaternium-22 (Merquat 295) 0.2 g Polyquaternium-37 & Mineral oil (Salcare SC95) 0.1 g Styrene-PVP Copolymer (Polectron(t 430) 0.1 g Xanthan gum 2.0 g Cetyl Alcohol 1.0 g Acrylates copolymer (Aculyn 33) X g Dyes (according to the below-mentioned table 2) ad 100.0 g Water The pH of the ready-to-use hair dye composition is about 9. The ready-to-use hair dye mixture is applied to bleached hair in the required amount. After an acting time of 40 minutes at 30 C the hair is washed with a shampoo, rinsed with water and dried.

Example lI to 3 1001: Hair Dye Dye carrier mass I: 0.1 g Sodium sulphite 0.1 g Ascorbic Acid 6.0 g Ammonium Carbonate 0.1 g Potassium Hydrogen Carbonate 0.2 g Ammonium Acetate 2.0 g Cetearyl Alcohol (and) Dicetyl Phosphate (and) Ceteth-10 Phosphate (Crodafos(V CES) 0.3 g Sodium Hydroxide (50% aqueous solution) 0.1 g Ethylenediaminetetraacetic acid tetrasodium salt 0.5 g Etidronic Acid 8.6 g Hydrogen Peroxide (35% aqueous solution) 1.0 g Amodimethicone (Belsil ADM1100) 0.5 g Styrene-PVP Copolymer (Polectron(V 430) 0.5 g Acrylates/C10-30 Alkyl Acrylate Crosspolymer 1.0 g Acrylates Steareth-20 Methacrylate Copolymer (Aculyn (V 22) 1.0 g Acrylates copolymer (Aculyn(V 33) X g Dyes (according to the below-mentioned table 2) ad 100.0 g Water The pH of the ready-to-use hair dye composition is about 9. The ready-to-use hair dye mixture is applied to bleached hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1K to 3100K: Hair Dye Synthesis of dye granules/pellets according to WO 2005/044208 (general method for producin~
granules/pellets of each dye mixture 1 to 3100): In a Glatt fluidized bed granulator and coater, 400 g of the respective dye mixture 1 to 3100 according to table 2 are heated to a product temperature of 34 C with air at an incoming air temperature of 90 C and an air flow rate of 18 m3/h. A 20 %
aqueous polyvinylpyrrolidone solution ("spraying solution") is then sprayed onto this mixture at an initial spraying rate of 8 g/min and at a spraying air pressure of 0.5 bar. In the course of the granulation process, the spraying rate is increased to 12 g/min and the incoming air temperature is increased to 100 C, while the air flow rate is raised to a maximum of 30 m3/h. The product temperature is kept at about 30-31 C throughout the entire procedure. After 310 g of the polyvinylpyrrolidone solution has been sprayed on, the granules/pellets are dried at a maximum product temperature of 57 C and then cooled to about 30 C and screened.

Before use these granules/pellets (comprising the dye combinations 1 to 3100 as described in the below-mentioned table 2) are mixed with the following peroxide solution or emulsion in a 1:1 ratio.
Hydrogen Peroxide Emulsion: 9.00 g Hydrogen peroxide 1.80 g Cetylstearyl alcohol 3.30 g Polyvinylpyrrolidone-styrene copolymer 0.20 g Disodium phosphate 0.20 g Sodium laurylsulfate 0.10 g Salicylic acid 0.08 g Phosphoric acid to 100.00 g Water, demineralized The resulting ready-to-apply dye mixture is applied to the hair in the required amount. After an acting time of 40 minutes at 30 C the hair is washed with a shampoo, rinsed with water and dried.

Example 1L to 3100 L: Hair Dye S3nthesis of dye rg anules/pellets according to WO 2005/044208 (general method for producing apr nules/pellets of each dye mixture 1 to 3100): In a Glatt fluidized bed granulator and coater, 400 g of the respective dye mixture 1 to 3100 according to table 2 are heated to a product temperature of 34 C with air at an incoming air temperature of 90 C and an air flow rate of 18 m3/h. A 20 %
aqueous polyvinylpyrrolidone solution ("spraying solution") is then sprayed onto this mixture at an initial spraying rate of 8 g/min and at a spraying air pressure of 0.5 bar. In the course of the granulation process, the spraying rate was increased to 12 g/min and the incoming air temperature is increased to 100 C, while the air flow rate was raised to a maximum of 30 m3/h. The product temperature is kept at about 30-31 C throughout the entire procedure. After 310 g of the polyvinylpyrrolidone solution has been sprayed on, the granules/pellets are dried at a maximum product temperature of 57 C and then cooled to about 30 C and screened.

Before use these granules/pellets (comprising one of the dye combinations 1 to 3100 as described in the below-mentioned table 2) are included in one of the above dye carrier masses A to I as the "Xg Dyes (according to the below-mentioned table 2)" in the needed ratio. Then 60 g of the resulting composition are mixed with 60 grams of a 6% by weight aqueous hydrogen peroxide solution.
The resulting ready-to-apply hair dye mixture is applied to the hair in the required amount. After an acting time of 30 minutes at 40 C the hair is washed with a shampoo, rinsed with water and dried.

Table 1: Dyes Used in Dye Combinations of Table 2 El 1,4-diamino-2-(methoxymethyl)benzene sulfate E2 1,4-diamino-2-methylbenzene sulfate E3 1, 4-diaminobenzene E4 1,4-diamino-2-(2-hydroxyethyl)benzene sulfate E5 3-methyl-4-aminophenol E6 4-aminophenol E7 N,N-bis(2'-hydroxyethyl)-p-phenylenediamine sulfate E8 4,5-diamino-l-(2-hydroxyethyl)-1H-pyrazole sulfate E9 4-(methylamino)phenol E10 2,4,5,6-pyrimidinetetramine E11 4-hydroxy-2,5,6-triaminopyrimidine sulfate Coupter substances Kl 2-amino-4-((2'-hydroxyethyl)amino)anisole sulfate K2 2,4-diamino-l-(2'-hydroxyethoxy)benzene sulfate K3 3-amino-2-methylamino-6-methoxypyridine K4 3,5-diamino-2,6-dimethoxypyridine dihydrochloride K5 1,3-Bis(2,4-diaminophenoxy)propane tetrahydrochloride K6 3-aminophenol K7 5-amino-2-methylphenol K8 5-amino-6-chlor-2-methylphenol K9 5-[(2-hydroxyethyl)amino]-2-methylphenol K10 5-amino-4-chloro-2-methylphenol Kl l 1-naphthol K12 resorcinol K13 2-methylresorcinol K14 4-chlororesorcinol K15 4-(2'-hydroxyethyl)amino-l,2-methylendioxybenzene*HCl K16 3-amino-2,6-dimethyl-phenol K17 1,5-naphthalenediol K18 2,7-naphthalenediol K19 3,4-dihydro-2H-1,4-benzoxazin-6-ol K20 5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one K21 3 -am ino-2, 4-dichlorophenol K22 2,6-Dihydroxy-3,4-dimethylpyridine K23 6-hydroxy-1 H-Indole K24 2-amino-3-hydroxypyridine K25 2-amino-5-ethylphenol Direct Dyes Dl 2,6-diamino-3-((pyridin-3 -yl)azo)pyridine D2 6-chloro-2-ethylamino-4-nitrophenol D3 2-amino-6-chloro-4-nitrophenol 3-((9,10-dihydro-9,10-dioxo-4-(methylamino)-1-anthracenyl)amino)-N,N-dimethyl-N-propyl-l-propanaminium bromide Table 2: Dye Combinations 1 to 3100 1. 0.250g El + 1.935g K16 + 0.263g K12 + 0.250g E8 + 0.263g K6 2. 2.500g E2 + 2.625g K12 + 1.673g K16 + 2.500g E8 + 2.625g K7 3. 1.250g E3 + 1.313g K12 + 1.250g E8 + 0.185g K16 + 1.313g K9 4. 0.250g E4 + 0.263g K12 + 0.250g E8 + 0.263g K13 + 0.057g K16 5. 0.250g El + 0.057g K16 + 0.263g K12 + 0.250g E8 + 0.263g K1 + 0.065g K3 6. 2.500g E2 + 2.625g K12 + 0.057g K16 + 2.500g E8 + 0.l00g K23 + 2.625g K11 7. 0.250g E3 + 0.263g K12 + 0.250g E8 + 0.057g K16 + 0.263g K14 8. 0.250g E4 + 0.263g K12 + 0.250g E8 + 0.263g K24 + 0.057g K16 9. 0.250g El + 0.057g K16 + 0.263g K12 + 0.250g E8 + 0.263g K2 10. 0.200g E2 + 0.210g K12 + 0.057g K16 + 0.200g E8 + 0.210g K6 + 0.210g K7 11. 0.200g E3 + 0.210g K12 + 0.200g E8 + 0.057g K16 + 0.210g K6 + 0.210g K9 12. 1.000g E4 + 1.050g K12 + 1.000g E8 + 1.050g K6 + 0.057g K16 + 1.050g K22 13. 2.000g El + 2.100g K12 + 2.000g E8 + 2.100g K6 + 2.100g K1 + 0.057g K16 14. 0.200gE10+0.057gK16+0.210gK12+0.200gE8+0.210gK6+0.210gK11 15. 0.200g E3 + 0.210g K12 + 0.057g K16 + 0.200g E8 + 0.210g K6 + 0.210g K14 16. 0.200g E4 + 0.210g K12 + 0.200g E8 + 0.057g K16 + 0.210g K6 + 0.210g K24 17. 1.000g E1 + 1.050g K12 + 1.000g E8 + 1.050g K6 + 0.057g K16 + 1.050g K2 18. 2.000g E2 + 2.100g K12 + 2.000g E8 + 2.100g K7 + 2.100g K9 + 0.057g K16 19. 2.000g E3 + 0.057g K16 + 2.100g K12 + 2.000g E8 + 2.100g K7 + 2.100g K13 20. 2.000g E4 + 2.100g K12 + 0.057g K16 + 2.000g E8 + 2.100g K7 + 2.100g K1 21. 1.000g El + 1.050g K12 + 1.000g E8 + 0.057g K16 + 1.050g K7 + 1.050g Kl 1 22. 1.000g E2 + 1.050g K12 + 1.000g E8 + 1.050g K7 + 0.057g K16 + 1.050g K14 23. 2.000g E3 + 2.100g K12 + 2.000g E8 + 2.100g K7 + 2.100g K24 + 0.057g K16 24. 2.000g E4 + 0.057g K16 + 2. l00g K12 + 2.000g E8 + 2.100g K8 + 2.100g K2 25. 1.000g El + 1.050g K12 + 0.057g K16 + 1.000g E8 + 1.050g K9 + 1.050g K13 26. 0.200g E2 + 0.210g K12 + 0.200g E8 + 0.057g K16 + 0.210g K9 + 0.210g K1 27. 1.000g E3 + 1.050g K12 + 1.000g E8 + 1.050g K9 + 0.057g K16 + 1.050g K11 28. 2.000g E4 + 2.100g K12 + 2.000g E8 + 2.l00g K9 + 2.l00g K14 + 0.057g K16 29. 0.200g El + 0.057g K16 + 0.210g K12 + 0.200g E8 + 0.210g K9 + 0.210g K24 30. 1.000g E2 + 1.050g K12 + 0.057g K16 + 1.000g E8 + 1.050g K9 + 1.050g K2 31. 2.000g E3 + 2.l00g K12 + 2.000g E8 + 0.057g K16 + 2.l00g K13 + 2.100g K1 32. 0.200g E4 + 0.210g K12 + 0.200g E8 + 0.210g K13 + 0.057g K16 + 0.210g Kl 1 33. 2.000gEl +2.100gK12+2.000gE8+2.100gK13+2.l00gK14+0.260gK16 34. 1.000g E2 + 0.260g K16 + 1.050g K12 + 1.000g E8 + 1.050g K13 + 1.050g K24 35. 2.000g E3 + 2.100g K12 + 0.260g K16 + 2.000g E8 + 2.l00g K13 + 2.100g K2 36. 0.200g E4 + 0.210g K12 + 0.200g E8 + 0.260g K16 + 0.210g K4 + 0.210g Kl 1 37. 1.000g El + 1.550g K12 + 1.000g E8 + 1.050g K1 + 0.050g K5 + 0.260g K16 +
1.050g K14 38. 1.000g E2 + 1.050g K12 + 1.000g E8 + 1.050g K1 + 1.050g K24 + 0.260g K16 39. 1.000g E3 + 0.260g K16 + 1.050g K12 + 1.000g E8 + 1.050g K1 + 1.050g K2 40. 0.200g E4 + 0.210g K12 + 0.260g K16 + 0.200g E8 + 0.210g K11 + 0.210g K14 41. 1.000g El + 1.050g K12 + 1.000g E8 + 0.260g K16 + 1.050g K11 + 1.050g K24 42. 0.200g E2 + 0.210g K12 + 0.200g E8 + 0.210g K11 + 0.260g K16 + 0.210g K2 43. 1.000g E3 + 1.050g K12 + 1.000g E8 + 1.050g K14 + 1.050g K24 + 0.260g K16 44. 2.000g E4 + 0.260g K16 + 2.100g K12 + 2.000g E8 + 2.100g K14 + 2.100g K2 45. 0.200g E1 + 0.210g K12 + 0.260g K16 + 0.200g E8 + 0.210g K24 + 0.210g K2 46. 2.500g E2 + 2.625g K12 + 2.500g E6 + 0.260g K16 + 2.625g K6 + 0.135g K20 47. 2.500g E3 + 2.625g K12 + 2.500g E6 + 2.625g K7 + 0.260g K16 48. 2.500g E4 + 0.260g K16 + 2.625g K12 + 2.500g E6 + 2.625g K9 + 0.150g K20 49. 1.250g El + 1.313g K12 + 0.260g K16 + 1.250g E6 + 1.313g K13 50. 2.500g E2 + 2.625g K12 + 2.500g E6 + 0.260g K16 + 2.625g KI

51. 0.250g E3 + 0.263g K12 + 0.250g E6 + 0.263g K11 + 0.260g K16 52. 0.250g E4 + 0.260g K16 + 0.263g K12 + 0.250g E6 + 0.263g K14 53. 2.500g El + 2.625g K12 + 0.260g K16 + 2.500g E6 + 2.625g K24 54. 0.250g E2 + 0.263g K12 + 0.250g E6 + 0.260g K16 + 0.109g E9 + 0.263g K2 55. 1.000g E3 + 1.050g K12 + 1.000g E6 + 1.050g K6 + 0.260g K16 + 1.050g K7 56. 0.200g E4 + 0.210g K12 + 0.200g E6 + 0.210g K6 + 0.210g K9 + 0.260g K16 57. 0.200g El + 0.260g K16 + 0.210g K12 + 0.200g E6 + 0.210g K6 + 0.210g K13 58. 1.000g E2 + 1.050g K12 + 0.260g K16 + 1.000g E6 + 1.050g K6 + 1.050g K1 59. 2.000g E3 + 2.100g K12 + 2.000g E6 + 0.260g K16 + 2.100g K6 + 2.100g Kl 1 60. 1.000g E4 + 1.050g K12 + 1.000g E6 + 1.050g K6 + 0.260g K16 + 1.050g K14 61. 1.000g El + 1.050g K12 + 1.000g E6 + 1.050g K6 + 1.050g K24 + 0.260g K16 62. 0.200g K6 + 0.210g K12 + 0.200g K8 + 0.210g K16 + 0.210g K2 + 0.060g K19 63. 2.000g E10 + 0.383g K16 + 2.100g K12 + 2.000g E6 + 2.100g K8 + 2.100g K9 64. 0.200g E3 + 0.210g K12 + 0.383g K16 + 0.200g E6 + 0.210g K7 + 0.210g K13 65. 2.000g E4 + 2.100g K12 + 2.000g E6 + 0.090g E9 + 0.383g K16 + 2.100g K7 +
2.100g Kl 66. 1.000g E11 + 1.050g K12 + 1.000g K7 + 1.050g K16 + 1.050g K11 67. 0.200gE10+0.210gK12+0.200gE6+0.210gK7+ 1.531gK16+0.210gK14 68. 2.000g E2 + 2. l00g K12 + 2.000g E6 + 2.100g K7 + 2.100g K24 + 1.53 lg K16 69. 0.200gE3+1.531gK16+0.210gK12+0.200gE6+0.210gK7+0.210gK2 70. 2.000g E11 + 2.100g K12 + 2.000g K6 + 2.l00g K16 + 2.100g K13 71. 0.200g E4 + 0.210g K12 + 1.970g K16 + 0.200g E6 + 0.210g K9 + 0.210g Kl 72. 1.000g E1 + 1.050g K12 + 1.000g E6 + 1.970g K16 + 1.050g K9 + 1.050g K11 73. 1.000g E2 + 1.050g K12 + 1.000g E6 + 1.050g K9 + 1.970g K16 + 1.050g K14 74. 0.200g E3 + 0.210g K12 + 0.200g E6 + 0.210g K9 + 0.210g K24 + 1.970g K16 75. 1.000g E4 + 1.970g K16 + 1.050g K12 + 1.000g E6 + 1.050g K9 + 1.050g K2 76. 2.000g E1 + 2.100g K12 + 1.970g K16 + 2.000g E6 + 2.100g K13 + 2.100g K1 77. 0.200g E2 + 0.210g K12 + 0.200g E6 + 1.970g K16 + 0.210g K13 + 0.210g K11 78. 2.000g E3 + 2.100g K12 + 2.000g E6 + 2.100g K13 + 1.970g K16 + 2.100g K14 79. 1.000g E4 + 1.050g K12 + 1.000g E6 + 1.050g K13 + 1.050g K24 + 1.970g K16 80. 0.200g El + 1.970g K16 + 0.210g K12 + 0.200g E6 + 0.210g K13 + 0.210g K2 81. 2.000g E2 + 2.100g K12 + 1.970g K16 + 2.000g E6 + 2.100g K1 + 2.100g K11 82. 1.000g E3 + 1.050g K12 + 1.000g E6 + 1.970g K16 + 1.050g Kl + 1.050g K14 83. 1.000g E4 + 1.050g K12 + 1.000g E6 + 1.050g Kl + 1.970g K16 + 1.050g K24 84. 1.000g El + 1.050g K12 + 1.000g E6 + 1.050g Kl + 1.050g K2 + 1.970g K16 85. 2.000g E2 + 1.970g K16 + 2.100g K12 + 2.000g E6 + 2.100g K11 + 2.100g K14 86. 1.000g E3 + 1.050g K12 + 1.970g K16 + 1.000g E6 + 1.050g Kl 1+ 1.050g K24 87. 2.000g E4 + 2.100g K12 + 2.000g E6 + 1.970g K16 + 2.100g K11 + 2.100g K2 88. 2.000g El + 2.100g K12 + 2.000g E6 + 2.100g K14 + 1.970g K16 + 2.100g K24 89. 0.200g E2 + 0.210g K12 + 0.200g E6 + 0.210g K14 + 0.210g K2 + 1.970g K16 90. 2.000g E3 + 1.970g K16 + 2.100g K12 + 2.000g E6 + 2.100g K24 + 2.100g K20 91. 1.250g E4 + 1.313g K12 + 1.970g K16 + 1.250g E5 + 1.313g K6 92. 0.250g El + 0.263g K12 + 0.250g E5 + 1.970g K16 + 0.263g K7 93. 2.500g E2 + 2.625g K12 + 2.500g E5 + 2.625g K9 + 1.970g K16 + O.OlOg K23 94. 0.250g E3 + 1.970g K16 + 0.263g K12 + 0.250g E5 + 0.263g K13 95. 0.250g E4 + 0.263g K12 + 1.970g K16 + 0.250g E5 + 0.263g K1 96. 1.250g E1 + 1.313g K12 + 1.250g E5 + 1.970g K16 + 1.313g K11 97. 1.250g E10 + 1.313g K12 + 1.250g E5 + 1.313g K14 + 1.970g K16 98. 0.250g E3 + 1.970g K16 + 0.263g K12 + 0.250g E5 + 0.263g K24 99. 0.250g E4 + 0.263g K12 + 0.173g K16 + 0.250g E5 + 0.263g K2 100. 1.000g El + 1.050g K12 + 1.000g E5 + 0.173g K16 + 1.050g K6 + 1'.050g K7 101. 2.000g E2 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 0.173g K16 + 2.100g K9 102. 2.000g E3 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 2.100g K13 + 0.173g K16 103. 1.000g E4 + 0.173g K16 + l.050g K12 + 1.000g E5 + 1.050g K6 + 1.050g K1 104. 2.000g El + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2.100g K6 + 2.100g K11 105. 1.000g E2 + 1.050g K12 + 1.000g E5 + 0.173g K16 + 1.050g K6 + 1.050g K14 106. 2.000g E3 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 0.173g K16 + 2.100g K24 107. 2.000g E4 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 0.173g K16 108. 0.200g El + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K7 + 0.210g K9 109. 1.000g E2 + 1.050g K12 + 0.173g K16 + 1.000g E5 + 1.050g K8 + 1.050g K13 110. 2.000g E3 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K7 + 2.100g Ki 111. 0.200g E4 + 0.210g K12 + 0.200g E5 + 0.210g K21 + 0.173g K16 + 0.210g K11 112. 1.000g El + 1.050g K12 + 1.000g E5 + 1.050g K8 + 1.050g K14 + 0.173g K16 113. 2.000g E2 + 0.173g K16 + 2.100g K12 + 2.000g E5 + 2.100g K7 + 2.100g K24 114. 1.000g E3 + 1.050g K12 + 0.173g K16 + 1.000g E5 + 1.050g K7 + 1.050g K2 115. 2.000g E4 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K9 + 2.100g K13 116. 0.200g El + 0.210g K12 + 0.200g E5 + 0.210g K9 + 0.173g K16 + 0.210g Kl 117. 0.200g E2 + 0.210g K12 + 0.200g E5 + 0.210g K9 + 0.210g K11 + 0.173g Kl6 118. 0.200g E3 + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K9 + 0.210g K14 119. 2.000g E4 + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2.100g K9 + 2.100g K24 120. 2.000g El + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K9 + 2.100g K2 121. 2.000g E2 + 2.100g K12 + 2.000g E5 + 2.100g K13 + 0.173g K16 + 2.100g K1 122. 2.000g E3 + 2.100g K12 + 2.000g E5 + 2.100g K13 + 2.100g K11 + 0.173g K16 123. 1.000g E4 + 0.173g K16 + 1.050g K12 + 1.000g E5 + 1.050g K13 + 1.050g K14 124. 2.000g El + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2. l00g K13 + 2.100g 125. 0.200g E2 + 0.210g K12 + 0.200g E5 + 0.173g K16 + 0.210g K13 + 0.210g K2 126. 0.200g E3 + 0.210g K12 + 0.200g E5 + 0.210g K1 + 0.173g K16 + 0.210g K11 127. 1.000g E4 + 1.050g K12 + 1.000g E5 + l.050g K1 + 1.050g K14 + 0.173g K16 128. 0.200g E1 + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K1 + 0.210g K24 129. 2.000g E2 + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2.100g K1 + 2.100g K2 130. 2.000g E3 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.IOOg K11 + 2.100g K14 131. 2.000g E4 + 2.100g K12 + 2.000g E5 + 2.100g K11 + 0.173g K16 + 2.100g K24 132. 0.200gE1 +0.210gK12+0.200gE5+0.210gK11 + 0.210g K2 + 0.173g K16 133. 0.200g E2 + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K14 + 0.210g K24 134. 0.200g E3 + 0.210g K12 + 0.173g K16 + 0.200g E5 + 0.210g K14 + 0.210g K2 135. 2.000g E4 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K24 + 2.100g K2 136. 1.250g El + 1.313g K12 + 1.250g E7 + 1.313g K6 + 0.173g K16 137. 1.250g E2 + 0.173g K16 + 1.313g K12 + 1.250g E7 + 1.313g K7 138. 0.250g E3 + 0.263g K12 + 0.173g K16 + 0.250g E7 + 0.263g K9 139. 1.250g E4 + 1.313g K12 + 1.250g E7 + 0.173g K16 + 1.313g K13 140. 2.500g El + 2.625g K12 + 2.500g E7 + 2.625g K4 + 0.173g K16 141. 2.500g E2 + 0.173g K16 + 2.625g K12 + 2.500g E7 + 2.625g Kl 1 142. 1.250g E3 + 1.313g K12 + 0.173g K16 + 1.250g E7 + 1.313g K14 143. 1.250g E4 + 1.313g K12 + 1.250g E7 + 0.173g K16 + 1.313g K24 144. 1.250g E1 + 1.313g K12 + 1.250g E7 + 1.313g K2 + 0.173g K16 145. 1.000g E2 + 0.173g K16 + 1.050g K12 + 1.000g E7 + 1.050g K6 + 1.050g K7 146. 1.000g E3 + 1.050g K12 + 0.173g K16 + 1.000g E7 + 1.050g K6 + 1.050g K9 147. 1.000g E4 + 1.050g K12 + 1.000g E7 + 0.173g K16 + 1.050g K6 + 1.050g K13 148. 2.000g El + 2.100g K12 + 2.000g E7 + 2.100g K6 + 0.173g K16 + 2.100g K1 149. 1.000g E2 + 1.050g K12 + 1.000g E7 + 1.050g K6 + 1.050g K11 + 0.173g K16 150. 2.000g E3 + 0.173g K16 + 2.100g K12 + 2.000g E7 + 2.100g K6 + 2.100g K14 151. 0.200g E4 + 0.210g K12 + 0.173g K16 + 0.200g E7 + 0.210g K6 + 0.210g K24 152. 0.200g E1 + 0.210g K12 + 0.200g E7 + 0.173g K16 + 0.210g K6 + 0.210g K2 153. 0.200g E2 + 0.210g K12 + 0.200g E7 + 0.210g K7 + 0.173g K16 + 0.210g K9 154. 0.200g E3 + 0.210g K12 + 0.200g E7 + 0.210g K7 + 0.210g K13 + 0.173g K16 155. 1.000g E4 + 0.173g K16 + 1.050g K12 + 1.000g E7 + 1.050g K7 + 1.050g K1 156. 0.200gE1 +0.210gK12+0.173gK16+0.200gE7+0.210gK7+0.210gK11 157. 0.200g E2 + 0.210g K12 + 0.200g E7 + 0.173g K16 + 0.210g K8 + 0.210g K14 158. 2.000g E3 + 2.100g K12 + 2.000g E7 + 2.100g K7 + 0.173g K16 + 2.100g K24 159. 2.000g E4 + 2.100g K12 + 2.000g E7 + 2.100g K7 + 2.100g K2 + 0.173g K16 160. 0.200gE1 + 0.173g K16 + 0.210g K12 + 0.200g E7 + 0.210g K9 + 0.210g K13 161. 2.000g E2 + 2.100g K12 + 0.173g K16 + 2.000g E7 + 2.100g K9 + 2.100g K1 162. 1.000g E3 + 1.050g K12 + 1.000g E7 + 0.173g K16 + 1.050g K9 + 1.050g K11 163. 0.200gE4+0.210gK12+0.200gE7+0.210gK9+0.173gK16+0.210gK14 164. 2.000g E1 + 2.100g K12 + 2.000g E7 + 2.100g K9 + 2.100g K24 + 0.173g K16 165. 2.000g E2 + 0.173g K16 + 2.100g K12 + 2.000g E7 + 2.100g K9 + 2.100g K2 166. 2.000g E3 + 2.100g K12 + 0.173g K16 + 2.000g E7 + 2.100g K13 + 2.100g K1 167. 1.000g E4 + 1.050g K12 + 1.000g E7 + 0.376g K16 + 1.050g K13 + 1.050g K11 168. 1.000g El + 1.050g K12 + 1.000g E7 + 1.050g K13 + 0.376g K16 + 1.050g K14 169. 2.000g E2 + 2.100g K12 + 2.000g E7 + 2.100g K13 + 2.100g K24 + 0.376g K16 170. 2.000g E3 + 0.376g K16 + 2.100g K12 + 2.000g E7 + 2.100g K13 + 2.100g K2 171. 0.200gE4+0.210gK12+0.376gK16+0.200gE7+0.210gK1+0.210gK11 172. 2.000g El + 2.100g K12 + 2.000g E7 + 0.376g K16 + 2.100g K1 + 2.100g K14 173. 1.000g E2 + 1.050g K12 + 1.000g E7 + 1.050g K1 + 0.376g K16 + 1.050g K24 174. 1.000g E3 + 1.050g K12 + 1.000g E7 + 1.050g K1 + 1.050g K2 + 0.376g K16 175. 0.200g E4 + 0.376g K16 + 0.210g K12 + 0.200g E7 + 0.210g K11 + 0.210g K14 176. 1.000g E1 + 1.050g K12 + 0.376g K16 + 1.000g E7 + 1.050g K11 + 1.050g K24 177. 0.200gE2+0.210gK12+0.200gE7+0.376gK16+0.210gK11 +0.210gK2 178. 1.000g E3 + 1.050g K12 + 1.000g E7 + 1.050g K14 + 0.376g K16 + 1.050g K24 179. 1.000g E4 + 1.050g K12 + 1.000g E7 + 1.050g K14 + 1.050g K2 + 0.376g K16 180. 0.200g El + 0.376g K16 + 0.210g K12 + 0.200g E7 + 0.210g K24 + 0.210g K2 181. 2.500g El + 2.625g K12 + 0.376g K16 182. 1.667g E3 + 0.376g K16 + 1.750g K12 + 1.750g K6 183. 3.333g E4 + 3.500g K12 + 0.376g K16 + 3.500g K7 + 0.110g K23 184. 1.667g El + 1.750g K12 + 1.750g K9 + 0.376g K16 185. 0.333g E2 + 0.376g K16 + 0.350g K12 + 0.350g K13 186. 1.667g E3 + 1.750g K12 + 0.376g K16 + 1.750g Kl 187. 0.333g E4 + 0.350g K12 + 0.350g Kl 1+ 0.376g K16 188. 3.333g El + 0.376g K16 + 3.500g K12 + 3.500g K14 189. 0.333g E2 + 0.350g K12 + 0.376g K16 + 0.350g K24 190. 0.333g E3 + 0.350g K12 + 0.350g K2 + 0.376g K16 191. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g K6 + 2.625g K7 192. 1.250gE1 + 1.313g K12 + 0.376g K16 + 1.313gK6+ 1.313g K9 193. 2.500g E2 + 2.625g K12 + 2.625g K6 + 0.376g K16 + 2.625g K13 194. 2.500g E3 + 2.625g K12 + 2.625g K6 + 2.625g K1 + 0.376g K16 195. 0.250g E4 + 0.376g K16 + 0.263g K12 + 0.263g K6 + 0.263g K11 196. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K6 + 0.263g K14 197. 1.250gE2+ 1.313gK12+ 1.313g K6 + 0.376g K16 + 1.313gK24 198. 1.250g E3 + 1.313g K12 + 1.313g K6 + 1.313g K2 + 0.376g K16 199. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g K7 + 2.625g K9 200. 1.250g El + 1.313g K12 + 0.376g K16 + 1.313g K7 + 1.313g K13 201. 0.250g E2 + 0.263g K12 + 0.263g K7 + 0.376g K16 + 0.263g KI

202. 0.250g E3 + 0.263g K12 + 0.263g K7 + 0.263g K11 + 0.376g K16 203. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g K7 + 2.625g K14 204. 1.250g E1 + 1.313g K12 + 0.376g K16 + 1.313g K7 + 1.313g K24 205. 1.250g E2 + 1.313g K12 + 1.313g K7 + 0.376g K16 + 1.313g K2 206. 2.500g E3 + 2.625g K12 + 2.625g K9 + 2.625g K13 + 0.376g K16 207. 1.250g E4 + 0.376g K16 + 1.313g K12 + 1.313g K9 + 1.313g K1 208. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K9 + 0.263g K11 209. 1.250g E2 + 1.313g K12 + 1.313g K9 + 0.376g K16 + 1.313g K14 210. 1.250gE3+ 1.313gK12+ 1.313gK9+ 1.313g K24 + 0.376g K16 211. 0.250g E4 + 0.376g K16 + 0.263g K12 + 0.263g K9 + 0.263g K2 212. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K13 + 0.263g KI

213. 1.250g E2 + 1.313g K12 + 1.313g K13 + 0.376g K16 + 1.313g K11 214. 1.250g E3 + 1.313g K12 + 1.313g K13 + 1.313g K14 + 0.376g K16 215. 1.250g E4 + 0.376g K16 + 1.313g K12 + 1.313g K13 + 1.313g K24 216. 2.500g El + 2.625g K12 + 0.376g K16 + 2.625g K13 + 2.625g K2 217. 2.500g E2 + 2.625g K12 + 2.625g K1 + 0.376g K16 + 2.625g Kl 1 218. 2.500g E3 + 2.625g K12 + 2.625g K1 + 2.625g K14 + 0.376g K16 219. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g Kl + 2.625g K24 220. 2.500g El + 2.625g K12 + 0.376g K16 + 2.625g Kl + 2.625g K2 221. 1.250g E2 + 1.313g K12 + 1.313g K17 + 0.376g K16 + 1.313g K14 222. 1.250g E3 + 1.313g K12 + 1.313g K18 + 1.313g K24 + 0.376g K16 223. 1.250gE4+0.376gK16+1.313gK12+1.313gK11+1.313gK2 224. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K14 + 0.263g K24 225. 2.500g E2 + 2.625g K12 + 2.625g K14 + 0.376g K16 + 2.625g K2 226. 1.250g E3 + 1.313g K12 + 1.313g K24 + 1.313g K2 + 0.376g K16 227. 2.000g E4 + 0.376g K16 + 2.100g K12 + 2.100g K6 + 2.100g K8 + 2.100g K9 228. 2.000g E1 + 2.100g K12 + 0.376g K16 + 2.100g K6 + 2.100g K21 + 2.100g K13 229. 1.000g E2 + 1.050g K12 + 1.050g K6 + 0.376g K16 + 1.050g K7 + 1.050g Ki 230. 1.000g E3 + 1.050g K12 + l.050g K6 + 1.050g K8 + 0.376g K16 + l.050g Kl 1 231. 1.000g E4 + 1.050g K12 + 1.050g K6 + 1.050g K7 + 1.050g K14 + 0.376g K16 232. 2.000g E1 + 0.376g K16 + 2.100g K12 + 2.100g K6 + 2.100g K7 + 2.100g K24 233. 0.200gE2+0.210gK12+0.376gK16+0.210gK6+0.2lOgK7+0.210gK2 234. 0.200gE3+0.210gK12+0.210gK6+0.376gK16+0.210gK9+0.210gK13 235. 1.000g E4 + 1.050g K12 + l.050g K6 + 1.050g K9 + 1.579g K16 + l.050g K1 236. 1.000g E1 + 1.050g K12 + 1.050g K6 + 1.050g K9 + 1.050g K11 + 1.579g K16 237. 0.200gE2+ 1.579gK16+0.210gK12+0.210gK6+0.210gK9+0.210gK14 238. 2.000g E3 + 2.100g K12 + 1.579g K16 + 2.100g K6 + 2.100g K9 + 2.100g K24 239. 2.000g E4 + 2.100g K12 + 2. l00g K6 + 1.579g K16 + 2.100g K9 + 2.100g K2 240. 2.000g El + 2.100g K12 + 2.100g K6 + 2.100g K13 + 1.579g K16 + 2.100g Kl 241. 0.200g E2 + 0.210g K12 + 0.210g K6 + 0.210g K13 + 0.210g K11 + 1.579g K16 242. 0.200g E3 + 1.579g K16 + 0.210g K12 + 0.210g K6 + 0.210g K13 + 0.210g K14 243. 1.000g E4 + 1.050g K12 + 1.579g K16 + 1.050g K6 + 1.050g K13 + 1.050g K24 244. 0.200gE1 + 0.210g K12 + 0.210g K6 + 1.579g K16 + 0.210g K13 +0.210gK2 245. 0.200g E2 + 0.210g K12 + 0.210g K6 + 0.210g Kl + 1.579g K16 + 0.210g K11 246. 2.000g E3 + 2.100g K12 + 2.100g K6 + 2.100g K1 + 2.100g K14 + 1.579g K16 247. 0.200g E4 + 1.579g K16 + 0.210g K12 + 0.210g K6 + 0.210g Kl + 0.210g K24 248. 1.000g E1 + 1.050g K12 + 1.579g K16 + 1.050g K6 + 1.050g K1 + 1.050g K2 249. 2.000g E2 + 2.l00g K12 + 2.l00g K6 + 1.579g K16 + 2.100g K11 + 2.l00g K14 250. 1.000g E3 + 1.050g K12 + 1.050g K6 + 1.050g Kl 1+ 1.579g K16 + 1.050g K24 251. 0.200gE4+0.210gK12+0.210gK6+0.210gK11+0.210gK2+1.579gK16 252. 0.200gE1 + 1.579g K16 + 0.210g K12 + 0.210g K6 + 0.210g K14 + 0.210g K24 253. 1.000g E2 + 1.050g K12 + 1.579g K16 + 1.050g K6 + 1.050g K14 + 1.050g K2 254. 2.000g E3 + 2.100g K12 + 2.100g K6 + 1.579g K16 + 2.100g K24 + 2.100g K2 255. 1.000g E4 + 1.050g K12 + 1.050g K7 + 1.050g K9 + 1.579g K16 + 1.050g K13 256. 0.200g E1 + 0.210g K12 + 0.210g K7 + 0.210g K9 + 0.210g K1 + 1.579g K16 257. 2.000g E2 + 1.579g K16 + 2.100g K12 + 2.100g K7 + 2.100g K9 + 2.100g K11 258. 0.200g E3 + 0.210g K12 + 1.579g K16 + 0.210g K7 + 0.210g K9 + 0.210g K14 259. 2.000g E4 + 2.100g K12 + 2.100g K7 + 1.579g K16 + 2.100g K9 + 2.100g K24 260. 2.000g E1 + 2.100g K12 + 2.100g K8 + 2.100g K9 + 1.579g K16 + 2.100g K2 261. 1.000g E2 + 1.050g K12 + 1.050g K7 + 1.050g K13 + 1.050g K1 + 1.579g K16 262. 0.200g E3 + 1.579g K16 + 0.210g K12 + 0.210g K7 + 0.210g K13 + 0.210g K11 263. 2.000g E4 + 2.100g K12 + 1.579g K16 + 2. l00g K7 + 2.100g K13 + 2.100g 264. 2.000g El + 2.l00g K12 + 2.l00g K7 + 1.579g K16 + 2.100g K13 + 2.100g K24 265. 1.000g E2 + 1.050g K12 + 1.050g K7 + 1.050g K13 + 1.579g K16 + 1.050g K2 266. 2.000g E3 + 2.l00g K12 + 2.l00g K7 + 2.l00g K1 + 2.100g K11 + 1.579g K16 267. 1.000g E4 + 1.579g K16 + 1.050g K12 + 1.050g K7 + 1.050g Kl + 1.050g K14 268. 1.000g E1 + 1.050g K12 + 1.579g K16 + 1.050g K7 + 1.050g Kl + 1.050g K24 269. 0.200g E2 + 0.210g K12 + 0.210g K7 + 1.579g K16 + 0.210g K1 + 0.210g K2 270. 1.000g E3 + l.050g K12 + l.050g K7 + 1.050g K11 + 1.579g K16 + 1.050g K14 271. 2.000g E4 + 2.1OOg K12 + 2.1OOg K21 + 2.100g Kl l+ 2.1OOg K24 + 1.579g 272. 2.000g El + 1.579g K16 + 2.100g K12 + 2.100g K7 + 2.100g Kl 1+ 2.100g K2 273. 1.000g E2 + 1.050g K12 + 1.579g K16 + 1.050g K8 + 1.050g K14 + 1.050g K24 274. 1.000g E3 + 1.050g K12 + 1.050g K7 + 1.579g K16 + 1.050g K14 + 1.050g K2 275. 0.200g E4 + 0.210g K12 + 0.210g K8 + 0.210g K24 + 1.579g K16 + 0.210g K2 276. 1.000g El + 1.050g K12 + 1.050g K9 + 1.050g K13 + 1.050g Kl + 1.579g K16 277. 1.000g E2 + 1.579g K16 + 1.050g K12 + 1.050g K9 + 1.050g K13 + 1.050g Kl 278. 0.200g E3 + 0.210g K12 + 1.579g K16 + 0.210g K9 + 0.210g K13 + 0.210g K14 279. 1.000g E4 + 1.050g K12 + 1.050g K9 + 1.579g K16 + 1.050g K13 + 1.050g K24 280. 0.200g E1 + 0.210g K12 + 0.210g K9 + 0.210g K13 + 1.579g K16 + 0.210g K2 281. 0.200g E2 + 0.210g K12 + 0.210g K9 + 0.210g K1 + 0.210g K11 + 1.579g K16 282. 0.200g E3 + 1.579g K16 + 0.210g K12 + 0.210g K9 + 0.210g K1 + 0.210g K14 283. 0.200g E4 + 0.210g K12 + 1.579g K16 + 0.210g K9 + 0.210g K1 + 0.210g K24 284. 2.000g El + 2.100g K12 + 2.100g K9 + 1.579g K16 + 2.100g K1 + 2.100g K2 285. 0.200g E2 + 0.210g K12 + 0.210g K9 + 0.210g K11 + 1.579g K16 + 0.210g K14 286. 2.000g E3 + 2.100g K12 + 2.100g K9 + 2.100g K11 + 2.100g K24 + 1.579g K16 287. 2.000g E4 + 1.579g K16 + 2.100g K12 + 2.100g K9 + 2.100g K11 + 2.100g K2 288. 0.200g E1 + 0.210g K12 + 1.579g K16 + 0.210g K9 + 0.210g K14 + 0.210g K24 289. 0.200g E2 + 0.210g K12 + 0.210g K9 + 1.579g K16 + 0.210g K14 + 0.210g K2 290. 2.000g E3 + 2.100g K12 + 2.100g K9 + 2.100g K24 + 1.579g K16 + 2.100g K2 291. 2.000g E4 + 2.100g K12 + 2.100g K13 + 2.100g K1 + 2.100g K11 + 1.579g K16 292. 2.000gE1 + 1.579gK16+2.100gK12+2.100gK13+2.100gK1 +2.100gK14 293. 0.200g E2 + 0.210g K12 + 1.579g K16 + 0.210g K13 + 0.210g K1 + 0.210g K24 294. 2.000g E3 + 2.100g K12 + 2.100g K13 + 1.579g K16 + 2.100g Kl + 2.100g K2 295. 2.000g E4 + 2.100g K12 + 2.100g K13 + 2.100g K11 + 1.579g K16 + 2.100g 296. 0.200g El + 0.210g K12 + 0.210g K13 + 0.210g K11 + 0.210g K24 + 1.579g 297. 1.000g E2 + 1.579g K16 + 1.050g K12 + 1.050g K13 + 1.050g K11 + 1.050g K2 298. 0.200g E3 + 0.210g K12 + 1.579g K16 + 0.210g K13 + 0.210g K14 + 0.210g 299. 0.200gE4+0.210gK12+0.210gK13+1.579gK16+0.210gK14+0.210gK2 300. 2.000g E1 + 2.100g K12 + 2.100g K13 + 2.100g K24 + 1.579g K16 + 2.100g K2 301. 0.200gE2+0.210gK12+0.2lOgK1 +0.210gK11 +0.210gK14+ 1.579gK16 302. 0.200g E3 + 1.782g K16 + 0.210g K12 + 0.210g K1 + 0.210g K11 + 0.210g K24 303. 0.200g E4 + 0.210g K12 + 1.782g K16 + 0.210g K1 + 0.210g K11 + 0.210g K2 304. 2.000g E1 + 2.100g K12 + 2.100g K1 + 1.782g K16 + 2.100g K14 + 2.100g K24 305. 1.000g E2 + 1.050g K12 + 1.050g K1 + 1.050g K14 + 1.782g K16 + 1.050g K2 306. 1.000g E3 + 1.050g K12 + 1.050g Kl + 1.050g K24 + 1.050g K2 + 1.782g K16 307. 1.000g E4 + 1.782g K16 + 1.050g K12 + 1.050g K11 + 1.050g K14 + 1.050g 308. 2.000g E1 + 2.100g K12 + 1.782g K16 + 2.l00g K11 + 2.100g K14 + 2.100g K2 309. 1.000g E2 + 1.050g K12 + 1.050g K11 + 1.782g K16 + 1.050g K24 + 1.050g K2 310. 1.000g E3 + 1.050g K12 + 1.050g K14 + 1.050g K24 + 1.782g K16 + 1.050g K2 311. 2.500g E4 + 2.625g K6 + 2.500g E8 + 2.625g K12 + 1.782g K16 312. 2.500g El + 1.782g K16 + 2.625g K6 + 2.500g E8 + 2.625g K7 313. 1.250g E2 + 1.313g K6 + 1.782g K16 + 1.250g E8 + 1.313g K9 314. 0.250g E3 + 0.263g K6 + 0.250g E8 + 1.782g K16 + 0.263g K13 315. 1.250g E4 + 1.313g K6 + 1.250g E8 + 1.313g K1 + 1.782g K16 316. 1.250g E1 + 1.782g K16 + 1.313g K6 + 1.250g E8 + 1.313g K11 317. 2.500g E2 + 2.625g K6 + 1.782g K16 + 2.500g E8 + 2.625g K14 318. 1.250g E3 + 1.313g K6 + 1.250g E8 + 1.782g K16 + 1.313g K24 319. 0.250g E4 + 0.263g K6 + 0.250g E8 + 0.263g K2 + 1.782g K16 320. 0.200g El + 1.782g K16 + 0.210g K6 + 0.200g E8 + 0.210g K12 + 0.210g K7 321. 1.000g E2 + 1.050g K6 + 1.782g K16 + 1.000g E8 + 1.050g K12 + 1.050g K9 322. 1.000g E3 + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K12 + 1.050g K13 323. 1.000g E4 + 1.050g K6 + 1.000g E8 + 1.050g K12 + 1.782g K16 + 1.050g K1 324. 0.200g El + 0.210g K6 + 0.200g E8 + 0.210g K12 + 0.210g Kl 1+ 1.782g K16 325. 2.000g E2 + 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K12 + 2.100g K14 326. 1.000g E3 + 1.050g K6 + 1.782g K16 + 1.000g E8 + 1.050g K12 + 1.050g K24 327. 0.200g E4 + 0.210g K6 + 0.200g E8 + 1.782g K16 + 0.210g K12 + 0.210g K2 328. 1.000g El + 1.050g K6 + 1.000g E8 + 1.050g K7 + 1.782g K16 + 1.050g K9 329. 2.000g E2 + 2.100g K6 + 2.000g E8 + 2.100g K7 + 2.100g K13 + 1.782g K16 330. 1.000g E3 + 1.782g K16 + 1.050g K6 + 1.000g E8 + 1.050g K7 + 1.050g Kl 331. 0.200g E4 + 0.210g K6 + 1.782g K16 + 0.200g E8 + 0.210g K7 + 0.210g KI I

332. 1.000g El + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K7 + 1.050g K14 333. 1.000g E2 + 1.050g K6 + 1.000g E8 + 1.050g K7 + 1.782g K16 + 1.050g K24 334. 0.200g E3 + 0.210g K6 + 0.200g E8 + 0.210g K7 + 0.210g K2 + 1.782g K16 335. 1.000g E4 + 1.782g K16 + 1.050g K6 + 1.000g E8 + 1.050g K9 + 1.050g K13 336. 0.200g E1 + 0.210g K6 + 1.782g K16 + 0.200g E8 + 0.210g K9 + 0.210g K1 337. 1.000g E2 + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K9 + 1.050g Kl 1 338. 2.000g E3 + 2.100g K6 + 2.000g E8 + 2.100g K9 + 1.782g K16 + 2.100g K14 339. 2.000g E4 + 2.100g K6 + 2.000g E8 + 2.100g K9 + 2.100g K24 + 1.782g K16 340. 2.000g E l+ 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K9 + 2.100g K2 341. 0.200g E2 + 0.210g K6 + 1.782g K16 + 0.200g E8 + 0.210g K13 + 0.210g K1 342. 2.000g E3 + 2.100g K6 + 2.000g E8 + 1.782g K16 + 2.100g K13 + 2.100g K11 343. 1.000g E4 + 1.050g K6 + 1.000g E8 + 1.050g K13 + 1.782g K16 + 1.050g K14 344. 2.000g El + 2.100g K6 + 2.000g E8 + 2.100g K13 + 2.100g K24 + 1.782g K16 345. 0.200g E2 + 1.782g K16 + 0.210g K6 + 0.200g E8 + 0.210g K13 + 0.210g K2 346. 2.000g E3 + 2.100g K6 + 1.782g K16 + 2.000g E8 + 2.100g K1 + 2.100g K11 347. 0.200g E4 + 0.210g K6 + 0.200g E8 + 1.782g K16 + 0.210g K1 + 0.210g K14 348. 2.000g El + 2.100g K6 + 2.000g E8 + 2.100g K1 + 1.782g K16 + 2.100g K24 349. 2.000g E2 + 2.100g K6 + 2.000g E8 + 2.100g K1 + 2.100g K2 + 1.782g K16 350. 2.000g E3 + 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K11 + 2.100g K14 351. 1.000g E4 + 1.050g K6 + 1.782g K16 + 1.000g E8 + 1.050g K11 + 1.050g K24 352. 1.000g El + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K11 + 1.050g K2 353. 1.000g E2 + 1.050g K6 + 1.000g E8 + 1.050g K14 + 1.782g K16 + 1.050g K24 354. 2.000g E3 + 2.100g K6 + 2.000g E8 + 2.100g K14 + 2.100g K2 + 1.782g K16 355. 2.000g E4 + 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K24 + 2.100g K2 356. 2.500g El + 2.625g K6 + 1.782g K16 + 2.500g E6 + 2.625g K12 357. 2.500g E2 + 2.625g K6 + 2.500g E6 + 1.782g K16 + 2.625g K7 358. 0.250g E3 + 0.263g K6 + 0.250g E6 + 0.263g K9 + 1.782g K16 359. 1.250gE4+ 1.782gK16+ 1.313gK6+ 1.250gE6+ 1.313gK13 360. 0.250g El + 0.263g K6 + 1.782g K16 + 0.250g E6 + 0.263g K1 361. 0.250g E2 + 0.263g K6 + 0.250g E6 + 1.782g K16 + 0.263g Kl 1 362. 1.250g E3 + 1.313g K6 + 1.250g E6 + 1.313g K14 + 1.782g K16 363. 1.250g E4 + 1.782g K16 + 1.313g K6 + 1.250g E6 + 1.313g K24 364. 2.500g El + 2.625g K6 + 1.782g K16 + 2.500g E6 + 2.625g K20 365. 0.200g E2 + 0.210g K6 + 0.200g E6 + 1.782g K16 + 0.210g K12 + 0.210g K7 366. 2.000g E3 + 2.100g K6 + 2.000g E6 + 2.100g K12 + 1.782g K16 + 2.100g K9 367. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.050g K12 + 1.050g K13 + 1.782g K16 368. 1.000g El + 1.782g K16 + 1.050g K6 + 1.000g E6 + 1.050g K12 + 1.050g K1 369. 0.200g E2 + 0.210g K6 + 1.782g K16 + 0.200g E6 + 0.210g K12 + 0.210g K11 370. 0.200g E3 + 0.210g K6 + 0.200g E6 + 1.985g K16 + 0.210g K12 + 0.210g K14 371. 0.200g E4 + 0.210g K6 + 0.200g E6 + 0.210g K12 + 1.985g K16 + 0.210g K24 372. 0.200g El + 0.210g K6 + 0.200g E6 + 0.210g K12 + 0.210g K2 + 1.985g K16 373. 2.000g E2 + 1.985g K16 + 2.100g K6 + 2.000g E6 + 2.100g K7 + 2.100g K9 374. 1.000g E3 + 1.050g K6 + 1.985g K16 + 1.000g E6 + 1.050g K7 + 1.050g K13 375. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K7 + 1.050g K1 376. 1.000g El + 1.050g K6 + 1.000g E6 + 1.050g K7 + 1.985g K16 + 1.050g K11 377. 2.000g E2 + 2.100g K6 + 2.000g E6 + 2.100g K7 + 2.100g K14 + 1.985g K16 378. 1.000g E3 + 1.985g K16 + 1.050g K6 + 1.000g E6 + 1.050g K7 + 1.050g K24 379. 1.000g E4 + 1.050g K6 + 1.985g K16 + 1.000g E6 + 1.050g K21 + 1.050g K2 380. 0.200g El + 0.210g K6 + 0.200g E6 + 1.985g K16 + 0.210g K9 + 0.210g K13 381. 1.000g E2 + 1.050g K6 + 1.000g E6 + 1.050g K9 + 1.985g K16 + 1.050g K1 382. 1.000g E3 + 1.050g K6 + 1.000g E6 + 1.050g K9 + 1.050g K11 + 1.985g K16 383. 1.000g E4 + 1.985g K16 + 1.050g K6 + 1.000g E6 + 1.050g K9 + 1.050g K14 384. 2.000g El + 2.100g K6 + 1.985g K16 + 2.000g E6 + 2.100g K9 + 2.100g K24 385. 1.000g E2 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K9 + 1.050g K2 386. 2.000g E3 + 2.100g K6 + 2.000g E6 + 2.100g K13 + 1.985g K16 + 2.100g K1 387. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.050g K13 + 1.050g K11 + 1.985g K16 388. 2.000g El + 1.985g K16 + 2.l00g K6 + 2.000g E6 + 2.100g K13 + 2.100g K14 389. 2.000g E2 + 2. l00g K6 + 1.985g K16 + 2.000g E6 + 2.100g K13 + 2.100g K24 390. 1.000g E3 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K13 + 1.050g K2 391. 2.000g E4 + 2.100g K6 + 2.000g E6 + 2.100g K1 + 1.985g K16 + 2.100g K11 392. 1.000g El + 1.050g K6 + 1.000g E6 + 1.050g K4 + 1.050g K14 + 1.985g K16 393. 0.200g E2 + 1.985g K16 + 0.210g K6 + 0.200g E6 + 0.210g Kl + 0.210g K24 394. 1.000g E3 + 1.050g K6 + 1.985g K16 + 1.000g E6 + 1.050g K1 + 1.050g K2 395. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K11 + 1.050g K14 396. 1.000g E1 + l.050g K6 + 1.000g E6 + 1.050g Kl 1+ 1.985g K16 + 1.050g K24 397. 0.200g E2 + 0.210g K6 + 0.200g E6 + 0.210g K11 + 0.210g K2 + 1.985g K16 398. 2.000g E3 + 1.985g K16 + 2.100g K6 + 2.000g E6 + 2.100g K14 + 2.100g K24 399. 2.000g E4 + 2.100g K6 + 1.985g K16 + 2.000g E6 + 2.100g K14 + 2.100g K2 400. 0.200g El + 0.210g K6 + 0.200g E6 + 1.985g K16 + 0.210g K24 + 0.210g K2 401. 2.500g E2 + 2.625g K6 + 2.500g E5 + 2.625g K12 + 1.985g K16 402. 1.250g E3 + 1.985g K16 + 1.313g K6 + 1.250g E5 + 1.313g K7 403. 0.250g E4 + 0.263g K6 + 1.985g K16 + 0.250g E5 + 0.263g K9 404. 0.250g El + 0.263g K6 + 0.250g E5 + 1.985g K16 + 0.263g K13 405. 0.250g E2 + 0.263g K6 + 0.250g E5 + 0.263g K1 + 1.985g K16 406. 2.500g E3 + 1.985g K16 + 2.625g K6 + 2.500g E5 + 2.625g Kl 1 407. 1.250g E4 + 1.313g K6 + 1.985g K16 + 1.250g E5 + 1.313g K14 408. 0.250g El + 0.263g K6 + 0.250g E5 + 1.985g K16 + 0.263g K24 409. 0.250g E2 + 0.263g K6 + 0.250g E5 + 0.263g K2 + 1.985g K16 410. 1.000g E3 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K12 + 1.050g K7 411. 1.000g E4 + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K12 + 1.050g K9 412. 1.000g E1 + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K12 + 1.050g K13 413. 2.000g E2 + 2.100g K6 + 2.000g E5 + 2.100g K12 + 1.985g K16 + 2.l00g K1 414. 0.200g E3 + 0.210g K6 + 0.200g E5 + 0.210g K12 + 0.210g K11 + 1.985g K16 415. 1.000g E4 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K12 + 1.050g K14 416. 1.000g El + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K12 + 1.050g K24 417. 1.000g E2 + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K12 + 1.050g K2 418. 2.000g E3 + 2. l00g K6 + 2.000g E5 + 2. l00g K7 + 1.985g K16 + 2.l00g K9 419. 0.200g E4 + 0.210g K6 + 0.200g E5 + 0.210g K8 + 0.210g K13 + 1.985g K16 420. 2.000g El + 1.985g K16 + 2.l00g K6 + 2.000g E5 + 2.l00g K7 + 2.l00g K1 421. 2.000g E2 + 2.100g K6 + 1.985g K16 + 2.000g E5 + 2.100g K7 + 2.100g K11 422. 2.000g E3 + 2.100g K6 + 2.000g E5 + 1.985g K16 + 2.100g K7 + 2.100g K14 423. 0.200g E4 + 0.210g K6 + 0.200g E5 + 0.210g K7 + 1.985g K16 + 0.210g K24 424. 2.000g E1 + 2.100g K6 + 2.000g E5 + 2.100g K7 + 2.100g K2 + 1.985g K16 425. 1.000g E2 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K9 + 1.050g K13 426. 1.000g E3 + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K9 + 1.050g Kl 427. 1.000g E4 + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K9 + 1.050g Kl l 428. 2.000g El + 2.100g K6 + 2.000g E5 + 2.100g K9 + 1.985g K16 + 2.100g K14 429. 2.000g E2 + 2.100g K6 + 2.000g E5 + 2.100g K9 + 2.100g K24 + 1.985g K16 430. 2.000g E3 + 1.985g K16 + 2.100g K6 + 2.000g E5 + 2.100g K9 + 2.100g K2 431. 1.000g E4 + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K13 + 1.050g K1 432. 1.000g El + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K13 + 1.050g K11 433. 2.000g E2 + 2. l00g K6 + 2.000g E5 + 2.100g K13 + 1.985g K16 + 2.100g K14 434. 0.200g E3 + 0.210g K6 + 0.200g E5 + 0.210g K13 + 0.210g K24 + 1.985g K16 435. 1.000g E4 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K13 + 1.050g K2 436. 1.000g El + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g Kl + 1.050g K11 437. 2.000g E2 + 2.100g K6 + 2.000g E5 + 0.187g K16 + 2.100g K1 + 2.100g K14 438. 2.000g E3 + 2.100g K6 + 2.000g E5 + 2.100g K1 + 0.187g K16 + 2.100g K24 439. 2.000g E4 + 2.100g K6 + 2.000g E5 + 2.100g K1 + 2.100g K2 + 0.187g K16 440. 2.000g El + 0.187g K16 + 2.100g K6 + 2.000g E5 + 2.100g K11 + 2.100g K14 441. 1.000g E2 + 1.050g K6 + 0.187g K16 + 1.000g E5 + 1.050g K11 + 1.050g K24 442. 1.000g E3 + 1.050g K6 + 1.000g E5 + 0.187g K16 + 1.050g K11 + 1.050g K2 443. 2.000g E4 + 2.100g K6 + 2.000g E5 + 2.100g K14 + 0.187g K16 + 2.100g K24 444. 0.200g El + 0.210g K6 + 0.200g E5 + 0.210g K14 + 0.210g K2 + 0.187g K16 445. 0.200g E2 + 0.187g K16 + 0.210g K6 + 0.200g E5 + 0.210g K24 + 0.210g K2 446. 1.250g E3 + 1.313g K6 + 0.187g K16 + 1.250g E7 + 1.313g K12 447. 1.250g E4 + 1.313g K6 + 1.250g E7 + 0.187g K16 + 1.313g K7 448. 2.500g El + 2.625g K6 + 2.500g E7 + 2.625g K9 + 0.187g K16 449. 2.500g E2 + 0.187g K16 + 2.625g K6 + 2.500g E7 + 2.625g K13 450. 2.500g E3 + 2.625g K6 + 0.187g K16 + 2.500g E7 + 2.625g K1 451. 1.250g E4 + 1.313g K6 + 1.250g E7 + 0.187g K16 + 1.313g K11 452. 0.250g El + 0.263g K6 + 0.250g E7 + 0.263g K14 + 0.187g K16 453. 2.500g E2 + 0.187g K16 + 2.625g K6 + 2.500g E7 + 2.625g K24 454. 2.500g E3 + 2.625g K6 + 0.187g K16 + 2.500g E7 + 2.625g K2 455. 0.200g E4 + 0.210g K6 + 0.200g E7 + 0.187g K16 + 0.210g K12 + 0.210g K7 456. 2.000g E1 + 2.100g K6 + 2.000g E7 + 2.100g K12 + 0.187g K16 + 2.100g K9 457. 1.000g E2 + 1.050g K6 + 1.000g E7 + 1.050g K12 + 1.050g K13 + 0.187g K16 458. 1.000g E3 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g K12 + 1.050g Kl 459. 1.000g E4 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K12 + 1.050g Kl 1 460. 0.200g E1 + 0.210g K6 + 0.200g E7 + 0.187g K16 + 0.210g K12 + 0.210g K14 461. 0.200g E2 + 0.210g K6 + 0.200g E7 + 0.210g K12 + 0.187g K16 + 0.210g K24 462. 2.000g E3 + 2.100g K6 + 2.000g E7 + 2.100g K12 + 2.100g K2 + 0.187g K16 463. 1.000g E4 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g K7 + 1.050g K9 464. 0.200g El + 0.210g K6 + 0.187g K16 + 0.200g E7 + 0.210g K7 + 0.210g K13 465. 2.000g E2 + 2.100g K6 + 2.000g E7 + 0.187g K16 + 2.100g K7 + 2.100g K1 466. 0.200g E3 + 0.210g K6 + 0.200g E7 + 0.210g K7 + 0.187g K16 + 0.210g K11 467. 1.000g E4 + 1.050g K6 + 1.000g E7 + 1.050g K7 + 1.050g K14 + 0.187g K16 468. 0.200g E1 + 0.187g K16 + 0.210g K6 + 0.200g E7 + 0.210g K8 + 0.210g K24 469. 1.000g E2 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K7 + 1.050g K2 470. 0.200g E3 + 0.210g K6 + 0.200g E7 + 0.187g K16 + 0.210g K9 + 0.210g K13 471. 2.000g E4 + 2.100g K6 + 2.000g E7 + 2.100g K9 + 0.187g K16 + 2.100g K1 472. 0.200g E1 + 0.210g K6 + 0.200g E7 + 0.210g K9 + 0.210g K11 + 0.187g K16 473. 0.200g E2 + 0.187g K16 + 0.210g K6 + 0.200g E7 + 0.210g K9 + 0.210g K14 474. 2.000g E3 + 2.100g K6 + 0.187g K16 + 2.000g E7 + 2.100g K9 + 2.100g K24 475. 0.200gE4+0.210gK6+0.200gE7+0.187gK16+0.210gK9+0.210gK2 476. 0.200g El + 0.210g K6 + 0.200g E7 + 0.210g K13 + 0.187g K16 + 0.210g K1 477. 0.200g E2 + 0.210g K6 + 0.200g E7 + 0.210g K13 + 0.210g Kl 1+ 0.187g K16 478. 1.000g E3 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g K13 + 1.050g K14 479. 1.000g E4 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K13 + 1.050g K24 480. 1.000g El + 1.050g K6 + 1.000g E7 + 0.187g K16 + 1.050g K13 + 1.050g K2 481. 2.000g E2 + 2.100g K6 + 2.000g E7 + 2.100g K1 + 0.187g K16 + 2.100g K11 482. 1.000g E3 + 1.050g K6 + 1.000g E7 + 1.050g K4 + 1.050g K14 + 0.187g K16 483. 1.000g E4 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g Kl + 1.050g K24 484. 0.200g E1 + 0.210g K6 + 0.187g K16 + 0.200g E7 + 0.210g K1 + 0.210g K2 485. 1.000g E2 + 1.050g K6 + 1.000g E7 + 0.187g K16 + 1.050g Kl 1+ 1.050g K14 486. 2.000g E3 + 2.100g K6 + 2.000g E7 + 2.100g K11 + 0.187g K16 + 2.100g K24 487. 1.000g E4 + 1.050g K6 + 1.000g E7 + 1.050g K11 + 1.050g K2 + 0.187g K16 488. 2.000g El + 0.187g K16 + 2.100g K6 + 2.000g E7 + 2.100g K14 + 2.100g K24 489. 1.000g E2 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K14 + 1.050g K2 490. 1.000g E3 + 1.050g K6 + 1.000g E7 + 0.187g K16 + 1.050g K24 + 1.050g K2 491. 3.333g E4 + 3.500g K6 + 3.500g K12 + 0.187g K16 + 0.015g K23 492. 0.250g El + 0.187g K16 + 0.263g K6 + 0.263g K12 + 0.263g K7 493. 2.500g E2 + 2.625g K6 + 0.187g K16 + 2.625g K12 + 2.625g K9 494. 1.250g E3 + 1.313g K6 + 1.313g K12 + 0.187g K16 + 1.313g K13 495. 1.250g E4 + 1.313g K6 + 1.313g K12 + 1.313g K1 + 0.187g K16 496. 1.250g E1 + 0.187g K16 + 1.313g K6 + 1.313g K12 + 1.313g K11 497. 2.500g E2 + 2.625g K6 + 0.187g K16 + 2.625g K12 + 2.625g K14 498. 0.250g E3 + 0.263g K6 + 0.263g K12 + 0.187g K16 + 0.263g K24 499. 2.500g E4 + 2.625g K6 + 2.625g K12 + 2.625g K2 + 0.187g K16 500. 0.200g E1 + 0.187g K16 + 0.210g K6 + 0.210g K12 + 0.210g K7 + 0.210g K9 501. 2.000g E2 + 2.100g K6 + 0.187g K16 + 2.100g K12 + 2.100g K7 + 2.100g K13 502. 1.000g E3 + 1.050g K6 + 1.050g K12 + 0.187g K16 + 1.050g K21 + 1.050g K1 503. 2.000g E4 + 2.100g K6 + 2.100g K12 + 2.100g K7 + 0.187g K16 + 2.100g K11 504. 1.000g E1 + 1.050g K6 + 1.050g K12 + 1.050g K7 + 1.050g K14 + 0.187g K16 505. 2.000g E2 + 0.390g K16 + 2.100g K6 + 2.100g K12 + 2.100g K7 + 2.100g K24 506. 1.000g E3 + 1.050g K6 + 0.390g K16 + 1.050g K12 + 1.050g K7 + 1.050g K2 507. 0.200g E4 + 0.210g K6 + 0.210g K12 + 0.390g K16 + 0.210g K9 + 0.210g K13 508. 2.000g E1 + 2.100g K6 + 2.100g K12 + 2.100g K9 + 0.390g K16 + 2.100g K1 509. 1.000g E2 + 1.050g K6 + 1.050g K12 + 1.050g K9 + 1.050g K11 + 0.390g K16 510. 1.000g E3 + 0.390g K16 + 1.050g K6 + 1.050g K12 + 1.050g K9 + 1.050g K14 511. 0.200g E4 + 0.210g K6 + 0.390g K16 + 0.210g K12 + 0.210g K9 + 0.210g K24 512. 0.200gE1 + 0.210g K6 + 0.210g K12 + 0.390g K16 + 0.210g K9 + 0.210g K2 513. 2.000g E2 + 2.100g K6 + 2.100g K12 + 2.100g K13 + 0.390g K16 + 2.100g Kl 514. 0.200gE3+0.210gK6+0.210gK12+0.210gK13+0.210gK11 +0.390gK16 515. 0.200g E4 + 0.390g K16 + 0.210g K6 + 0.210g K12 + 0.210g K13 +0.210gK14 516. 1.000g E1 + 1.050g K6 + 0.390g K16 + 1.050g K12 + 1.050g K13 + 1.050g K24 517. 1.000g E2 + 1.050g K6 + 1.050g K12 + 0.390g K16 + 1.050g K13 + 1.050g K2 518. 1.000g E3 + 1.050g K6 + 1.050g K12 + 1.050g K1 + 0.390g K16 + 1.050g K11 519. 1.000g E4 + 1.050g K6 + 1.050g K12 + 1.050g K1 + 1.050g K14 + 0.390g K16 520. 2.000g El + 0.390g K16 + 2.100g K6 + 2.100g K12 + 2.100g K1 + 2.100g K24 521. 0.200gE2+0.210gK6+0.390gK16+0.210gK12+0.210gK1 +0.210gK2 522. 2.000g E3 + 2.100g K6 + 2.100g K12 + 0.390g K16 + 2.100g Kl 1+ 2.100g K14 523. 1.000g E4 + 1.050g K6 + 1.050g K12 + 1.050g K11 + 0.390g K16 + 1.050g K24 524. 0.200g E1 + 0.210g K6 + 0.210g K12 + 0.210g K11 + 0.210g K2 + 0.390g K16 525. 2.000g E2 + 0.390g K16 + 2. l00g K6 + 2.100g K12 + 2.100g K14 + 2.100g 526. 1.000g E3 + 1.050g K6 + 0.390g K16 + 1.050g K12 + 1.050g K14 + 1.050g K2 527. 0.200g E4 + 0.210g K6 + 0.210g K12 + 0.390g K16 + 0.210g K24 + 0.210g K2 528. 0.500g El + 0.525g K6 + 0.390g K16 529. 1.667g E2 + 0.390g K16 + 1.750g K6 + 1.750g K8 530. 3.333g E3 + 3.500g K6 + 0.390g K16 + 3.500g K9 531. 1.667g E4 + 1.750g K6 + 1.750g K13 + 0.390g K16 532. 1.667g El + 0.390g K16 + 1.750g K6 + 1.750g K1 533. 3.333gE2+3.500gK6+0.390gK16+3.500gK11 534. 1.667g E3 + 1.750g K6 + 1.750g K14 + 0.390g K16 535. 3.333g E4 + 0.390g K16 + 3.500g K6 + 3.500g K24 536. 3.333g El + 3.500g K6 + 0.390g K16 + 3.500g K2 537. 2.500g E2 + 2.625g K6 + 2.625g K7 + 0.390g K16 + 2.625g K9 538. 0.250g E3 + 0.263g K6 + 0.263g K7 + 0.263g K13 + 0.390g K16 539. 1.250g E4 + 0.390g K16 + 1.313g K6 + 1.313g K7 + 1.313g K1 540. 2.500g El + 2.625g K6 + 0.390g K16 + 2.625g K7 + 2.625g K11 541. 1.250g E2 + 1.313g K6 + 1.313g K7 + 0.390g K16 + 1.313g K14 542. 1.250g E3 + 1.313g K6 + 1.313g K7 + 1.313g K24 + 0.390g K16 543. 2.500g E4 + 0.390g K16 + 2.625g K6 + 2.625g K7 + 2.625g K2 544. 1.250g El + 1.313g K6 + 0.390g K16 + 1.313g K9 + 1.313g K13 545. 1.250g E2 + 1.313g K6 + 1.313g K9 + 0.390g K16 + 1.313g K1 546. 0.250g E3 + 0.263g K6 + 0.263g K9 + 0.263g Kl 1+ 0.390g K16 547. 2.500g E4 + 0.390g K16 + 2.625g K6 + 2.625g K9 + 2.625g K14 548. 2.500g El + 2.625g K6 + 0.390g K16 + 2.625g K9 + 2.625g K24 549. 1.250g E2 + 1.313g K6 + 1.313g K9 + 0.390g K16 + 1.313g K2 550. 1.250g E3 + 1.313g K6 + 1.313g K13 + 1.313g K1 + 0.390g K16 551. 1.250gE4+0.390gK16+1.313gK6+1.313gK13+1.313gK11 552. 1.250gE1+1.313gK6+0.390gK16+1.313gK13+1.313gK14 553. 2.500g E2 + 2.625g K6 + 2.625g K13 + 0.390g K16 + 2.625g K24 554. 2.500g E3 + 2.625g K6 + 2.625g K13 + 2.625g K2 + 0.390g K16 555. 1.250g E4 + 0.390g K16 + 1.313g K6 + 1.313g K1 + 1.313g K11 556. 1.250gE1+1.313gK6+0.390gK16+1.313gK1+1.313gK14 557. 1.250gE2+ 1.313gK6+ 1.313gK1+0.390gK16+ 1.313g K24 + 0.313g K17 558. 0.250g E3 + 0.263g K6 + 0.263g KI + 0.263g K2 + 0.090g K16 + 0.313g K18 559. 1.250g E4 + 0.390g K16 + 1.313g K6 + 1.313g K11 + 1.313g K14 560. 1.250g E1 + 1.313g K6 + 0.390g K16 + 1.313g K11 + 1.313g K24 561. 1.250g E2 + 1.313g K6 + 1.313g K11 + 0.390g K16 + 1.313g K2 562. 2.500g E3 + 2.625g K6 + 2.625g K14 + 2.625g K24 + 0.390g K16 563. 2.500g E4 + 0.390g K16 + 2.625g K6 + 2.625g K14 + 2.625g K2 564. 2.500g El + 2.625g K6 + 0.390g K16 + 2.625g K24 + 2.625g K2 565. 2.000gE2+2.100gK6+2.l00gK7+0.390gK16+2.100gK9+2.100gK13 566. 0.200g E3 + 0.210g K6 + 0.210g K7 + 0.210g K9 + 0.390g K16 + 0.210g K1 567. 2.000g E4 + 2.100g K6 + 2.100g K7 + 2.100g K9 + 2.100g Kl l+ 0.390g K16 568. 2.000g E1 + 0.390g K16 + 2.l00g K6 + 2.100g K7 + 2.100g K9 + 2.100g K14 569. 2.000g E2 + 2.100g K6 + 0.390g K16 + 2.100g K7 + 2.100g K9 + 2.100g K24 570. 0.200g E3 + 0.210g K6 + 0.210g K7 + 0.390g K16 + 0.210g K9 + 0.210g K2 571. 0.200g E4 + 0.210g K6 + 0.210g K7 + 0.210g K13 + 0.390g K16 + 0.210g K1 572. 1.000g El + 1.050g K6 + 1.050g K7 + 1.050g K13 + 1.050g Kl 1+ 0.390g K16 573. 0.200gE2+1.593gK16+0.210gK6+0.210gK21+0.210gK13+0.210gK14 574. 0.200g E3 + 0.210g K6 + 1.593g K16 + 0.210g K7 + 0.210g K13 + 0.210g K24 575. 1.000g E4 + 1.050g K6 + 1.050g K7 + 1.593g K16 + 1.050g K13 + l.050g K2 576. 2.000g E1 + 2.100g K6 + 2.100g K7 + 2.100g K1 + 1.593g K16 + 2.100g K11 577. 1.000g E2 + 1.050g K6 + 1.050g K7 + 1.050g K1 + 1.050g K14 + 1.593g K16 578. 2.000g E3 + 1.593g K16 + 2.100g K6 + 2.100g K7 + 2.100g K1 + 2.100g K24 579. 2.000g E4 + 2.100g K6 + 1.593g K16 + 2.100g K8 + 2.100g K1 + 2.100g K2 580. 0.200g E1 + 0.210g K6 + 0.210g K7 + 1.593g K16 + 0.210g K11 + 0.210g K14 581. 1.000g E2 + 1.050g K6 + 1.050g K7 + 1.050g Kl 1+ 1.593g K16 + 1.050g K24 582. 1.000g E3 + 1.050g K6 + 1.050g K7 + 1.050g K11 + 1.050g K2 + 1.593g K16 583. 2.000g E4 + 1.593g K16 + 2.100g K6 + 2.100g K7 + 2.100g K14 + 2.100g K24 584. 0.200gE11 +0.210gK6+ 1.593gK16+0.210gK7+0.210gK14+0.210gK2 585. 2.000g E2 + 2.100g K6 + 2.100g K7 + 1.593g K16 + 2.100g K24 + 2.100g K2 586. 1.000g E3 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.593g K16 + 1.050g K1 587. 1.000g E4 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.050g K11 + 1.593g K16 588. 1.000g El + 1.593g K16 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.050g K14 589. 0.200g E2 + 0.210g K6 + 1.593g K16 + 0.210g K9 + 0.210g K13 + 0.210g K24 590. 2.000g E3 + 2.100g K6 + 2.100g K9 + 1.593g K16 + 2.100g Kl3 + 2.100g K2 591. 2.000g E4 + 2.100g K6 + 2.100g K9 + 2.100g Kl + 1.593g K16 + 2.100g K11 592. 2.000g E1 + 2.100g K6 + 2.100g K9 + 2.100g Kl + 2.100g K14 + 1.593g Kl6 593. 0.200g E2 + 1.593g K16 + 0.2l0g K6 + 0.2lOg K9 + 0.210g K1 + 0.2lOg K24 594. 0.200g E3 + 0.210g K6 + 1.593g K16 + 0.210g K9 + 0.210g K1 + 0.210g K2 595. 2.000g E4 + 2.100g K6 + 2.100g K9 + 1.593g K16 + 2.100g Kl 1+ 2.100g K14 596. 2.000g E1 + 2.100g K6 + 2.100g K9 + 2.100g Kl l+ 1.593g K16 + 2.100g K24 597. 0.200gE2+0.210gK6+0.210gK9+0.210gK11 + 0.210g K2 + 1.593gK16 598. 2.000g E3 + 1.593g K16 + 2.100g K6 + 2.100g K9 + 2.100g K14 + 2.100g K24 599. 1.000g E4 + 1.050g K6 + 1.593g K16 + 1.050g K9 + 1.050g K14 + 1.050g K2 600. 1.000g El + 1.050g K6 + 1.050g K9 + 1.593g K16 + 1.050g K24 + 1.050g K2 601. 2.000g E2 + 2.100g K6 + 2.100g K13 + 2.100g K1 + 1.593g K16 + 2.100g K11 602. 0.200gE3+0.210gK6+0.210gK13+0.210gK1 +0.210gK14+ 1.593gK16 603. 1.000g E4 + 1.593g K16 + 1.050g K6 + 1.050g K13 + 1.050g Kl + 1.050g K24 604. 1.000g El + 1.050g K6 + 1.593g K16 + 1.050g K13 + 1.050g K1 + 1.050g K2 605. 2.000g E2 + 2.100g K6 + 2.100g K13 + 1.593g K16 + 2.100g K11 + 2.100g K14 606. 0.200g E3 + 0.210g K6 + 0.210g K13 + 0.210g K11 + 1.593g K16 + 0.210g K24 607. 2.000g E4 + 2.100g K6 + 2.l00g K13 + 2.100g K11 + 2.100g K2 + 1.593g K16 608. 0.200g El + 1.593g K16 + 0.210g K6 + 0.210g K13 + 0.210g K14 + 0.210g K24 609. 0.200g E2 + 0.2lOg K6 + 1.593g K16 + 0.210g K13 + 0.210g K14 + 0.2l0g K2 610. 2.000g E3 + 2.100g K6 + 2.100g K13 + 1.593g K16 + 2.100g K24 + 2.100g K2 611. 0.200gE4+0.210gK6+0.210gK1+0.210gK11+1.593gK16+0.210gK14 612. 1.000g El + l.050g K6 + 1.050g K1 + 1.050g K11 + 1.050g K24 + 1.593g K16 613. 0.200gE2+1.593gK16+0.210gK6+0.210gK1+0.210gKl1 +0.210gK2 614. 1.000g E3 + 1.050g K6 + 1.593g K16 + 1.050g K1 + 1.050g K14 + 1.050g K24 615. 2.000g E4 + 2.100g K6 + 2.100g K1 + 1.593g K16 + 2.100g K14 + 2.100g K2 616. 1.000g El + l.050g K6 + 1.050g Kl + 1.050g K24 + 1.593g K16 + 1.050g K2 617. 1.000g E2 + 1.050g K6 + l.050g K1 l+ 1.050g K14 + l.050g K24 + 1.593g K16 618. 1.000g E3 + 1.593g K16 + 1.050g K6 + l.050g Kl l+ 1.050g Kl4 + l.050g K2 1 619. 1.000g E4 + 1.050g K6 + 1.593g K16 + 1.050g K11 + 1.050g K24 + 1.050g 620. 0.200gE1 + 0.210g K6 + 0.210g K14 + 1.593g K16 + 0.210g K24 + 0.210g K2 621. 2.500g E2 + 2.625g K7 + 2.500g E8 + 2.625g K12 + 1.593g K16 622. 2.500g E3 + 1.593g K16 + 2.625g K8 + 2.500g E8 + 2.625g K6 623. 2.500g E4 + 2.625g K7 + 1.796g K16 + 2.500g E8 + 2.625g K9 624. 2.500g E1 + 2.625g K7 + 2.500g E8 + 1.796g K16 + 2.625g K13 625. 1.250g E2 + 1.313g K7 + 1.250g E8 + 1.313g K1 + 1.796g K16 626. 0.250g E3 + 1.796g K16 + 0.263g K7 + 0.250g E8 + 0.263g K11 627. 2.500g E4 + 2.625g K7 + 1.796g K16 + 2.500g E8 + 2.625g K14 628. 1.250g E1 + 1.313g K7 + 1.250g E8 + 1.796g K16 + 1.313g K24 629. 0.250g E2 + 0.263g K7 + 0.250g E8 + 0.263g K2 + 1.796g K16 630. 1.000g E3 + 1.796g K16 + 1.050g K21 + 1.000g E8 + 1.050g K12 + 1.050g K6 631. 2.000g E4 + 2.100g K7 + 1.796g K16 + 2.000g E8 + 2.100g K12 + 2.100g K9 632. 0.200g El + 0.210g K7 + 0.200g E8 + 1.796g K16 + 0.210g K12 + 0.210g K13 633. 2.000g E2 + 2.100g K7 + 2.000g E8 + 2.100g K12 + 1.796g K16 + 2.100g Kl 634. 2.000g E3 + 2.100g K7 + 2.000g E8 + 2.100g K12 + 2.100g K11 + 1.796g K16 635. 0.200g E4 + 1.796g K16 + 0.210g K7 + 0.200g E8 + 0.210g K12 + 0.210g K14 636. 0.200g E1 + 0.210g K7 + 1.796g K16 + 0.200g E8 + 0.210g K12 + 0.210g K24 637. 0.200g E2 + 0.210g K8 + 0.200g E8 + 1.796g K16 + 0.210g K12 + 0.210g K2 638. 0.200g E3 + 0.210g K7 + 0.200g E8 + 0.210g K6 + 1.796g K16 + 0.210g K9 639. 2.000g E4 + 2.100g K7 + 2.000g E8 + 2.100g K6 + 2.100g K13 + 1.796g K16 640. 1.000g E1 + 1.796g K16 + 1.050g K7 + 1.000g E8 + 1.050g K6 + 1.050g Kl 641. 1.000g E2 + 1.050g K7 + 1.796g K16 + 1.000g E8 + l.050g K6 + l.050g K11 642. 0.200g E3 + 0.210g K7 + 0.200g E8 + 1.796g K16 + 0.210g K6 + 0.210g K14 643. 1.000g E4 + 1.050g K7 + 1.000g E8 + 1.050g K6 + 1.796g K16 + 1.050g K24 644. 2.000g E 1+ 2.100g K7 + 2.000g E8 + 2.100g K6 + 2.100g K2 + 1.796g K 16 645. 0.200g E2 + 1.796g K16 + 0.210g K7 + 0.200g E8 + 0.210g K9 + 0.210g K22 646. 2.000g E3 + 2.100g K7 + 1.796g K16 + 2.000g E8 + 2.100g K9 + 2.l00g Kl 647. 2.000g E4 + 2.100g K7 + 2.000g E8 + 1.796g K16 + 2.100g K9 + 2.100g K11 648. 1.000g El + 1.050g K7 + 1.000g E8 + 1.050g K9 + 1.796g K16 + 1.050g K14 649. 1.000g E2 + 1.050g K7 + 1.000g E8 + 1.050g K9 + 1.050g K24 + 1.796g K16 650. 1.000g E3 + 1.796g K16 + 1.050g K7 + 1.000g E8 + 1.050g K9 + 1.050g K2 651. 0.200g E4 + 0.210g K21 + 1.796g K16 + 0.200g E8 + 0.210g K13 + 0.210g Kl 652. 1.000g El + 1.050g K7 + 1.000g E8 + 1.796g K16 + 1.050g K13 + 1.050g K11 653. 0.200g E2 + 0.210g K7 + 0.200g E8 + 0.210g K13 + 1.796g K16 + 0.210g K14 654. 0.200g E3 + 0.210g K7 + 0.200g E8 + 0.210g K13 + 0.210g K24 + 1.796g K16 655. 1.000g E4 + 1.796g K16 + 1.050g K7 + 1.000g E8 + 1.050g K13 + 1.050g K2 656. 0.200g El + 0.210g K7 + 1.796g K16 + 0.200g E8 + 0.210g Kl + 0.210g Kl 1 657. 1.000g E2 + 1.050g K7 + 1.000g E8 + 1.796g K16 + 1.050g K1 + 1.050g K14 658. 1.000g E3 + 1.050g K7 + 1.000g E8 + 1.050g K1 + 1.796g K16 + 1.050g K24 659. 2.000g E4 + 2.100g K8 + 2.000g E8 + 2.100g K1 + 2.100g K2 + 1.796g K16 660. 2.000g El + 1.796g K16 + 2.100g K7 + 2.000g E8 + 2.100g K11 + 2.100g K14 661. 1.000g E2 + 1.050g K7 + 1.796g K16 + 1.000g E8 + 1.050g K11 + 1.050g K24 662. 1.000g E3 + 1.050g K7 + 1.000g E8 + 1.796g K16 + 1.050g Kl 1+ 1.050g K2 663. 1.000g E4 + 1.050g K7 + 1.000g E8 + 1.050g K14 + 1.796g K16 + 1.050g K24 664. 1.000g El + 1.050g K7 + 1.000g E8 + 1.050g K14 + 1.050g K2 + 1.796g K16 665. 2.000g E2 + 1.796g K16 + 2. l00g K7 + 2.000g E8 + 2.100g K24 + 2.100g K2 666. 1.250g E11 + 1.313g K7 + 1.796g K16 + 1.250g E6 + 1.313g K12 667. 2.500g E10 + 2.625g K7 + 2.500g E6 + 1.796g K16 + 2.625g K6 668. 0.250g El + 0.263g K7 + 0.250g E6 + 0.263g K9 + 1.796g K16 669. 2.500g E2 + 1.796g K16 + 2.625g K7 + 2.500g E6 + 2.625g K13 670. 2.500g E3 + 2.625g K7 + 1.796g K16 + 2.500g E6 + 2.625g Kl 671. 0.250g E4 + 0.263g K7 + 0.250g E6 + 1.796g K16 + 0.263g K11 672. 0.250g El + 0.263g K21 + 0.250g E6 + 0.263g K14 + 1.796g K16 673. 2.500g E2 + 1.796g K16 + 2.625g K7 + 2.500g E6 + 2.625g K24 674. 0.250g E3 + 0.263g K7 + 1.796g K16 + 0.250g E6 + 0.263g K2 675. 0.200g E4 + 0.210g K7 + 0.200g E6 + 1.796g K16 + 0.210g K12 + 0.210g K6 676. 0.200gE1+0.210g1(7+0.200gE6+0.210gK12+1.796gK16+0.210gK9 677. 2.000g E2 + 2.100g K7 + 2.000g E6 + 2.100g K12 + 2.100g K13 + 1.796g K16 678. 1.000g E3 + 1.796g K16 + 1.050g K7 + 1.000g E6 + 1.050g K12 + 1.050g K1 679. 0.200g E4 + 0.210g K8 + 1.796g K16 + 0.200g E6 + 0.210g K12 + 0.210g 1(11 680. 0.200g El + 0.210g K7 + 0.200g E6 + 1.796g K16 + 0.210g K12 + 0.210g K14 681. 1.000g E2 + 1.050g K7 + 1.000g E6 + 1.050g K12 + 1.796g K16 + 1.050g K24 682. 0.200g E3 + 0.210g K8 + 0.200g E6 + 0.210g K12 + 0.210g K2 + 1.796g K16 683. 1.000g E4 + 1.796g K16 + 1.050g K7 + 1.000g E6 + 1.050g K6 + 1.050g K9 684. 1.000g E1 + 1.050g K7 + 1.796g K16 + 1.000g E6 + 1.050g K6 + 1.050g K13 685. 0.200g E2 + 0.210g K7 + 0.200g E6 + 1.796g K16 + 0.210g K6 + 0.210g K1 686. 0.200g E3 + 0.210g K7 + 0.200g E6 + 0.210g K6 + 1.796g K16 + 0.210g K11 687. 0.200g E4 + 0.210g K7 + 0.200g E6 + 0.210g K6 + 0.210g K14 + 1.796g K16 688. 2.000g El + 1.796g K16 + 2.100g K7 + 2.000g E6 + 2.100g K6 + 2.100g K24 689. 0.200g E2 + 0.210g K7 + 1.796g K16 + 0.200g E6 + 0.210g K6 + 0.210g K2 690. 1.000g E3 + 1.050g K7 + 1.000g E6 + 1.796g K16 + 1.050g K9 + 1.050g K13 691. 0.200g E4 + 0.210g K7 + 0.200g E6 + 0.210g K9 + 1.999g K 16 + 0.210g K 1 692. 0.200g E 1+ 0.210g K7 + 0.200g E6 + 0.210g K9 + 0.210g K 11 + 1.999g K16 693. 0.200g E2 + 1.999g K16 + 0.210g K7 + 0.200g E6 + 0.210g K9 + 0.210g K14 694. 0.200g E 10 + 0.210g K21 + 1.999g K 16 + 0.200g E6 + 0.210g K9 + 0.210g 695. 1.000g E4 + 1.050g K7 + 1.000g E6 + 1.999g K16 + 1.050g K9 + 1.050g K2 696. 0.200g El + 0.210g K7 + 0.200g E6 + 0.210g K13 + 1.999g K16 + 0.210g K1 697. 1.000g E2 + 1.050g K7 + 1.000g E6 + 1.050g K13 + 1.050g K11 + 1.999g K16 698. 2.000g E3 + 1.999g K16 + 2.100g K8 + 2.000g E6 + 2.100g K13 + 2.100g K14 699. 2.000g E4 + 2.100g K7 + 1.999g K16 + 2.000g E6 + 2.100g K13 + 2.100g K24 700. 1.000g E1 + 1.050g K7 + 1.000g E6 + 1.999g K16 + 1.050g K13 + 1.050g K2 701. 0.200g E2 + 0.210g K7 + 0.200g E6 + 0.210g K1 + 1.999g K16 + 0.210g K11 702. 0.200g E3 + 0.210g K7 + 0.200g E6 + 0.210g K1 + 0.210g K14 + 1.999g K16 703. 1.000g E4 + 1.999g K16 + 1.050g K7 + 1.000g E6 + 1.050g Kl + 1.050g K24 704. 0.200g E1 + 0.210g K7 + 1.999g K16 + 0.200g E6 + 0.210g K1 + 0.210g K2 705. 1.0009 E2 + 1.050g K8 + 1.000g E6 + 1.999g K16 + 1.050g K11 + 1.050g K14 706. 0.200g E3 + 0.210g K7 + 0.200g E6 + 0.210g Kl 1 + 1.999g K16 + 0.210g K24 707. 1.000g E4 + 1.050g K7 + 1.000g E6 + 1.050g K11 + 1.050g K2 + 1.999g K16 708. 0.200g E1 + 1.999g K16 + 0.210g K7 + 0.200g E6 + 0.210g K14 + 0.210g K24 709. 2.000g E2 + 2.100g K7 + 1.999g K16 + 2.000g E6 + 2.100g K14 + 2.l00g K2 710. 2.000g E3 + 2.100g K7 + 2.000g E6 + 1.999g K16 + 2.100g K24 + 2.100g K2 711. 0.250g E4 + 0.263g K7 + 0.250g E5 + 0.263g K12 + 1.999g K16 712. 1.250g E1 + 1.999g K16 + 1.313g K7 + 1.250g E5 + 1.313g K6 713. 0.250g E2 + 0.263g K7 + 1.999g K16 + 0.250g E5 + 0.263g K9 714. 0.250g E3 + 0.263g K7 + 0.250g E5 + 1.999g K16 + 0.263g K13 715. 0.250g E4 + 0.263g K7 + 0.250g E5 + 0.263g K1 + 1.999g K16 716. 0.250g El + 1.999g K16 + 0.263g K21 + 0.250g E5 + 0.263g K11 717. 2.500g E2 + 2.625g K7 + 1.999g K16 + 2.500g E5 + 2.625g K14 718. 0.250g E3 + 0.263g K7 + 0.250g E5 + 1.999g K16 + 0.263g K24 719. 2.500g E4 + 2.625g K7 + 2.500g E5 + 2.625g K2 + 1.999g K16 720. 2.000g E1 + 1.999g K16 + 2.100g K7 + 2.000g E5 + 2.100g K12 + 2.100g K6 721. 2.000g E2 + 2.100g K7 + 1.999g K16 + 2.000g E5 + 2.100g K12 + 2.100g K9 722. 0.200g E3 + 0.210g K7 + 0.200g E5 + 1.999g K16 + 0.210g K12 + 0.210g K13 723. 0.200g E4 + 0.210g K7 + 0.200g E5 + 0.210g K12 + 1.999g K16 + 0.210g K1 724. 2.000g E1 + 2.100g K7 + 2.000g E5 + 2.100g K12 + 2.100g Kl 1+ 0.009g K17 +
1.999g K16 725. 1.000g E2 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K12 + 1.050g K14 726. 1.000g E3 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K12 + 1.050g K24 727. 2.000g E4 + 2.100g K8 + 2.000g E5 + 1.999g K16 + 2.100g K12 + 2.100g K2 728. 2.000g El + 2.100g K7 + 2.000g E5 + 2.100g K6 + 1.999g K16 + 2.100g K9 729. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K6 + 2.100g K13 + 1.999g K16 730. 1.000g E3 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K6 + 1.050g Kl 731. 1.000g E4 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K6 + 1.050g K11 732. 0.200g El + 0.210g K7 + 0.200g E5 + 2.009g K16 + 0.210g K6 + 0.210g K14 733. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K6 + 1.999g K16 + 2.100g K24 734. 2.000g E3 + 2.100g K7 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 1.999g K16 735. 1.000g E4 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K9 + 1.050g K13 736. 1.000g El + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K9 + 0.050g K17 737. 2.000g E2 + 2.100g K8 + 2.000g E5 + 1.999g K16 + 2.100g K9 + 2.100g K11 738. 0.200g E3 + 0.210g K21 + 0.200g E5 + 0.210g K9 + 1.999g K16 + 0.210g K14 739. 2.000g E4 + 2.100g K7 + 2.000g E5 + 2.100g K9 + 2.100g K24 + 1.999g K16 740. 0.200g E1 + 1.999g K16 + 0.210g K7 + 0.200g E5 + 0.210g K9 + 0.210g K2 741. 1.000g E2 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K13 + 1.050g K1 742. 0.200g E3 + 0.210g K7 + 0.200g E5 + 1.999g K16 + 0.210g K13 + 0.210g K11 743. 0.200g E4 + 0.210g K7 + 0.200g E5 + 0.210g K13 + 1.999g K16 + 0.210g K14 744. 1.000g El + 1.050g K7 + 1.000g E5 + 1.050g K13 + 1.050g K24 + 1.999g K16 745. 1.000g E2 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K13 + 1.050g K2 746. 1.000g E3 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K1 + 1.050g Kl 1 747. 1.000g E4 + 1.050g K7 + 1.000g E5 + 1.999g K16 + 1.050g Kl + 1.050g K14 748. 1.000g El + 1.050g K7 + 1.000g E5 + 1.050g Kl + 1.999g K16 + 1.050g K24 749. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K1 + 2.100g K2 + 1.999g K16 750. 0.200g E3 + 1.999g K16 + 0.210g K8 + 0.200g E5 + 0.210g K11 + 0.210g K14 751. 2.000g E4 + 2.100g K7 + 0.202g K16 + 2.000g E5 + 2. l00g Kl 1+ 2.100g K24 752. 2.000g E1 + 2.100g K7 + 2.000g E5 + 0.202g K16 + 2.100g K11 + 2.100g K2 753. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K14 + 0.202g K16 + 2.100g K24 754. 1.000g E3 + 1.050g K7 + 1.000g E5 + 1.050g K14 + 1.050g K2 + 0.202g K16 755. 1.000g E4 + 0.202g K16 + 1.050g K7 + 1.000g E5 + 1.050g K24 + 1.050g K2 756. 0.250g El + 0.263g K7 + 0.202g K16 + 0.250g E7 + 0.263g K12 757. 2.500g E2 + 2.625g K7 + 2.500g E7 + 0.202g K16 + 2.625g K6 758. 0.250g E3 + 0.263g K7 + 0.250g E7 + 0.263g K9 + 0.202g K16 759. 2.500g E4 + 0.202g K16 + 2.625g K21 + 2.500g E7 + 2.625g K13 760. 2.500g El + 2.625g K7 + 0.202g K16 + 2.500g E7 + 2.625g Kl 761. 0.250g E2 + 0.263g K7 + 0.250g E7 + 0.202g K16 + 0.263g K11 762. 2.500g E3 + 2.625g K7 + 2.500g E7 + 2.625g K14 + 0.202g K16 763. 2.500g E4 + 0.202g K16 + 2.625g K7 + 2.500g E7 + 2.625g K24 764. 0.250g El + 0.263g K7 + 0.202g K16 + 0.250g E7 + 0.263g K2 765. 2.000g E2 + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K12 + 2.100g K6 766. 0.200g E3 + 0.210g K7 + 0.200g E7 + 0.210g K12 + 0.202g K16 + 0.210g K9 767. 2.000g E4 + 2.100g K7 + 2.000g E7 + 2.100g K12 + 2.100g K13 + 0.202g K16 768. 2.000g E1 + 0.202g K16 + 2.100g K7 + 2.000g E7 + 2.100g K12 + 2.100g K1 769. 1.000g E2 + 1.050g K7 + 0.202g K16 + 1.000g E7 + 1.050g K12 + 1.050g K11 770. 1.000g E3 + 1.050g K7 + 1.000g E7 + 0.202g K16 + 1.050g K12 + 1.050g K14 771. 1.000g E4 + 1.050g K7 + 1.000g E7 + 1.050g K12 + 0.202g K16 + 1.050g K24 772. 2.000g E 1+ 2.100g K8 + 2.000g E7 + 2.100g K12 + 2.100g K2 + 0.202g K16 773. 0.2009 E2 + 0.202g K16 + 0.210g K7 + 0.200g E7 + 0.210g K6 + 0.210g K9 774. 1.000g E3 + 1.050g K7 + 0.202g K16 + 1.000g E7 + 1.050g K6 + 1.050g K13 775. 1.000g E4 + 1.050g K7 + 1.000g E7 + 0.202g K16 + 1.050g K6 + 1.050g Kl 776. 2.000g E1 + 2.100g K7 + 2.000g E7 + 2.100g K6 + 0.202g K16 + 2.100g K11 777. 0.200g E2 + 0.210g K7 + 0.200g E7 + 0.210g K6 + 0.210g K14 + 0.202g K16 778. 1.000g E3 + 0.202g K16 + 1.050g K7 + 1.000g E7 + 1.050g K6 + 1.050g K24 779. 1.000g E4 + 1.050g K7 + 0.202g K16 + 1.000g E7 + 1.050g K6 + 1.050g K2 780. 0.200g E1 + 0.210g K21 + 0.200g E7 + 0.202g K16 + 0.210g K9 + 0.210g K13 781. 2.000g E2 + 2.100g K7 + 2.000g E7 + 2.100g K9 + 0.202g K16 + 2.100g Kl 782. 1.000g E3 + 1.050g K7 + 1.000g E7 + 1.050g K9 + 1.050g K11 + 0.202g K16 783. 2.000g E4 + 0.202g K16 + 2. l00g K7 + 2.000g E7 + 2.l00g K9 + 2.l00g K14 784. 0.200g E1 + 0.210g K7 + 0.202g K16 + 0.200g E7 + 0.210g K9 + 0.210g K24 785. 1.000g E2 + 1.050g K7 + 1.000g E7 + 0.202g K16 + 1.050g K9 + 1.050g K2 786. 1.000g E3 + 1.050g K7 + 1.000g E7 + 1.050g K13 + 0.202g K16 + 1.050g K1 787. 1.000g E4 + 1.050g K7 + 1.000g E7 + 1.050g K13 + 1.050g K11 + 0.202g K16 788. 2.000g El + 0.202g K16 + 2.100g K7 + 2.000g E7 + 2.100g K13 + 2.100g K14 789. 0.200g E2 + 0.210g K7 + 0.202g K16 + 0.200g E7 + 0.210g K13 + 0.210g K24 790. 2.000g E3 + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K13 + 2.100g K2 791. 2.000g E4 + 2.100g K7 + 2.000g E7 + 2.100g Kl + 0.202g K16 + 2.100g K11 792. 2.000g E1 + 2.100g K7 + 2.000g E7 + 2.100g Kl + 2.100g K14 + 0.202g K16 793. 1.000g E2 + 0.202g K16 + 1.050g K7 + 1.000g E7 + 1.050g Kl + 1.050g K24 794. 0.200g E3 + 0.210g K8 + 0.202g K16 + 0.200g E7 + 0.210g K1 + 0.210g K2 795. 2.000g E4 + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K11 + 2.100g K14 796. 1.000g E1 + 1.050g K7 + 1.000g E7 + 1.050g K11 + 0.202g K16 + 1.050g K24 797. 0.200g E2 + 0.210g K7 + 0.200g E7 + 0.210g Kl 1+ 0.210g K2 + 0.202g K16 798. 1.000g E3 + 0.202g K16 + 1.050g K7 + 1.000g E7 + 1.050g K14 + 1.050g K24 799. 0.200g E4 + 0.210g K7 + 0.202g K16 + 0.200g E7 + 0.210g K14 + 0.210g K2 800. 2.000g El + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K24 + 2.100g K2 801. 3.333g E2 + 3.500g K21 + 3.500g K12 + 0.202g K16 802. 1.250g E3 + 0.202g K16 + 1.313g K7 + 1.313g K12 + 1.313g K6 803. 1.250g E4 + 1.313g K7 + 0.202g K16 + 1.313g K12 + 1.313g K9 804. 0.250g El + 0.263g K7 + 0.263g K12 + 0.202g K16 + 0.263g K13 805. 1.250g E2 + 1.313g K7 + 1.313g K12 + 1.313g K1 + 0.202g K16 806. 1.250g E3 + 0.202g K16 + 1.313g K7 + 1.313g K12 + 1.313g K11 807. 2.500g E4 + 2.625g K7 + 0.202g K16 + 2.625g K12 + 2.625g K14 808. 0.250g El + 0.263g K8 + 0.263g K12 + 0.202g K16 + 0.263g K24 809. 1.250g E2 + 1.313g K7 + 1.313g K12 + 1.313g K5 + 0.202g K16 810. 0.200gE3 +0.202gK16+0.210gK7+0.210gK12+0.210gK6+0.210gK9 811. 2.000g E4 + 2.100g K7 + 0.202g K16 + 2.100g K12 + 2.100g K6 + 2.100g K13 812. 1.000g El + 1.050g K7 + 1.050g K12 + 0.202g K16 + 1.050g K6 + 1.050g Kl 813. 2.000g E2 + 2.100g K7 + 2.l00g K12 + 2.100g K6 + 0.202g K16 + 2.100g K11 814. 0.200gE3 +0.210gK7+0.210gK12+0.210gK6+0.210gK14+0.202gK16 815. 0.200g E4 + 0.202g K16 + 0.210g K7 + 0.210g K12 + 0.210g K6 + 0.210g K24 816. 2.000g E 1+ 2.100g K7 + 0.202g K16 + 2.100g K12 + 2.100g K6 + 2.100g K2 817. 1.000g E2 + 1.050g K8 + 1.050g K12 + 0.202g K16 + 1.050g K9 + 1.050g K13 818. 1.000g E3 + 1.050g K7 + 1.050g K12 + 1.050g K9 + 0.202g K16 + 1.050g Ki 819. 2.000g E4 + 2.100g K7 + 2.100g K12 + 2.100g K9 + 2.100g K11 + 0.405g K16 820. 1.000g El + 0.405g K16 + 1.050g K7 + 1.050g K12 + 1.050g K9 + 1.050g K14 821. 0.200g E2 + 0.210g K7 + 0.405g K16 + 0.210g K12 + 0.210g K9 + 0.210g K24 822. 2.000g E3 + 2.100g K7 + 2.100g K12 + 0.405g K16 + 2.100g K9 + 2.100g K2 823. 0.200g E4 + 0.210g K21 +0.210gK12+0.210gK13+0.405gK16+0.210gK1 824. 2.000g E1 + 2.100g K7 + 2.100g K12 + 2.100g K13 + 2.100g K11 + 0.405g K16 825. 0.200g E2 + 0.405g K16 + 0.210g K7 + 0.210g K12 + 0.210g K13 + 0.210g K14 826. 0.200g E3 + 0.210g K7 + 0.405g K16 + 0.210g K12 + 0.210g K13 + 0.210g K24 827. 0.200gE4+0.210gK7+0.2lOgK12+0.405gK16+0.210gK13+0.210gK2 828. 0.200gE1 +0.210gK7+0.210gK12+0.210gK1 +0.405gK16+0.210gK11 829. 2.000g E2 + 2.100g K7 + 2.100g K12 + 2.l00g K1 + 2.100g K14 + 0.405g K16 830. 2.000g E3 + 0.405g K16 + 2.100g K7 + 2.100g K12 + 2.100g K1 + 2.100g K24 831. 0.200gE4+0.210gK7+0.405gK16+0.210gK12+0.210gK1 +0.210gK2 832. 0.200g E1 + 0.210g K7 + 0.210g K12 + 0.405g K16 + 0.210g Kl 1+ 0.210g K14 833. 0.200gE2+0.2lOgK7+0.210gK12+0.210gK11 +0.405gK16+0.210gK24 834. 2.000g E3 + 2.100g K7 + 2.100g K12 + 2.100g Kl l+ 2.100g K2 + 0.405g K16 835. 2.000g E4 + 0.405g K16 + 2.100g K7 + 2.100g K12 + 2.100g K14 + 2.100g K24 836. 2.000g El + 2.100g K7 + 0.405g K16 + 2.100g K12 + 2.100g K14 + 2.100g K2 837. 2.000g E2 + 2.100g K7 + 2.100g K12 + 0.405g K16 + 2.100g K24 + 2.100g K2 838. 3.333g E3 + 3.500g K7 + 3.500g K6 + 0.405g K16 839. 0.250g E4 + 0.405g K16 + 0.263g K8 + 0.263g K6 + 0.263g K9 840. 2.500g El + 2.625g K7 + 0.405g K16 + 0.625g K3 + 2.625g K6 + 2.625g K13 841. 0.250g E2 + 0.263g K7 + 0.263g K6 + 0.405g K16 + 0.263g K19 842. 0.250g E3 + 0.263g K7 + 0.263g K6 + 0.263g K11 + 0.405g K16 843. 2.500g E4 + 0.405g K16 + 2.625g K7 + 2.625g K6 + 2.625g K14 844. 0.250g El + 0.263g K21 + 0.405g K16 + 0.263g K6 + 0.263g K24 845. 0.250g E2 + 0.263g K7 + 0.263g K6 + 0.405g K16 + 0.263g K2 846. 2.000g E3 + 2.100g K7 + 2.100g K6 + 2.100g K9 + 0.405g K16 + 2.100g K13 847. 2.000g E4 + 2.100g K7 + 2.100g K6 + 2.100g K9 + 2.100g K1 + 0.405g K16 848. 1.000g El + 0.405g K16 + 1.050g K7 + 1.050g K6 + 1.050g K9 + 1.050g K11 849. 2.000g E2 + 2.100g K7 + 0.405g K16 + 2.100g K6 + 2.100g K9 + 2.100g K14 850. 1.000g E3 + 1.050g K7 + 1.050g K6 + 0.405g K16 + 1.050g K9 + 1.050g K24 851. 1.000g E4 + 1.050g K7 + 1.050g K6 + 1.050g K9 + 0.405g K16 + 1.050g K2 852. 0.200g El + 0.210g K7 + 0.210g K6 + 0.210g K13 + 0.210g Kl + 0.405g K16 853. 2.000g E2 + 0.405g K16 + 2.100g K7 + 2.100g K6 + 2.100g K13 + 2.100g K11 854. 2.000g E3 + 2.100g K7 + 0.405g K16 + 2.100g K6 + 2.100g K13 + 2.100g K14 855. 1.000g E4 + 1.050g K7 + 1.050g K6 + 0.405g K16 + 1.050g K13 + 1.050g K24 856. 2.000g El + 2.100g K7 + 2.100g K6 + 2.100g K13 + 0.405g K16 + 2.100g K2 857. 2.000g E2 + 2.100g K7 + 2.100g K6 + 2.100g K1 + 2.100g K11 + 0.405g K16 858. 2.000g E3 + 0.405g K16 + 2.100g K7 + 2.100g K6 + 2.100g Kl + 2.100g K14 859. 2.000g E4 + 2.100g K7 + 0.405g K16 + 2.100g K6 + 2.100g Kl + 2.100g K24 860. 0.200g El + 0.210g K7 + 0.210g K6 + 0.405g K16 + 0.210g KI + 0.210g K2 861. 0.200g E2 + 0.210g K8 + 0.210g K6 + 0.210g K11 + 0.405g K16 + 0.210g K14 862. 1.000g E3 + 1.050g K7 + 1.050g K6 + 1.050g K11 + 1.050g K24 + 0.405g K16 863. 1.000g E4 + 0.405g K16 + 1.050g K7 + 1.050g K6 + 1.050g K11 + 1.050g K2 864. 1.000g El + 1.050g K7 + 0.405g K16 + 1.050g K6 + 1.050g K14 + 1.050g K24 865. 0.200g E2 + 0.210g K21 + 0.210g K6 + 0.405g K16 + 0.210g K14 + 0.210g K2 866. 1.000g E3 + 1.050g K7 + 1.050g K6 + 1.050g K24 + 0.405g K16 + 1.050g K2 867. 0.500g El + 0.525g K7 + 0.405g K16 + 0.040g K17 + 0.045g K18 868. 1.667g El + 0.405g K16 + 1.750g K7 + 1.750g K9 869. 1.667g E2 + 1.750g K7 + 0.405g K16 + 1.750g K13 870. 3.333g E3 + 3.500g K7 + 3.500g K1 + 0.405g K16 871. 3.333g E4 + 0.405g K16 + 3.500g K7 + 3.500g K11 872. 3.333g El + 3.500g K7 + 0.405g K16 + 3.500g K14 873. 0.333g E2 + 0.350g K7 + 0.350g K24 + 0.405g K16 874. 0.333g E3 + 0.405g K16 + 0.350g K7 + 0.350g K2 875. 2.500g E4 + 2.625g K7 + 0.405g K16 + 2.625g K9 + 2.625g K13 876. 1.250gE1+1.313gK7+1.313gK9+0.405gK16+1.313gK1 877. 0.250g E2 + 0.263g K7 + 0.263g K9 + 0.263g K11 + 0.405g K16 878. 0.250g E3 + 0.405g K16 + 0.263g K7 + 0.263g K9 + 0.263g K14 879. 1.250gE4+ 1.313g K7 + 0.405g K16 + 1.313g K9 + 1.313g K24 880. 0.250g El + 0.263g K7 + 0.263g K9 + 0.405g K16 + 0.263g K2 881. 1.250gE2+1.313gK7+1.313gK13+1.313gK1+0.405gK16 882. 2.500g E3 + 0.405g K16 + 2.625g K7 + 2.625g K13 + 2.625g Kl 1 883. 0.250g E4 + 0.263g K8 + 0.405g K16 + 0.263g K13 + 0.263g K14 884. 1.250g E1 + 1.313g K7 + 1.313g K13 + 0.405g K16 + 1.313g K24 885. 0.250g E2 + 0.263g K7 + 0.263g K13 + 0.263g K2 + 0.405g K16 886. 1.250gE3+1.608gK16+1.313gK21+1.313gK1+1.313gK11 887. 1.250gE4+1.313gK7+1.608gK16+1.313gK1+1.313gK14 888. 0.250g El + 0.263g K7 + 0.263g K1 + 1.608g K16 + 0.263g K24 889. 1.250g E2 + 1.313g K7 + 1.313g K1 + 1.313g K2 + 1.608g K16 890. 2.500g E3 + 1.608g K16 + 2.625g K7 + 2.625g K11 + 2.625g K14 891. 2.500g E4 + 2.625g K7 + 1.608g K16 + 2.625g K11 + 2.625g K24 892. 0.250g El + 0.263g K7 + 0.263g K11 + 1.608g K16 + 0.263g K2 893. 0.250g E2 + 0.263g K7 + 0.263g K14 + 0.263g K24 + 1.608g K16 894. 2.500g E3 + 1.608g K16 + 2.625g K7 + 2.625g K14 + 2.625g K2 895. 0.250g E4 + 0.263g K7 + 1.608g K16 + 0.263g K24 + 0.263g K2 896. 1.000g El + 1.050g K7 + 1.050g K9 + 1.608g K16 + 1.050g K13 + 1.050g K1 897. 0.200g E2 + 0.210g K7 + 0.210g K9 + 0.210g K13 + 1.608g K16 + 0.210g K11 898. 0.200g E3 + 0.210g K7 + 0.210g K9 + 0.210g K13 + 0.210g K14 + 1.608g K16 899. 2.000g E4 + 1.608g K16 + 2.l00g K7 + 2.l00g K9 + 2.l00g K13 + 2.100g K24 900. 1.000g E1 + 1.050g K7 + 1.608g K16 + 1.050g K9 + 1.050g K13 + 1.050g K2 901. 0.200g E2 + 0.210g K7 + 0.210g K9 + 1.608g K16 + 0.210g K1 + 0.210g K11 902. 2.000g E3 + 2.100g K7 + 2.100g K9 + 2.100g K1 + 1.608g Kl6 + 2.100g K14 903. 0.200g E4 + 0.210g K7 + 0.210g K9 + 0.210g K1 + 0.210g K24 + 1.608g K16 904. 1.000g El + 1.608g K16 + 1.050g K7 + 1.050g K9 + 1.050g Kl + 1.050g K2 905. 1.000g E2 + 1.050g K8 + 1.608g K16 + 1.050g K9 + 1.050g 1(11 + 1.050g K14 906. 2.000g E3 + 2.100g K7 + 2.100g K9 + 1.608g K16 + 2.100g Kl l+ 2.100g K24 907. 2.000g E4 + 2.100g K21 + 2.100g K9 + 2.100g K11 + 1.608g K16 + 2.I OOg K2 908. 0.200g El + 0.210g K7 + 0.210g K9 + 0.210g K14 + 0.210g K24 + 1.608g K16 909. 0.200g E2 + 1.608g K16 + 0.210g K7 + 0.210g K9 + 0.210g K14 + 0.210g K2 910. 2.000g E3 + 2.100g K8 + 1.608g K16 + 2.100g K9 + 2.100g K24 + 2.100g K2 911. 1.000g E4 + 1.050g K7 + 1.050g K13 + 1.608g K16 + 1.050g K1 + 1.050g Kl 1 912. 0.200gE1+0.210gK7+0.210gK13+0.210gK1+1.608gK16+0.210gK14 913. 2.000g E2 + 2.100g K7 + 2.100g K13 + 2.100g K1 + 2.100g K24 + 1.608g K16 914. 1.000g E3 + 1.608g K16 + 1.050g K7 + 1.050g K13 + 1.050g K1 + 1.050g K2 915. 1.000g E4 + 1.050g K7 + 1.608g K16 + 1.050g K13 + 1.050g K11 + 1.050g K14 916. 0.200g E1 + 0.210g K7 + 0.210g K13 + 1.608g K16 + 0.210g K11 + 0.210g K24 917. 2.000g E2 + 2.100g K7 + 2.100g K13 + 2.100g K11 + 1.608g K16 + 2.100g K2 918. 0.200g E3 + 0.210g K7 + 0.210g K13 + 0.210g K14 + 0.210g K24 + 1.608g K16 919. 1.000g E4 + 1.608g K16 + 1.050g K7 + 1.050g K13 + 1.050g K14 + 1.050g K2 920. 2.000g E1 + 2.100g K7 + 1.608g K16 + 2.100g K13 + 2.100g K24 + 2.100g K2 921. 2.000g E2 + 2.l00g K7 + 2.100g Kl + 1.608g K16 + 2.100g K11 + 2.100g K14 922. 0.200g E3 + 0.210g K7 + 0.210g K1 + 0.210g K11 + 1.608g K16 + 0.210g K24 923. 1.000g E4 + 1.050g K7 + 1.050g K1 + 1.050g K11 + 1.050g K2 + 1.608g K16 924. 0.200g E1 + 1.608g K16 + 0.210g K7 + 0.210g K1 + 0.210g K14 + 0.210g K24 925. 2.000g E2 + 2.100g K7 + 1.608g K16 + 2.100g K1 + 2.100g K14 + 2.100g K2 926. 2.000g E3 + 2.100g K7 + 2.100g K1 + 1.608g K16 + 2.100g K24 + 2.100g K2 927. 0.200g E4 + 0.210g K7 + 0.210g K11 + 0.210g K14 + 1.608g K16 + 0.210g K24 928. 2.000g El + 2.100g K8 + 2.100g K11 + 2.100g K14 + 2.100g K2 + 1.608g K16 929. 0.200g E2 + 1.608g K16 + 0.210g K21 + 0.210g K11 + 0.210g K24 + 0.210g K2 930. 1.000g E3 + 1.050g K7 + 1.608g K16 + 1.050g K14 + 1.050g K24 + 1.050g K2 931. 2.500g E4 + 2.625g K9 + 2.500g E8 + 1.608g K16 + 2.625g K12 + 0.655g K10 932. 2.500g El + 2.625g K9 + 2.500g E8 + 2.625g K6 + 1.608g K16 933. 0.250g E2 + 1.608g K16 + 0.263g K9 + 0.250g E8 + 0.263g K7 934. 0.250g E3 + 0.263g K9 + 1.608g K16 + 0.250g E8 + 0.263g K13 935. 2.500g E4 + 2.625g K9 + 2.500g E8 + 1.608g K16 + 2.625g K1 936. 1.250g El + 1.313g K9 + 1.250g E8 + 1.313g K11 + 1.608g K16 937. 0.250g E2 + 1.608g K16 + 0.263g K9 + 0.250g E8 + 0.263g K14 938. 0.250g E3 + 0.263g K9 + 1.608g K16 + 0.250g E8 + 0.263g K24 939. 1.250g E4 + 1.313g K9 + 1.250g E8 + 1.608g K16 + 1.313g K2 940. 1.000g El + 1.050g K9 + 1.000g E8 + 1.050g K12 + 1.608g K16 + 1.050g K6 941. 2.000g E2 + 2.100g K9 + 2.000g E8 + 2.100g K12 + 2.100g K7 + 1.608g K16 942. 0.200g E3 + 1.608g K16 + 0.210g K9 + 0.200g E8 + 0.210g K12 + 0.210g K13 943. 2.000g E4 + 2.100g K9 + 1.608g K16 + 2.000g E8 + 2.100g K12 + 2.100g Kl 944. 2.000g El + 2.100g K9 + 2.000g E8 + 1.608g K16 + 2.100g K12 + 2.100g K11 945. 2.000g E2 + 2.100g K9 + 2.000g E8 + 2.100g K12 + 1.608g K16 + 2.100g K14 946. 1.000g E3 + 1.050g K9 + 1.000g E8 + 1.050g K12 + 1.050g K24 + 1.608g K16 947. 1.000g E4 + 1.608g K16 + 1.050g K9 + 1.000g E8 + 1.050g K12 + 1.050g K2 948. 1.000g El + 1.050g K9 + 1.608g K16 + 1.000g E8 + 1.050g K6 + 1.050g K7 949. 0.200g E2 + 0.210g K9 + 0.200g E8 + 1.608g K16 + 0.210g K6 + 0.210g K13 950. 0.200g E3 + 0.210g K9 + 0.200g E8 + 0.210g K6 + 1.608g K16 + 0.210g KI
951. 2.000g E4 + 2.100g K9 + 2.000g E8 + 2.100g K6 + 2.100g K1 l+ 1.608g K16 952. 2.000g E1 + 1.608g K16 + 2.100g K9 + 2.000g E8 + 2.100g K6 + 2.100g K14 953. 2.000g E2 + 2.100g K9 + 1.608g K16 + 2.000g E8 + 2.100g K6 + 2.100g K24 954. 2.000g E3 + 2. l 00g K9 + 2.000g E8 + 1.811 g K16 + 2.100g K6 + 2.100g K2 955. 0.200g E4 + 0.210g K9 + 0.200g E8 + 0.210g K7 + 1.811g K16 + 0.210g K13 956. 2.000g El + 2.100g K9 + 2.000g E8 + 2.100g K7 + 2.100g K1 + 1.811g K16 957. 1.000g E2 + 1.811g K16 + 1.050g K9 + 1.000g E8 + 1.054g K7 + 1.050g K11 958. 0.200g E3 + 0.210g K9 + 1.811g K16 + 0.200g E8 + 0.210g K7 + 0.210g K14 959. 2.000g E4 + 2.100g K9 + 2.000g E8 + 1.811g K16 + 2.100g K7 + 2.100g K24 960. 2.000g E1 + 2.100g K9 + 2.000g E8 + 2.100g K7 + 1.811g K16 + 2.100g K2 961. 0.200g E2 + 0.210g K9 + 0.200g E8 + 0.210g K13 + 0.210g K1 + 1.811g K16 962. 0.200gE3+ 1.811gK16+0.210gK9+0.200gE8+0.210gK13+0.210gK11 963. 1.000g E4 + 1.050g K9 + 1.811g K16 + 1.000g E8 + 1.050g K13 + 1.050g K14 964. 2.000g E1 + 2. l00g K9 + 2.000g E8 + 1.811g K16 + 2.100g K13 + 2.100g K24 965. 1.000g E2 + 1.050g K9 + 1.000g E8 + 1.050g K13 + 1.811g K16 + 1.050g K2 966. 2.000g E3 + 2.100g K9 + 2.000g E8 + 2.100g K1 + 2.100g K11 + 1.811g K16 967. 2.000g E4 + 1.811g K16 + 2.100g K9 + 2.000g E8 + 2.100g Kl + 2.100g K14 968. 0.200g El + 0.210g K9 + 1.81 lg K16 + 0.200g E8 + 0.210g Kl + 0.210g K24 969. 0.200g E2 + 0.210g K9 + 0.200g E8 + 1.811g K16 + 0.210g K1 + 0.210g K2 970. 1.000g E3 + 1.050g K9 + 1.000g E8 + 1.050g K11 + 1.81 lg K16 + 1.050g K14 971. 1.000g E4 + 1.050g K9 + 1.000g E8 + 1.050g K11 + 1.050g K24 + 1.811g K16 972. 2.000g El + 1.811g K16 + 2.100g K9 + 2.000g E8 + 2.100g K1 l+ 2.100g K2 973. 2.000g E2 + 2.100g K9 + 1.811 g K16 + 2.000g E8 + 2.100g K14 + 2.100g K24 974. 2.000g E3 + 2.100g K9 + 2.000g E8 + 1.811g K16 + 2.100g K14 + 2.100g K2 975. 0.200g E4 + 0.210g K9 + 0.200g E8 + 0.210g K24 + 1.811g K16 + 0.210g K2 976. 2.500g E1 + 2.625g K9 + 2.500g E6 + 2.625g K12 + 1.811g K16 977. 0.250g E2 + 1.811g K16 + 0.263g K9 + 0.250g E6 + 0.263g K6 978. 2.500g E3 + 2.625g K9 + 1.811gK16+2.500gE6+2.625gK7 979. 0.250g E4 + 0.263g K9 + 0.250g E6 + 1.81 lg K16 + 0.263g K13 980. 2.500g E1 + 2.625g K9 + 2.500g E6 + 2.625g Kl + 1.81 lg K16 981. 0.250g E2 + 1.811g K16 + 0.263g K9 + 0.250g E6 + 0.263g K11 + 0.050g K23 982. 2.500g E3 + 2.625g K9 + 1.811g K16 + 2.500g E6 + 2.625g K14 983. 1.250g E4 + 1.313g K9 + 1.250g E6 + 1.811g K16 + 1.313g K24 984. 1.250gE1 + 1.313gK9+ 1.250gE6+ 1.313gK2+ 1.811gK16 985. 0.200g E2 + 1.811 g K16 + 0.210g K9 + 0.200g E6 + 0.210g K12 + 0.210g K6 986. 1.000g E3 + 1.050g K9 + 1.811g K16 + 1.000g E6 + 1.050g K12 + 1.050g K7 987. 0.200gE4+0.210gK9+0.200gE6+ 1.811gK16+0.210gK12+0.210gK13 988. 0.200gE1 + 0.210g K9 + 0.200g E6 + 0.210g K12 + 1.811gK16+0.210gK1 989. 2.000g E2 + 2.100g K9 + 2.000g E6 + 2.100g K12 + 2.100g K11 + 1.811g K16 990. 1.000g E3 + 1.811g K16 + 1.050g K9 + 1.000g E6 + 1.050g K12 + 1.050g K14 991. 1.000g E4 + 1.050g K9 + 1.811g K16 + 1.000g E6 + 1.050g K12 + 1.050g K24 992. 0.200gE1 +0.210gK9+0.200gE6+ 1.811gK16+0.210gK12+0.210gK2 993. 1.000g E2 + 1.050g K9 + 1.000g E6 + 1.050g K6 + 1.811g K16 + 1.050g K7 994. 0.200g E3 + 0.210g K9 + 0.200g E6 + 0.210g K6 + 0.210g K13 + 1.811g K16 995. 2.000g E4 + 1.811g K16 + 2.100g K9 + 2.000g E6 + 2.100g K6 + 0.100g K18 996. 0.200gE1+0.210gK9+1.811gK16+0.200gE6+0.210gK6+0.2lOgK11 997. 0.200g E2 + 0.210g K9 + 0.200g E6 + 1.811g K16 + 0.210g K6 + 0.210g K14 998. 0.200g E3 + 0.210g K9 + 0.200g E6 + 0.210g K6 + 1.811g K16 + 0.210g K24 999. 1.000g E4 + 1.050g K9 + 1.000g E6 + 1.050g K6 + 1.050g K2 + 1.811g K16 1000 0.200g E1 + 1.811g K16 + 0.210g K9 + 0.200g E6 + 0.2l Og K7 + 0.210g K13 1001 0.200g E2 + 0.210g K9 + 1.811g K16 + 0.200g E6 + 0.210g K7 + 0.210g K1 1002 2.000g E3 + 2.100g K9 + 2.000g E6 + 1.811 g K16 + 2.100g K7 + 2.100g K11 1003 1.000g E4 + 1.050g K9 + 1.000g E6 + 1.050g K7 + 1.811g K16 + 1.050g K14 1004 2.000g E 1+ 2.100g K9 + 2.000g E6 + 2. l 00g K7 + 2.100g K24 + 1.811 g K

1005 0.200g E2 + 1.811g K16 + 0.210g K9 + 0.200g E6 + 0.210g K7 + 0.210g K2 1006 0.200gE3+0.210gK9+1.811gK16+0.200gE6+0.210gK13+0.210gK1 1007 1.000g E4 + 1.050g K9 + 1.000g E6 + 1.811g K16 + 1.050g K13 + 1.050g K11 1008 2.000gE1 +2.100gK9+2.000gE6+2.100gK13+1.811gK16+2.100gK14 1009 1.000g E2 + 1.050g K9 + 1.000g E6 + 1.050g K13 + 1.050g K24 + 1.81 lg K16 1010 2.000g E3 + 1.811g K16 + 2.100g K9 + 2.000g E6 + 2.100g K13 + 2.100g K2 1011 0.200g E4 + 0.210g K9 + 1.811 g K16 + 0.200g E6 + 0.210g K1 + 0.210g K11 1012 2.000g E1 + 2.100g K9 + 2.000g E6 + 1.811g K16 + 2.100g Kl + 2.100g K14 1013 2.000g E2 + 2.100g K9 + 2.000g E6 + 2.100g K1 + 1.811g K16 + 2.100g K24 1014 1.000g E3 + 1.050g K9 + 1.000g E6 + 1.050g K1 + 1.050g K2 + 1.81 lg K16 1015 1.000g E4 + 1.81 lg K16 + 1.050g K9 + 1.000g E6 + 1.050g K11 + l.050g K14 1016 1.000g El + 1.050g K9 + 1.81 lg K16 + 1.000g E6 + 1.050g K11 + 1.050g K24 1017 0.200gE2+0.210gK9+0.200gE6+ 1.811gK16+0.210gK11 +0.210gK2 1018 0.200gE3+0.210gK9+0.200gE6+0.210gK14+1.811gK16+0.210gK24 1019 2.000g E4 + 2.100g K9 + 2.000g E6 + 2.100g K14 + 2.100g K2 + 1.811 g K16 1020 2.000g E 1+ 1.811 g K16 + 2. l 00g K9 + 2.000g E6 + 2.100g K24 + 2.100g 1021 0.250g E2 + 0.263g K9 + 1.811g K16 + 0.250g E5 + 0.263g K12 1022 0.250g E3 + 0.263g K9 + 0.250g E5 + 0.013g K16 + 0.263g K6 1023 2.500g E4 + 2.625g K9 + 2.500g E5 + 2.625g K7 + 0.013g K16 1024 0.250g El + 0.013g K16 + 0.263g K9 + 0.250g E5 + 0.263g K13 1025 0.250g E2 + 0.263g K9 + 0.013g K16 + 0.250g E5 + 0.263g K1 1026 1.250g E3 + 1.313g K9 + 1.250g E5 + 0.013g K16 + 1.313g K11 1027 1.250g E4 + 1.313g K9 + 1.250g E5 + 1.313g K14 + 0.013g K16 1028 1.250g E1 + 0.013g K16 + 1.313g K9 + 1.250g E5 + 1.313g K24 1029 1.250g E2 + 1.313g K9 + 0.013g K16 + 1.250g E5 + 1.313g K2 1030 1.000g E3 + 1.050g K9 + 1.000g E5 + 0.013g K16 + 1.050g K12 + 1.050g K6 1031 1.000g E4 + 1.050g K9 + 1.000g E5 + 1.050g K12 + 0.013g K16 + 1.050g K21 1032 0.200gE1 + 0.210g K9 + 0.200g E5 + 0.210g K12 + 0.210g K13 + 0.013g K16 1033 2.000g E2 + 0.013g K16 + 2.l00g K9 + 2.000g E5 + 2.l00g K12 + 2.100g K1 1 1034 2.000g E3 + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K12 + 2.100g 1035 0.200gE4+0.210gK9+0.200gE5+0.013gK16+0.210gK12+0.210gK14 1036 2.000g E1 + 2.100g K9 + 2.000g E5 + 2.100g K12 + 0.013g K16 + 2.100g K24 1037 2.000g E2 + 2.100g K9 + 2.000g E5 + 2.100g K12 + 2.100g K2 + 0.013g K16 1038 2.000g E3 + 0.013g K16 + 2.100g K9 + 2.000g E5 + 2.100g K6 + 2.100g K8 1039 2.000g E4 + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K6 + 2.100g K13 1040 2.000g E1 + 2.100g K9 + 2.000g E5 + 0.013g K16 + 2.100g K6 + 2.100g Kl 1041 1.000g E2 + 1.050g K9 + 1.000g E5 + 1.050g K6 + 0.013g K16 + 1.050g K11 1042 0.200g E3 + 0.210g K9 + 0.200g E5 + 0.210g K6 + 0.210g K14 + 0.013g K16 1043 1.000g E4 + 0.013g K16 + 1.050g K9 + 1.000g E5 + 1.050g K6 + 1.050g K24 1044 2.000g El + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K6 + 2.100g K2 1045 0.200g E2 + 0.210g K9 + 0.200g E5 + 0.013g K16 + 0.210g K7 + 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K7 + 1.050g K2 1753 2.000g E2 + 2.100g K1 + 2.100g K12 + 2.100g K9 + 1.636g K16 + 2.100g K13 1754 0.200g E3 + 0.210g K1 + 0.210g K12 + 0.210g K9 + 0.210g K11 + 1.636g K16 1755 1.000g E4 + 1.636g K16 + 1.050g K1 + 1.050g K12 + l.050g K9 + 1.050g K14 1756 2.000g E1 + 2.100g K1 + 1.636g K16 + 2.100g K12 + 2.100g K9 + 2.100g K24 1757 1.000g E2 + 1.050g K1 + 1.050g K12 + 1.636g K16 + 1.050g K9 + 1.050g K2 1758 0.200g E3 + 0.210g K1 + 0.210g K12 + 0.210g K13 + 1.636g K16 + 0.210g K11 1759 1.000g E4 + 1.050g Kl + 1.050g K12 + 1.050g K13 + 1.050g K14 + 1.636g K16 1760 0.200g E1 + 1.636g K16 + 0.210g K1 + 0.210g K12 + 0.210g K13 + 0.210g K24 1761 0.200gE2+0.210gK1 + 1.636g K16 + 0.210g K12 + 0.210g K13 +0.210gK2 1762 2.000g E3 + 2.100g Kl + 2.100g K12 + 1.839g K16 + 2.100g Kl l+ 2.100g K14 1763 1.000g E4 + l.050g Kl + 1.050g K12 + 1.050g K11 + 1.839g K16 + 1.050g K24 1764 2.000g E1 + 2.100g Kl + 2.100g K12 + 2.100g K11 + 2.100g K2 + 1.839g K16 1765 2.000g E2 + 1.839g K16 + 2.100g Kl + 2.100g K12 + 2.100g K14 + 2.100g K24 1766 0.200gE3+0.210gK1 + 1.839g K16 + 0.210g K12 + 0.210g K14 + 0.210g K2 1767 0.200gE4+0.210gK1 +0.210gK12+ 1.839g K16 + 0.210g K24 + 0.210g K2 1768 3.333g El + 3.500g Ki + 3.500g K6 + 1.839g K16 1 1769 1.250g E2 + 1.839g K16 + 1.313g K1 + 1.313g K6 + 1.313g K7 1770 1.250g E3 + 1.313g K1 + 1.839g K16 + 1.313g K6 + 1.313g K9 1771 1.250gE4+1.313gK1+1.313gK6+1.839gK16+1.313gK13 1772 0.250g E1 + 0.263g K1 + 0.263g K6 + 0.263g K11 + 1.839g K16 1773 0.250g E2 + 1.839g K16 + 0.263g K1 + 0.263g K6 + 0.263g K14 1774 1.250g E3 + 1.313g K1 + 1.839g K16 + 1.313g K6 + 1.313g K24 1775 0.250g E4 + 0.263g KI + 0.263g K6 + 1.839g K16 + 0.263g K2 1776 0.200gE1 +0.210gK1 + 0.210g K6 + 0.210g K7 + 1.839g K16 + 0.210g K9 1777 1.000g E2 + 0.850g K1 + 1.050g K6 + 1.050g K7 + 1.050g K4 + 1.050g K13 +
1.839g K16 1778 0.200g E3 + 1.839g K16 + 0.210g K1 + 0.210g K6 + 0.210g K7 + 0.210g K11 1779 2.000g E4 + 2.100g K1 + 1.839g K16 + 2.100g K6 + 2.100g K7 + 2.100g K14 1780 2.000g E1 + 2.100g Kl + 2.100g K6 + 1.839g K16 + 2.100g K7 + 2.100g K24 1781 0.200g E2 + 0.210g K1 + 0.210g K6 + 0.210g K8 + 1.839g K16 + 0.210g K2 1782 2.000g E3 + 2.100g Kl + 2. l00g K6 + 2.100g K9 + 2.100g K13 + 1.839g K16 1783 0.200g E4 + 1.839g K16 + 0.210g K1 + 0.210g K6 + 0.210g K9 + 0.210g K11 1784 2.000g E1 + 2.100g K1 + 1.839g K16 + 2.100g K6 + 2.100g K9 + 2.100g K14 1785 2.000g E2 + 2.100g Kl + 2.100g K6 + 1.839g K16 + 2.100g K9 + 2.100g K24 1786 1.000g E3 + 1.050g K1 + 1.050g K6 + 1.050g K9 + 1.839g K16 + 1.050g K2 1787 2.000g E4 + 2.100g Kl + 2. l00g K6 + 2.100g K13 + 2.100g K11 + 1.839g K16 1788 2.000g E1 + 1.839g K16 + 2.100g K1 + 2.100g K6 + 2.100g K13 + 2.100g K14 1789 0.200g E2 + 0.210g Kl + 1.839g K16 + 0.210g K6 + 0.210g K13 + 0.210g K24 1790 0.200g E3 + 0.210g K1 + 0.210g K6 + 1.839g K16 + 0.210g K13 + 0.210g K2 1791 0.200g E4 + 0.210g K1 + 0.210g K6 + 0.210g K1 l+ 1.839g K16 + 0.210g K14 1792 0.200g El + 0.210g K1 + 0.210g K6 + 0.210g Kl 1+ 0.210g K24 + 1.839g K16 1793 0.200g E2 + 1.839g K16 + 0.210g K1 + 0.210g K6 + 0.210g K11 + 0.210g K2 1794 1.000g E3 + 1.050g Kl + 1.839g K16 + 1.050g K6 + 1.050g K14 + 1.050g K24 1795 1.000g E4 + 1.050g K1 + 1.050g K6 + 1.839g K16 + 1.050g K14 + 1.050g K2 1796 1.000g E1 + 1.050g K1 + 1.050g K6 + 1.050g K24 + 1.839g K16 + 1.050g K2 1797 0.333g E2 + 0.350g K1 + 0.350g K7 + 1.839g K16 1798 0.250g E3 + 1.839g K16 + 0.263g K5 + 0.263g K7 + 0.263g K9 1799 1.250gE4+1.313gK1+1.839gK16+1.313gK7+1.313gK13 1800 0.250g El + 0.263g K1 + 0.263g K7 + 1.839g K16 + 0.263g K11 1801 0.250g E2 + 0.263g Kl + 0.263g K7 + 0.263g K14 + 1.839g K16 1802 2.500g E3 + 1.839g K16 + 2.625g K1 + 2.625g K7 + 2.625g K24 1803 2.500g E4 + 2.625g Kl + 1.839g K16 + 2.625g K7 + 2.625g K2 1804 0.200g E1 + 0.210g K1 + 0.210g K7 + 1.839g K16 + 0.210g K9 + 0.210g K13 1805 1.000g E2 + 1.050g K1 + 1.050g K7 + 1.050g K9 + 1.839g K16 + 1.050g K11 1806 2.000g E3 + 2.100g K1 + 2.100g K7 + 2.100g K9 + 2.100g K14 + 1.839g K16 1807 2.000g E4 + 1.839g K16 + 2.100g K1 + 2.100g K7 + 2.100g K9 + 2.100g K24 1808 2.000g E1 + 2.100g Kl + 1.839g K16 + 2.100g K21 + 2.100g K9 + 2.100g K2 1809 0.200g E2 + 0.210g K1 + 0.210g K7 + 1.839g K16 + 0.210g K13 + 0.210g K11 1810 0.200g E3 + 0.210g K1 + 0.210g K7 + 0.210g K13 + 1.839g K16 + 0.210g K14 1811 2.000g E4 + 2.100g K1 + 2.100g K7 + 2.100g K13 + 2.100g K24 + 1.839g K16 1812 2.000g El + 1.839g K16 + 2.l00g K1 + 2.100g K7 + 2.100g K13 + 2.100g K2 1813 2.000g E2 + 2.100g K1 + 1.839g K16 + 2.100g K7 + 2.100g K11 + 2.100g K14 1814 1.000g E3 + 1.050g K1 + 1.050g K7 + 1.839g K16 + 1.050g Kl l+ 1.050g K24 1815 1.000g E4 + 1.050g K1 + 1.050g K7 + 1.050g K11 + 1.839g K16 + 1.050g K2 1816 2.000g E1 + 2.100g K1 + 2.100g K7 + 2.100g Kl4 + 2.100g K24 + 1.839g K16 1817 2.000g E2 + 1.839g K16 + 2.100g Kl + 2.100g K7 + 2.100g K14 + 2.100g K2 1818 2.000g E3 + 2.100g K1 + 1.839g K16 + 2.100g K8 + 2.100g K24 + 2.100g K2 1819 1.667g E4 + 1.750g Kl + 1.750g K9 + 1.839g K16 1820 0.250g El + 1.839g K16 + 0.263g K1 + 0.263g K9 + 0.263g K13 1821 2.500g E2 + 2.625g K1 + 1.839g K16 + 2.625g K9 + 2.625g K11 1822 2.500g E3 + 2.625g Kl + 2.625g K9 + 1.839g K16 + 2.625g K14 1823 1.250g E4 + 1.313g K1 + 1.313g K9 + 1.313g K24 + 1.839g K16 1824 0.250g El + 1.839g K16 + 0.263g K1 + 0.263g K9 + 0.263g K2 1825 0.200g E2 + 0.210g K1 + 1.839g K16 + 0.210g K9 + 0.210g K13 + 0.210g K11 1826 0.200g E3 + 0.210g K1 + 0.210g K9 + 1.839g K16 + 0.210g K13 + 0.210g K14 1827 0.200g E4 + 0.210g K1 + 0.210g K9 + 0.210g K13 + 1.839g K16 + 0.210g K24 1828 1.000g El + 1.050g K1 + 1.050g K9 + 1.050g K13 + 1.050g K2 + 1.839g K16 1829 1.000g E2 + 1.839g K16 + 1.050g K1 + l.050g K9 + 1.050g Kl l+ 1.050g Kl4 1830 0.200g E3 + 0.210g Kl + 1.839g K16 + 0.210g K9 + 0.210g Kl l+ 0.210g K24 1831 1.000g E4 + 1.050g K1 + 1.050g K9 + 1.839g K16 + 1.050g K11 + 1.050g K2 1832 2.000g E1 + 2.100g Kl + 2.100g K9 + 2.100g K14 + 1.839g K16 + 2.100g K24 1833 0.200gE2+0.210gK1 + 0.210g K9 + 0.210g K14 + 0.210g K2 + 1.839gK16 1834 1.000g E3 + 1.839g K16 + 1.050g K1 + 1.050g K9 + 1.050g K24 + 1.050g K2 1835 1.667g E4 + 1.750g K1 + 1.839g K16 + 1.750g K13 1836 0.250g El + 0.263g Kl + 0.263g K13 + 1.839g K16 + 0.263g Kl 1 1837 1.250g E2 + 1.313g K1 + 1.313g K13 + 1.313g K14 + 1.839g K16 1838 2.500g E3 + 1.839g K16 + 2.625g K1 + 2.625g K13 + 2.625g K24 1839 2.500g E4 + 2.625g Kl + 1.839g K16 + 2.625g K13 + 2.625g K2 1840 1.000g E1 + 1.050g Kl + 1.050g K13 + 1.839g K16 + 1.050g Kl l+ 1.050g K14 1841 0.200g E2 + 0.210g Kl + 0.210g K13 + 0.210g K11 + 1.839g K16 + 0.210g K24 1842 0.200g E3 + 0.210g K1 + 0.210g K13 + 0.210g K11 + 0.210g K2 + 1.839g K16 1843 0.200g E4 + 1.839g K16 + 0.210g Kl + 0.210g K13 + 0.210g K14 + 0.210g K24 1844 1.000g El + 1.050g Kl + 1.839g K16 + 1.050g K13 + 1.050g K14 + 1.050g K2 1845 0.200g E2 + 0.210g Kl + 0.210g K13 + 1.839g K16 + 0.210g K24 + 0.210g K2 1846 5.000g El + 5.250g K1 + 1.839g K16 + O.OlOg D1 1847 0.333g E4 + 1.839g K16 + 0.350g K1 + 0.350g K11 1848 1.667g E1 + 1.750g Kl + 1.839g K16 + 1.750g K14 1849 0.333g E2 + 0.350g KI + 0.350g K24 + 1.839g K16 1850 1.667g E3 + 1.839g K16 + 0.750g K18 + 1.750g K2 1851 1.250gE4+1.313gK1+1.839gK16+1.313gK11+1.313gK14 1852 2.500g El + 2.625g K1 + 2.625g K11 + 0.042g K16 + 2.625g K24 1853 1.250gE2+ 1.313gK1 +0.313gK4+ 1.313gK11 + 1.313gK2+0.042gK16 1854 0.250g E3 + 0.042g K16 + 0.263g Kl + 0.263g K14 + 0.263g K24 1855 1.250gE4+1.313gK1 + 0.042g K16 + 1.313g K14 + 1.313g K2 1856 1.250g El + 1.313g K1 + 1.313g K24 + 0.042g K16 + 1.313g K2 1857 2.000g E2 + 2.100g K1 + 2.100g K11 + 2.100g K14 + 0.042g K16 + 2.100g K24 1858 0.200g E3 + 0.210g K1 + 0.210g K11 + 0.210g K14 + 0.210g K2 + 0.042g K16 1859 2.000g E4 + 0.042g K16 + 2.100g K1 + 2.100g K11 + 2.100g K24 + 2.100g K2 1860 1.000g El + 1.050g Kl + 0.042g K16 + 1.050g K14 + 1.050g K24 + 1.050g K2 1861 2.500g E2 + 2.625g Kl 1 + 2.500g E8 + 0.042g K16 + 2.625g K12 1862 2.500g E3 + 2.625g Kl 1+ 2.500g E8 + 2.625g K6 + 0.042g K16 1863 1.250g E4 + 0.042g K16 + 1.313g K11 + 1.250g E8 + 1.313g K7 1864 0.250g El + 0.263g K11 + 0.042g K16 + 0.250g E8 + 0.263g K9 1865 2.500g E2 + 2.625g K11 + 2.500g E8 + 0.042g K16 + 2.625g K13 1866 2.500g E3 + 2.625g K11 + 2.500g E8 + 2.625g K1 + 0.042g K16 1867 1.250g E4 + 0.042g K16 + 1.313g K11 + 1.250g E8 + 1.313g K14 1868 0.250g El + 0.263g K11 + 0.042g K16 + 0.250g E8 + 0.263g K24 1869 0.250g E2 + 0.263g K11 + 0.250g E8 + 0.042g K16 + 0.263g K2 1870 1.000g E3 + 1.050g Kl 1+ 1.000g E8 + 1.050g K12 + 0.042g K16 + 1.050g K6 1871 2.000g E4 + 2.100g K11 + 2.000g E8 + 2.100g K12 + 2.100g K7 + 0.042g K16 1872 1.000g E1 + 0.042g K16 + 1.050g K11 + 1.000g E8 + 1.050g K12 + 1.050g K9 1873 1.000g E2 + 1.050g K11 + 0.042g K16 + 1.000g E8 + 1.050g K12 + 1.050g K13 1874 0.200g E3 + 0.210g K11 + 0.200g E8 + 0.042g K16 + 0.210g K12 + 0.210g K1 1875 1.000g E4 + 1.050g K11 + 1.000g E8 + 1.050g K12 + 0.042g K16 + 1.050g K14 1876 1.000g El + 1.050g K11 + 1.000g E8 + 1.050g K12 + 1.050g K24 + 0.042g K16 1877 0.200g E2 + 0.042g K16 + 0.210g K11 + 0.200g E8 + 0.210g K12 + 0.210g K2 1878 0.200g E3 + 0.210g Kl 1+ 0.042g K16 + 0.200g E8 + 0.210g K6 + 0.210g K7 1879 2.000g E4 + 2.100g K11 + 2.000g E8 + 0.042g K16 + 2.l00g K6 + 2.l00g K9 1880 2.000g E1 + 2.100g K11 + 2.000g E8 + 2.100g K6 + 0.042g K16 + 2.100g K13 1881 1.000g E2 + 1.050g Kl 1 + 1.000g E8 + 1.050g K6 + 1.050g KI + 0.042g K16 1882 2.000g E3 + 0.042g K16 + 2.100g K11 + 2.000g E8 + 2.100g K6 + 2.100g K14 1883 2.000g E4 + 2.100g Kl l+ 0.042g K16 + 2.000g E8 + 2.100g K6 + 2.100g K24 1884 1.000g E1 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K6 + 1.050g K2 1885 0.200g E2 + 0.210g K11 + 0.200g E8 + 0.210g K7 + 0.042g K16 + 0.210g K9 1886 1.000g E3 + 1.050g Kl l+ 1.000g E8 + 1.050g K7 + 1.050g K13 + 0.042g K16 1887 2.000g E4 + 0.042g K16 + 2.100g K11 + 2.000g E8 + 2.100g K7 + 2.100g Kl 1888 1.000g E1 + 1.050g Kl l+ 0.042g K16 + 1.000g E8 + 1.050g K7 + 1.050g K14 1889 1.000g E2 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K7 + 1.050g K24 1890 1.000g E3 + 1.050g Kl l+ 1.000g E8 + 1.050g K7 + 0.042g K16 + 1.050g K2 1891 2.000g E4 + 2. l00g K11 + 2.000g E8 + 2.100g K9 + 2. l00g K13 + 0.042g 1892 0.200g El + 0.042g K16 + 0.210g Kl 1+ 0.200g E8 + 0.210g K9 + 0.210g Kl 1893 0.200g E2 + 0.210g K11 + 0.042g K16 + 0.200g E8 + 0.210g K9 + 0.210g K14 1894 1.000g E3 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K9 + 1.050g K24 1895 2.000g E4 + 2.100g K11 + 2.000g E8 + 2.100g K9 + 0.042g K16 + 2.100g K2 1896 2.000g E1 + 2.100g K11 + 2.000g E8 + 2.100g K13 + 0. l00g K5 + 1.900g K1 +

0.042g K16 1897 0.200gE2+0.042gK16+0.210gK11+0.200gE8+0.210gK13+0.210gK14 1898 0.200g E3 + 0.210g K11 + 0.042g K16 + 0.200g E8 + 0.210g K13 + 0.210g K24 1899 1.000g E4 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K13 + 1.050g K2 1900 0.200g El + 0.210g Kl 1 + 0.200g E8 + 0.210g K1 + 0.042g K16 + 0.210g K14 1901 1.000g E2 + 1.050g K11 + 1.000g E8 + 1.050g K1 + 1.050g K24 + 0.042g K16 1902 0.200g E3 + 0.042g K16 + 0.210g K11 + 0.200g E8 + 0.210g K1 + 0.210g K2 1903 0.200g E4 + 0.210g Kl 1 + 0.042g K16 + 0.200g E8 + 0.210g K14 + 0.210g 1904 2.000g El + 2.100g K11 + 2.000g E8 + 0.042g K16 + 2.100g K14 + 2.100g K2 1905 0.200g E2 + 0.210g K11 + 0.200g E8 + 0.210g K24 + 0.042g K16 + 0.210g K2 1906 1.250g E3 + 1.313g K11 + 1.250g E6 + 1.313g K12 + 0.042g K16 1907 2.500g E4 + 0.042g K16 + 2.625g K11 + 2.500g E6 + 2.625g K6 1908 0.250g El + 0.263g KI 1 + 0.042g K16 + 0.250g E6 + 0.263g K7 1909 2.500g E2 + 2.625g Kl 1 + 2.500g E6 + 0.042g K16 + 2.625g K9 1910 2.500g E3 + 2.625g K11 + 2.500g E6 + 2.625g K13 + 0.042g K16 1911 0.250g E4 + 0.042g K16 + 0.263g K11 + 0.250g E6 + 0.263g Kl 1912 0.250g El + 0.263g Ki 1+ 0.042g K16 + 0.250g E6 + 0.263g K14 + 0.090g D2 1913 0.250g E2 + 0.263g Kl 1+ 0.250g E6 + 0.042g K16 + 0.263g K24 1914 1.250g E3 + 1.313g K11 + 1.250g E6 + 1.313g K2 + 0.042g K16 1915 1.000g E4 + 0.042g K16 + 1.050g Kl 1+ 1.000g E6 + 1.050g K12 + 1.050g K6 1916 2.000g El + 2.100g K11 + 0.042g K16 + 2.000g E6 + 2.100g K12 + 2.100g K21 1917 0.200gE2+0.210gK11 + 0.200g E6 + 0.042g K16 + 0.210g K12 + 0.210g K9 1918 1.000g E3 + 1.050g Kl l+ 1.000g E6 + 1.050g K12 + 0.042g K16 + 1.050g K13 1919 1.000g E4 + 1.050g K11 + 1.000g E6 + 1.050g K12 + 1.050g K1 + 0.042g K16 1920 0.200gE1 +0.042gK16+0.210gK11 + 0.200g E6 + 0.210g K12 + 0.210g K14 1921 2.000g E2 + 2.100g Kl l+ 0.042g K16 + 2.000g E6 + 2.100g K12 + 2.100g K24 1922 1.000g E3 + 1.050g Kl l+ 1.000g E6 + 0.042g K16 + 1.050g K12 + 1.050g K2 1923 1.000g E4 + 1.050g K11 + 1.000g E6 + 1.050g K6 + 0.042g K16 + 1.050g K7 1924 2.000g El + 2.100g K11 + 2.000g E6 + 2.100g K6 + 2.100g K9 + 0.042g K16 1925 2.000g E2 + 0.042g K16 + 2.100g K11 + 2.000g E6 + 2.100g K6 + 2.100g K13 1926 2.000g E3 + 2.100g Kl 1+ 0.042g K16 + 2.000g E6 + 2.100g K6 + 2.100g K1 1927 0.200g E4 + 0.210g K11 + 0.200g E6 + 0.042g K16 + 0.210g K6 + 0.210g K14 1928 0.200g El + 0.210g Kl 1+ 0.200g E6 + 0.210g K6 + 0.042g K16 + 0.210g K24 1929 1.000g E2 + 1.050g K11 + 1.000g E6 + 1.050g K6 + 1.050g K2 + 0.042g K16 1930 0.200g E3 + 0.042g K16 + 0.210g K11 + 0.200g E6 + 0.214g K7 + 0.210g K9 1931 2.000g E4 + 2.100g K1 l+ 0.042g K16 + 2.000g E6 + 2.100g K7 + 2.100g K13 1932 0.200g El + 0.210g K11 + 0.200g E6 + 0.042g K16 + 0.210g K7 + 0.210g K1 1933 0.200g E2 + 0.210g K11 + 0.200g E6 + 0.210g K7 + 0.042g K16 + 0.210g K14 1934 2.000g E3 + 2.100g K11 + 2.000g E6 + 2.100g K7 + 2.100g K24 + 0.042g K16 1935 1.000g E4 + 0.042g K16 + 1.050g K11 + 1.000g E6 + 1.050g K7 + 1.050g K2 1936 2.000g El + 2.100g Kl 1 + 0.042g K16 + 2.000g E6 + 2.100g K9 + 2.100g K13 1937 1.000g E2 + 1.050g Kl l+ 1.000g E6 + 0.042g K16 + 1.050g K9 + 1.050g K1 1938 0.200gE3+0.210gK11 + 0.200g E6 + 0.210g K9 + 0.042g K16 + 0.210g K14 1939 0.200g E4 + 0.210g K11 + 0.200g E6 + 0.210g K9 + 0.210g K24 + 0.042g K16 1940 2.000g El + 0.042g K16 + 2.100g K11 + 2.000g E6 + 2.100g K9 + 2.100g K2 1941 2.000g E2 + 2.100g K11 + 0.042g K16 + 2.000g E6 + 2.100g K13 + 2.100g K1 1942 1.000g E3 + 1.050g K11 + 1.000g E6 + 0.245g K16 + 1.050g K13 + 1.050g K14 1943 0.200g E4 + 0.210g K11 + 0.200g E6 + 0.210g K13 + 0.245g K16 + 0.210g K24 1944 0.200g El + 0.210g KI 1+ 0.200g E6 + 0.210g K13 + 0.210g K2 + 0.245g K16 1945 0.200g E2 + 0.245g K16 + 0.210g K11 + 0.200g E6 + 0.210g K1 + 0.210g K14 1946 1.000g E3 + 1.050g Kl l+ 0.245g K16 + 1.000g E6 + 1.050g K1 + 1.050g K24 1947 2.000g E4 + 2.100g Kl l+ 2.000g E6 + 0.245g K16 + 2.100g K1 + 2.100g K2 1948 2.000g E1 + 2.100g K11 + 2.000g E6 + 2.100g K14 + 0.245g K16 + 2.100g K24 1949 0.200g E2 + 0.210g K11 + 0.200g E6 + 0.210g K14 + 0.210g K2 + 0.245g K16 1950 0.200g E3 + 0.245g K16 + 0.210g K11 + 0.200g E6 + 0.210g K24 + 0.210g K2 1951 1.250g E4 + 1.313g K11 + 0.245g K16 + 1.250g E5 + 1.313g K12 1952 1.250g E1 + 1.313g Kl 1+ 1.250g E5 + 0.245g K16 + 1.313g K6 1953 1.250g E2 + 1.313g K11 + 1.250g E5 + 1.313g K7 + 0.245g K16 1954 1.250g E3 + 0.245g K16 + 1.313g K11 + 1.250g E5 + 1.313g K9 1955 0.250g E4 + 0.263g Kl 1+ 0.245g K16 + 0.250g E5 + 0.263g K13 1956 2.500g El + 2.625g KI 1+ 2.500g E5 + 0.245g K16 + 2.625g K1 1957 2.500g E2 + 2.625g K11 + 2.500g E5 + 2.625g K14 + 0.245g K16 1958 1.250g E3 + 0.245g K16 + 1.313g K11 + 1.250g E5 + 1.313g K24 1959 1.250g E4 + 1.313g K11 + 0.245g K16 + 1.250g E5 + 1.313g K2 1960 2.000g E1 + 2.100g K11 + 2.000g E5 + 0.245g K16 + 2.100g K12 + 2.100g K6 1961 1.000g E2 + 1.050g K11 + 1.000g E5 + 1.050g K15 + 0.245g K16 + 1.050g K7 1962 2.000g E3 + 2.100g K11 + 2.000g E5 + 2.100g K12 + 2.100g K9 + 0.245g K16 1963 2.000g E4 + 0.245g K16 + 2.100g K11 + 2.000g E5 + 2.000g K15 + 2.l00g K12 +
2.100g K13 1964 2.000g El + 2.100g K11 + 0.245g K16 + 2.000g E5 + 2.100g K12 + 2.100g Kl 1965 2.000g E2 + 2.100g Kl 1+ 2.000g E5 + 0.245g K16 + 2.100g K12 + 2.100g K14 1966 0.200g E3 + 0.210g K11 + 0.200g E5 + 0.210g K12 + 0.245g K16 + 0.210g K24 1967 1.000g E4 + 1.050g K11 + 1.000g E5 + 1.050g K12 + 1.050g K2 + 0.245g K16 1968 0.200g E1 + 0.245g K16 + 0.210g K11 + 0.200g E5 + 0.210g K6 + 0.210g K7 1969 0.200g E2 + 0.210g K11 + 0.245g K16 + 0.200g E5 + 0.210g K6 + 0.210g K9 1970 0.200g E3 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K6 + 0.210g K13 1971 1.000g E4 + 1.050g K11 + 1.000g E5 + 1.050g K6 + 0.245g K16 + 1.050g Kl 1972 1.000g El + 1.050g K11 + 1.000g E5 + 1.050g K6 + 1.050g K14 + 0.245g K16 1973 2.000g E2 + 0.245g K16 + 2.l00g K11 + 2.000g E5 + 2.l00g K6 + 2.100g K24 1974 1.000g E3 + 1.050g Kl 1 + 0.245g K16 + 1.000g E5 + 1.050g K6 + 1.050g K2 1975 0.200g E4 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K8 + 0.210g K9 1976 1.000g E1 + 1.050g Kl 1+ 1.000g E5 + 1.050g K7 + 0.245g K16 + 1.050g K13 1977 2.000g E2 + 2.100g K11 + 2.000g E5 + 2.100g K7 + 2.100g K1 + 0.245g K16 1978 0.200g E3 + 0.245g K16 + 0.210g K11 + 0.200g E5 + 0.210g K7 + 0.210g K14 1979 2.000g E4 + 2.100g Kl l+ 0.245g K16 + 2.000g E5 + 2.100g K7 + 2.100g K24 1980 0.200g E1 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K7 + 0.210g K2 1981 1.000g E2 + 1.050g Kl 1 + 1.000g E5 + 1.050g K9 + 0.245g K16 + 1.050g K13 1982 2.000g E3 + 2.100g KI l+ 2.000g E5 + 2.100g K9 + 2.100g Kl + 0.245g K16 1983 0.200g E4 + 0.245g K16 + 0.210g K11 + 0.200g E5 + 0.210g K9 + 0.210g K14 1984 0.200g El + 0.210g Kl 1 + 0.245g K16 + 0.200g E5 + 0.210g K9 + 0.210g K24 1985 0.200g E2 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K9 + 0.210g K2 1986 1.000g E3 + 1.050g Kl l+ 1.000g E5 + 1.050g K13 + 0.245g K16 + 1.050g K1 1987 1.000g E4 + 1.050g K11 + 1.000g E5 + 1.050g K13 + 1.050g K14 + 0.245g K16 1988 1.000g E1 + 0.245g K16 + 1.050g Kl l+ 1.000g E5 + 1.050g K13 + 1.050g K24 1989 2.000g E2 + 2.l00g K11 + 0.245g K16 + 2.000g E5 + 2.l00g K13 + 2.l00g K2 1990 2.000g E3 + 2.l00g K11 + 2.000g E5 + 0.245g K16 + 2.l00g K1 + 2.l00g K14 1991 0.200g E4 + 0.210g K11 + 0.200g E5 + 0.210g K1 + 0.245g K16 + 0.210g K24 1992 2.000g El + 2.100g K11 + 2.000g E5 + 2.100g K1 + 2.100g K2 + 0.245g K16 1993 2.000g E2 + 0.245g K16 + 2.100g K11 + 2.000g E5 + 2.100g K14 + 2.100g K24 1994 1.000g E3 + 1.050g K11 + 0.245g K16 + 1.000g E5 + 1.050g K14 + 1.050g K2 1995 2.000g E4 + 2.100g K11 + 2.000g E5 + 0.245g K16 + 2.100g K24 + 2.100g K2 1996 2.500g El + 2.625g K11 + 2.500g E7 + 2.625g K12 + 0.245g K16 1997 1.250g E2 + 0.245g K16 + 1.313g K11 + 1.250g E7 + 1.313g K6 1998 2.500g E3 + 2.625g K11 + 0.245g K16 + 2.500g E7 + 2.625g K7 1999 0.250g E4 + 0.263g K11 + 0.250g E7 + 0.245g K16 + 0.263g K9 2000 1.250g El + 1.313g Kl 1+ 1.250g E7 + 1.313g K13 + 0.245g K16 2001 2.500g E2 + 0.245g K16 + 2.625g Kl 1+ 2.500g E7 + 2.625g K1 2002 2.500g E3 + 2.625g Kl 1+ 0.245g K16 + 2.500g E7 + 2.625g K14 2003 2.500g E4 + 2.625g K11 + 2.500g E7 + 0.245g K16 + 2.625g K24 2004 2.500g El + 2.625g K11 + 2.500g E7 + 2.625g K2 + 0.245g K16 2005 2.000g E2 + 0.245g K16 + 2.100g K11 + 2.000g E7 + 2.100g K15 + 2.100g K6 2006 0.200g E3 + 0.210g K11 + 0.245g K16 + 0.200g E7 + 0.210g K12 + 0.210g K7 2007 2.000g E4 + 2.100g K11 + 2.000g E7 + 0.245g K16 + 2.100g K12 + 2.100g K9 2008 0.200g E1 + 0.210g K11 + 0.200g E7 + 0.210g K15 + 0.245g K16 + 0.210g K13 2009 2.000g E2 + 2.100g K11 + 2.000g E7 + 2.100g K12 + 2.100g Kl + 0.245g K16 2010 1.000g E3 + 0.245g K16 + 1.050g K11 + 1.000g E7 + 1.050g K12 + 1.050g K14 2011 2.000g E4 + 2.100g K11 + 0.245g K16 + 2.000g E7 + 2.100g K12 + 2.100g K24 2012 1.000g E1 + 1.050g K11 + 1.000g E7 + 0.245g K16 + 1.050g K12 + 1.050g K2 2013 1.000g E2 + 1.050g Kl 1+ 1.000g E7 + 1.050g K6 + 0.245g K16 + 1.050g K7 2014 2.000g E3 + 2.100g K11 + 2.000g E7 + 2.100g K6 + 2.100g K9 + 0.245g K16 2015 0.200gE4+0.245gK16+0.210gK11 + 0.200g E7 + 0.210g K6 + 0.210g K13 2016 1.000g E1 + 1.050g K11 + 0.245g K16 + 1.000g E7 + 1.050g K6 + 1.050g K1 2017 2.000g E2 + 2.100g K11 + 2.000g E7 + 0.245g K16 + 2.100g K6 + 2.l00g K14 2018 2.000g E3 + 2.100g Kl 1+ 2.000g E7 + 2.100g K6 + 0.245g K16 + 2.100g K24 2019 0.200g E4 + 0.210g K11 + 0.200g E7 + 0.210g K6 + 0.210g K2 + 0.245g K16 2020 2.000g E1 + 0.245g K16 + 2.100g K11 + 2.000g E7 + 2.100g K7 + 2.100g K9 2021 1.000g E2 + 1.050g K11 + 0.245g K16 + 1.000g E7 + 1.050g K21 + 1.050g K13 2022 1.000g E3 + 1.050g K11 + 1.000g E7 + 0.245g K16 + 1.050g K7 + 1.050g Kl 2023 2.000g E4 + 2.100g K11 + 2.000g E7 + 2.100g K7 + 0.245g K16 + 2.100g K14 2024 0.200g El + 0.210g K11 + 0.200g E7 + 0.210g K7 + 0.210g K24 + 0.245g K16 2025 0.200g E2 + 0.245g K16 + 0.210g K11 + 0.200g E7 + 0.210g K7 + 0.210g K2 2026 2.000g E3 + 2.100g Kl 1 + 0.245g K16 + 2.000g E7 + 2.100g K9 + 2.100g K13 2027 2.000g E4 + 2.100g K11 + 2.000g E7 + 0.245g K16 + 2.100g K9 + 2.100g K1 2028 0.200g El + 0.210g K11 + 0.200g E7 + 0.210g K9 + 0.245g K16 + 0.210g K14 2029 0.200g E2 + 0.210g K11 + 0.200g E7 + 0.210g K9 + 0.210g K24 + 0.245g K16 2030 1.000g E3 + 0.245g K16 + 1.050g K11 + 1.000g E7 + 1.050g K9 + 1.050g K2 2031 1.000g E4 + 1.050g K11 + 0.245g K16 + 1.000g E7 + 1.050g K13 + l.050g K1 2032 2.000g El + 2.100g Kl 1+ 2.000g E7 + 0.245g K16 + 2.100g K13 + 2.100g K14 2033 0.200g E2 + 0.210g K11 + 0.200g E7 + 0.210g K13 + 0.448g K16 + 0.210g K24 2034 2.000g E3 + 2.100g K11 + 2.000g E7 + 2.100g K13 + 2.100g K15 + 0.048g K16 2035 2.000g E4 + 0.448g K16 + 2.100g Kl l+ 2.000g E7 + 2.100g Kl + 2.100g K14 2036 0.200g El + 0.210g K11 + 0.448g K16 + 0.200g E7 + 0.210g Kl + 0.210g K24 2037 0.200g E2 + 0.210g Kl 1 + 0.200g E7 + 0.448g K16 + 0.210g K1 + 0.210g K2 2038 1.000g E3 + 1.050g K11 + 1.000g E7 + 1.050g K14 + 0.448g K16 + 1.050g K24 2039 0.200g E4 + 0.210g Kl 1+ 0.200g E7 + 0.210g K14 + 0.210g K2 + 0.448g K16 2040 0.200g El + 0.448g K16 + 0.210g K11 + 0.200g E7 + 0.210g K24 + 0.210g K2 2041 3.333g E2 + 3.500g K11 + 0.448g K16 + 3.500g K12 + 0.100g D3 2042 2.500g E3 + 2.625g K11 + 2.625g K12 + 0.448g K16 + 2.625g K6 2043 0.250g E4 + 0.263g K11 + 0.263g K12 + 0.263g K7 + 0.448g K16 2044 0.250g El + 0.448g K16 + 0.263g K11 + 0.263g K12 + 0.263g K9 2045 2.500g E2 + 2.625g Kl 1 + 0.448g K16 + 2.625g K12 + 2.625g K15 2046 0.250g E3 + 0.263g Kl 1 + 0.263g K12 + 0.448g K16 + 0.263g K1 2047 0.250g E4 + 0.263g Kl 1 + 0.263g K12 + 0.263g K14 + 0.448g K16 2048 1.250g E1 + 0.448g K16 + 1.313g K11 + 1.313g K12 + 1.313g K24 2049 2.500g E2 + 2.625g K11 + 0.448g K16 + 2.625g K12 + 2.625g K2 2050 0.200g E3 + 0.210g K11 + 0.210g K12 + 0.448g K16 + 0.210g K6 + 0.210g K7 2051 0.200g E4 + 0.210g K11 + 0.210g K12 + 0.210g K6 + 0.448g K16 + 0.210g K9 2052 2.000g El + 2.100g Kl 1 + 2.100g K12 + 2.100g K6 + 2.100g K13 + 0.448g 2053 1.000g E2 + 0.448g K16 + 1.050g K11 + 1.050g K12 + 1.050g K6 + 1.050g Kl 2054 0.200gE3+0.210gK11 + 0.448g K16 + 0.210g K12 + 0.210g K6 + 0.210g K14 2055 1.000g E4 + 1.050g K11 + 1.050g K12 + 0.448g K16 + 1.050g K6 + 1.050g K24 2056 0.200g E1 + 0.210g K11 + 0.210g 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2540 2.000g El + 2.100g K24 + 2.000g E6 + 0.462g K16 + 2.100g K12 + 2.100g Kl 2541 0.200g E2 + 0.210g K24 + 0.200g E6 + 0.210g K12 + 0.462g K16 + 0.210g K14 2542 0.200g E3 + 0.210g K24 + 0.200g E6 + 0.210g K12 + 0.210g K2 + 0.462g K16 2543 2.000g E4 + 0.462g K 16 + 2. l 00g K24 + 2.000g E6 + 2. l 00g K6 + 2.100g 2544 1.000g El + 1.050g K24 + 0.462g K16 + 1.000g E6 + 1.050g K6 + 1.050g K9 2545 0.200g E2 + 0.210g K24 + 0.200g E6 + 0.462g K16 + 0.210g K6 + 0.210g K13 2546 2.000g E3 + 2.100g K24 + 2.000g E6 + 2.100g K6 + 0.462g K16 + 2.100g 1(1 2547 2.000g E4 + 2.100g K24 + 2.000g E6 + 2.100g K6 + 2.100g K11 + 0.462g K16 2548 2.000g E1 + 0.462g K16 + 2.100g K24 + 2.000g E6 + 2.100g K6 + 2.100g K14 2549 0.200g E2 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K6 + 0.210g K2 2550 2.000g E3 + 2.100g K24 + 2.000g E6 + 0.462g K16 + 2.100g K7 + 2.100g K9 2551 1.000g E4 + 1.050g K24 + 1.000g E6 + 1.050g K7 + 0.462g K16 + 1.050g K13 2552 2.000g El + 2.100g K24 + 2.000g E6 + 2.100g K7 + 2.100g K1 + 0.462g K16 2553 2.000g E2 + 0.462g K16 + 2.100g K24 + 2.000g E6 + 2.100g K7 + 2.100g Kl 1 2554 0.200g E3 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K7 + 0.210g K14 2555 2.000g E4 + 2.100g K24 + 2.000g E6 + 0.462g K16 + 2.100g K7 + 2.100g K2 2556 1.000g El + 1.050g K24 + 1.000g E6 + 1.050g K9 + 0.462g K16 + 1.050g K13 2557 1.000g E2 + 1.050g K24 + 1.000g E6 + 1.050g K9 + 1.050g Kl + 0.462g K16 2558 1.000g E3 + 0.462g K16 + 1.050g K24 + 1.000g E6 + 1.050g K9 + 1.050g K11 2559 0.200g E4 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K9 + 0.210g K14 2560 1.000g El + 1.050g K24 + 1.000g E6 + 0.462g K16 + 1.050g K9 + 1.050g K2 2561 0.200g E2 + 0.210g K24 + 0.200g E6 + 0.210g K13 + 0.462g K16 + 0.210g K1 2562 0.200g E3 + 0.210g K24 + 0.200g E6 + 0.210g K22 + 0.210g K11 + 0.462g K16 2563 1.000g E4 + 0.462g K16 + 1.050g K24 + 1.000g E6 + 1.050g K13 + 1.050g K14 2564 2.000g El + 2.100g K24 + 0.462g K16 + 2.000g E6 + 2.100g K13 + 2.100g K2 2565 1.000g E2 + 1.050g K24 + 1.000g E6 + 0.462g K16 + 1.050g Kl + 1.050g K11 2566 2.000g E3 + 2.100g K24 + 2.000g E6 + 2.100g K1 + 0.462g K16 + 2.100g K14 2567 2.000g E4 + 2.100g K24 + 2.000g E6 + 2.100g K1 + 2.100g K2 + 0.462g K16 2568 1.000g E1 + 0.462g K16 + 1.050g K24 + 1.000g E6 + 1.050g K11 + 1.050g K14 2569 0.200g E2 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K11 + 0.210g K2 2570 1.000g E3 + 1.050g K24 + 1.000g E6 + 0.462g K16 + 1.050g K14 + 1.050g K2 2571 2.500g E4 + 2.625g K24 + 2.500g E5 + 2.625g K12 + 0.462g K16 2572 0.250g E1 + 0.462g K16 + 0.263g K24 + 0.250g E5 + 0.263g K6 2573 0.250g E2 + 0.263g K24 + 0.462g K16 + 0.250g E5 + 0.263g K7 2574 1.250g E3 + 1.313g K24 + 1.250g E5 + 1.665g K16 + 1.313g K9 2575 2.500g E4 + 2.625g K24 + 2.500g E5 + 2.625g K13 + 1.665g K16 2576 2.500g E1 + 1.665g K16 + 2.625g K24 + 2.500g E5 + 2.625g K1 2577 2.500g E2 + 2.625g K24 + 1.665g K16 + 2.500g E5 + 2.625g K11 2578 1.250g E3 + 1.313g K24 + 1.250g E5 + 1.665g K16 + 1.313g K14 2579 1.250g E4 + 1.313g K24 + 1.250g E5 + 1.313g K2 + 1.665g K16 2580 1.000g El + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K12 + 1.050g K6 2581 0.200g E2 + 0.210g K24 + 1.665g K16 + 0.200g E5 + 0.210g K12 + 0.210g K7 2582 1.000g E3 + 1.050g K24 + 1.000g E5 + 1.665g K16 + 1.050g K12 + 1.050g K9 2583 0.200g E4 + 0.210g K24 + 0.200g E5 + 0.210g K12 + 1.665g K16 + 0.210g K13 2584 0.200g El + 0.210g K24 + 0.200g E5 + 0.210g K12 + 0.210g K1 + 1.665g K16 2585 1.000g E2 + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K12 + 1.050g K11 2586 0.200g E3 + 0.210g K24 + 1.665g K16 + 0.200g E5 + 0.210g K12 + 0.210g K14 2587 1.000g E4 + 1.050g K24 + 1.000g E5 + 1.665g K16 + 1.050g K12 + 1.050g K2 2588 0.200g El + 0.210g K24 + 0.200g E5 + 0.210g K6 + 1.665g K16 + 0.210g K7 2589 2.000g E2 + 2.100g K24 + 2.000g E5 + 2.100g K6 + 2.100g K9 + 1.665g K16 2590 0.200g E3 + 1.665g K16 + 0.210g K24 + 0.200g E5 + 0.210g K6 + 0.210g K13 2591 1.000g E4 + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K6 + 1.050g KI
2592 2.000g E1 + 2.100g K24 + 2.000g E5 + 1.665g K16 + 2.100g K6 + 2.100g Kl 1 2593 0.200g E2 + 0.210g K24 + 0.200g E5 + 0.210g K6 + 1.665g K16 + 0.210g K14 2594 2.000g E3 + 2.100g K24 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 1.665g K16 2595 2.000g E4 + 1.665g K16 + 2.100g K24 + 2.000g E5 + 2.100g K7 + 2.100g K9 2596 1.000g El + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K7 + 1.050g K13 2597 0.200g E2 + 0.210g K24 + 0.200g E5 + 1.665g K16 + 0.210g K7 + 0.210g K1 2598 1.000g E3 + 1.050g K24 + 1.000g E5 + 1.050g K7 + 1.665g K16 + 1.050g Kl 1 2599 1.000g E4 + 1.050g K24 + 1.000g E5 + 1.050g K7 + 1.050g K14 + 1.665g K16 2600 1.000g E1 + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K7 + 1.050g K2 2601 1.000g E2 + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K9 + 1.050g K13 2602 0.200g E3 + 0.210g K24 + 0.200g E5 + 1.665g K16 + 0.210g K9 + 0.210g K1 2603 0.200g E4 + 0.210g K24 + 0.200g E5 + 0.210g K9 + 1.665g K16 + 0.210g K11 2604 1.000g El + 1.050g K24 + 1.000g E5 + 1.050g K9 + 1.050g K14 + 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0.200gE4+0.497gK16+0.210gK2+0.210gK6+0.210gK1 +0.210gK11 3032 0.200g E1 + 0.210g K2 + 0.497g K16 + 0.210g K6 + 0.210g K1 + 0.210g K14 3033 1.000g E2 + 1.050g K2 + 1.050g K6 + 0.497g K16 + 1.050g K1 + 1.050g K24 3034 1.000g E3 + 1.050g K2 + 1.050g K6 + 1.050g K11 + 0.497g K16 + 1.050g K14 3035 0.200g E4 + 0.210g K2 + 0.210g K6 + 0.210g K11 + 0.210g K24 + 0.497g K16 3036 1.000g El + 0.497g K16 + 1.050g K2 + 1.050g K6 + 1.050g K14 + 1.050g K24 3037 1.667g E2 + 1.750g K2 + 0.497g K16 + 1.750g K7 3038 0.250g E3 + 0.263g K2 + 0.263g K7 + 0.497g K16 + 0.263g K9 3039 1.250g E4 + 1.313g K2 + 1.313g K7 + 1.313g K13 + 0.497g K16 3040 2.500g El + 0.497g K16 + 2.625g K2 + 2.625g K7 + 2.625g K1 3041 2.500g E2 + 2.625g K2 + 0.497g K16 + 2.625g K7 + 2.625g Kl 1 3042 1.250g E3 + 1.313g K2 + 1.313g K7 + 0.497g K16 + 1.313g K14 3043 0.250g E4 + 0.263g K2 + 0.263g K7 + 0.263g K24 + 0.497g K16 3044 2.000g El + 0.497g K16 + 2.100g K2 + 2.100g K7 + 2.100g K9 + 2.100g K13 3045 1.000g E2 + 1.050g K2 + 0.497g K16 + 1.050g K7 + 1.050g K9 + 1.050g Kl 3046 1.000g E3 + 1.050g K2 + 1.050g K7 + 0.497g K16 + 1.050g K9 + 1.050g K11 3047 2.000g E4 + 2.100g K2 + 2.100g K7 + 2.100g K9 + 0.497g K16 + 2.100g K14 3048 0.200g E 1+ 0.210g K2 + 0.210g K7 + 0.210g K9 + 0.210g K24 + 0.497g K 16 3049 1.000g E2 + 0.497g K16 + 1.050g K2 + 1.050g K7 + 1.050g K13 + 1.050g K1 3050 2.000g E3 + 2.100g K2 + 0.497g K16 + 2.100g K21 + 2.100g K13 + 2.100g K11 3051 0.200g E4 + 0.210g K2 + 0.210g K7 + 0.497g K16 + 0.210g K13 + 0.210g K14 3052 1.000g El + 1.050g K2 + 1.050g K7 + 1.050g K13 + 0.497g K16 + 1.050g K24 3053 0.200g E2 + 0.210g K2 + 0.210g K8 + 0.210g K1 + 0.210g K11 + 0.497g K16 3054 2.000g E3 + 0.497g K16 + 2.l00g K2 + 2.l00g K7 + 2.l00g K1 + 2.l00g K14 3055 2.000g E4 + 2.100g K2 + 0.497g K16 + 2.100g K7 + 2.100g K1 + 2.100g K24 3056 1.000g E1 + 1.050g K2 + 1.050g K7 + 0.497g K16 + 1.050g K11 + 1.050g K14 3057 1.000g E2 + 1.050g K2 + 1.050g K7 + 1.050g K11 + 0.497g K16 + 1.050g K24 3058 0.200g E3 + 0.210g K2 + 0.210g K7 + 0.210g K14 + 0.210g K24 + 0.497g K16 3059 0.333g E4 + 0.497g K16 + 0.350g K2 + 0.350g K9 3060 0.250g El + 0.263g K2 + 0.497g K16 + 0.263g K9 + 0.263g K13 3061 0.250g E2 + 0.263g K2 + 0.263g K9 + 0.497g K16 + 0.263g K1 3062 0.250g E3 + 0.263g K2 + 0.263g K9 + 0.263g K11 + 0.497g K16 3063 2.500g E4 + 0.497g K16 + 2.625g K2 + 2.625g K9 + 2.625g K14 3064 1.250g E1 + 1.313g K2 + 0.497g K16 + 1.313g K9 + 1.313g K24 3065 0.200g E2 + 0.210g K2 + 0.210g K9 + 0.497g K16 + 0.210g K13 + 0.210g K1 3066 1.000g E3 + 1.050g K2 + 1.050g K9 + 1.050g K13 + 1.700g K16 + 1.050g Ki 1 3067 0.200g E4 + 0.210g K2 + 0.210g K9 + 0.210g K13 + 0.210g K14 + 1.700g K16 3068 0.200g E1 + 1.700g K16 + 0.210g K2 + 0.210g K9 + 0.210g K13 + 0.210g K24 3069 0.200g E2 + 0.210g K2 + 1.700g K16 + 0.210g K9 + 0.210g Kl + 0.210g K11 3070 0.200g E3 + 0.210g K2 + 0.210g K9 + 1.700g K16 + 0.210g K1 + 0.210g K14 3071 2.000g E4 + 2.100g K2 + 2.100g K9 + 2.100g K1 + 1.700g K16 + 2.100g K24 3072 1.000g E1 + 1.050g K2 + 1.050g K9 + 1.050g K11 + 1.050g K14 + 1.700g K16 3073 1.000g E2 + 1.700g K16 + 1.050g K2 + 1.050g K9 + 1.050g K11 + 1.050g K24 3074 0.200g E3 + 0.210g K2 + 1.700g K16 + 0.210g K9 + 0.210g K14 + 0.210g K24 3075 1.333g E8 + 0.020g K2 + 0.050g K25 + 1.700g K16 3076 2.500g El + 1.700g K16 + 2.625g K2 + 2.625g K13 + 2.625g K1 3077 0.250g E2 + 0.263g K2 + 1.700g K16 + 0.263g K13 + 0.263g K11 3078 1.250g E3 + 1.313g K2 + 1.313g K13 + 1.700g K16 + 1.313g K14 3079 1.250g E4 + 1.313g K2 + 1.313g K13 + 1.313g K24 + 1.700g K16 3080 1.000g E1 + 1.700g K16 + 1.050g K2 + 1.050g K13 + 1.050g K1 + 1.050g K11 3081 2.000g E2 + 2.100g K2 + 1.700g K16 + 2.100g K13 + 2.100g K1 + 2.100g K14 3082 0.200g E3 + 0.210g K2 + 0.210g K13 + 1.700g K16 + 0.210g Kl + 0.210g K24 3083 1.000g E4 + 1.050g K2 + 1.050g K13 + 1.050g K11 + 1.700g K16 + 1.050g K14 3084 0.200g E1 + 0.210g K2 + 0.210g K13 + 0.210g K11 + 0.210g K24 + 1.700g K16 3085 0.200g E2 + 1.700g K16 + 0.210g K2 + 0.210g K13 + 0.210g K14 + 0.210g K24 3086 3.333g E3 + 3.500g K2 + 1.700g K16 + 3.500g K1 3087 0.250g E4 + 0.263g K2 + 0.263g K1 + 1.700g K16 + 0.263g K11 3088 1.250gE1+1.313gK2+1.313gK1+1.313gK14+1.700gK16 3089 1.250g E2 + 1.700g K16 + 1.313g K2 + 1.313g K1 + 1.313g K24 3090 1.000g E3 + 1.050g K2 + 1.700g K16 + 1.050g K1 + 1.050g K11 + 1.050g K14 3091 1.000g E4 + 1.050g K2 + 1.050g K1 + 1.700g K16 + 1.050g K11 + 1.050g K24 3092 2.000g E1 + 2.100g K2 + 2.100g K1 + 2.100g K14 + 1.700g K16 + 2.100g K24 3093 0.333g E2 + 0.350g K2 + 0.350g Kl 1+ 1.700g K16 3094 1.250g E3 + 1.700g K16 + 1.313g K2 + 1.313g K11 + 1.313g K14 3095 1.250g E4 + 1.313g K2 + 1.700g K16 + 1.313g K11 + 1.313g K24 3096 2.000g El + 2.100g K2 + 2.l00g K11 + 1.700g K16 + 2.l00g K14 + 2.100g K24 3097 1.667g E2 + 1.750g K2 + 1.750g K14 + 1.700g K16 3098 0.250g E3 + 1.700g K16 + 0.263g K2 + 0.263g K14 + 0.263g K24 3099 1.667g E4 + 1.750g K2 + 1.700g K16 + 1.750g K24 3100 0.300g E1 + 0.100g E2 + 0.100g K8 + 0.100g K12 + 0.100g K13 + 0.100g Kl4 +
0.700g K16 + 0.200g J1 The large number of examples shown is based on the enormous flexibility for the formulator due to the sheer unlimited ability to use 3-amino-2,6-dimethylphenol in the context of keratin fiber coloring compositions. Many more compositions similar to those exemplified are possible by modification of compounds (dyes or additives) and their amount in the composition as such. All these are obvious alterations for the skilled person from those exemplified and are not included for the sake of conciseness.

Unless stated otherwise, all of the percentages given in the present application are percentages by weight.

The dimensions and values disclosed herein are not to be understood as being strictly limited to the exact numerical values recited. Instead, unless otherwise specified, each such dimension is intended to mean both the recited value and a functionally equivalent range surrounding that value. For example, a dimension disclosed as "40 mm" is intended to mean "about 40 mm".

Claims (6)

1. An aqueous or aqueous-alcoholic oxidation dye precursor composition comprising water, at least one coupler compound and at least one developer compound, wherein said at least one coupler compound includes at least one coupler selected from the group consisiting of 3-amino-

2,6-dimethylphenol and its inorganic or organic salt.

2. The aqueous or aqueous-alcoholic oxidation dye precursor composition as defined in claim 1, wherein said at least one coupler compound is present in a total amount of from 0.001 to 15 percent by weight.

3. A ready-to-apply hair dye mixture made by a method comprising the steps of:
a) providing an oxidation dye precursor composition comprising at least one coupler compound and at least one developer compound, said at least one coupler compound including at least one coupler selected from the group consisiting of 3-amino-2,6-dimethylphenol and its inorganic or organic salt;
b) mixing the oxidation dye precursor composition provided in step a) with an oxidizing agent immediately prior to application to form the ready-to-apply hair dye mixture.

4. The ready-to-apply hair dye mixture as defined in claim 3, wherein the oxidation dye precursor composition and the oxidizing agent are mixed with each other in a weight ratio of from 5:1 to 1:3 during the mixing.

5. A method of dyeing keratin fibers, said method comprising the steps of:
a) providing an oxidation dye precursor composition containing at least one coupler compound and at least one developer compound, said at least one coupler compound including at least one coupler selected from the group consisiting of 3-amino-2,6-dimethylphenol and its inorganic or organic salt;
b) mixing the oxidation dye precursor composition provided in step a) with an oxidizing agent to form a ready-to-apply dye mixture;
c) applying the ready-to-apply dye mixture to the keratin fibers to dye the keratin fibers

6. A method of dyeing keratin fibers, said method comprising the steps of:
a) providing a dye-carrying composition comprising at least one member selected from the group consisting of oxidation dye precursor compounds and direct-dyeing dye compounds, said dye-carrying composition including at least one ingredient selected from the group consisting of 3-amino-2,6-dimethylphenol and its inorganic or organic salt;
and b) applying the dye-carrying composition to the keratin fibers in order to dye the keratin fibers.