CA2553926C - Process and plant for electrodepositing copper - Google Patents

Process and plant for electrodepositing copper Download PDF

Info

Publication number: CA2553926C
Authority: CA; Canada
Prior art keywords: bars; cathode; electrolytic cell; contact; electrolysis
Prior art date: 2004-02-20
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA2553926A

Other languages

English (en)

French (fr)

Other versions

CA2553926A1 (en

Inventor

Nikola Anastasijevic

Jean-Paul Nepper

Martin Koeneke

Dirk Lohrberg

Tom Marttila

Henri Virtanen

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Metso Outotec Oyj

Original Assignee

Outokumpu Technology Oyj

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2004-02-20

Filing date

2005-02-04

Publication date

2012-06-05

2005-02-04 Application filed by Outokumpu Technology Oyj filed Critical Outokumpu Technology Oyj

2005-09-01 Publication of CA2553926A1 publication Critical patent/CA2553926A1/en

2012-06-05 Application granted granted Critical

2012-06-05 Publication of CA2553926C publication Critical patent/CA2553926C/en

Status Expired - Fee Related legal-status Critical Current

2025-02-04 Anticipated expiration legal-status Critical

Links

RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 77
239000010949 copper Substances 0.000 title claims abstract description 76
229910052802 copper Inorganic materials 0.000 title claims abstract description 75
238000000034 method Methods 0.000 title claims abstract description 63
238000005868 electrolysis reaction Methods 0.000 claims abstract description 59
239000003792 electrolyte Substances 0.000 claims abstract description 46
239000008151 electrolyte solution Substances 0.000 claims abstract description 27
239000012530 fluid Substances 0.000 claims description 48
239000000498 cooling water Substances 0.000 claims description 20
230000000284 resting effect Effects 0.000 claims description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
239000000203 mixture Substances 0.000 claims description 7
238000001816 cooling Methods 0.000 claims description 6
238000007373 indentation Methods 0.000 claims description 6
229910000831 Steel Inorganic materials 0.000 claims description 4
239000000463 material Substances 0.000 claims description 4
239000010959 steel Substances 0.000 claims description 4
241000711981 Sais Species 0.000 claims description 2
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 2
229920002554 vinyl polymer Polymers 0.000 claims description 2
239000008213 purified water Substances 0.000 claims 1
238000007670 refining Methods 0.000 abstract description 10
239000002184 metal Substances 0.000 abstract description 3
229910052751 metal Inorganic materials 0.000 abstract description 3
210000004027 cell Anatomy 0.000 description 55
241000196324 Embryophyta Species 0.000 description 21
229940021013 electrolyte solution Drugs 0.000 description 14
238000000605 extraction Methods 0.000 description 10
230000000875 corresponding effect Effects 0.000 description 8
239000007789 gas Substances 0.000 description 8
238000007654 immersion Methods 0.000 description 8
238000012545 processing Methods 0.000 description 8
238000012360 testing method Methods 0.000 description 8
238000000151 deposition Methods 0.000 description 7
230000008021 deposition Effects 0.000 description 7
238000004519 manufacturing process Methods 0.000 description 6
238000002844 melting Methods 0.000 description 6
230000008018 melting Effects 0.000 description 6
239000000243 solution Substances 0.000 description 6
230000003247 decreasing effect Effects 0.000 description 5
238000009826 distribution Methods 0.000 description 5
238000011161 development Methods 0.000 description 4
238000002386 leaching Methods 0.000 description 4
230000002829 reductive effect Effects 0.000 description 4
JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
229910001431 copper ion Inorganic materials 0.000 description 3
230000000694 effects Effects 0.000 description 3
239000007788 liquid Substances 0.000 description 3
239000010935 stainless steel Substances 0.000 description 3
229910001220 stainless steel Inorganic materials 0.000 description 3
QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 description 2
239000005751 Copper oxide Substances 0.000 description 2
239000004020 conductor Substances 0.000 description 2
229910000431 copper oxide Inorganic materials 0.000 description 2
239000007772 electrode material Substances 0.000 description 2
238000009854 hydrometallurgy Methods 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000011068 loading method Methods 0.000 description 2
238000012423 maintenance Methods 0.000 description 2
238000009853 pyrometallurgy Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
239000010802 sludge Substances 0.000 description 2
238000012546 transfer Methods 0.000 description 2
244000007835 Cyamopsis tetragonoloba Species 0.000 description 1
229910000978 Pb alloy Inorganic materials 0.000 description 1
239000010405 anode material Substances 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
238000005452 bending Methods 0.000 description 1
230000005540 biological transmission Effects 0.000 description 1
238000007664 blowing Methods 0.000 description 1
239000010406 cathode material Substances 0.000 description 1
210000002421 cell wall Anatomy 0.000 description 1
DVRDHUBQLOKMHZ-UHFFFAOYSA-N chalcopyrite Chemical compound [S-2].[S-2].[Fe+2].[Cu+2] DVRDHUBQLOKMHZ-UHFFFAOYSA-N 0.000 description 1
229910052951 chalcopyrite Inorganic materials 0.000 description 1
238000000576 coating method Methods 0.000 description 1
238000010276 construction Methods 0.000 description 1
239000002826 coolant Substances 0.000 description 1
229910000365 copper sulfate Inorganic materials 0.000 description 1
ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
BQJTUDIVKSVBDU-UHFFFAOYSA-L copper;sulfuric acid;sulfate Chemical compound [Cu+2].OS(O)(=O)=O.[O-]S([O-])(=O)=O BQJTUDIVKSVBDU-UHFFFAOYSA-L 0.000 description 1
238000005260 corrosion Methods 0.000 description 1
230000007797 corrosion Effects 0.000 description 1
238000000280 densification Methods 0.000 description 1
238000013461 design Methods 0.000 description 1
230000005518 electrochemistry Effects 0.000 description 1
238000005363 electrowinning Methods 0.000 description 1
239000000284 extract Substances 0.000 description 1
238000005188 flotation Methods 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
230000003455 independent Effects 0.000 description 1
239000011810 insulating material Substances 0.000 description 1
239000011159 matrix material Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
230000036961 partial effect Effects 0.000 description 1
238000011020 pilot scale process Methods 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000001223 reverse osmosis Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
125000006850 spacer group Chemical group 0.000 description 1
239000007858 starting material Substances 0.000 description 1
229940032330 sulfuric acid Drugs 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
239000000725 suspension Substances 0.000 description 1
238000002604 ultrasonography Methods 0.000 description 1
238000009827 uniform distribution Methods 0.000 description 1
238000012795 verification Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/06—Operating or servicing
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/12—Electrolytic production, recovery or refining of metals by electrolysis of solutions of copper
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/02—Electrodes; Connections thereof

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Electrochemistry (AREA)
Materials Engineering (AREA)
Metallurgy (AREA)
Organic Chemistry (AREA)
Electrolytic Production Of Metals (AREA)

CA2553926A 2004-02-20 2005-02-04 Process and plant for electrodepositing copper Expired - Fee Related CA2553926C (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DE102004008813.6		2004-02-20
DE102004008813A DE102004008813B3 (de)	2004-02-20	2004-02-20	Verfahren und Anlage zum elektrochemischen Abscheiden von Kupfer
PCT/EP2005/001127 WO2005080640A2 (en)	2004-02-20	2005-02-04	Process and plant for electrodepositing copper

Publications (2)

Publication Number	Publication Date
CA2553926A1 CA2553926A1 (en)	2005-09-01
CA2553926C true CA2553926C (en)	2012-06-05

Family

ID=34877080

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA2553926A Expired - Fee Related CA2553926C (en)	2004-02-20	2005-02-04	Process and plant for electrodepositing copper

Country Status (6)

Country	Link
US (1)	US20080035473A1 (de)
AU (1)	AU2005214817B2 (de)
CA (1)	CA2553926C (de)
DE (1)	DE102004008813B3 (de)
PE (1)	PE20060033A1 (de)
WO (1)	WO2005080640A2 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NO324587B1 (no) *	2006-03-15	2007-11-26	Advanced Hydrocarbon Mapping A	Elektrisk feltsensor for marine omgivelser
LU91518B1 (en) *	2009-01-21	2010-01-21	Wurth Paul Sa	Hydrometallurgical production of metal
PL410261A1 (pl) *	2010-08-11	2015-05-11	Outotec Oyj	Urządzenie do elektroprodukcji lub elektrorafinacji materiału
BG110844A (bg) *	2011-02-04	2012-10-31	"Кцм" Ад	Метод и устройство за електроекстракция на цинк от сулфатни разтвори
US8597477B2 (en) *	2011-02-16	2013-12-03	Freeport-Mcmoran Corporation	Contact bar assembly, system including the contact bar assembly, and method of using same
US9234287B2 (en) *	2011-07-12	2016-01-12	Pultrusion Technique Inc.	Contact bar and capping board for supporting symmetrical electrodes for enhanced electrolytic refining of metals
CN113122895B (zh) *	2021-03-19	2022-09-20	同济大学	一种阴极并联调控电化学诱导矿物沉积速率的方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2443112A (en) *	1942-05-30	1948-06-08	American Smelting Refining	Contact structure for electrolytic cells
US3530047A (en) *	1968-10-15	1970-09-22	American Smelting Refining	Stripping of sheet metal electrodeposits from starting sheet blanks
GB1468889A (en) *	1973-04-12	1977-03-30	Crucible Inc	Method and assembly for use in making powder metallurgy articles having internal passages
US4098668A (en) *	1974-08-21	1978-07-04	Continental Copper & Steel Industries, Inc.	Electrolyte metal extraction
GB1460089A (en) *	1974-11-08	1976-12-31	Imp Metal Ind Kynoch Ltd	Cathode assembly for electrolysis
US4066520A (en) *	1976-09-01	1978-01-03	Envirotech Corporation	Slurry electrowinning process
CA1140892A (en) *	1980-01-28	1983-02-08	Cominco Ltd.	Increased spacing of end electrodes in electro-deposition of metals
IT1267237B1 (it) *	1994-05-11	1997-01-28	Danieli Off Mecc	Elettrodo di fondo raffreddato per un forno elettrico in corrente continua
DE19525360A1 (de) *	1995-07-12	1997-01-16	Metallgesellschaft Ag	Anode zur elektrolytischen Gewinnung von Metallen
JPH09228090A (ja) *	1996-02-21	1997-09-02	Nikko Kinzoku Kk	湿式電解採取または電解精製用陰極板
FI104839B (fi) *	1998-05-06	2000-04-14	Outokumpu Oy	Elektrolyysialtaan virtakiskorakenne
FI982569A (fi) *	1998-11-27	2000-05-28	Outokumpu Oy	Laite metallisaostuman erottamiseksi katodilta
DE19940698C2 (de) *	1999-08-27	2002-08-01	Mg Technologies Ag	Elektrolyseanlage für die Metallgewinnung
AUPQ584800A0 (en) *	2000-02-25	2000-03-16	Comalco Aluminium Limited	An electrical reduction cell
US6398939B1 (en) *	2001-03-09	2002-06-04	Phelps Dodge Corporation	Method and apparatus for controlling flow in an electrodeposition process

2004
- 2004-02-20 DE DE102004008813A patent/DE102004008813B3/de not_active Expired - Fee Related
2005
- 2005-02-04 CA CA2553926A patent/CA2553926C/en not_active Expired - Fee Related
- 2005-02-04 US US10/589,592 patent/US20080035473A1/en not_active Abandoned
- 2005-02-04 WO PCT/EP2005/001127 patent/WO2005080640A2/en active Application Filing
- 2005-02-04 AU AU2005214817A patent/AU2005214817B2/en not_active Ceased
- 2005-02-14 PE PE2005000173A patent/PE20060033A1/es active IP Right Grant

Also Published As

Publication number	Publication date
DE102004008813B3 (de)	2005-12-01
WO2005080640A3 (en)	2006-06-22
US20080035473A1 (en)	2008-02-14
AU2005214817B2 (en)	2010-11-11
AU2005214817A1 (en)	2005-09-01
CA2553926A1 (en)	2005-09-01
PE20060033A1 (es)	2006-03-01
WO2005080640A2 (en)	2005-09-01

Legal Events

Date	Code	Title	Description
2010-02-01	EEER	Examination request
2022-09-15	MKLA	Lapsed	Effective date: 20210204

Publication	Publication Date	Title
CA2553926C (en)	2012-06-05	Process and plant for electrodepositing copper
US3875041A (en)	1975-04-01	Apparatus for the electrolytic recovery of metal employing improved electrolyte convection
US11060199B2 (en)	2021-07-13	Electrode configurations for electrolytic cells and related methods
CN105132944A (zh)	2015-12-09	一种制备高纯铜的方法及装置
FI60039B (fi)	1981-07-31	Elektrokemisk anordning
BR112018007493B1 (pt)	2022-11-08	Dispositivo do tipo prensa filtro para eletrodeposição de metal a partir de soluções que o contêm
CN203890449U (zh)	2014-10-22	一种高纯铜的制备装置
CA1072055A (en)	1980-02-19	Electrolytic cell and circulating method for electrolyte
CN101680102B (zh)	2011-11-09	电解槽及其操作方法
CA1232868A (en)	1988-02-16	Arrangement of busbars for electrolytic reduction cell
US3928152A (en)	1975-12-23	Method for the electrolytic recovery of metal employing improved electrolyte convection
US4110179A (en)	1978-08-29	Process and device for the production of aluminium by the electrolysis of a molten charge
US4313811A (en)	1982-02-02	Arrangement of busbars for electrolytic cells
WO2017144912A1 (en)	2017-08-31	Equipment for a metal electrowinning or liberator process and way of operating the process
US3775281A (en)	1973-11-27	Plant for production of aluminum by electrolysis
CA1126684A (en)	1982-06-29	Bipolar refining of lead
EP3452640B1 (de)	2020-03-25	Ausrüstung zur entkupferung eines elektroraffinationsverfahrens und verfahren zum betrieb des verfahrens
US20150034491A1 (en)	2015-02-05	Anode and method of operating an electrolysis cell
US4359377A (en)	1982-11-16	Busbar arrangement for electrolytic cells
MXPA06009412A (en)	2007-04-10	Process and plant for electrodepositing copper
US4891105A (en)	1990-01-02	Method and apparatus for electrolytic refining of copper and production of copper wires for electrical purposes
US4196067A (en)	1980-04-01	Absorption of magnetic field lines in electrolytic reduction cells
CN213624406U (zh)	2021-07-06	带有通孔锡锭的电解装置
RU2022717C1 (ru)	1994-11-15	Способ получения медного порошка электролизом из сульфатных растворов и устройством для его осуществления
US10584423B2 (en)	2020-03-10	EWS module device for electro-winning and/or electro-refining, interconnection process, and operating process thereof