CA2362955C - Multi-phase detergent tablet - Google Patents

Multi-phase detergent tablet Download PDF

Info

Publication number: CA2362955C
Authority: CA; Canada
Prior art keywords: phase; weight; acid; alkali metal; mixtures
Prior art date: 1999-03-04
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA002362955A

Other languages

English (en)

French (fr)

Other versions

CA2362955A1 (en

Inventor

Steven Baldwin Mcgowan

James Iain Kinloch

Alasdair Duncan Mcgregor

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Procter and Gamble Co

Original Assignee

Procter and Gamble Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1999-03-04

Filing date

2000-02-29

Publication date

2005-07-05

2000-02-29 Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co

2000-09-08 Publication of CA2362955A1 publication Critical patent/CA2362955A1/en

2005-07-05 Application granted granted Critical

2005-07-05 Publication of CA2362955C publication Critical patent/CA2362955C/en

2020-02-29 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

239000003599 detergent Substances 0.000 title claims abstract description 127
239000000203 mixture Substances 0.000 claims abstract description 243
239000000654 additive Substances 0.000 claims abstract description 40
230000000996 additive effect Effects 0.000 claims abstract description 40
229920005646 polycarboxylate Polymers 0.000 claims abstract description 37
239000007787 solid Substances 0.000 claims abstract description 18
238000005406 washing Methods 0.000 claims abstract description 10
239000000853 adhesive Substances 0.000 claims abstract description 6
230000001070 adhesive effect Effects 0.000 claims abstract description 6
-1 solubility aids Substances 0.000 claims description 154
239000004094 surface-active agent Substances 0.000 claims description 76
150000003839 salts Chemical class 0.000 claims description 60
239000002253 acid Substances 0.000 claims description 44
238000000034 method Methods 0.000 claims description 34
239000000843 powder Substances 0.000 claims description 34
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 34
239000007788 liquid Substances 0.000 claims description 27
229910052783 alkali metal Inorganic materials 0.000 claims description 26
229920001577 copolymer Polymers 0.000 claims description 23
239000000243 solution Substances 0.000 claims description 20
239000002245 particle Substances 0.000 claims description 17
150000001340 alkali metals Chemical class 0.000 claims description 16
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 14
239000000178 monomer Substances 0.000 claims description 13
TTZMPOZCBFTTPR-UHFFFAOYSA-N O=P1OCO1 Chemical compound O=P1OCO1 TTZMPOZCBFTTPR-UHFFFAOYSA-N 0.000 claims description 12
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 10
229910000288 alkali metal carbonate Inorganic materials 0.000 claims description 10
239000002738 chelating agent Substances 0.000 claims description 10
239000008187 granular material Substances 0.000 claims description 10
150000008041 alkali metal carbonates Chemical class 0.000 claims description 9
229910052936 alkali metal sulfate Inorganic materials 0.000 claims description 9
150000001408 amides Chemical class 0.000 claims description 9
150000002148 esters Chemical class 0.000 claims description 9
PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims description 8
229920002678 cellulose Polymers 0.000 claims description 8
239000001913 cellulose Substances 0.000 claims description 8
NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 claims description 8
229910052757 nitrogen Inorganic materials 0.000 claims description 8
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 7
229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 7
235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 7
229940071207 sesquicarbonate Drugs 0.000 claims description 7
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 7
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 6
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 6
238000009826 distribution Methods 0.000 claims description 6
239000004615 ingredient Substances 0.000 claims description 6
238000004519 manufacturing process Methods 0.000 claims description 6
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 5
KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 5
229910052910 alkali metal silicate Inorganic materials 0.000 claims description 5
150000001860 citric acid derivatives Chemical class 0.000 claims description 5
239000007884 disintegrant Substances 0.000 claims description 5
235000019832 sodium triphosphate Nutrition 0.000 claims description 5
HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 claims description 4
RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 4
VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims description 4
229920002472 Starch Polymers 0.000 claims description 4
235000010443 alginic acid Nutrition 0.000 claims description 4
229920000615 alginic acid Polymers 0.000 claims description 4
FUSUHKVFWTUUBE-UHFFFAOYSA-N buten-2-one Chemical compound CC(=O)C=C FUSUHKVFWTUUBE-UHFFFAOYSA-N 0.000 claims description 4
239000006185 dispersion Substances 0.000 claims description 4
238000001035 drying Methods 0.000 claims description 4
239000000839 emulsion Substances 0.000 claims description 4
ROBFUDYVXSDBQM-UHFFFAOYSA-N hydroxymalonic acid Chemical compound OC(=O)C(O)C(O)=O ROBFUDYVXSDBQM-UHFFFAOYSA-N 0.000 claims description 4
MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 claims description 4
239000002002 slurry Substances 0.000 claims description 4
235000019698 starch Nutrition 0.000 claims description 4
239000008107 starch Substances 0.000 claims description 4
235000000346 sugar Nutrition 0.000 claims description 4
229920001567 vinyl ester resin Polymers 0.000 claims description 4
CIEZZGWIJBXOTE-UHFFFAOYSA-N 2-[bis(carboxymethyl)amino]propanoic acid Chemical compound OC(=O)C(C)N(CC(O)=O)CC(O)=O CIEZZGWIJBXOTE-UHFFFAOYSA-N 0.000 claims description 3
HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 3
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
UJHYZJSRAHZNFM-UHFFFAOYSA-N O=P1OCCOP(=O)O1 Chemical compound O=P1OCCOP(=O)O1 UJHYZJSRAHZNFM-UHFFFAOYSA-N 0.000 claims description 3
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 3
238000013019 agitation Methods 0.000 claims description 3
239000012153 distilled water Substances 0.000 claims description 3
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 3
239000011976 maleic acid Substances 0.000 claims description 3
239000001632 sodium acetate Substances 0.000 claims description 3
235000017281 sodium acetate Nutrition 0.000 claims description 3
150000008163 sugars Chemical class 0.000 claims description 3
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 3
JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 claims description 2
CQWXKASOCUAEOW-UHFFFAOYSA-N 2-[2-(carboxymethoxy)ethoxy]acetic acid Chemical compound OC(=O)COCCOCC(O)=O CQWXKASOCUAEOW-UHFFFAOYSA-N 0.000 claims description 2
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 2
QEVGZEDELICMKH-UHFFFAOYSA-N Diglycolic acid Chemical compound OC(=O)COCC(O)=O QEVGZEDELICMKH-UHFFFAOYSA-N 0.000 claims description 2
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
XYLMUPLGERFSHI-UHFFFAOYSA-N alpha-Methylstyrene Chemical compound CC(=C)C1=CC=CC=C1 XYLMUPLGERFSHI-UHFFFAOYSA-N 0.000 claims description 2
KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical class O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 2
239000001530 fumaric acid Substances 0.000 claims description 2
150000004677 hydrates Chemical class 0.000 claims description 2
LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 claims description 2
235000002906 tartaric acid Nutrition 0.000 claims description 2
239000011975 tartaric acid Substances 0.000 claims description 2
DWPPQBRQGKAHDL-UHFFFAOYSA-K potassium disodium 3-carboxy-3-hydroxypentanedioate 2,3,4-trihydroxy-4-oxobutanoate Chemical compound C(CC(O)(C(=O)[O-])CC(=O)[O-])(=O)[O-].[Na+].C(=O)(O)C(O)C(O)C(=O)O.[K+].[Na+] DWPPQBRQGKAHDL-UHFFFAOYSA-K 0.000 claims 1
238000004090 dissolution Methods 0.000 abstract description 17
238000004140 cleaning Methods 0.000 abstract description 11
230000016507 interphase Effects 0.000 abstract description 4
150000001875 compounds Chemical class 0.000 description 69
102000004190 Enzymes Human genes 0.000 description 60
108090000790 Enzymes Proteins 0.000 description 60
229940088598 enzyme Drugs 0.000 description 60
239000002243 precursor Substances 0.000 description 57
239000007844 bleaching agent Substances 0.000 description 56
125000004432 carbon atom Chemical group C* 0.000 description 49
125000000217 alkyl group Chemical group 0.000 description 48
239000003795 chemical substances by application Substances 0.000 description 41
239000000463 material Substances 0.000 description 41
239000003054 catalyst Substances 0.000 description 38
108010065511 Amylases Proteins 0.000 description 32
102000013142 Amylases Human genes 0.000 description 32
239000011248 coating agent Substances 0.000 description 31
235000019418 amylase Nutrition 0.000 description 30
239000000047 product Substances 0.000 description 27
229940025131 amylases Drugs 0.000 description 26
238000007906 compression Methods 0.000 description 26
230000006835 compression Effects 0.000 description 26
108091005804 Peptidases Proteins 0.000 description 24
102000035195 Peptidases Human genes 0.000 description 24
238000000576 coating method Methods 0.000 description 24
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 24
239000002736 nonionic surfactant Substances 0.000 description 23
239000002689 soil Substances 0.000 description 22
108010084185 Cellulases Proteins 0.000 description 21
102000005575 Cellulases Human genes 0.000 description 21
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 21
229920000642 polymer Polymers 0.000 description 21
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 20
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 20
229910017052 cobalt Inorganic materials 0.000 description 20
239000010941 cobalt Substances 0.000 description 20
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 20
239000011734 sodium Substances 0.000 description 20
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 19
239000004365 Protease Substances 0.000 description 19
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 19
229910052708 sodium Inorganic materials 0.000 description 19
239000003446 ligand Substances 0.000 description 18
108090001060 Lipase Proteins 0.000 description 17
102000004882 Lipase Human genes 0.000 description 17
238000004851 dishwashing Methods 0.000 description 17
239000010457 zeolite Substances 0.000 description 17
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 16
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 16
239000004367 Lipase Substances 0.000 description 16
230000007797 corrosion Effects 0.000 description 16
238000005260 corrosion Methods 0.000 description 16
235000019421 lipase Nutrition 0.000 description 16
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 15
239000004115 Sodium Silicate Substances 0.000 description 15
229910000323 aluminium silicate Inorganic materials 0.000 description 15
230000000694 effects Effects 0.000 description 15
239000003112 inhibitor Substances 0.000 description 15
239000010410 layer Substances 0.000 description 15
239000011572 manganese Substances 0.000 description 15
229910052709 silver Inorganic materials 0.000 description 15
239000004332 silver Substances 0.000 description 15
239000004382 Amylase Substances 0.000 description 14
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 14
125000003118 aryl group Chemical group 0.000 description 14
235000014113 dietary fatty acids Nutrition 0.000 description 14
239000000194 fatty acid Substances 0.000 description 14
229930195729 fatty acid Natural products 0.000 description 14
150000007513 acids Chemical class 0.000 description 13
239000011230 binding agent Substances 0.000 description 13
239000000975 dye Substances 0.000 description 13
229910001385 heavy metal Inorganic materials 0.000 description 13
239000000344 soap Substances 0.000 description 13
229910052911 sodium silicate Inorganic materials 0.000 description 13
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 12
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 12
125000000129 anionic group Chemical group 0.000 description 12
150000002500 ions Chemical class 0.000 description 12
229910052748 manganese Inorganic materials 0.000 description 12
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 12
235000019419 proteases Nutrition 0.000 description 12
239000003352 sequestering agent Substances 0.000 description 12
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 12
YNJSNEKCXVFDKW-UHFFFAOYSA-N 3-(5-amino-1h-indol-3-yl)-2-azaniumylpropanoate Chemical compound C1=C(N)C=C2C(CC(N)C(O)=O)=CNC2=C1 YNJSNEKCXVFDKW-UHFFFAOYSA-N 0.000 description 11
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 11
229920003171 Poly (ethylene oxide) Polymers 0.000 description 11
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 11
125000002947 alkylene group Chemical group 0.000 description 11
150000001768 cations Chemical class 0.000 description 11
239000001257 hydrogen Chemical group 0.000 description 11
229910052739 hydrogen Chemical group 0.000 description 11
150000004967 organic peroxy acids Chemical class 0.000 description 11
150000004965 peroxy acids Chemical class 0.000 description 11
241000894007 species Species 0.000 description 11
150000008051 alkyl sulfates Chemical class 0.000 description 10
150000007942 carboxylates Chemical class 0.000 description 10
150000002191 fatty alcohols Chemical class 0.000 description 10
JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 9
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 9
WAEMQWOKJMHJLA-UHFFFAOYSA-N Manganese(2+) Chemical class [Mn+2] WAEMQWOKJMHJLA-UHFFFAOYSA-N 0.000 description 9
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 9
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 9
229910021536 Zeolite Inorganic materials 0.000 description 9
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 9
150000004665 fatty acids Chemical class 0.000 description 9
RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 9
239000011591 potassium Substances 0.000 description 9
229910052700 potassium Inorganic materials 0.000 description 9
125000001424 substituent group Chemical group 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
229910019142 PO4 Inorganic materials 0.000 description 8
150000001298 alcohols Chemical class 0.000 description 8
125000002877 alkyl aryl group Chemical group 0.000 description 8
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 8
235000021317 phosphate Nutrition 0.000 description 8
229920001223 polyethylene glycol Polymers 0.000 description 8
150000003467 sulfuric acid derivatives Chemical class 0.000 description 8
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 7
102000003992 Peroxidases Human genes 0.000 description 7
229920002125 Sokalan® Polymers 0.000 description 7
150000001450 anions Chemical group 0.000 description 7
125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 7
235000010980 cellulose Nutrition 0.000 description 7
238000013270 controlled release Methods 0.000 description 7
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150000002430 hydrocarbons Chemical class 0.000 description 7
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NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 7
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235000008733 Citrus aurantifolia Nutrition 0.000 description 6
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 6
BGRWYDHXPHLNKA-UHFFFAOYSA-N Tetraacetylethylenediamine Chemical compound CC(=O)N(C(C)=O)CCN(C(C)=O)C(C)=O BGRWYDHXPHLNKA-UHFFFAOYSA-N 0.000 description 6
235000011941 Tilia x europaea Nutrition 0.000 description 6
239000012190 activator Substances 0.000 description 6
229910052784 alkaline earth metal Inorganic materials 0.000 description 6
150000001412 amines Chemical class 0.000 description 6
239000003945 anionic surfactant Substances 0.000 description 6
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 6
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239000000460 chlorine Substances 0.000 description 6
239000004927 clay Substances 0.000 description 6
230000000295 complement effect Effects 0.000 description 6
108010005400 cutinase Proteins 0.000 description 6
229910052736 halogen Inorganic materials 0.000 description 6
150000002367 halogens Chemical class 0.000 description 6
XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
239000004571 lime Substances 0.000 description 6
229910052751 metal Inorganic materials 0.000 description 6
239000002184 metal Substances 0.000 description 6
230000003287 optical effect Effects 0.000 description 6
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239000001301 oxygen Substances 0.000 description 6
MWNQXXOSWHCCOZ-UHFFFAOYSA-L sodium;oxido carbonate Chemical compound [Na+].[O-]OC([O-])=O MWNQXXOSWHCCOZ-UHFFFAOYSA-L 0.000 description 6
229940100515 sorbitan Drugs 0.000 description 6
230000000087 stabilizing effect Effects 0.000 description 6
238000006467 substitution reaction Methods 0.000 description 6
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 6
239000007916 tablet composition Substances 0.000 description 6
238000012546 transfer Methods 0.000 description 6
241000193830 Bacillus <bacterium> Species 0.000 description 5
229920002134 Carboxymethyl cellulose Polymers 0.000 description 5
108010059892 Cellulase Proteins 0.000 description 5
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 5
DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 description 5
102000004157 Hydrolases Human genes 0.000 description 5
108090000604 Hydrolases Proteins 0.000 description 5
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 5
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 5
ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 5
125000000539 amino acid group Chemical group 0.000 description 5
150000001413 amino acids Chemical class 0.000 description 5
150000008064 anhydrides Chemical class 0.000 description 5
230000001580 bacterial effect Effects 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
229910052801 chlorine Inorganic materials 0.000 description 5
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238000005507 spraying Methods 0.000 description 1
150000003890 succinate salts Chemical class 0.000 description 1
KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
239000005720 sucrose Substances 0.000 description 1
229960004793 sucrose Drugs 0.000 description 1
229940035023 sucrose monostearate Drugs 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000002600 sunflower oil Substances 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1
239000000271 synthetic detergent Substances 0.000 description 1
108010038851 tannase Proteins 0.000 description 1
229940095064 tartrate Drugs 0.000 description 1
229960003080 taurine Drugs 0.000 description 1
235000013616 tea Nutrition 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1
150000004026 tertiary sulfonium compounds Chemical class 0.000 description 1
TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
ODBLHEXUDAPZAU-UHFFFAOYSA-N threo-D-isocitric acid Natural products OC(=O)C(O)C(C(O)=O)CC(O)=O ODBLHEXUDAPZAU-UHFFFAOYSA-N 0.000 description 1
125000000341 threoninyl group Chemical group [H]OC([H])(C([H])([H])[H])C([H])(N([H])[H])C(*)=O 0.000 description 1
JOXIMZWYDAKGHI-UHFFFAOYSA-M toluene-4-sulfonate Chemical compound CC1=CC=C(S([O-])(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-M 0.000 description 1
230000001052 transient effect Effects 0.000 description 1
150000003852 triazoles Chemical group 0.000 description 1
150000005691 triesters Chemical class 0.000 description 1
ITMCEJHCFYSIIV-UHFFFAOYSA-M triflate Chemical compound [O-]S(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-M 0.000 description 1
JSPLKZUTYZBBKA-UHFFFAOYSA-N trioxidane Chemical class OOO JSPLKZUTYZBBKA-UHFFFAOYSA-N 0.000 description 1
HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 1
WCTAGTRAWPDFQO-UHFFFAOYSA-K trisodium;hydrogen carbonate;carbonate Chemical compound [Na+].[Na+].[Na+].OC([O-])=O.[O-]C([O-])=O WCTAGTRAWPDFQO-UHFFFAOYSA-K 0.000 description 1
239000010981 turquoise Substances 0.000 description 1
OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
235000013799 ultramarine blue Nutrition 0.000 description 1
150000003672 ureas Chemical class 0.000 description 1
229940005605 valeric acid Drugs 0.000 description 1
239000004474 valine Substances 0.000 description 1
125000002987 valine group Chemical group [H]N([H])C([H])(C(*)=O)C([H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
235000015112 vegetable and seed oil Nutrition 0.000 description 1
239000008158 vegetable oil Substances 0.000 description 1
235000014101 wine Nutrition 0.000 description 1
229910052727 yttrium Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
- C11D17/0065—Solid detergents containing builders
- C11D17/0073—Tablets
- C11D17/0078—Multilayered tablets
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/36—Organic compounds containing phosphorus
- C11D3/364—Organic compounds containing phosphorus containing nitrogen
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
- C11D3/3761—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in solid compositions
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Emergency Medicine (AREA)
Detergent Compositions (AREA)

CA002362955A 1999-03-04 2000-02-29 Multi-phase detergent tablet Expired - Fee Related CA2362955C (en)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
GB9904882.9		1999-03-04
GB9904882A GB2347431A (en)	1999-03-04	1999-03-04	Detergent tablet
PCT/US2000/005302 WO2000052130A1 (en)	1999-03-04	2000-02-29	Detergent tablet

Publications (2)

Publication Number	Publication Date
CA2362955A1 CA2362955A1 (en)	2000-09-08
CA2362955C true CA2362955C (en)	2005-07-05

Family

ID=10848878

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002362955A Expired - Fee Related CA2362955C (en)	1999-03-04	2000-02-29	Multi-phase detergent tablet

Country Status (7)

Country	Link
EP (1)	EP1159396A1 (es)
JP (1)	JP2002538270A (es)
AU (1)	AU3862100A (es)
CA (1)	CA2362955C (es)
GB (1)	GB2347431A (es)
MX (1)	MXPA01008901A (es)
WO (1)	WO2000052130A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE10010760A1 (de) *	2000-03-04	2001-09-20	Henkel Kgaa	Mehrphasige Wasch- und Reinigungsmittelformkörper mit nicht-gepreßten Anteilen
DE102004011256B4 (de) *	2004-03-09	2007-11-15	Henkel Kgaa	Mehrphasentabletten mit verbesserter Duftwahrnehmung
EP2190969B1 (en)	2007-05-04	2014-08-20	Ecolab Inc.	Pressed, self-solidifying, solid cleaning compositions and methods of making them
US7759300B2 (en) *	2007-07-02	2010-07-20	Ecolab Inc.	Solidification matrix including a salt of a straight chain saturated mono-, di-, or tri- carboxylic acid
MX2010003825A (es)	2007-10-18	2010-04-27	Ecolab Inc	Composiciones de limpieza solidas, auto-solidificables, comprimidas, y metodos para hacerlas.
CN110317681A (zh) *	2019-07-12	2019-10-11	广州立白企业集团有限公司	提升黏合性能的组合物及自动洗碗机洗涤剂组合物

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB1333042A (en) *	1969-08-22	1973-10-10	Unilever Ltd	Detergent bars
GB8830010D0 (en) *	1988-12-22	1989-02-15	Unilever Plc	Detergent composition
AU4324693A (en) *	1992-06-18	1994-01-04	Unilever Plc	Machine dishwashing composition
BR9405916A (pt) *	1993-04-01	1995-12-12	Unilever Nv	Composição detergente sólida na forma de pastilhas de material detergente granular comprimido processo para a fabricação de uma composição detergente sólido e uso da composição
AU702040B2 (en) *	1994-01-25	1999-02-11	Unilever Plc	Co-granules and detergent tablets formed therefrom
US5490949A (en) *	1994-07-22	1996-02-13	Monsanto Company	Block detergent containing nitrilotriacetic acid
DE19710254A1 (de) *	1997-03-13	1998-09-17	Henkel Kgaa	Wasch- oder reinigungsaktive Formkörper für den Gebrauch im Haushalt
ZA984570B (en) *	1997-06-06	1999-11-29	Unilever Plc	Cleaning compositions.
GB9815525D0 (en) *	1998-07-17	1998-09-16	Procter & Gamble	Detergent tablet
WO2000004117A2 (en) *	1998-07-17	2000-01-27	The Procter & Gamble Company	Detergent tablet

1999
- 1999-03-04 GB GB9904882A patent/GB2347431A/en not_active Withdrawn
2000
- 2000-02-29 AU AU38621/00A patent/AU3862100A/en not_active Abandoned
- 2000-02-29 MX MXPA01008901A patent/MXPA01008901A/es active IP Right Grant
- 2000-02-29 WO PCT/US2000/005302 patent/WO2000052130A1/en not_active Application Discontinuation
- 2000-02-29 JP JP2000602742A patent/JP2002538270A/ja active Pending
- 2000-02-29 EP EP00917687A patent/EP1159396A1/en not_active Withdrawn
- 2000-02-29 CA CA002362955A patent/CA2362955C/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
GB9904882D0 (en)	1999-04-28
GB2347431A (en)	2000-09-06
AU3862100A (en)	2000-09-21
CA2362955A1 (en)	2000-09-08
WO2000052130A1 (en)	2000-09-08
EP1159396A1 (en)	2001-12-05
MXPA01008901A (es)	2002-04-24
JP2002538270A (ja)	2002-11-12

Legal Events

Date	Code	Title	Description
2001-08-23	EEER	Examination request
2009-03-02	MKLA	Lapsed

Publication	Publication Date	Title
US6686328B1 (en)	2004-02-03	Detergent tablet
US6770616B1 (en)	2004-08-03	Detergent tablet
CA2337402C (en)	2004-05-04	Detergent tablet
US20020160930A1 (en)	2002-10-31	Detergent tablet
CA2358872C (en)	2005-03-29	Detergent tablet
CA2333388C (en)	2005-04-05	Detergent tablet
US6974789B1 (en)	2005-12-13	Detergent tablet
US6551982B1 (en)	2003-04-22	Detergent tablet
CA2337427C (en)	2004-04-27	Detergent tablet
EP0922756B1 (en)	2001-09-19	Detergent composition
CA2337401C (en)	2005-10-11	A multi-phase detergent tablet
EP1327676B1 (en)	2006-10-18	Detergent tablet
CA2337408C (en)	2005-11-15	A multi-phase detergent tablet
WO2000004124A2 (en)	2000-01-27	Detergent tablet
CA2362955C (en)	2005-07-05	Multi-phase detergent tablet
WO2002033037A1 (en)	2002-04-25	Detergent tablet
CA2455703C (en)	2006-10-03	A multi-phase detergent tablet
WO2001060965A1 (en)	2001-08-23	Detergent tablet
GB2340842A (en)	2000-03-01	Detergent tablet
WO2004003124A1 (en)	2004-01-08	Detergent compositions
GB2340841A (en)	2000-03-01	Detergent Tablet
CA2510479A1 (en)	2000-01-27	A multi-phase detergent tablet
GB2340840A (en)	2000-03-01	Detergent tablet